CN106745358A - A kind of heavy metal-polluted water treatment agent and preparation method thereof - Google Patents
A kind of heavy metal-polluted water treatment agent and preparation method thereof Download PDFInfo
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- CN106745358A CN106745358A CN201611048609.1A CN201611048609A CN106745358A CN 106745358 A CN106745358 A CN 106745358A CN 201611048609 A CN201611048609 A CN 201611048609A CN 106745358 A CN106745358 A CN 106745358A
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- heavy metal
- treatment agent
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- C—CHEMISTRY; METALLURGY
- C02—TREATMENT OF WATER, WASTE WATER, SEWAGE, OR SLUDGE
- C02F—TREATMENT OF WATER, WASTE WATER, SEWAGE, OR SLUDGE
- C02F1/00—Treatment of water, waste water, or sewage
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- C—CHEMISTRY; METALLURGY
- C02—TREATMENT OF WATER, WASTE WATER, SEWAGE, OR SLUDGE
- C02F—TREATMENT OF WATER, WASTE WATER, SEWAGE, OR SLUDGE
- C02F1/00—Treatment of water, waste water, or sewage
- C02F1/52—Treatment of water, waste water, or sewage by flocculation or precipitation of suspended impurities
-
- C—CHEMISTRY; METALLURGY
- C02—TREATMENT OF WATER, WASTE WATER, SEWAGE, OR SLUDGE
- C02F—TREATMENT OF WATER, WASTE WATER, SEWAGE, OR SLUDGE
- C02F2101/00—Nature of the contaminant
- C02F2101/10—Inorganic compounds
- C02F2101/20—Heavy metals or heavy metal compounds
Abstract
Component the invention discloses a kind of heavy metal-polluted water treatment agent and preparation method thereof, including following parts by weight is constituted:15 25 parts of Sodium Polyacrylate, 10 30 parts of aluminum sulfate, 10 15 parts of iron chloride, 20 25 parts of activated sludge, 5 10 parts of tealeaves, 5 10 parts of sodium alginate, 13 parts of plant ash, 70 200 parts of deionized water.Many kinds of metal ions in the heavy metal-polluted water treatment agent heavy metal sewage has good clearance, and governance efficiency is high;And stable performance, sedimentation effect is good, and effluent quality is good, and processing method is simple, and processing cost is low;It is non-toxic and the heavy metal-polluted water treatment agent purity is high, on operator without influence, do not result in biological pollution and secondary pollution problem.
Description
Technical field
The present invention relates to technical field of sewage, specifically a kind of heavy metal-polluted water treatment agent and preparation method thereof.
Background technology
Heavy metal wastewater thereby refers to discharge in the industrial processes such as mining and metallurgy, machine-building, chemical industry, electronics, instrument containing weight
The waste water of metal.Heavy metal wastewater thereby is arranged essentially from enterprises such as mine, smelting, electrolysis, plating, agricultural chemicals, medicine, paint, pigment
The waste water for going out.The species of heavy metal in waste water, content and existing forms are different with different manufacturing enterprises.Heavy metal wastewater thereby is to one
One of environmental pollution most serious and the industrial wastewater maximum to mankind's harm, its water quality and quantity is relevant with production technology.In waste water
Heavy metal can not typically decompose destruction, can only shift its existence position and change its Material Form.Heavy metal pollution and other
The pollution of organic compound is different.Many organic compounds can be by the net of nature physics, chemistry or biology in itself
Change, make harmfulness reduction or release.And heavy metal has enriching, it is difficult to degrade in the environment.Current China is due in a huge sum of money
In exploitation, smelting, the process of category, many heavy metals such as lead, mercury, cadmium, cobalt etc. is caused to cause sternly into big gas and water, soil
The environmental pollution of weight.The heavy metal such as discharged with useless heavy metal mercury water, even if concentration is small, can also accumulate in algae and bed mud
It is tired, adsorbed by fish and shellfish body surface, food chain concentration is produced, so as to cause public hazards.Metal is favourable in water body or harmful not only takes
Depending on the species of metal, physicochemical property, but also concentration and the valence state of presence and form depending on metal, even if beneficial
Metallic element concentration also has violent toxicity more than a certain numerical value, animals and plants is poisoned, or even dead.
