CN106769390A - A kind of micro-wave digestion equipment - Google Patents
A kind of micro-wave digestion equipment Download PDFInfo
- Publication number
- CN106769390A CN106769390A CN201710087132.6A CN201710087132A CN106769390A CN 106769390 A CN106769390 A CN 106769390A CN 201710087132 A CN201710087132 A CN 201710087132A CN 106769390 A CN106769390 A CN 106769390A
- Authority
- CN
- China
- Prior art keywords
- test tube
- micro
- lid
- hole
- wave digestion
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Granted
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Classifications
-
- G—PHYSICS
- G01—MEASURING; TESTING
- G01N—INVESTIGATING OR ANALYSING MATERIALS BY DETERMINING THEIR CHEMICAL OR PHYSICAL PROPERTIES
- G01N1/00—Sampling; Preparing specimens for investigation
- G01N1/28—Preparing specimens for investigation including physical details of (bio-)chemical methods covered elsewhere, e.g. G01N33/50, C12Q
- G01N1/44—Sample treatment involving radiation, e.g. heat
-
- Y—GENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
- Y02—TECHNOLOGIES OR APPLICATIONS FOR MITIGATION OR ADAPTATION AGAINST CLIMATE CHANGE
- Y02E—REDUCTION OF GREENHOUSE GAS [GHG] EMISSIONS, RELATED TO ENERGY GENERATION, TRANSMISSION OR DISTRIBUTION
- Y02E50/00—Technologies for the production of fuel of non-fossil origin
- Y02E50/30—Fuel from waste, e.g. synthetic alcohol or diesel
Abstract
The invention discloses a kind of micro-wave digestion equipment, including test tube container and lid, also include nitrogen access tube and blast pipe, sealing gland is provided with the body of nitrogen access tube, lid is provided with the stepped hole of more than 2, sealing gland is arranged at a upper part for stepped hole, and the bottom of nitrogen access tube enters the inside of test tube container through stepped hole, and the entrance of blast pipe is connected to the upper part of stepped hole.Lid sets stepped hole, nitrogen access tube sets sealing gland, sealing gland is arranged at the upper part of stepped hole, ensure that sealing effectiveness, nitrogen access tube enters the inside of test tube container through lid, air can in time be drained, can be good at creating good inert gas environment, it is ensured that fast and efficiently carry out substance decomposition.
Description
Technical field
The present invention relates to micro-wave digestion equipment technical field, and in particular to a kind of micro-wave digestion equipment.
Background technology
In order to improve the analysis efficiency of material, it is necessary to be decomposed under high-temperature and high-pressure conditions to material.
High-temperature and high-pressure conditions need simultaneously coordinate inert gas environment, how to create good inert gas environment be can
Quickly, the key factor efficiently decomposed.
The content of the invention
The technical problem to be solved in the present invention is：A kind of micro-wave digestion equipment is proposed, can be good at creating good lazy
Property gaseous environment, it is ensured that fast and efficiently carry out substance decomposition.
It is that, up to this purpose, the present invention uses following technical scheme：
A kind of micro-wave digestion equipment, including test tube container and lid, also including nitrogen access tube and blast pipe, nitrogen access tube
Sealing gland is provided with body, lid is provided with the stepped hole of more than 2, and sealing gland is arranged at a top for stepped hole
Point, the bottom of nitrogen access tube enters the inside of test tube container through stepped hole, and the entrance of blast pipe is connected to stepped hole
Upper part.
Preferably, test tube container includes test tube distributing disc, and the outer of test tube distributing disc is connected to the inside of test tube container, tries
Offered on pipe distributing disc in the test tube hole clipping of array distribution.
Preferably, cap bore is also offered in the middle part of supporting plate including supporting plate；Lid includes post body and connection step,
Connection step is arranged at the top of post body, and the leave from office for connecting step is provided with screwed hole；
The surrounding of cap bore offers connecting hole corresponding with the screwed hole of the leave from office of connection step, and appearing on the stage for step of connection is arranged at
In cap bore.
