CN106753872B - Cleaning fluid for cleaning and recovering healing abutment and using method thereof - Google Patents
Cleaning fluid for cleaning and recovering healing abutment and using method thereof Download PDFInfo
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- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
- C11D1/00—Detergent compositions based essentially on surface-active compounds; Use of these compounds as a detergent
- C11D1/66—Non-ionic compounds
- C11D1/83—Mixtures of non-ionic with anionic compounds
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61L—METHODS OR APPARATUS FOR STERILISING MATERIALS OR OBJECTS IN GENERAL; DISINFECTION, STERILISATION OR DEODORISATION OF AIR; CHEMICAL ASPECTS OF BANDAGES, DRESSINGS, ABSORBENT PADS OR SURGICAL ARTICLES; MATERIALS FOR BANDAGES, DRESSINGS, ABSORBENT PADS OR SURGICAL ARTICLES
- A61L2/00—Methods or apparatus for disinfecting or sterilising materials or objects other than foodstuffs or contact lenses; Accessories therefor
- A61L2/02—Methods or apparatus for disinfecting or sterilising materials or objects other than foodstuffs or contact lenses; Accessories therefor using physical phenomena
- A61L2/04—Heat
- A61L2/06—Hot gas
- A61L2/07—Steam
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- B—PERFORMING OPERATIONS; TRANSPORTING
- B08—CLEANING
- B08B—CLEANING IN GENERAL; PREVENTION OF FOULING IN GENERAL
- B08B3/00—Cleaning by methods involving the use or presence of liquid or steam
- B08B3/04—Cleaning involving contact with liquid
- B08B3/08—Cleaning involving contact with liquid the liquid having chemical or dissolving effect
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- C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
- C11D3/00—Other compounding ingredients of detergent compositions covered in group C11D1/00
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- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
- C11D3/00—Other compounding ingredients of detergent compositions covered in group C11D1/00
- C11D3/02—Inorganic compounds ; Elemental compounds
- C11D3/04—Water-soluble compounds
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- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
- C11D3/00—Other compounding ingredients of detergent compositions covered in group C11D1/00
- C11D3/02—Inorganic compounds ; Elemental compounds
- C11D3/04—Water-soluble compounds
- C11D3/046—Salts
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- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
- C11D3/00—Other compounding ingredients of detergent compositions covered in group C11D1/00
- C11D3/02—Inorganic compounds ; Elemental compounds
- C11D3/12—Water-insoluble compounds
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- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
- C11D3/00—Other compounding ingredients of detergent compositions covered in group C11D1/00
- C11D3/16—Organic compounds
- C11D3/20—Organic compounds containing oxygen
- C11D3/2003—Alcohols; Phenols
- C11D3/2006—Monohydric alcohols
- C11D3/201—Monohydric alcohols linear
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- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
- C11D3/00—Other compounding ingredients of detergent compositions covered in group C11D1/00
- C11D3/16—Organic compounds
- C11D3/20—Organic compounds containing oxygen
- C11D3/2003—Alcohols; Phenols
- C11D3/2041—Dihydric alcohols
- C11D3/2044—Dihydric alcohols linear
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- C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
- C11D3/00—Other compounding ingredients of detergent compositions covered in group C11D1/00
- C11D3/16—Organic compounds
- C11D3/20—Organic compounds containing oxygen
- C11D3/2075—Carboxylic acids-salts thereof
- C11D3/2086—Hydroxy carboxylic acids-salts thereof
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- C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
- C11D3/00—Other compounding ingredients of detergent compositions covered in group C11D1/00
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- C11D3/00—Other compounding ingredients of detergent compositions covered in group C11D1/00
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- C11D3/38—Products with no well-defined composition, e.g. natural products
- C11D3/386—Preparations containing enzymes, e.g. protease or amylase
- C11D3/38663—Stabilised liquid enzyme compositions
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- A61L—METHODS OR APPARATUS FOR STERILISING MATERIALS OR OBJECTS IN GENERAL; DISINFECTION, STERILISATION OR DEODORISATION OF AIR; CHEMICAL ASPECTS OF BANDAGES, DRESSINGS, ABSORBENT PADS OR SURGICAL ARTICLES; MATERIALS FOR BANDAGES, DRESSINGS, ABSORBENT PADS OR SURGICAL ARTICLES
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Abstract
The invention provides a cleaning fluid for cleaning and recovering a healing abutment and a using method thereof, and the cleaning fluid comprises a composition 1 and a composition 2 which are used in cooperation. The novel multienzyme cleaning solution and the cleaning process provided by the invention are suitable for the healing abutment which is recycled clinically, the problem that the cleaning effect of the traditional cleaning process on pollutants such as tartar, dental plaque, blood and the like on the surface of the healing abutment is poor is solved, the propagation of germs is avoided, and the novel multienzyme cleaning solution and the cleaning process have the advantages of low cost, safety and good cleaning effect.
