CN106768514A - The preparation method and pressure sensor of pressure sensor - Google Patents

The preparation method and pressure sensor of pressure sensor Download PDF

Info

Publication number
CN106768514A
CN106768514A CN201611218453.7A CN201611218453A CN106768514A CN 106768514 A CN106768514 A CN 106768514A CN 201611218453 A CN201611218453 A CN 201611218453A CN 106768514 A CN106768514 A CN 106768514A
Authority
CN
China
Prior art keywords
wafer
pressure sensor
pressure
preparation
back side
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Pending
Application number
CN201611218453.7A
Other languages
Chinese (zh)
Inventor
马清杰
李文翔
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
Suzhou Industrial Park Co Ltd Of Industries Based On Nanotechnology Institute For Research And Technology
Original Assignee
Suzhou Industrial Park Co Ltd Of Industries Based On Nanotechnology Institute For Research And Technology
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by Suzhou Industrial Park Co Ltd Of Industries Based On Nanotechnology Institute For Research And Technology filed Critical Suzhou Industrial Park Co Ltd Of Industries Based On Nanotechnology Institute For Research And Technology
Priority to CN201611218453.7A priority Critical patent/CN106768514A/en
Publication of CN106768514A publication Critical patent/CN106768514A/en
Pending legal-status Critical Current

Links

Classifications

    • GPHYSICS
    • G01MEASURING; TESTING
    • G01LMEASURING FORCE, STRESS, TORQUE, WORK, MECHANICAL POWER, MECHANICAL EFFICIENCY, OR FLUID PRESSURE
    • G01L1/00Measuring force or stress, in general
    • G01L1/18Measuring force or stress, in general using properties of piezo-resistive materials, i.e. materials of which the ohmic resistance varies according to changes in magnitude or direction of force applied to the material

Landscapes

  • Physics & Mathematics (AREA)
  • General Physics & Mathematics (AREA)
  • Measuring Fluid Pressure (AREA)

Abstract

The present invention relates to the preparation method and pressure sensor of a kind of pressure sensor, the preparation method comprises the following steps:S1:There is provided has the back side and positive wafer;Pressure drag bar and heavily doped contact zone are formed in the front of wafer;Pressure depth chamber is formed by the back-etching of wafer;S2:Support chip is bonded at the back side of wafer;S3:Fairlead and metal connecting line are made in the front of wafer, connection pressure drag bar forms Wheatstone bridge;S4:Deposit to form passivation layer in the front of wafer, open portion of the passivating layer to form metal pad region.Be placed on bonding technology after high-temperature diffusion process by the preparation method of the pressure sensor, before metal connecting line technique, so as to avoid the influence of high-temperature diffusion process para-linkage technique, the pressure sensitive film for preventing high-temperature diffusion process to destroy on vacuum chamber, and avoid bonding technology to weigh metal connecting line wounded, and then improve the fine ratio of product of product.