Preferably, also including location-plate, through hole is offered in the middle part of location-plate, 3 is offered in the card of location-plate
Location hole above, appearing on the stage for step of connection is provided with connection blind hole corresponding with location hole；
Arc notch is provided with the outside of location-plate, arc notch is used for clamping sealing gland.
Preferably, the first convex edge is provided with the outside of the top of test tube container, is set on the outside of the bottom of the post body of lid
The second convex edge is equipped with, the bottom of supporting plate is provided with clamping mechanism, and clamping mechanism is used for the convex edge of clamping first and the second convex edge.
Preferably, clamping mechanism includes the first half clips, the second half clip, the first push rod, the second push rod, the first connecting plates
With the second connecting plate；The first notch and the second notch are offered in the supporting plate of the both sides of cap bore respectively；
The clip of lower end connection the first half of the first connecting plate, the upper end of the first connecting plate connects the first push rod, and the first push rod is set
In in supporting plate, the first connecting plate passes through the first notch；
The clip of lower end connection the second half of the second connecting plate, the upper end of the second connecting plate connects the second push rod, and the second push rod is set
In in supporting plate, the second connecting plate passes through the second notch.
Preferably, the first half clips are semicircular arc, and the madial wall of the first half clips is provided with the draw-in groove of circular arc, draw-in groove
For the convex edge of clamping first and the second convex edge, the lateral wall of the first half clips is vertical wall, and vertical wall is provided with for connecting the
The screwed hole of one connecting plate；
The second half clips are semicircular arc, and the madial wall of the second half clips is provided with the draw-in groove of circular arc, the second half clips it is outer
Side wall is vertical wall, and vertical wall is provided with the screwed hole for connecting the second connecting plate.
Preferably, the bottom of the second convex edge of lid is provided with plunger body, and plunger body is cylinder, and the week side of boss of plunger body sets
Rubber cushion ring recess is equipped with, rubber cushion is connected with rubber cushion ring recess；The external diameter of plunger body is equal with the internal diameter of test tube container, and plunger body is filled in
The top of test tube container.
Preferably, test tube container also includes inner chamber, and the bottom of the plunger body of lid is provided with bottom, and bottom is provided with down convex
Platform, the external diameter of lower convex platform is introversive equal with inner chamber, and lower convex platform fills in the top of inner chamber.
Preferably, the side of test tube container is provided with cold wind mouthful.
Beneficial effects of the present invention：A kind of micro-wave digestion equipment, including test tube container and lid are proposed, it is also logical including nitrogen
Enter pipe and blast pipe, sealing gland is provided with the body of nitrogen access tube, lid is provided with the stepped hole of more than 2, sealing
Gland is arranged at a upper part for stepped hole, and the bottom of nitrogen access tube enters the inside of test tube container through stepped hole,
The entrance of blast pipe is connected to the upper part of stepped hole.Lid sets stepped hole, and nitrogen access tube sets sealing gland, sealing gland
The upper part of stepped hole is arranged at, sealing effectiveness is ensure that, nitrogen access tube enters the inside of test tube container, energy through lid
It is enough to drain air in time, can be good at creating good inert gas environment, it is ensured that fast and efficiently carry out material point
Solution.
Brief description of the drawings
Fig. 1 is the structural representation of the test tube container, inner chamber and bottom of a kind of micro-wave digestion equipment of the invention.
Fig. 2 is a kind of structural representation at visual angle of the bottom of micro-wave digestion equipment of the invention.
Fig. 3 is a kind of structural representation at another visual angle of the bottom of micro-wave digestion equipment of the invention.
Fig. 4 is a kind of structural representation at visual angle of the lid of micro-wave digestion equipment of the invention.
Fig. 5 is a kind of structural representation at another visual angle of the lid of micro-wave digestion equipment of the invention.
Fig. 6 is a kind of structural representation at visual angle of the test tube container of micro-wave digestion equipment of the invention.
Fig. 7 is a kind of explosive view 1 of micro-wave digestion environment division structure of the invention.
Fig. 8 is a kind of explosive view 2 of micro-wave digestion environment division structure of the invention.
