CN106758191A - Mulberry silk fiber deoils and protects the process of glue - Google Patents
Mulberry silk fiber deoils and protects the process of glue Download PDFInfo
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- CN106758191A CN106758191A CN201611141156.7A CN201611141156A CN106758191A CN 106758191 A CN106758191 A CN 106758191A CN 201611141156 A CN201611141156 A CN 201611141156A CN 106758191 A CN106758191 A CN 106758191A
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- silk
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- percent concentration
- mulberry
- sodium carbonate
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Classifications
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- D—TEXTILES; PAPER
- D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
- D06M—TREATMENT, NOT PROVIDED FOR ELSEWHERE IN CLASS D06, OF FIBRES, THREADS, YARNS, FABRICS, FEATHERS OR FIBROUS GOODS MADE FROM SUCH MATERIALS
- D06M13/00—Treating fibres, threads, yarns, fabrics or fibrous goods made from such materials, with non-macromolecular organic compounds; Such treatment combined with mechanical treatment
- D06M13/10—Treating fibres, threads, yarns, fabrics or fibrous goods made from such materials, with non-macromolecular organic compounds; Such treatment combined with mechanical treatment with compounds containing oxygen
- D06M13/12—Aldehydes; Ketones
- D06M13/123—Polyaldehydes; Polyketones
-
- D—TEXTILES; PAPER
- D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
- D06M—TREATMENT, NOT PROVIDED FOR ELSEWHERE IN CLASS D06, OF FIBRES, THREADS, YARNS, FABRICS, FEATHERS OR FIBROUS GOODS MADE FROM SUCH MATERIALS
- D06M11/00—Treating fibres, threads, yarns, fabrics or fibrous goods made from such materials, with inorganic substances or complexes thereof; Such treatment combined with mechanical treatment, e.g. mercerising
- D06M11/73—Treating fibres, threads, yarns, fabrics or fibrous goods made from such materials, with inorganic substances or complexes thereof; Such treatment combined with mechanical treatment, e.g. mercerising with carbon or compounds thereof
- D06M11/76—Treating fibres, threads, yarns, fabrics or fibrous goods made from such materials, with inorganic substances or complexes thereof; Such treatment combined with mechanical treatment, e.g. mercerising with carbon or compounds thereof with carbon oxides or carbonates
-
- D—TEXTILES; PAPER
- D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
- D06M—TREATMENT, NOT PROVIDED FOR ELSEWHERE IN CLASS D06, OF FIBRES, THREADS, YARNS, FABRICS, FEATHERS OR FIBROUS GOODS MADE FROM SUCH MATERIALS
- D06M15/00—Treating fibres, threads, yarns, fabrics, or fibrous goods made from such materials, with macromolecular compounds; Such treatment combined with mechanical treatment
- D06M15/19—Treating fibres, threads, yarns, fabrics, or fibrous goods made from such materials, with macromolecular compounds; Such treatment combined with mechanical treatment with synthetic macromolecular compounds
- D06M15/37—Macromolecular compounds obtained otherwise than by reactions only involving carbon-to-carbon unsaturated bonds
- D06M15/643—Macromolecular compounds obtained otherwise than by reactions only involving carbon-to-carbon unsaturated bonds containing silicon in the main chain
-
- D—TEXTILES; PAPER
- D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
- D06M—TREATMENT, NOT PROVIDED FOR ELSEWHERE IN CLASS D06, OF FIBRES, THREADS, YARNS, FABRICS, FEATHERS OR FIBROUS GOODS MADE FROM SUCH MATERIALS
- D06M2101/00—Chemical constitution of the fibres, threads, yarns, fabrics or fibrous goods made from such materials, to be treated
- D06M2101/02—Natural fibres, other than mineral fibres
- D06M2101/10—Animal fibres
-
- D—TEXTILES; PAPER
- D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
- D06M—TREATMENT, NOT PROVIDED FOR ELSEWHERE IN CLASS D06, OF FIBRES, THREADS, YARNS, FABRICS, FEATHERS OR FIBROUS GOODS MADE FROM SUCH MATERIALS
- D06M2200/00—Functionality of the treatment composition and/or properties imparted to the textile material
- D06M2200/50—Modified hand or grip properties; Softening compositions
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- Engineering & Computer Science (AREA)
- Textile Engineering (AREA)
- Chemical & Material Sciences (AREA)
- Chemical Kinetics & Catalysis (AREA)
- Treatments For Attaching Organic Compounds To Fibrous Goods (AREA)
Abstract
Deoiled the invention discloses a kind of mulberry silk fiber and protect the process of glue, be related to textile technology field.The step such as refining, biological corruption, cocoon cooking, bleaching, softening, dewatered drying at the beginning of including using glutaraldehyde solid glue silk, softened water that this mulberry silk fiber deoils the process for protecting glue, mulberry silk after treated is after measured, content of silk gum reaches more than 3.7%, and fat content is no more than 0.42%.The present invention is solved being told to silk spinning raw material spoiled cocoon, bar, in the refinery practice of basinetto silk, on the premise of grease is removed（Oil content is controlled in 0 below .5%）, how glue fat could be retained in the problem in the range of 3 5%.