Description

The preparation method and pressure sensor of pressure sensor
Technical field
The present invention relates to the preparation method and pressure sensor of a kind of pressure sensor, belong to micro code-lock field.
Background technology
1962, the first time such as Tufte diffusion silicon pressure drag bar and silicon fiml structure processed piezoresistive pressure sensor, open Begin the research of piezoresistive pressure sensor.Beginning of the seventies late 1960s, silicon anisotropic etching technology, ion implanting The appearance of technology and the big technology of anode linkage technology three brings huge change to pressure sensor, and they are improving pressure Played the important and pivotal role in the performance of sensor.From the eighties in 20th century so far, the further development of micro-processing technology, Such as anisotropic etch, photoetching, diffusing, doping, ion implanting, bonding and plated film technology so that the size of pressure sensor Constantly reduce, sensitivity is improved, yield is high and excellent performance.Meanwhile, the development and application of new micro fabrication makes The thickness for obtaining pressure sensor is precisely controlled.Jackson etc. and Kim and Wise have studied the electrochemistry of P-N junction respectively Property, the difference (3000 of the rate of corrosion in corrosive liquid using P-type silicon and N-type silicon:1 in the corrosive liquid based on ethylenediamine) make Standby silicon fiml.Kloeck etc. reports using electrochemistry self-stopping technology technology to improve the output characteristics of piezoresistive pressure sensor. In the later stage eighties 20th century, NovaSensor starts with the technology and produces substantial amounts of pressure sensor.
So far, the manufacture of pressure sensor has evolved to a new stage, and more new technologies will be applied to It is below most representational three kinds of prior arts in the production of pressure sensor.
Prior art one, Freescale Manifold Air Pressure (MAP) sensor is each to different using KOH etc. Property the deep chamber of wet etch techniques etching form pressure sensitive film, finally overleaf deep chamber side switch combined glass glass or silicon chip form pressure Chamber.But, using the wet etching solution such as KOH, K ionic soils are had, device performance is influenceed, pollute producing line;Other time control Corrosion depth, makes presser sensor film thickness be difficult to precise control;Bonding technology can cause to weigh wounded to the positive metal level of disk;
Prior art two, NovaSensor pressure sensor corrode on substrate disk first pressure depth chamber, Then in pressure depth chamber side switch unification piece N-type disk, by the N-type disk above attenuated polishing, pressure sensitive film is formed, then The techniques such as diffusion are injected on pressure sensitive film and forms pressure drag, the structure such as metal connecting line and passivation layer finally subtracts to the back side The technique such as thin opens pressure chamber from the back side.But, there are the following problems for the technology:Pressure depth chamber, pressure sensitive film are completed first It is sealed in above, subsequent high temperature processes can deform pressure sensitive film, or even rupture, influence subsequent technique and yield rate;Pressure , using the technique such as wafer bonding is thinning, technology difficulty is big, it is difficult to manufacture relatively thin and flat pressure sensitive film for sensitive membrane;
Prior art three, piezoresistive pressure sensor prepared by Bosch porous epitaxial silicons technology, its technique uses porous silicon Epitaxial monocrystalline silicon forms annular seal space and pressure sensitive film.But, the related process technologies such as porous epitaxial silicon single silicon, including its Its epitaxy single-crystal silicon technology on cavity forms annular seal space and presser sensor membrane technology, and technology difficulty is high, is hardly formed flat Pressure sensitive film, and do not apply to the manufacture of gauge sensor.
The content of the invention
It is an object of the invention to provide a kind of preparation method of pressure sensor, high temperature is avoided by the preparation method The influence of diffusion technique para-linkage technique, it is therefore prevented that the pressure sensitive film on high-temperature diffusion process destruction vacuum chamber, and avoid Bonding technology is weighed wounded to metal connecting line.
To reach above-mentioned purpose, the present invention provides following technical scheme:A kind of preparation method of pressure sensor, including such as Lower step:
S1:There is provided has the back side and positive wafer;
Pressure drag bar and heavily doped contact zone are formed in the front of the wafer;
Pressure depth chamber is formed by the back-etching of the wafer;
S2:Support chip is bonded at the back side of the wafer;
S3:Fairlead and metal connecting line are made in the front of the wafer, connection pressure drag bar forms Wheatstone bridge;
S4:Deposit to form passivation layer in the front of the wafer, open portion of the passivating layer to form metal pad region.
Further:The S1 specifically includes following steps:
S11:There is provided has the back side and positive wafer, and the thickness of pressure sensitive film is defined on the wafer;
S12:Ion implanting is used in the front of the wafer, pressure drag bar, heavily doped contact are made using high-temperature diffusion process Area;
S13:Deposit to form protective layer in the front of wafer;
S14:Etch to form pressure depth chamber to form pressure sensitive film in the wafer rear.
Further:The wafer is SOI.
Further:The pressure depth chamber is formed by deep reactive ion etch technique.
Further:The S13 is specifically included:Protective layer is formed with oxide layer and nitration case in the front deposition of wafer.
Further:Include between the S13 and S14:The thinning back side of the wafer is polished to reduce wafer thickness.
Further:In the S3, also include:After the back side of wafer is bonded support chip, beaten on the support chip Hole is forming and the through hole that is connected of pressure depth chamber.
Further:The support chip is silicon chip or sheet glass.
Further:In the S4, the passivation layer is formed by cvd silicon oxide and silicon nitride.
Present invention also offers a kind of pressure sensor, formed by the preparation method of above-mentioned pressure sensor.
The beneficial effects of the present invention are:Bonding technology is placed on high temperature and expanded by the preparation method of pressure sensor of the invention After day labor skill, before metal connecting line technique, so as to avoid the influence of high-temperature diffusion process para-linkage technique, it is therefore prevented that high temperature Pressure sensitive film on diffusion technique destruction vacuum chamber, and avoid bonding technology metal connecting line is weighed wounded, and then lifted The fine ratio of product of product.
