CN106726666A - A kind of nursing type hairspray and preparation method thereof - Google Patents
A kind of nursing type hairspray and preparation method thereof Download PDFInfo
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- CN106726666A CN106726666A CN201611209674.8A CN201611209674A CN106726666A CN 106726666 A CN106726666 A CN 106726666A CN 201611209674 A CN201611209674 A CN 201611209674A CN 106726666 A CN106726666 A CN 106726666A
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- nursing type
- film forming
- forming agent
- hair
- conditioner
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/30—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
- A61K8/60—Sugars; Derivatives thereof
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/30—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
- A61K8/33—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing oxygen
- A61K8/34—Alcohols
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/30—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
- A61K8/40—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing nitrogen
- A61K8/41—Amines
- A61K8/416—Quaternary ammonium compounds
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/30—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
- A61K8/64—Proteins; Peptides; Derivatives or degradation products thereof
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/72—Cosmetics or similar toiletry preparations characterised by the composition containing organic macromolecular compounds
- A61K8/73—Polysaccharides
- A61K8/733—Alginic acid; Salts thereof
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/72—Cosmetics or similar toiletry preparations characterised by the composition containing organic macromolecular compounds
- A61K8/73—Polysaccharides
- A61K8/736—Chitin; Chitosan; Derivatives thereof
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
- A61Q5/00—Preparations for care of the hair
- A61Q5/06—Preparations for styling the hair, e.g. by temporary shaping or colouring
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K2800/00—Properties of cosmetic compositions or active ingredients thereof or formulation aids used therein and process related aspects
- A61K2800/40—Chemical, physico-chemical or functional or structural properties of particular ingredients
- A61K2800/59—Mixtures
- A61K2800/592—Mixtures of compounds complementing their respective functions
- A61K2800/5922—At least two compounds being classified in the same subclass of A61K8/18
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- Health & Medical Sciences (AREA)
- Life Sciences & Earth Sciences (AREA)
- Animal Behavior & Ethology (AREA)
- General Health & Medical Sciences (AREA)
- Public Health (AREA)
- Veterinary Medicine (AREA)
- Birds (AREA)
- Epidemiology (AREA)
- Emergency Medicine (AREA)
- Cosmetics (AREA)
Abstract
The invention belongs to daily chemical product technical field, and in particular to a kind of nursing type hairspray and preparation method thereof.The nursing type hairspray that the present invention is provided, including following components and its mass percent：Film forming agent 15~20%, the, of conditioner 11~15% treatment oil composition 15~20%, NMF 10~16%, preservative 0.5~1% and water 28~48.5%.It is of the invention it is a technical advantage that：The drawbacks of film forming agent for compounding formation by a certain percentage using shitosan and maltose avoids silicon-oxygen polymer and synthesising macromolecule copolymer film forming agent, the correct effect initiated to nutrition and nursing such as addition conditioner and treatment oil composition.
Description
Technical field
The invention belongs to daily chemical product technical field, and in particular to a kind of nursing type hairspray and preparation method thereof.
Background technology
In daily life, having under many occasions is needed to shape hair, such as, for needs attractive in appearance, performer is carried out
Make up etc., generally it is required for realizing the sizing to hair by hairspray, at present hairspray common on the market
Product is relatively more, but mostly exist be not easy by who clean, to hair easily cause injury etc. weak point.
Chinese patent CN101474138B discloses a kind of hair setting composition, in addition to water including accounting for composition weight
The setting agent of 0.02%-15.0%, the suspension thickener for accounting for composition weight 0.02%-1.5%, account for composition weight 0.0%-
6.0% white oil and dimethyl silicone polymer composition containing composed of the following components：Account for composition weight 0.01%-5.0%'s
Interior phase viscosity is the dimethyl silicone polymer of 5cs-1000cs, the interior phase viscosity that accounts for composition weight 0.01%-5.0% is
The dimethiconol of 2000cs-5000cs, the phenyl trimethicone polysiloxanes for accounting for composition weight 0.01%-5.0%,
Account for the polyether-modified dimethyl silicone polymer of composition weight 0.01%-5.0%.Although silica class compound can in the present invention
Completely cut off the osmotic efficiency enhancing hair texture of other harmful components, but long-term use influences the hair quality of hair, easily causes alopecia
With the generation of dandruff.