Description
Technical field
Deoiled the present invention relates to textile technology field, especially a kind of mulberry silk fiber and protect the process of glue.
Background technology
Silk is constituted by wrapping up in silk gum outside 2 fibroins, and silk gum weight accounts for 25%, fibroin weight and accounts for 75%, and silk gum is structure
Into silk fiber outer tissue protein, it is wrapped in around two fibroins, protective effect is played to fibroin and silk fiber is bonded
Effect.Silk gum have water solubility, be soluble in hot water, acid, aqueous slkali, and fibroin in water can only part swelling and can not be molten
Solution.On silk product, printing and dyeing practice and the dress of dress ornament for many years prove that content of silk gum can influence the gloss of silk more than 5%,
Silk product easily decolourizes hardened jaundice, and content of silk gum is less than 3%, and silk fiber pulling force is inadequate, the crisp easy fracture of silk, have a strong impact on product
Service life.Silk fiber oil content is more than 0 .5%, and spinnability is poor, easily causes entanglement, adhesion, hardened, drafting.Therefore right
In the refinery practice of mulberry silk fiber, deoil（Oil content is controlled in 0 below .5%）Protect glue（Glue fat is retained in 3-5% scopes
It is interior）It is extremely important.
Silk spinning raw material can be divided into three major types：Spoiled cocoon, bar Tuhe basinetto silk, spoiled cocoon are mainly Shuan Gong, Chai Yin, oily rotten cocoon etc., this
Class cocoon fat content is high, silk fiber severe contamination, is available for the silk fiber of silk spinning there was only 30%；Practice folding general 40% or so；Bar
Tell be reeling mill byproduct, be to be formed through manual tension by beating sleave out in silk reeling process, bar general 1-1 .5 long
Rice or so, two ends slightly have indivedual extension cocoons, practice folding general 80% or so, and basinetto silk is the left pelettes of reeling mill, through basinetto silk mechanism piece
Form, above with broken rotten silkworm chrysalis, glue fat is extremely weighed, practice one class of folding 50% or so.Just because of silk spinning raw material species is a lot, fibroin with
Content of silk gum is differed again, there is very big difference on refining process.No matter but what silk spinning raw material, biography general at present
Refining production technology of uniting all is directly boiling, directly practicing after biology is degenerated, the difference is that height, the length of action time of kiering liquid temperature
Short, chemical industry dosage use number with proportioning ratio it is different.According to incompletely statistics, the silkworm spoiled cocoon of the annual production in the whole nation is in 5-
60000 tons, mulberry shoot is told, 50,000 tons of basinetto silk agreement that contracts a film or TV play to an actor or actress.Therefore being told to silk spinning raw material spoiled cocoon, bar, in the refinery practice of basinetto silk, in removal
On the premise of grease（Oil content is controlled in 0 below .5%）, how glue fat could be retained in the range of 3-5%, silk fiber
The grease difficulty fat that removes photoresist is difficult to ensure the technical barrier of always silk spinning production.
The content of the invention
The present invention provides the process that a kind of mulberry silk fiber deoils guarantor's glue, and it can be solved under to silk spinning raw material
Cocoon, bar are told, in the refinery practice of basinetto silk, on the premise of grease is removed（Oil content is controlled in 0 below .5%）, how could
Glue fat is retained in the problem in the range of 3-5%.