Described above is only the general introduction of technical solution of the present invention, in order to better understand technological means of the invention, And can be practiced according to the content of specification, below with presently preferred embodiments of the present invention and coordinate accompanying drawing describe in detail as after.
Brief description of the drawings
Fig. 1 is the gauge sensor shown in one embodiment of the invention;
Fig. 2A to Fig. 2 I is the preparation method of the gauge sensor shown in Fig. 1;
Fig. 3 is the absolute pressure pressure sensor shown in another embodiment of the present invention.
Specific embodiment
With reference to the accompanying drawings and examples, specific embodiment of the invention is described in further detail.Hereinafter implement Example is not limited to the scope of the present invention for illustrating the present invention.
Refer to Fig. 1 and combine Fig. 2A to Fig. 2 I, the gauge sensor 100 shown in a preferred embodiment of the present invention Preparation method includes as follows:
Incorporated by reference to Fig. 2A, the first step:Wafer 1 is provided, the wafer 1 is SOI (the silicon on of (100) crystal face insulator).The wafer 1 sequentially consists of lower floor's silicon 15, buried oxide 2 and the upper layer of silicon in buried oxide 2 3;The material of the buried oxide 2 is silica.By the thickness explication of upper layer of silicon 3 in buried oxide 2 for gauge is sensed The thickness of the pressure sensitive film 4 of device 100;
Incorporated by reference to Fig. 2 B, second step:Zero layer alignment mark 5 is made in the front of the wafer 1, before subsequent technique Layer alignment mark;
Incorporated by reference to Fig. 2 C, the 3rd step:Ion implanting is used in the front of wafer 1, pressure drag is made using high-temperature diffusion process Bar 6, heavily doped contact zone 7;
Incorporated by reference to Fig. 2 D, the 4th step:Deposited oxide layer and nitration case on wafer 1, as follow-up attenuated polishing technique Protective layer 8, likewise, the protective layer 8 again can be as the insulating barrier of gauge sensor 100;
Incorporated by reference to Fig. 2 E, the 5th step:By the thinning back side polishing of wafer 1 to reduce the thickness of wafer 1, and then reduce follow-up The depth in etching pressure depth chamber, reduces the gross thickness of gauge sensor 100;
Incorporated by reference to Fig. 2 F, the 6th step:Etched by deep reactive ion etch technique (DRIE) at the back side of wafer 1 and form pressure Power depth chamber 9, etching stopping forms pressure sensitive film 4 in buried oxide 2;Because etching oxidation silicon and silicon have choosing very high Ratio is selected, so the thickness of pressure sensitive film 4 can be precisely controlled by deep reactive ion etch technique;
Incorporated by reference to Fig. 2 G, the 7th step:The back side of wafer 1 be bonded support chip 10, the material of support chip 10 can with but do not limit to In silicon chip or sheet glass.In the present embodiment, after the back side of wafer 1 is bonded support chip 10, beaten on the support chip 10 Hole is forming the through hole 16 with the UNICOMs of pressure Shen Qiang 9;
Incorporated by reference to Fig. 2 H, the 8th step:Perforate to form fairlead 11 to make on the positive protective layer 8 of wafer 1, is drawing Metal connecting line 12 is formed in string holes 11 and protective layer 8 and forms Wheatstone bridge to connect pressure drag bar 6, for measurement presser sensor Film 4 changes the resistance variations for causing;
Incorporated by reference to Fig. 2 I, the 9th step:Wafer 1 front cvd silicon oxide and silicon nitride as passivation layer 13, opening portion Divide passivation layer 13 to form the region of metal pad 14, for follow-up routing.
In other embodiments, the 3rd step can be placed on after the 6th step, but, the 6th step is put by the present embodiment Before the 3rd step (i.e.:By high-temperature diffusion process be placed on pressure depth chamber 9 prepare before), can avoid causing due to fuel factor Pressure sensitive film 4 is destroyed, and can improve finished product rate and technological feasibility.In addition, in the present embodiment, by by deeply instead Answer ion etching etching pressure depth chamber 9 to be used in combination SOI and prepare pressure sensitive film, can be with precise control pressure sensitive film 4 Thickness, improve the uniformity of pressure sensor, it is to avoid metal ion pollution, and reduce the area of pressure sensor, And, compared with prior art, can also avoid directly using the technologies such as attenuated polishing, can be with more precise control pressure sensitive film 4 thickness, is more easy to obtain flat pressure sensitive film 4.
Above-mentioned preparation technology can form gauge sensor 100, in other embodiments, if in the 7th step, when After the back side bonding support chip 10 of wafer 1, do not punched on the support chip 10, then can form absolute pressure pressure sensor 200 (please Referring to Fig. 3).
In sum:Following advantage can obtain by the preparation method of the preparation method of above-mentioned pressure sensor:
1st, by before bonding technology is moved into metal layer process, it is to avoid bonding technology is to metal level (metal connecting line 12) Weigh wounded;
2nd, it is placed on after high-temperature diffusion process by by bonding technology, it is to avoid the shadow of high-temperature diffusion process para-linkage technique Ring, it is therefore prevented that the pressure sensitive film 4 on high-temperature diffusion process breakdown pressure depth chamber 9;
3rd, by by high-temperature diffusion process be placed on pressure depth chamber 9 prepare before, can avoid causing pressure quick due to fuel factor Sense film 4 is destroyed, and improves finished product rate and technological feasibility;
4th, pressure sensitive film 4 is prepared by the way that the deep chamber of deep reactive ion etch technique etching is used in combination into SOI, can be accurate The thickness of control pressure sensitive membrane 4, improves the uniformity of pressure sensor, it is to avoid metal ion pollution, and reduce pressure The area of force snesor, and, compared with prior art, can also avoid directly using the technologies such as attenuated polishing, can be more accurate Control pressure sensitive membrane 4 thickness, be more easy to obtain flat pressure sensitive film 4.
Each technical characteristic of embodiment described above can be combined arbitrarily, to make description succinct, not to above-mentioned reality Apply all possible combination of each technical characteristic in example to be all described, as long as however, the combination of these technical characteristics is not deposited In contradiction, the scope of this specification record is all considered to be.
Embodiment described above only expresses several embodiments of the invention, and its description is more specific and detailed, but simultaneously Can not therefore be construed as limiting the scope of the patent.It should be pointed out that coming for one of ordinary skill in the art Say, without departing from the inventive concept of the premise, various modifications and improvements can be made, these belong to protection of the invention Scope.Therefore, the protection domain of patent of the present invention should be determined by the appended claims.