At present, countries in the world process for treating heavy-metal waste water mainly has three classes:The first kind is that heavy metal ions in wastewater is led to
Cross and the method that chemical reaction is removed occurs, including neutralization precipitation method, sulphide precipitation, ferrite coprecipitation, electronation
Method, electrochemical reducing and high molecular heavy metals trapping agent method etc., but this method reaction time is more long, governance efficiency compared with
It is low;Equations of The Second Kind is the side for making the heavy metal in waste water be adsorbed under conditions of its chemical form is not changed, concentrated, be separate
Method, including absorption, solvent extraction, evaporation and freezing method, ion exchange and UF membrane etc., complex treatment process, treatment cost compared with
It is high;3rd class is the method by the effect removal heavy metal in waste water such as flocculation, absorption, accumulation, enrichment of microorganism or plant,
Including bioflocculation, biochemical process and plant ecological repair etc., this method exist high cost, technology it is immature, hold
Easily cause the shortcoming of biological pollution.Therefore, in the urgent need to a kind of governance efficiency is high, low cost, administering method are simple, do not result in
The heavy metal-polluted water treatment agent of biological pollution.
The content of the invention
It is an object of the invention to provide a kind of heavy metal-polluted water treatment agent and preparation method thereof, to solve above-mentioned background skill
The problem proposed in art.
To achieve the above object, the present invention provides following technical scheme:
A kind of heavy metal-polluted water treatment agent, including the component of following parts by weight is constituted:Sodium Polyacrylate 15-25 parts, aluminum sulfate
10-30 parts, iron chloride 10-15 parts, activated sludge 20-25 parts, tealeaves 5-10 parts, sodium alginate 5-10 parts, plant ash 1-3 parts,
Deionized water 70-200 parts.
As further scheme of the invention:Component composition including following parts by weight:22 parts of Sodium Polyacrylate, sulfuric acid
25 parts of aluminium, 13 parts of iron chloride, 22 parts of activated sludge, 9 parts of tealeaves, 6 parts of sodium alginate, 2 parts of plant ash, 90 parts of deionized water.
A kind of preparation method of heavy metal-polluted water treatment agent, concretely comprises the following steps:(1)It is first according to parts by weight and weighs poly- third
Olefin(e) acid sodium, aluminum sulfate, iron chloride, activated sludge, tealeaves, sodium alginate, plant ash, it is standby;(2)By activated sludge, tealeaves, grass
Wood ash is added in pulverizer, and it is 80-110 mesh powder to crush, standby;(3)Sodium Polyacrylate, aluminum sulfate, iron chloride are added and gone
In ionized water, using vibration of ultrasonic wave 15-20 minutes, mixed liquor I is obtained;(4)Sodium alginate, and side are added in mixed liquor I
The stirring of addition side, obtains mixed liquor II;(5)Above-mentioned powder is added in mixed liquor II, is stirred 10-15 minutes, using ultrasound
Ripple shakes 5-10 minutes, gets product.
As further scheme of the invention:The step(2)Activated sludge, tealeaves, plant ash are added into pulverizer
In, it is 90 mesh powder to crush.
As further scheme of the invention:The step(3)Sodium Polyacrylate, aluminum sulfate, iron chloride are added and gone
In ionized water, using vibration of ultrasonic wave 16 minutes, mixed liquor I is obtained.
As further scheme of the invention:The step(5)Above-mentioned powder is added in mixed liquor II, stirring 12
Minute, using vibration of ultrasonic wave 8 minutes.
Compared with prior art, the beneficial effects of the invention are as follows:
The heavy metal-polluted water treatment agent is compounded by above-mentioned raw materials, plays synergy, can capture the various metals in water body
Many kinds of metal ions in ion, and heavy metal sewage has good clearance, and governance efficiency is high;Heavy metal of the invention
Sewage-treating agent treatment effect is good, and stable performance, sedimentation effect is good, and effluent quality is good;And processing method is simple, is using
When, only need to be by the dirty inorganic agent input water, processing cost is low;Sewage after treatment can reach discharge standard, floc sedimentation
Intensity is high, and hydrophobic performance is good;Heavy metal-polluted water treatment agent purity of the invention is high, non-toxic, on operator without influence, will not
Cause biological pollution and secondary pollution problem.
Specific embodiment
The technical scheme of this patent is described in more detail with reference to specific embodiment.