In order to solve the above problems, the technical solution adopted in the present invention is：This mulberry silk fiber deoils and protects the work of glue
Process, comprises the following steps：
A, solid glue silk：Mulberry silk is put into baking oven, 50 DEG C~65 DEG C constant temperature 20 hours~26 hours；Taking-up is then placed in percentage
Specific concentration be 0.1%~1% glutaraldehyde water solution in soak 1 hour~24 hours, soaking temperature be 0 DEG C~50 DEG C；Then use
Clear water is rinsed, and places into drying in 50 DEG C~65 DEG C baking ovens；
Refined at the beginning of B, softened water：Step A gained mulberry silks are immersed in 90 DEG C~105 DEG C of the water for being mixed with sodium carbonate and detergent
5 minutes~15 minutes in solution, wherein the percent concentration of sodium carbonate is 0.01%~0.05%, and the percent concentration of detergent is
0.005%~0.025%；Then rinse well and dewatered and washed point；
C, biological corruption：Step B gained mulberry silks are put into and are mixed with 35 DEG C~38 DEG C in the aqueous solution of sodium carbonate and Lamepon A
Constant temperature immersion corruption 48 hours~96 hours, the wherein percent concentration of sodium carbonate are 0.01%~0.05%, the percentage of Lamepon A
Specific concentration is 0.02%~0.01%, and regulation pH value is 8.5~9.5；Then rinse well and dewatered and washed point；
D, cocoon cooking：Add cocoon cooking aid to carry out cocoon cooking in step C gained mulberry silks to process 1 time~2 times, then rinse well and take off
Solid carbon dioxide point；
E, bleaching：Mulberry silk obtained by step D is put into and is mixed with the Bellmer that sodium carbonate, hydrogen peroxide, sodium metasilicate and pancreas add drift
Carry out bleaching 6 hours~7.5 hours, the percent concentration of sodium carbonate is 0.2%~0.3%, the hundred of hydrogen peroxide in Bellmer
Point specific concentration is 25%~30%, and the percent concentration of sodium metasilicate is 10%~15%, pancreas add the percent concentration of drift for 0.3%~
0.5%, control temperature is at 75 DEG C~85 DEG C；Then rinse well and dewatered and washed point；
F, softening：The cationic softener aqueous solution that mulberry silk obtained by step E is not higher than 4% with concentration is carried out at softening
Reason, it is 4~4.5 to soften pH value；The cationic softener can be various modified mailing polysiloxanes；
G, dewatered drying：Mulberry silk just obtained by step E is rinsed well, dewatered drying to regain is not higher than 10%.
By adopting the above-described technical solution, the present invention has the advantages that compared with prior art：
The present invention first carries out adhering sericin with glutaraldehyde to mulberry silk, and glutaraldehyde belongs to saturated straight chain binary aliphatic aldehyde, contains
Two aldehyde radicals can be good at adding the series crosslinking such as layer with some amino in sericin molecule side base and hydroxyl generation nucleophilic
Reaction, reaches the effect of adhering sericin, and its anchor effect is good, and the protein after crosslinking is refined in general treatment, Bu Huiyin
Play a large amount of molten mistakes of silk gum；And the glutaraldehyde fixing protein of low concentration is separated out without aldehyde, harmless.
Specific embodiment
Below in conjunction with specific embodiment, the invention will be further described：
Embodiment one：
A kind of mulberry silk fiber deoils and protects the process of glue, comprises the following steps：
A, solid glue silk：Mulberry silk is put into baking oven, 60 DEG C or so constant temperature 20 hours；Taking-up is then placed in percent concentration
Soaked 2 hours in 0.1% glutaraldehyde water solution, soaking temperature is 50 DEG C；Then rinsed with clear water, place into 50 DEG C~65 DEG C
Dried in baking oven；
Refined at the beginning of B, softened water：Step A gained mulberry silks are immersed in 90 DEG C~105 DEG C of the water for being mixed with sodium carbonate and detergent
5 minutes in solution, wherein the percent concentration of sodium carbonate is 0.05%, and the percent concentration of detergent is 0.025%；Then rinse
Clean and dewatered and washed point；
C, biological corruption：Step B gained mulberry silks are put into and are mixed with 35 DEG C of constant temperature leachings in the aqueous solution of sodium carbonate and Lamepon A
Bubble corruption 96 hours, the wherein percent concentration of sodium carbonate are 0.01%, and the percent concentration of Lamepon A is 0.02%, adjusts pH
Be worth is 8.5~9.5；Then rinse well and dewatered and washed point；
D, cocoon cooking：By 9 grams of mulberry silk addition perfluorinated sulfonic acid sodium obtained by step C, 1 gram of glacial acetic acid carries out cocoon cooking and processes 1 time, Ran Houchong
Wash clean and dewatered and washed point；
E, bleaching：Mulberry silk obtained by step D is put into and is mixed with the Bellmer that sodium carbonate, hydrogen peroxide, sodium metasilicate and pancreas add drift
Carry out bleaching 6 hours, the percent concentration of sodium carbonate is 0.3% in Bellmer, the percent concentration of hydrogen peroxide is 30%, silicon
The percent concentration of sour sodium is 115%, and pancreas adds the percent concentration of drift to be 0.5%, and control temperature is at 75 DEG C~85 DEG C；Then rinse
Clean and dewatered and washed point；
F, softening：Mulberry silk obtained by step E is carried out into sofening treatment with the amino-modified silicone oil solution of concentration 2%, softens pH value
It is 4；
G, dewatered drying：Mulberry silk just obtained by step E is rinsed well, dewatered drying to regain is not higher than 10%.