Chinese patent CN103781458B discloses a kind of aerosol hair jelly product for shaping and/or shaping hair,
Its hair shaping copolymer is selected from：The acrylic acid of two or more monomers of one of (methyl) acrylic acid or their monoesters is total to
Polymers；The propylene of butyl acrylate, methyl methacrylate, methacrylic acid, ethyl acrylate and hydroxyethyl methacrylate
Acid esters/hydroxy acrylate copolymer；Polyurethane -14/AMP- acrylate polymer blends, use macromolecule resin type
Hair style agent can make firmly to be fixed around hair using macromolecule resin, as a result, can make not destructible hair style, but
It is that synthesising macromolecule copolymer has the defect of air impermeability and moisture impermeability.
The content of the invention
To solve problems of the prior art, the present invention provides a kind of nursing type hairspray and its preparation side
Method.
Nursing type hairspray of the present invention, including following components and its mass percent：
Film forming agent 15~20%, the, of conditioner 11~15% treatment oil composition 15~20%, NMF 10~16%, preservative
0.5~1% and water 28~48.5%.
Preferably, described nursing type hairspray is made up of following components and its mass percent：
Film forming agent 18%, the, of conditioner 13% treatment oil composition 18%, NMF 12%, preservative 0.7% and water 38.3%.
Preferably, described film forming agent is by maltose and shitosan in mass ratio 2:3 compositions.
Preferably, described conditioner is double cocounut oil alkane acyl ethyl-hydroxyethyl ester quats.
Preferably, Suo Shu treatment oil composition is silk peptide.
Preferably, described NMF is by sodium alginate and trimethylglycine in mass ratio 2:3 compositions.
Further preferably, described preservative is Phenoxyethanol.
In addition, present invention also offers a kind of preparation method of nursing type hairspray, comprising the following steps：
S1, weigh raw material according to mass percent；
In S2, film forming agent, conditioner, are treated with oil composition and water addition emulsification pot, 70-80 DEG C is warming up to, stirred,
Matter 10-20min；
S3, it is cooled to 40-50 DEG C, adds NMF, stirs, homogeneous 5-10min；
S4, continue to be down to room temperature, add preservative, stir, obtain final product.
Maltose CAS：69-79-4；Shitosan CAS：9012-76-4；Sodium alginate CAS：9005-38-3；Three
Methylglycine CAS：107-43-7；Phenoxyethanol CAS：122-99-6.
Film forming matter uses maltose and natural copolymer chitosan in the present invention, and the addition of maltose makes hair more beautiful
It is beautiful, and do not result in the sticky sense of setting agent not only after head perspiration but also hair can be made more shinny, and maltose meeting
Portion of water is absorbed, makes hair moist；Shitosan overcomes synthesising macromolecule copolymer air impermeability and moisture impermeability
Defect, and because the acylate of shitosan has cationic, be applied on the hair for be in negative charge state compared with anion
Polymer is easily adhered to hair surface, makes the mutual tight union of hair, forms hard without viscous, ventilative, moisture-inhibiting thin transparent
Film, hair style, the purpose of fixed hairdo are kept so as to reach, due also to shitosan has antistatic and bactericidal properties, are difficult hair
Dye dirt, reduces the frictional resistance of hair, it is easy to combing, with logic and hair care aesthetic effect.
Double cocounut oil alkane acyl ethyl-hydroxyethyl ester quats are high concentration liquid ester quat, are the cation opsonizing agents of a new generation,
The shortcomings of it effectively overcomes excitant high, the difficult for biological degradation that conventional quaternary ammonium salts have, can be effectively improved the combing of hair
Property and tangling property, minimizing electrostatic, more significantly improve hair quality, increase the glossiness and tensile strength of hair, reduce hair bifurcated, especially
It is notable to the hair repairing effect and effect of color protection after dye.