Description
Technical Field
The invention designs a cleaning solution and a using method thereof, and particularly relates to a cleaning solution for cleaning and recovering a healing abutment and a using method thereof.
Background
The oral cavity is a complex environment, and plaque and soft scale can form dental calculus after being deposited on saliva and gingival crevicular fluid and can be attached to the surfaces of teeth and restorations.
The healing abutment is a structure which is arranged above an implant and ensures the formation of the appearance of gingival tissue around the implant, and when the healing abutment is exposed in the oral environment, the surface of the healing abutment can be adhered with components such as bacterial plaque, dental calculus, food residues, histiocyte, saliva, gingival crevicular fluid and the like, and blood and the like can be adhered during the process of taking the healing abutment out of the mouth, so the surface pollution components are complex, and the healing abutment has specificity compared with pollutants on other medical instruments.
At present, the cleaning method clinically used for the healing abutment which is recycled is mainly to use multienzyme cleaning agent with neutral or alkaline PH to soak for hours to soften dirt, then to carry out ultrasonic cleaning and rinsing, so that inorganic pollutants containing calcified components on the surface of the healing abutment, such as dental calculus, can not be effectively removed, and the cleaning period is prolonged; the unremoved pollutants on the surface of the healing abutment can reduce the biocompatibility of the healing abutment and influence the adhesion, the extension and the proliferation of the fibroblasts of epithelial cells and connective tissues; the recovery and reuse of the healing abutment by harmful microorganisms contained in the contaminants presents a risk of disease transmission.
Disclosure of Invention
The invention mainly aims to provide a method for cleaning a healing abutment, which aims to solve the problem of cleaning the healing abutment recycled and improve the surface cleanliness of the healing abutment.
In order to achieve the purpose, the specific technical scheme of the invention is as follows:
a cleaning solution for cleaning and recovering healing abutment comprises a composition 1 and a composition 2 which are used in cooperation; the composition 1 consists of citric acid, hydrogen peroxide and deionized water, and the mass ratio of the citric acid to the hydrogen peroxide to the deionized water is 1: 3; the composition 2 comprises the following raw materials in percentage by mass: 1.5 to 2 percent of complex enzyme component; 4-6% of surfactant component; 0.5 to 1 percent of tea saponin; 6 to 7 percent of propylene glycol; 1% -2% of borax; 0.1 to 0.3 percent of anhydrous calcium chloride; 5 to 6 percent of ethanol; 1% -2% of triethanolamine; the balance being deionized water.
The composite enzyme is preferably a composition of (1) alkaline protease, cellulase, α -amylase, fatty triglyceride lipase and mannanase, and (2) the surfactant comprises fatty alcohol-polyoxyethylene ether sodium sulfate and alkyl glycoside in a mass ratio of 1: 1.
Preferably, the ratio of the alkaline protease, the cellulase, the α -amylase, the fatty triglyceride lipase and the mannanase in the complex enzyme is any ratio.
The HIA provided by the invention is a method for cleaning a recovered healing abutment by using the cleaning solution, and the method comprises the following steps: step 1: ultrasonically cleaning the healing abutment with composition 1;
step 2: rinsing and wiping the cleaned healing abutment;
and step 3: ultrasonically cleaning the healing abutment with composition 2;
and 4, step 4: rinsing and wiping the cleaned healing abutment;
and 5: putting the healed base station which is rinsed and wiped dry into a medical drying oven for drying;
step 6: and (5) performing steam sterilization on the dried healing base.
As the preferred items: the temperature of ultrasonic cleaning in the step 1 is 50-60 ℃, and the cleaning time is 15 minutes.