Embodiment two：
A kind of mulberry silk fiber deoils and protects the process of glue, comprises the following steps：
A, solid glue silk：Mulberry silk is put into baking oven, 50 DEG C or so constant temperature 26 hours；It is 1% that taking-up is then placed in percent concentration
Glutaraldehyde water solution in soak 24 hours, soaking temperature be 0 DEG C；Then rinsed with clear water, place into 50 DEG C~65 DEG C baking ovens
Middle drying；
Refined at the beginning of B, softened water：Step A gained mulberry silks are immersed in 90 DEG C~105 DEG C of the water for being mixed with sodium carbonate and detergent
15 minutes in solution, wherein the percent concentration of sodium carbonate is 0.01%, and the percent concentration of detergent is 0.005%；Then rush
Wash clean and dewatered and washed point；
C, biological corruption：Step B gained mulberry silks are put into and are mixed with 38 DEG C of constant temperature leachings in the aqueous solution of sodium carbonate and Lamepon A
Bubble corruption 48 hours, the wherein percent concentration of sodium carbonate are 0.05%, and the percent concentration of Lamepon A is 0.01%, adjusts pH
Be worth is 8.5~9.5；Then rinse well and dewatered and washed point；
D, cocoon cooking：Add cocoon cooking aid to carry out cocoon cooking in step C gained mulberry silks to process 1 time~2 times, then rinse well and take off
Solid carbon dioxide point；
E, bleaching：Mulberry silk obtained by step D is put into and is mixed with the Bellmer that sodium carbonate, hydrogen peroxide, sodium metasilicate and pancreas add drift
Carry out bleaching 7.5 hours, the percent concentration of sodium carbonate is 0.2% in Bellmer, the percent concentration of hydrogen peroxide is 25%,
The percent concentration of sodium metasilicate is 10%, and pancreas adds the percent concentration of drift to be 0.3%, and control temperature is at 75 DEG C~85 DEG C；Then rush
Wash clean and dewatered and washed point；
F, softening：Mulberry silk obtained by step E is carried out into sofening treatment with the amino-modified silicone oil solution of concentration 3%, softens pH value
It is 4；The cationic softener can be various modified mailing polysiloxanes；
G, dewatered drying：Mulberry silk just obtained by step E is rinsed well, dewatered drying to regain is not higher than 10%.
After measured, content of silk gum reaches more than 3.7% to the treated mulberry silk of embodiment one and two, and fat content is no more than
0.42%。
Claims (1)
1. a kind of mulberry silk fiber deoils and protects the process of glue, it is characterised in that comprise the following steps：
A, solid glue silk：Mulberry silk is put into baking oven, 50 DEG C~65 DEG C constant temperature 20 hours~26 hours；Taking-up is then placed in percentage
Specific concentration be 0.1%~1% glutaraldehyde water solution in soak 1 hour~24 hours, soaking temperature be 0 DEG C~50 DEG C；Then use
Clear water is rinsed, and places into drying in 50 DEG C~65 DEG C baking ovens；
Refined at the beginning of B, softened water：Step A gained mulberry silks are immersed in 90 DEG C~105 DEG C of the water for being mixed with sodium carbonate and detergent
5 minutes~15 minutes in solution, wherein the percent concentration of sodium carbonate is 0.01%~0.05%, and the percent concentration of detergent is
0.005%~0.025%；Then rinse well and dewatered and washed point；
C, biological corruption：Step B gained mulberry silks are put into and are mixed with 35 DEG C~38 DEG C in the aqueous solution of sodium carbonate and Lamepon A
Constant temperature immersion corruption 48 hours~96 hours, wherein wherein the percent concentration of sodium carbonate is 0.01%~0.05%, Lamepon A
Percent concentration is 0.02%~0.01%, and regulation pH value is 8.5~9.5；Then rinse well and dewatered and washed point；
D, cocoon cooking：Add cocoon cooking aid to carry out cocoon cooking in step C gained mulberry silks to process 1 time~2 times, then rinse well and take off
Solid carbon dioxide point；