Claims (10)

1. a kind of preparation method of pressure sensor, it is characterised in that the preparation method comprises the following steps:
S1:There is provided has the back side and positive wafer;
Pressure drag bar and heavily doped contact zone are formed in the front of the wafer;
Pressure depth chamber is formed by the back-etching of the wafer;
S2:Support chip is bonded at the back side of the wafer;
S3:Fairlead and metal connecting line are made in the front of the wafer, connection pressure drag bar forms Wheatstone bridge;
S4:Deposit to form passivation layer in the front of the wafer, open portion of the passivating layer to form metal pad region.
2. the preparation method of pressure sensor as claimed in claim 1, it is characterised in that the S1 specifically includes following step Suddenly:
S11:There is provided has the back side and positive wafer, and the thickness of pressure sensitive film is defined on the wafer;
S12:Ion implanting is used in the front of the wafer, pressure drag bar, heavily doped contact zone are made using high-temperature diffusion process;
S13:Deposit to form protective layer in the front of wafer;
S14:Etch to form pressure depth chamber to form pressure sensitive film in the wafer rear.
3. the preparation method of pressure sensor as claimed in claim 1 or 2, it is characterised in that the wafer is SOI.
4. the preparation method of pressure sensor as claimed in claim 3, it is characterised in that reacted by deep in the pressure depth chamber Ion etching is formed.
5. the preparation method of pressure sensor as claimed in claim 2, it is characterised in that the S13 is specifically included:In wafer Front deposition protective layer is formed with oxide layer and nitration case.
6. the preparation method of pressure sensor as claimed in claim 2, it is characterised in that include between the S13 and S14: The thinning back side of the wafer is polished to reduce wafer thickness.
7. the preparation method of pressure sensor as claimed in claim 1, it is characterised in that in the S3, also include:Work as crystalline substance After round back side bonding support chip, punch to form the through hole being connected with pressure depth chamber on the support chip.
8. the preparation method of the pressure sensor as described in claim 1 or 7, it is characterised in that the support chip be silicon chip or Person's sheet glass.
9. the preparation method of pressure sensor as claimed in claim 1, it is characterised in that in the S4, the passivation layer Formed by cvd silicon oxide and silicon nitride.
10. a kind of pressure sensor, it is characterised in that the pressure sensor is by as any one in claim 1 to 9 The preparation method of the pressure sensor described in is formed.
CN201611218453.7A 2016-12-26 2016-12-26 The preparation method and pressure sensor of pressure sensor Pending CN106768514A (en)