As the preferred items: and rinsing the cleaned healing abutment in the steps 2 and 4, and rinsing the healing abutment at normal temperature by using deionized water for 10 minutes.
As the preferred items: and 3, carrying out ultrasonic cleaning at the temperature of 30-40 ℃ and the pH of 9-11 for 15 minutes.
As the preferred items: and 5, putting the healed base station which is cleaned and wiped dry into a medical drying oven, controlling the drying temperature to be 70-90 ℃ and the drying time to be 20-30 minutes.
The invention provides a novel multienzyme cleaning solution for cleaning a recovered healing abutment and a cleaning process, which aim at the characteristics of pollutants on the surface of the healing abutment and improve the traditional cleaning process. On the basis of a cleaning method mainly based on ultrasonic cleaning by using a traditional multienzyme cleaning agent, the step of ultrasonic cleaning by using citric acid and hydrogen peroxide replaces the long-time multienzyme cleaning liquid soaking treatment process, the citric acid is beneficial to cleaning inorganic pollutants on the surface of a healing abutment, and the hydrogen peroxide has the functions of sterilization, disinfection and decontamination, can form an oxide layer with bioactivity on the surface of the healing abutment, and promotes cell adhesion; meanwhile, a novel multi-enzyme cleaning solution formula, namely a component 2, is provided, and a nonionic surfactant APG and an anionic surfactant AES are used in a composite mode, so that the cleaning agent has the characteristics of higher decontamination capability and easiness in rinsing, and the pollution to the environment is reduced, wherein the tea saponin has the effects of emulsifying, dispersing, foaming, moistening and dissolving red blood cells, and the cleaning effect on organic pollutants such as blood is enhanced. The cleaning process and the novel multienzyme cleaning solution solve the cleaning problem of the healing base station which is recycled, improve the surface cleanliness of the healing base station, shorten the cleaning period and obtain better cleaning effect.
Drawings
Fig. 1 is a picture of a healing abutment retrieved after clinical use;
FIG. 2 is a flow diagram of a typical conventional cleaning procedure employed in a healing abutment;
FIG. 3 is a flow chart of the present invention providing cleaning of a healing abutment;
figure 4 is a photograph of a healing abutment before and after cleaning using the present invention.
Detailed Description
The invention is further illustrated by the following examples and figures.
Example 1
Step 1: ultrasonically cleaning the healing abutment with composition 1; the composition 1 consists of citric acid, hydrogen peroxide and deionized water, and the mass ratio of the citric acid to the hydrogen peroxide to the deionized water is 1: 3;
step 2: rinsing and wiping the cleaned healing abutment;
and step 3: ultrasonically cleaning the healing abutment with composition 2; the composition 2 comprises the following raw materials in percentage by mass: 1.5 percent of complex enzyme component; surfactant component, 6%; 0.5 percent of tea saponin; 7% of propylene glycol; 2% of borax; anhydrous calcium chloride, 0.1% >; 6 percent of ethanol; triethanolamine, 2%; the balance of deionized water;
and 4, step 4: rinsing and wiping the cleaned healing abutment;
and 5: putting the healed base station which is rinsed and wiped dry into a medical drying oven for drying;
step 6: and (5) performing steam sterilization on the dried healing base.
The compound enzyme comprises 20 percent of alkaline protease, 20 percent of cellulase, 20 percent of α -amylase, 20 percent of fatty triglyceride lipase and 20 percent of mannanase by mass percentage;
the surfactant component comprises fatty alcohol-polyoxyethylene ether sodium sulfate and alkyl glycoside in a mass ratio of 1: 1.
The temperature of ultrasonic cleaning in the step 1 is 50-60 ℃, and the cleaning time is 15 minutes.
And rinsing the cleaned healing abutment in the steps 2 and 4, and rinsing the healing abutment at normal temperature by using deionized water for 10 minutes.
And 3, carrying out ultrasonic cleaning at the temperature of 30-40 ℃ and the pH of 9-11 for 15 minutes.
And 5, putting the healed base station which is cleaned and wiped dry into a medical drying oven, controlling the drying temperature to be 70-90 ℃ and the drying time to be 20-30 minutes.