E, bleaching：Mulberry silk obtained by step D is put into and is mixed with the Bellmer that sodium carbonate, hydrogen peroxide, sodium metasilicate and pancreas add drift
Carry out bleaching 6 hours~7.5 hours, the percent concentration of sodium carbonate is 0.2%~0.3%, the hundred of hydrogen peroxide in Bellmer
Point specific concentration is 25%~30%, and the percent concentration of sodium metasilicate is 10%~15%, pancreas add the percent concentration of drift for 0.3%~
0.5%, control temperature is at 75 DEG C~85 DEG C；Then rinse well and dewatered and washed point；
F, softening：The cationic softener aqueous solution that mulberry silk obtained by step E is not higher than 4% with concentration is carried out at softening
Reason, it is 4~4.5 to soften pH value；
G, dewatered drying：Mulberry silk just obtained by step E is rinsed well, dewatered drying to regain is not higher than 10%.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201611141156.7A CN106758191A (en) | 2016-12-12 | 2016-12-12 | Mulberry silk fiber deoils and protects the process of glue |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201611141156.7A CN106758191A (en) | 2016-12-12 | 2016-12-12 | Mulberry silk fiber deoils and protects the process of glue |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| CN106758191A true CN106758191A (en) | 2017-05-31 |
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Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN201611141156.7A Pending CN106758191A (en) | 2016-12-12 | 2016-12-12 | Mulberry silk fiber deoils and protects the process of glue |
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Cited By (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN111809283A (en) * | 2020-07-16 | 2020-10-23 | 苏州市星京泽纤维科技有限公司 | Blended yarn for deep development of silkworm mulberry and spinning process |
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|---|---|---|---|---|
| CN1563520A (en) * | 2004-03-17 | 2005-01-12 | 席星航 | Technical method for fabricating refined waste silk of silk spinning through softening solid glue on blaze silk |
| CN102031569A (en) * | 2010-11-16 | 2011-04-27 | 席星航 | Method for producing silk glue-enriched silk spinning refined waste silk |
| CN102605438A (en) * | 2012-04-05 | 2012-07-25 | 常德诺雅蚕丝制品有限公司 | Manufacture method of washable mulberry silkworm long silk floss with high sericin content |
| CN102936757A (en) * | 2012-11-16 | 2013-02-20 | 南阳市民兴茧丝绸有限责任公司 | Refining technology of silkworm oil rotten cocoons |
| CN104223527A (en) * | 2014-09-03 | 2014-12-24 | 苏州印丝特纺织数码科技有限公司 | Manufacturing method for puncture-proof protective fabric containing silk |
| CN104611771A (en) * | 2015-01-19 | 2015-05-13 | 河南省民兴茧丝绸有限责任公司 | Mulberry silk fiber oil removing and adhesive preserving process |
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2016
- 2016-12-12 CN CN201611141156.7A patent/CN106758191A/en active Pending
Patent Citations (6)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN1563520A (en) * | 2004-03-17 | 2005-01-12 | 席星航 | Technical method for fabricating refined waste silk of silk spinning through softening solid glue on blaze silk |
| CN102031569A (en) * | 2010-11-16 | 2011-04-27 | 席星航 | Method for producing silk glue-enriched silk spinning refined waste silk |
| CN102605438A (en) * | 2012-04-05 | 2012-07-25 | 常德诺雅蚕丝制品有限公司 | Manufacture method of washable mulberry silkworm long silk floss with high sericin content |
| CN102936757A (en) * | 2012-11-16 | 2013-02-20 | 南阳市民兴茧丝绸有限责任公司 | Refining technology of silkworm oil rotten cocoons |
| CN104223527A (en) * | 2014-09-03 | 2014-12-24 | 苏州印丝特纺织数码科技有限公司 | Manufacturing method for puncture-proof protective fabric containing silk |
| CN104611771A (en) * | 2015-01-19 | 2015-05-13 | 河南省民兴茧丝绸有限责任公司 | Mulberry silk fiber oil removing and adhesive preserving process |
Non-Patent Citations (1)
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Cited By (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN111809283A (en) * | 2020-07-16 | 2020-10-23 | 苏州市星京泽纤维科技有限公司 | Blended yarn for deep development of silkworm mulberry and spinning process |
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