Priority Applications (1)

Application Number Priority Date Filing Date Title
CN201611218453.7A CN106768514A (en) 2016-12-26 2016-12-26 The preparation method and pressure sensor of pressure sensor

Applications Claiming Priority (1)

Application Number Priority Date Filing Date Title
CN201611218453.7A CN106768514A (en) 2016-12-26 2016-12-26 The preparation method and pressure sensor of pressure sensor

Publications (1)

Publication Number Publication Date
CN106768514A true CN106768514A (en) 2017-05-31

Family

ID=58926146

Family Applications (1)

Application Number Title Priority Date Filing Date
CN201611218453.7A Pending CN106768514A (en) 2016-12-26 2016-12-26 The preparation method and pressure sensor of pressure sensor

Country Status (1)

Country Link
CN (1) CN106768514A (en)

Cited By (5)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN107673306A (en) * 2017-08-12 2018-02-09 北方电子研究院安徽有限公司 A kind of preparation method of MEMS pressure sensor
CN108147361A (en) * 2017-12-22 2018-06-12 中国科学院半导体研究所 The preparation method of dense boron-doping silicon nano wire MEMS Piezoresistive Pressure Sensor
CN109342836A (en) * 2018-10-24 2019-02-15 清华大学 Production technology based on piezoelectricity pressure resistance type wideband high field intensity micro field sensor
CN110243501A (en) * 2019-06-28 2019-09-17 华中科技大学 The quantum pressure sensor and preparation method of a kind of diamond nitrogen vacancy colour center
CN110730905A (en) * 2017-06-13 2020-01-24 株式会社电装 Semiconductor device and method for manufacturing the same

Citations (5)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN101520350A (en) * 2009-03-24 2009-09-02 无锡市纳微电子有限公司 Process for manufacturing improved high-sensitivity low pressure sensor chip
CN202305094U (en) * 2011-07-14 2012-07-04 无锡芯感智半导体有限公司 High temperature pressure sensor with silicon-on-insulator (SOI) structure
CN105021328A (en) * 2015-07-13 2015-11-04 厦门大学 Piezoresistive pressure sensor compatible with CMOS process and preparation method of piezoresistive pressure sensor
CN106017751A (en) * 2016-05-25 2016-10-12 东南大学 High-sensitivity piezoresistive pressure sensor and preparation method thereof
CN106153221A (en) * 2016-08-26 2016-11-23 沈阳仪表科学研究院有限公司 A kind of manufacture method of high-precision pressure sensor based on Si-Si bonding

Patent Citations (5)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN101520350A (en) * 2009-03-24 2009-09-02 无锡市纳微电子有限公司 Process for manufacturing improved high-sensitivity low pressure sensor chip
CN202305094U (en) * 2011-07-14 2012-07-04 无锡芯感智半导体有限公司 High temperature pressure sensor with silicon-on-insulator (SOI) structure
CN105021328A (en) * 2015-07-13 2015-11-04 厦门大学 Piezoresistive pressure sensor compatible with CMOS process and preparation method of piezoresistive pressure sensor
CN106017751A (en) * 2016-05-25 2016-10-12 东南大学 High-sensitivity piezoresistive pressure sensor and preparation method thereof
CN106153221A (en) * 2016-08-26 2016-11-23 沈阳仪表科学研究院有限公司 A kind of manufacture method of high-precision pressure sensor based on Si-Si bonding