Fig. 9 is a kind of explosive view 3 of micro-wave digestion environment division structure of the invention.
In figure：
1- test tube containers；11- test tube distributing discs；111- test tube hole clippings；The convex edges of 12- first；13- inner chambers；2- lids；21- post sheets
Body；22- connects step；The convex edges of 23- second；24- plunger bodies；241- rubber cushion ring recess；25- bottoms；251- lower convex platforms；3- nitrogen leads to
Enter pipe；31- sealing glands；4- blast pipes；5- supporting plates；51- cap bore；The notches of 52- first；The notches of 53- second；6- location-plates；
61- arc notch；7- clamping mechanisms；The clips of 71- the first half；The clips of 72- the second half；The push rods of 73- first；The push rods of 74- second；
The connecting plates of 75- first；The connecting plates of 76- second.
Specific embodiment
1 ~ 9 and technical scheme is further illustrated by specific embodiment below in conjunction with the accompanying drawings.
A kind of micro-wave digestion equipment, including test tube container 1 and lid 2, also including nitrogen access tube 3 and blast pipe 4, nitrogen
Sealing gland 31 is provided with the body of access tube 3, lid 2 is provided with the stepped hole of more than 2, and sealing gland 31 is arranged at one
The upper part of individual stepped hole, the bottom of nitrogen access tube 3 enters the inside of test tube container 1 through stepped hole, and blast pipe 4 enters
Mouth is connected to the upper part of stepped hole.
Lid 2 sets stepped hole, and nitrogen access tube 3 sets sealing gland 31, and sealing gland 31 is arranged at the top of stepped hole
Point, sealing effectiveness is ensure that, nitrogen access tube 3 enters the inside of test tube container 1 through the stepped hole of lid 2, can be by sky
Gas is drained in time, can be good at creating good inert gas environment, it is ensured that fast and efficiently carry out substance decomposition.
In the present embodiment, test tube container 1 includes test tube distributing disc 11, and the outer of test tube distributing disc 11 is connected to test tube container
1 inside, offers in the test tube hole clipping 111 of array distribution on test tube distributing disc 11.
In the present embodiment, also including supporting plate 5, the middle part of supporting plate 5 offers cap bore 51；Lid 2 includes post body 21
With connection step 22, the top that step 22 is arranged at post body 21 is connected, the leave from office for connecting step 22 is provided with screwed hole；
The surrounding of cap bore 51 offers connecting hole corresponding with the screwed hole of the leave from office of connection step 22, connects appearing on the stage for step 22
It is arranged in cap bore 51.
In the present embodiment, also including location-plate 6, the middle part of location-plate 6 offers through hole, is opened in the card of location-plate 6
The location hole of more than 3 is provided with, appearing on the stage for step 22 of connection is provided with connection blind hole corresponding with location hole；
The outside of location-plate 6 is provided with arc notch 61, and arc notch 61 is used for clamping sealing gland 31.
In the present embodiment, the first convex edge 12 is provided with the outside of the top of test tube container 1, under the post body 21 of lid 2
The second convex edge 23 is provided with the outside of portion, the bottom of supporting plate 5 is provided with clamping mechanism 7, and it is convex that clamping mechanism 7 is used for clamping first
Along 12 and second convex edge 23.
In the present embodiment, clamping mechanism 7 includes the first half clips 71, the second half clip 72, the first push rod 73, the second push rods
74th, the first connecting plate 75 and the second connecting plate 76；The first notch 52 and are offered in the supporting plate 5 of the both sides of cap bore 51 respectively
Two notches 53；
The clip 71 of lower end connection the first half of the first connecting plate 75, the upper end of the first connecting plate 75 connects the first push rod 73, first
Push rod 73 is arranged in supporting plate 5, and the first connecting plate 75 passes through the first notch 52；
The clip 72 of lower end connection the second half of the second connecting plate 76, the upper end of the second connecting plate 76 connects the second push rod 74, second
Push rod 74 is arranged in supporting plate 5, and the second connecting plate 76 passes through the second notch 53.