Embodiment 1
A kind of preparation method of heavy metal-polluted water treatment agent, concretely comprises the following steps:(1)It is first according to parts by weight and weighs polyacrylic acid
15 parts of sodium, 10 parts of aluminum sulfate, 10 parts of iron chloride, 20 parts of activated sludge, 5 parts of tealeaves, 5 parts of sodium alginate, 1 part of plant ash, go from
70 parts of sub- water, it is standby;(2)By in activated sludge, tealeaves, plant ash addition pulverizer, it is 80 mesh powder to crush, standby;(3)Will
Sodium Polyacrylate, aluminum sulfate, iron chloride are added in deionized water, using vibration of ultrasonic wave 15 minutes, obtain mixed liquor I;(4)
Sodium alginate is added in mixed liquor I, and is stirred in addition, obtain mixed liquor II;(5)Above-mentioned powder is added to mixed liquor II
In, stir 10 minutes, using vibration of ultrasonic wave 5 minutes, get product.
Embodiment 2
A kind of preparation method of heavy metal-polluted water treatment agent, concretely comprises the following steps:(1)It is first according to parts by weight and weighs polyacrylic acid
25 parts of sodium, 30 parts of aluminum sulfate, 15 parts of iron chloride, 25 parts of activated sludge, 10 parts of tealeaves, 10 parts of sodium alginate, 3 parts of plant ash, go
200 parts of ionized water, it is standby;(2)By in activated sludge, tealeaves, plant ash addition pulverizer, it is 110 mesh powder to crush, standby;
(3)During Sodium Polyacrylate, aluminum sulfate, iron chloride added into deionized water, using vibration of ultrasonic wave 20 minutes, mixed liquor I is obtained;
(4)Sodium alginate is added in mixed liquor I, and is stirred in addition, obtain mixed liquor II;(5)Above-mentioned powder is added to mixed
Close in liquid II, stir 15 minutes, using vibration of ultrasonic wave 10 minutes, get product.
Embodiment 3
A kind of preparation method of heavy metal-polluted water treatment agent, concretely comprises the following steps:(1)It is first according to parts by weight and weighs polyacrylic acid
22 parts of sodium, 25 parts of aluminum sulfate, 13 parts of iron chloride, 22 parts of activated sludge, 9 parts of tealeaves, 6 parts of sodium alginate, 2 parts of plant ash, go from
90 parts of sub- water, it is standby;(2)By in activated sludge, tealeaves, plant ash addition pulverizer, it is 90 mesh powder to crush, standby;(3)Will
Sodium Polyacrylate, aluminum sulfate, iron chloride are added in deionized water, using vibration of ultrasonic wave 16 minutes, obtain mixed liquor I;(4)
Sodium alginate is added in mixed liquor I, and is stirred in addition, obtain mixed liquor II;(5)Above-mentioned powder is added to mixed liquor II
In, stir 12 minutes, using vibration of ultrasonic wave 8 minutes, get product.
Embodiment 4
A kind of preparation method of heavy metal-polluted water treatment agent, concretely comprises the following steps:(1)It is first according to parts by weight and weighs polyacrylic acid
18 parts of sodium, 19 parts of aluminum sulfate, 14 parts of iron chloride, 24 parts of activated sludge, 7 parts of tealeaves, 8 parts of sodium alginate, 2 parts of plant ash, go from
180 parts of sub- water, it is standby;(2)By in activated sludge, tealeaves, plant ash addition pulverizer, it is 100 mesh powder to crush, standby;(3)
During Sodium Polyacrylate, aluminum sulfate, iron chloride added into deionized water, using vibration of ultrasonic wave 16 minutes, mixed liquor I is obtained;(4)
Sodium alginate is added in mixed liquor I, and is stirred in addition, obtain mixed liquor II;(5)Above-mentioned powder is added to mixed liquor
In II, stir 12 minutes, using vibration of ultrasonic wave 9 minutes, get product.
Embodiment 5
A kind of preparation method of heavy metal-polluted water treatment agent, concretely comprises the following steps:(1)It is first according to parts by weight and weighs polyacrylic acid
16 parts of sodium, 29 parts of aluminum sulfate, 12 parts of iron chloride, 24 parts of activated sludge, 9 parts of tealeaves, 6 parts of sodium alginate, 2 parts of plant ash, go from
155 parts of sub- water, it is standby;(2)By in activated sludge, tealeaves, plant ash addition pulverizer, it is 90 mesh powder to crush, standby;(3)
During Sodium Polyacrylate, aluminum sulfate, iron chloride added into deionized water, using vibration of ultrasonic wave 19 minutes, mixed liquor I is obtained;(4)
Sodium alginate is added in mixed liquor I, and is stirred in addition, obtain mixed liquor II;(5)Above-mentioned powder is added to mixed liquor
In II, stir 13 minutes, using vibration of ultrasonic wave 6 minutes, get product.