Treat with oil composition silk peptide structure and hair structure closely, and active ingredient amino acid therein is easy to
Absorbed by hair, so as to play a part of nourishing hair, while the SP of HMW is easy to form transparent on hair again
Film, and be difficult to be washed out by water, thus it has good hair care performance again.
Sodium alginate hydrophily is strong, can be dissolved in cold water and warm water, forms very sticky uniform solution, is formed
Solution there are other analogs to be difficult to flexibility, homogeneity and other good characteristics for obtaining, with very strong protecting colloid
Effect；Trimethylglycine also known as glycine betaine, are natural moisture preserving agent, tool high biological compatibility, for personal care product
The middle water holding capacity that can rapidly improve skin hair, makes that hair quality is moist, smooth, prevent drying.
The addition of micro preservative Phenoxyethanol is avoiding hairspray from being gone mouldy in long-term storage.
Compatibility of the present invention is reasonable, science, and each component cooperates, act synergistically the nursing and sizing played jointly to hair
Effect.
Compared with prior art, it is of the invention it is a technical advantage that：Compounded by a certain percentage with maltose using shitosan
The drawbacks of film forming agent of formation avoids silicon-oxygen polymer and synthesising macromolecule copolymer film forming agent, addition conditioner are He treatment oil
The correct effect initiated to nutrition and nursing such as composition.
Specific embodiment
The present invention is described in further details below by specific embodiment, these embodiments are only used for the mesh of illustration
, it is in no way intended to limit protection scope of the present invention.
Double cocounut oil alkane acyl ethyl-hydroxyethyl ester quat producers：Member of Imperial Academy Chemical Co., Ltd.；Silk peptide producer：Xuancheng is brilliant auspicious new
Materials Co., Ltd.
Embodiment 1-3, comparative example 1-2
Table 1 lists the group of the specific embodiment 1-3 and comparative example 1-2 of nursing type hairspray provided by the present invention
Divide and mass percent.
The embodiment of table 1 and comparative example component and mass percent
Comparative example 1 is with the difference of embodiment 2：Film forming agent is by maltose and shitosan in mass ratio 1:1 composition.
Comparative example 2 is with the difference of embodiment 2：Film forming agent is changed to dimethyl silicone polymer.
The preparation method of the nursing type hairspray of embodiment 1：
S1, weigh raw material according to mass percent；
In S2, film forming agent, conditioner, are treated with oil composition and water addition emulsification pot, 70 DEG C are warming up to, stirred, homogeneous
10min；
S3, it is cooled to 40 DEG C, adds NMF, stirs, homogeneous 5min；
S4, continue to be down to room temperature, add preservative, stir, obtain final product.
The preparation method of the nursing type hairspray of embodiment 2：
S1, weigh raw material according to mass percent；
In S2, film forming agent, conditioner, are treated with oil composition and water addition emulsification pot, 75 DEG C are warming up to, stirred, homogeneous
15min；
S3, it is cooled to 45 DEG C, adds NMF, stirs, homogeneous 7.5min；
S4, continue to be down to room temperature, add preservative, stir, obtain final product.
The preparation method of the nursing type hairspray of embodiment 3：
S1, weigh raw material according to mass percent；
In S2, film forming agent, conditioner, are treated with oil composition and water addition emulsification pot, 80 DEG C are warming up to, stirred, homogeneous
20min；
S3, it is cooled to 50 DEG C, adds NMF, stirs, homogeneous 10min；
S4, continue to be down to room temperature, add preservative, stir, obtain final product.
The preparation method of comparative example 1-2 hairsprays is similar to Example 2.
Properties of product evaluation test
Test example 1：Water solubility test
Test method：The hairspray that embodiment 1-3 and comparative example 1-2 are prepared is added to 50 times of water of volume
In, temperature be 50 DEG C when stirring and dissolving 30min, then cool down rear solution can be in uniform state, by the aqueous solution pour into 1cm ×
In 1cm cuvettes, the transmitance under 655nm, transmitance 70~100%, good water solubility are determined with ultraviolet specrophotometer；Through
Rate 30~70% is water-soluble general；Transmitance 0~30%, poorly water-soluble, concrete outcome is as shown in table 2.