In the present embodiment, the first half clips 71 are semicircular arc, and the madial wall of the first half clips 71 is provided with circular arc
Draw-in groove, draw-in groove is used for clamping the first convex edge 12 and the second convex edge 23, and the lateral wall of the first half clips 71 is vertical wall, and vertical wall sets
It is equipped with the screwed hole for connecting the first connecting plate 75；
The second half clips 72 are semicircular arc, and the madial wall of the second half clips 72 is provided with the draw-in groove of circular arc, the second half clips
72 lateral wall is vertical wall, and vertical wall is provided with the screwed hole for connecting the second connecting plate 76.
In the present embodiment, the bottom of the second convex edge 23 of lid 2 is provided with plunger body 24, and plunger body 24 is cylinder, post
The week side of boss of cock body 24 is provided with rubber cushion ring recess 241, rubber cushion ring recess 241 and is connected with rubber cushion；The external diameter of plunger body 24 holds with test tube
The internal diameter of device 1 is equal, and plunger body 24 fills in the top of test tube container 1.
In the present embodiment, rubber cushion is annular rubber cushion, and the surface of rubber cushion is embedded in the miniature stainless shot of the nm of particle diameter 50 ~ 80, micro-
The spacing of type stainless shot is 100 ~ 120 nm, it is ensured that the intensity and elasticity of rubber cushion.It is corresponding to match somebody with somebody in test tube container 1 and rubber cushion
The position of conjunction, sets miniature pit, and the aperture of miniature pit is 80 ~ 100 nm, and the spacing of miniature pit is 100 ~ 120 nm guarantors
The bonding strength and sealing property of card rubber cushion and test tube container 1.
In the present embodiment, rubber cushion is internally provided with cavity, is provided with inflation inlet, can ensure that rubber cushion has foot by inflation
Enough intensity and diameter.
In the present embodiment, test tube container 1 also includes inner chamber 13, and the bottom of the plunger body 24 of lid 2 is provided with bottom 25, bottom
Lid 25 is provided with lower convex platform 251, and the external diameter of lower convex platform 251 is introversive equal with inner chamber 13, and lower convex platform 251 fills in the upper of inner chamber 13
Portion.
In the present embodiment, the side of test tube container 1 is provided with cold wind mouthful.
Know-why of the invention is described above in association with specific embodiment.These descriptions are intended merely to explain of the invention
Principle, and can not by any way be construed to limiting the scope of the invention.Based on explanation herein, the technology of this area
Personnel associate other specific embodiments of the invention by would not require any inventive effort, these modes fall within
Within protection scope of the present invention.
Claims (10)
1. a kind of micro-wave digestion equipment, including test tube container（1）And lid（2）, it is characterised in that also including nitrogen access tube
（3）And blast pipe（4）, the nitrogen access tube（3）Body on be provided with sealing gland（31）, the lid（2）It is provided with 2
Stepped hole more than individual, the sealing gland（31）It is arranged at a upper part for the stepped hole, the nitrogen access tube（3）
Bottom through stepped hole enter the test tube container（1）Inside, the blast pipe（4）Entrance be connected to the step
The upper part in hole.
2. micro-wave digestion equipment as claimed in claim 1, it is characterised in that the test tube container（1）Including test tube distributing disc
（11）, the test tube distributing disc（11）Outer be connected to the test tube container（1）Inside, the test tube distributing disc（11）On
Offer in the test tube hole clipping of array distribution（111）.
3. micro-wave digestion equipment as claimed in claim 1, it is characterised in that also including supporting plate（5）, the supporting plate（5）'s
Middle part offers cap bore（51）；The lid（2）Including post body（21）With connection step（22）, the connection step（22）If
It is placed in the post body（21）Top, the connection step（22）Leave from office be provided with screwed hole；
The cap bore（51）Surrounding offer and the connection step（22）Leave from office the corresponding connecting hole of screwed hole, it is described
Connection step（22）Appear on the stage and be arranged at the cap bore（51）It is interior.