Comparative example 1
A kind of preparation method of heavy metal-polluted water treatment agent, concretely comprises the following steps:(1)It is first according to parts by weight and weighs polyacrylic acid
22 parts of sodium, 25 parts of aluminum sulfate, 13 parts of iron chloride, 22 parts of activated sludge, 2 parts of plant ash, 90 parts of deionized water, it is standby;(2)Will be living
Property sludge, plant ash add pulverizer in, it is 90 mesh powder to crush, standby;(3)Sodium Polyacrylate, aluminum sulfate, iron chloride are added
In entering deionized water, using vibration of ultrasonic wave 16 minutes, mixed liquor is obtained;(4)Above-mentioned powder is added in mixed liquor, is stirred
12 minutes, using vibration of ultrasonic wave 8 minutes, get product.
Comparative example 2
A kind of preparation method of heavy metal-polluted water treatment agent, concretely comprises the following steps:(1)It is first according to parts by weight and weighs polyacrylic acid
22 parts of sodium, 25 parts of aluminum sulfate, 13 parts of iron chloride, 22 parts of activated sludge, 6 parts of sodium alginate, 2 parts of plant ash, 90 parts of deionized water,
It is standby;(2)By in activated sludge, plant ash addition pulverizer, it is 90 mesh powder to crush, standby;(3)By Sodium Polyacrylate, sulphur
Sour aluminium, iron chloride are added in deionized water, using vibration of ultrasonic wave 16 minutes, obtain mixed liquor I;(4)Added in mixed liquor I
Sodium alginate, and stirred in addition, obtain mixed liquor II;(5)Above-mentioned powder is added in mixed liquor II, 12 points are stirred
Clock, using vibration of ultrasonic wave 8 minutes, gets product.
Comparative example 3
A kind of preparation method of heavy metal-polluted water treatment agent, concretely comprises the following steps:(1)It is first according to parts by weight and weighs polyacrylic acid
22 parts of sodium, 25 parts of aluminum sulfate, 13 parts of iron chloride, 22 parts of activated sludge, 9 parts of tealeaves, 2 parts of plant ash, 90 parts of deionized water, it is standby
With;(2)By in activated sludge, tealeaves, plant ash addition pulverizer, it is 90 mesh powder to crush, standby;(3)By Sodium Polyacrylate,
Aluminum sulfate, iron chloride are added in deionized water, using vibration of ultrasonic wave 16 minutes, obtain mixed liquor;(4)By the addition of above-mentioned powder
To in mixed liquor, stir 12 minutes, using vibration of ultrasonic wave 8 minutes, get product.
First, test method
The finished product being made of embodiment 1-5 and comparative example 1-3 carries out heavy metal-polluted water process, and water quality situation is such as after sewage disposal
Shown in following table:(Unit:mg/L)
Project | COD | SS | CU2+ | Cd2+ | Chromium |
Embodiment 1 | 25 | 6 | 0.12 | 0.05 | 0.04 |
Embodiment 2 | 26 | 5 | 0.15 | 0.07 | 0.02 |
Embodiment 3 | 23 | 5 | 0.11 | 0.04 | 0.03 |
Embodiment 4 | 27 | 7 | 0.16 | 0.05 | 0.05 |
Embodiment 5 | 28 | 6 | 0.13 | 0.06 | 0.04 |
Comparative example 1 | 213 | 53 | 13.5 | 7.2 | 1.2 |
Comparative example 2 | 176 | 42 | 10.5 | 5.4 | 0.68 |
Comparative example 3 | 165 | 39 | 7.6 | 2.5 | 0.54 |
Wherein:Tealeaves and sodium alginate are not added with comparative example 1, tealeaves is not added with comparative example 2, sea is not added with comparative example 3
Mosanom.
2nd, experimental result
As can be seen from the above table:Embodiment 1-5 can capture many in many kinds of metal ions in water body, and heavy metal sewage
Metal ion species have good clearance, and governance efficiency is high, and many kinds of metal ions in comparative example 1-3 heavy metal sewage
Clearance substantially clearance than embodiment 1-5 is low, governance efficiency is relatively low.May certify that only addition tealeaves and sodium alginate are not
The many kinds of metal ions in heavy metal containing sewage can be preferably removed, and the synergy for passing through tealeaves and sodium alginate can be notable
Improve the clearance of many kinds of metal ions in the heavy metal-polluted water treatment agent heavy metal sewage, and stable performance.