Example 2
Step 1: ultrasonically cleaning the healing abutment with composition 1; the composition 1 consists of citric acid, hydrogen peroxide and deionized water, and the mass ratio of the citric acid to the hydrogen peroxide to the deionized water is 1: 3;
step 2: rinsing and wiping the cleaned healing abutment;
and step 3: ultrasonically cleaning the healing abutment with composition 2; the composition 2 comprises the following raw materials in percentage by mass: complex enzyme component, 2%; surfactant component, 4%; 1% of tea saponin; 6% of propylene glycol; 2% of borax; 0.1 percent of anhydrous calcium chloride; 6 percent of ethanol; triethanolamine, 2%; the balance of deionized water;
and 4, step 4: rinsing and wiping the cleaned healing abutment;
and 5: putting the healed base station which is rinsed and wiped dry into a medical drying oven for drying;
step 6: and (5) performing steam sterilization on the dried healing base.
The compound enzyme comprises 15% of alkaline protease, 30% of cellulase, 19% of α -amylase, 25% of fatty triglyceride lipase and 11% of mannanase by mass percentage;
the surfactant component comprises fatty alcohol-polyoxyethylene ether sodium sulfate and alkyl glycoside in a mass ratio of 1: 1.
The temperature of ultrasonic cleaning in the step 1 is 50-60 ℃, and the cleaning time is 15 minutes.
And rinsing the cleaned healing abutment in the steps 2 and 4, and rinsing the healing abutment at normal temperature by using deionized water for 10 minutes.
And 3, carrying out ultrasonic cleaning at the temperature of 30-40 ℃ and the pH of 9-11 for 15 minutes.
And 5, putting the healed base station which is cleaned and wiped dry into a medical drying oven, controlling the drying temperature to be 70-90 ℃ and the drying time to be 20-30 minutes.
Fig. 1 is a picture of a healing abutment recovered after clinical use, and it can be seen from fig. 1 that there are a large amount of inorganic calcifications, such as dental calculus, on the surface of the healing abutment after clinical use.
Fig. 2 is a flow chart of a typical conventional cleaning method applied to a healing abutment, as can be seen from fig. 1, in the conventional cleaning process, mainly ultrasonic cleaning and rinsing after soaking for several hours in a multienzyme cleaning agent having a neutral or alkaline PH to soften dirt, inorganic contaminants containing calcified components, such as dental calculus, on the surface of the healing abutment cannot be effectively removed, and the cleaning cycle is lengthened.
Fig. 3 is a flow chart of cleaning the healing abutment provided by the present invention, which is an improvement of the conventional cleaning process according to the characteristics of the contamination on the surface of the healing abutment. On the basis of a cleaning method mainly based on ultrasonic cleaning by using a traditional multienzyme cleaning agent, the step of ultrasonic cleaning by using citric acid and hydrogen peroxide replaces the long-time multienzyme cleaning liquid soaking treatment process, the citric acid is beneficial to cleaning inorganic pollutants on the surface of a healing abutment, and the hydrogen peroxide has the functions of sterilization, disinfection and decontamination, can form an oxide layer with bioactivity on the surface of the healing abutment, and promotes cell adhesion; the tea saponin cleaning liquid has the characteristics of stronger decontamination capability and easy rinsing, and reduces the pollution to the environment by adopting the nonionic surfactant APG and the anionic surfactant AES in a composite way, wherein the tea saponin has the functions of emulsifying, dispersing, foaming, wetting and dissolving red blood cells, and the cleaning effect on organic pollutants such as blood is enhanced. The cleaning process and the novel multienzyme cleaning solution solve the cleaning problem of the healing base station which is recycled, improve the surface cleanliness of the healing base station, shorten the cleaning period and obtain better cleaning effect.
The healing abutment is cleaned by citric acid, hydrogen peroxide, multienzyme cleaning liquid and an ultrasonic cleaning method, and physical and chemical methods are comprehensively utilized for cleaning, so that the surface cleanliness of the healing abutment is effectively improved.
Fig. 4 is a picture of a healing abutment before and after cleaning according to the present invention, as shown in fig. 4. As can be seen from FIG. 4, after the healing abutment is cleaned by the cleaning method provided by the invention, pollutants are obviously reduced, and the cleanliness is improved, so that the cleaning method provided by the invention has a good cleaning effect and high cleanliness.