4. micro-wave digestion equipment as claimed in claim 3, it is characterised in that also including location-plate（6）, the location-plate（6）'s
Middle part offers through hole, the location-plate（6）Card on offer the location hole of more than 3, the connection step（22）
Appear on the stage and be provided with connection blind hole corresponding with the location hole；
The location-plate（6）Outside be provided with arc notch（61）, the arc notch（61）For sealing pressure described in clamping
Lid（31）.
5. micro-wave digestion equipment as claimed in claim 3, it is characterised in that the test tube container（1）Top outside set
There is the first convex edge（12）, the lid（2）Post body（21）Bottom on the outside of be provided with the second convex edge（23）, the support
Plate（5）Bottom be provided with clamping mechanism（7）, the clamping mechanism（7）For the first convex edge described in clamping（12）It is convex with second
Edge（23）.
6. micro-wave digestion equipment as claimed in claim 5, it is characterised in that the clamping mechanism（7）Including the first half clips
（71）, the second half clips（72）, the first push rod（73）, the second push rod（74）, the first connecting plate（75）With the second connecting plate（76）；
The cap bore（51）Both sides supporting plate（5）It is upper to offer the first notch respectively（52）With the second notch（53）；
First connecting plate（75）Lower end connection the first half clip（71）, first connecting plate（75）Upper end connect
Connect first push rod（73）, first push rod（73）It is arranged at the supporting plate（5）On, first connecting plate（75）Wear
Cross first notch（52）；
Second connecting plate（76）Lower end connection the second half clip（72）, second connecting plate（76）Upper end connect
Connect second push rod（74）, second push rod（74）It is arranged at the supporting plate（5）On, second connecting plate（76）Wear
Cross second notch（53）.
7. micro-wave digestion equipment as claimed in claim 6, it is characterised in that the first half clip（71）It is semicircular arc, institute
State the first half clips（71）Madial wall be provided with the draw-in groove of circular arc, the draw-in groove is used for the first convex edge described in clamping（12）With
Second convex edge（23）, the first half clip（71）Lateral wall be vertical wall, the vertical wall is provided with described for connecting
First connecting plate（75）Screwed hole；
The second half clip（72）It is semicircular arc, the second half clip（72）Madial wall be provided with the card of circular arc
Groove, the second half clip（72）Lateral wall be vertical wall, the vertical wall is provided with for connecting second connecting plate
（76）Screwed hole.
8. micro-wave digestion equipment as claimed in claim 3, it is characterised in that the lid（2）The second convex edge（23）Bottom
It is provided with plunger body（24）, the plunger body（24）It is cylinder, the plunger body（24）The week side of boss be provided with rubber cushion ring recess
（241）, the rubber cushion ring recess（241）Inside it is connected with rubber cushion；The plunger body（24）External diameter and the test tube container（1）It is interior
Footpath is equal, the plunger body（24）Fill in the test tube container（1）Top.
9. micro-wave digestion equipment as claimed in claim 8, it is characterised in that the test tube container（1）Also include inner chamber（13）, institute
State lid（2）Plunger body（24）Bottom be provided with bottom（25）, the bottom（25）It is provided with lower convex platform（251）, it is described
Lower convex platform（251）External diameter and the inner chamber（13）Introversive equal, the lower convex platform（251）Fill in the inner chamber（13）It is upper
Portion.
10. micro-wave digestion equipment as claimed in claim 1, it is characterised in that the test tube container（1）Side be provided with cold wind
Mouthful.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201710087132.6A CN106769390B (en) | 2017-02-17 | 2017-02-17 | Microwave digestion equipment |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201710087132.6A CN106769390B (en) | 2017-02-17 | 2017-02-17 | Microwave digestion equipment |
Publications (2)
| Publication Number | Publication Date |
|---|---|
| CN106769390A true CN106769390A (en) | 2017-05-31 |
| CN106769390B CN106769390B (en) | 2023-09-05 |
Family
ID=58958026
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN201710087132.6A Active CN106769390B (en) | 2017-02-17 | 2017-02-17 | Microwave digestion equipment |
Country Status (1)
| Country | Link |
|---|---|
| CN (1) | CN106769390B (en) |
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| Publication number | Publication date |
|---|---|
| CN106769390B (en) | 2023-09-05 |
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