The heavy metal-polluted water treatment agent is compounded by above-mentioned raw materials, plays synergy, can capture various in water body
Many kinds of metal ions in metal ion, and heavy metal sewage has good clearance, and governance efficiency is high;It is of the invention heavy
Metal sewage-treating agent treatment effect is good, and stable performance, sedimentation effect is good, and effluent quality is good;And processing method is simple,
When using, only need to be by the dirty inorganic agent input water, processing cost is low;Sewage after treatment can reach discharge standard,
Floc strength is high, and hydrophobic performance is good;Heavy metal-polluted water treatment agent purity of the invention is high, non-toxic, on operator without influence,
Biological pollution and secondary pollution problem are not resulted in.
The better embodiment to this patent is explained in detail above, but this patent is not limited to above-mentioned embodiment party
Formula, in the ken that one skilled in the relevant art possesses, can also be on the premise of this patent objective not be departed from
Make a variety of changes.
Claims (6)
1. a kind of heavy metal-polluted water treatment agent, it is characterised in that the component composition including following parts by weight:Sodium Polyacrylate
15-25 parts, aluminum sulfate 10-30 parts, iron chloride 10-15 parts, activated sludge 20-25 parts, tealeaves 5-10 parts, sodium alginate 5-10
Part, plant ash 1-3 parts, deionized water 70-200 parts.
2. heavy metal-polluted water treatment agent according to claim 1, it is characterised in that the component group including following parts by weight
Into:22 parts of Sodium Polyacrylate, 25 parts of aluminum sulfate, 13 parts of iron chloride, 22 parts of activated sludge, 9 parts of tealeaves, 6 parts of sodium alginate, vegetation
2 parts of ash, 90 parts of deionized water.
3. a kind of preparation method of heavy metal-polluted water treatment agent as described in claim 1-2 is any, it is characterised in that specific step
Suddenly it is:(1)Be first according to parts by weight weigh Sodium Polyacrylate, aluminum sulfate, iron chloride, activated sludge, tealeaves, sodium alginate,
Plant ash, it is standby;(2)By in activated sludge, tealeaves, plant ash addition pulverizer, it is 80-110 mesh powder to crush, standby;(3)
By in Sodium Polyacrylate, aluminum sulfate, iron chloride addition deionized water, using vibration of ultrasonic wave 15-20 minutes, mixed liquor I is obtained;
(4)Sodium alginate is added in mixed liquor I, and is stirred in addition, obtain mixed liquor II;(5)Above-mentioned powder is added to mixed
Close in liquid II, stir 10-15 minutes, using vibration of ultrasonic wave 5-10 minutes, get product.
4. the preparation method of heavy metal-polluted water treatment agent according to claim 3, it is characterised in that the step(2)Will
Activated sludge, tealeaves, plant ash are added in pulverizer, and it is 90 mesh powder to crush.
5. the preparation method of heavy metal-polluted water treatment agent according to claim 3, it is characterised in that the step(3)Will
Sodium Polyacrylate, aluminum sulfate, iron chloride are added in deionized water, using vibration of ultrasonic wave 16 minutes, obtain mixed liquor I.
6. the preparation method of heavy metal-polluted water treatment agent according to claim 3, it is characterised in that the step(5)Will
Above-mentioned powder was added in mixed liquor II, stirs 12 minutes, using vibration of ultrasonic wave 8 minutes.
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Cited By (3)
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CN108910983A (en) * | 2018-08-06 | 2018-11-30 | 邹泽深 | A kind of sewage-treating agent and preparation method thereof for purifying domestic sewage |
CN111875450A (en) * | 2020-08-17 | 2020-11-03 | 鄂尔多斯市蒙康元生物科技研究有限公司 | Soil repairing agent and repairing method for backfill area of coal mining pit |
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CN108910983A (en) * | 2018-08-06 | 2018-11-30 | 邹泽深 | A kind of sewage-treating agent and preparation method thereof for purifying domestic sewage |
CN111875450A (en) * | 2020-08-17 | 2020-11-03 | 鄂尔多斯市蒙康元生物科技研究有限公司 | Soil repairing agent and repairing method for backfill area of coal mining pit |
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