Cited By (7)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN110730905A (en) * 2017-06-13 2020-01-24 株式会社电装 Semiconductor device and method for manufacturing the same
CN107673306A (en) * 2017-08-12 2018-02-09 北方电子研究院安徽有限公司 A kind of preparation method of MEMS pressure sensor
CN107673306B (en) * 2017-08-12 2019-06-21 北方电子研究院安徽有限公司 A kind of preparation method of MEMS pressure sensor
CN108147361A (en) * 2017-12-22 2018-06-12 中国科学院半导体研究所 The preparation method of dense boron-doping silicon nano wire MEMS Piezoresistive Pressure Sensor
CN109342836A (en) * 2018-10-24 2019-02-15 清华大学 Production technology based on piezoelectricity pressure resistance type wideband high field intensity micro field sensor
CN109342836B (en) * 2018-10-24 2021-03-26 清华大学 Production process based on piezoelectric piezoresistive broadband high-field-intensity miniature electric field sensor
CN110243501A (en) * 2019-06-28 2019-09-17 华中科技大学 The quantum pressure sensor and preparation method of a kind of diamond nitrogen vacancy colour center

Similar Documents

Publication Publication Date Title
CN106768514A (en) The preparation method and pressure sensor of pressure sensor
CN104931163B (en) A kind of double soi structure MEMS pressure sensor chips and preparation method thereof
US6928879B2 (en) Episeal pressure sensor and method for making an episeal pressure sensor
JP3444639B2 (en) Manufacturing method and apparatus for integrated pressure transducer
CN100374838C (en) Monolithic silicon based SOI high-temperature low-drift pressure sensor
CN106153221B (en) A kind of manufacturing method of the high-precision pressure sensor based on Si-Si bonding
CN101289160B (en) 0-100Pa monolithic silicon based SOI high-temperature low drift micropressure sensor and processing method thereof
CN101290255B (en) Preparing method of 0-50pa single slice silicon based SOI ultra-low micro pressure sensor
CN102980694B (en) Without the MEMS piezoresistive pressure transducer and preparation method thereof of strain films structure
CN104330196B (en) Cavity film piezoresistive pressure sensor and manufacturing method thereof
JP3506932B2 (en) Semiconductor pressure sensor and method of manufacturing the same
CN104864988B (en) MEMS pressure sensor of silicon island membrane structure and preparation method thereof
JPS6197572A (en) Manufacture of semiconductor acceleration sensor
CN103604538A (en) MEMS pressure sensor chip based on SOI technology and manufacturing method thereof
CN104058361A (en) Processing method of integrated piezoresistive accelerometer and pressure meter which are based on prefabricated cavity SOI (silicon on insulator) substrate
CN108254106B (en) Preparation method of silicon-glass-silicon four-layer structure resonant MEMS pressure sensor
CN202305094U (en) High temperature pressure sensor with silicon-on-insulator (SOI) structure
CN104297520A (en) Monolithic embedded integrated silicon acceleration and pressure composite sensor
CN111076856A (en) Float self-compensating SOI pressure sensor
CN109545953A (en) A kind of preparation method of chip of high-temp pressure sensor
CN114684774A (en) Silicon piezoresistive pressure sensor chip and preparation method thereof
CN108981982A (en) A kind of MEMS pressure sensor and preparation method thereof
CN114275731A (en) MEMS-based double-beam type micro-pressure sensing core and preparation process thereof
CN204855051U (en) Two SOI structure MEMS pressure sensor chips
CN204718717U (en) The MEMS pressure sensor of silicon island membrane structure

Legal Events

Date Code Title Description
PB01 Publication
PB01 Publication
SE01 Entry into force of request for substantive examination
SE01 Entry into force of request for substantive examination
RJ01 Rejection of invention patent application after publication

Application publication date: 20170531

RJ01 Rejection of invention patent application after publication