It should be understood that parts of the specification not set forth in detail are well within the prior art.
It should be understood that the above description of the preferred embodiments is given for clarity and not for any purpose of limitation, and that various changes, substitutions and alterations can be made herein without departing from the spirit and scope of the invention as defined by the appended claims.
Claims (5)
1. The utility model provides a wash and retrieve washing liquid for healing base station which characterized in that: comprises a composition 1 and a composition 2 which are used in a matching way; the composition 1 consists of citric acid, hydrogen peroxide and deionized water, and the mass ratio of the citric acid to the hydrogen peroxide to the deionized water is 1: 3; the composition 2 comprises the following raw materials in percentage by mass: 1.5 to 2 percent of complex enzyme component; 4-6% of surfactant component; 0.5 to 1 percent of tea saponin; 6 to 7 percent of propylene glycol; 1% -2% of borax; 0.1 to 0.3 percent of anhydrous calcium chloride; 5 to 6 percent of ethanol; 1% -2% of triethanolamine; the balance being deionized water.
The cleaning solution is characterized in that (1) the complex enzyme is a composition of alkaline protease, cellulase, α -amylase, fatty triglyceride lipase and mannase, and (2) the surfactant is composed of fatty alcohol-polyoxyethylene ether sodium sulfate and alkyl glycoside in a mass ratio of 1: 1.
The alkaline protease, the cellulase, the α -amylase, the fatty triglyceride lipase and the mannase in the compound enzyme are in any ratio.
2. A method of cleaning a recovered healing abutment using the cleaning solution of claim 1, wherein: the method comprises the following steps: step 1: ultrasonically cleaning the healing abutment with composition 1;
step 2: rinsing and wiping the cleaned healing abutment;
and step 3: ultrasonically cleaning the healing abutment with composition 2;
and 4, step 4: rinsing and wiping the cleaned healing abutment;
and 5: putting the healed base station which is rinsed and wiped dry into a medical drying oven for drying;
step 6: and (5) performing steam sterilization on the dried healing base.
And 5, putting the healed base station which is cleaned and wiped dry into a medical drying oven, controlling the drying temperature to be 70-90 ℃ and the drying time to be 20-30 minutes.
3. The method of claim 2, wherein: the temperature of ultrasonic cleaning in the step 1 is 50-60 ℃, and the cleaning time is 15 minutes.
4. The method of claim 2, wherein: and rinsing the cleaned healing abutment in the steps 2 and 4, and rinsing the healing abutment at normal temperature by using deionized water for 10 minutes.
5. The method according to claim 2, wherein the ultrasonic cleaning in step 3 is carried out at a temperature of 30 to 40 ℃ and a pH of 9 to 11 for 15 minutes.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201710004747.8A CN106753872B (en) | 2017-01-04 | 2017-01-04 | Cleaning fluid for cleaning and recovering healing abutment and using method thereof |
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| Application Number | Priority Date | Filing Date | Title |
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| CN201710004747.8A CN106753872B (en) | 2017-01-04 | 2017-01-04 | Cleaning fluid for cleaning and recovering healing abutment and using method thereof |
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| CN106753872A CN106753872A (en) | 2017-05-31 |
| CN106753872B true CN106753872B (en) | 2020-05-26 |
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| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US5489531A (en) * | 1990-10-15 | 1996-02-06 | E. R. Squibb And Sons, Inc. | Combined two stage method for cleaning and decontaminating surgical instruments |
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|---|---|---|---|---|
| CN1339959A (en) * | 1999-03-26 | 2002-03-13 | 前技术专业产品公司 | Anticmicrobial denture cleaning compositions |
| CN1509704A (en) * | 2002-12-25 | 2004-07-07 | 朱素真 | Artificial tooth cleaning agent |
| CN101428281A (en) * | 2007-11-08 | 2009-05-13 | 上海市卢湾区东南医院 | Method for cleaning artificial tooth with ultrasonic |
| CN107184414A (en) * | 2017-05-11 | 2017-09-22 | 江苏苏沃尚新材料科技有限公司 | A kind of artificial tooth cleaning agent |
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| 离体牙结石溶解性的研究;李晓晔等;《实用口腔医学杂志》;19981231;第14卷(第4期);第279-280页 * |
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