Test example 2：Curl retention is determined
Test products：The hairspray that embodiment 1-3 and comparative example 1-2 are prepared.
Test method：The setting agent of 0.7g is applied on 25cm long, the hair of weight 3g, being so post-rolled on 5cm long, internal diameter is
On the curling iron of 1cm, fixed with hair clip and be placed in 40 DEG C of oven for drying.Topknot is removed after drying, the initial crimp of topknot is measured
Length L1.Then topknot is hung in 30 DEG C, humidity is the final lengths for determining topknot in 90% climatic chamber after 12 hours
L2, curl retention=[(25-L2)/(25-L1)] × 100%, curl retention is more than 70%, and effect is good, curl retention
Between 40~70%, effect is general；Curl retention is between 20~40%, and effect is poor, and concrete outcome is as shown in table 2.
The water solubility of table 2 and curl retention result of the test
From table 2 it can be seen that the setting agent good water solubility that the present invention is prepared, and curl retention is high.
Test example 3：Human body long hair is tested
Subjects：Female, 25 ± 2 years old, 50 people, hair lengths were 30 ± 3cm.Test method：It is continuous to use embodiment 1-3
The setting agent prepared with comparative example 1-2 30 days, observes behaviour in service, and test the strength carried using hair before and after 30 days
(3 hairs exert a force from the 1cm of two ends, power when calculating is broken), every group is averaged, and concrete outcome is as shown in table 3.
The setting agent behaviour in service of table 3 and carrying strength
| Group | With preceding bearing capacity/N | With rear bearing capacity/N | With state after 30 days |
| Embodiment 1 | 5.1 | 5.0 | Hair is submissive glossy, using rear flexible, is considered to be worth doing without white, and dandruff is normal level |
| Embodiment 2 | 5.4 | 5.8 | Hair is submissive glossy, is shaped after use, and without white bits, dandruff is normal level |
| Embodiment 3 | 5.0 | 4.8 | Hair is submissive glossy, there is very much type after use, and without white bits, dandruff is normal level |
| Comparative example 1 | 4.5 | 4.4 | Hair is submissive glossy, using rear flexible, there is a small amount of white bits, and dandruff is normal level |
| Comparative example 2 | 4.2 | 4.3 | Hair is short-tempered, intense darkness without light, using rear nonelastic, there is a large amount of white bits, has dandruff to produce |
From table 3 it can be seen that the setting agent that embodiment of the present invention 1-3 is prepared bears pulling force base using front and rear hair
This is constant, but the setting agents that prepare of comparative example 1-2 bear pulling force and diminish using rear hair, illustrate to be made using comparative example 2
The standby setting agent for obtaining has injured hair, hair toughness is diminished, and comparative example 1-3 and comparative example 1-2 use states
It was found that, comparative example 2 is scared hot-tempered, intense darkness without light using back, using rear nonelastic, there is a large amount of white bits, has dandruff to produce, explanation
In the case where formula is changed, effect is deteriorated comparative example 2.The setting agent that embodiment 1-3 prepares is further illustrated more
Make hair submissive glossy, white bits are not produced, and dandruff is normal.
The above is only the preferred embodiment of the present invention, it is noted that it is right that above-mentioned preferred embodiment is not construed as
Limitation of the invention, protection scope of the present invention should be defined by claim limited range.For the art
For those of ordinary skill, without departing from the spirit and scope of the present invention, some improvements and modifications can also be made, these change
Enter and retouch and also should be regarded as protection scope of the present invention.
Claims (8)
1. a kind of nursing type hairspray, it is characterised in that including following components and its mass percent：
Film forming agent 15~20%, the, of conditioner 11~15% treatment oil composition 15~20%, NMF 10~16%, preservative 0.5~
1% and water 28~48.5%.
2. nursing type hairspray according to claim 1, it is characterised in that by following components and its mass percent
Composition：
Film forming agent 18%, the, of conditioner 13% treatment oil composition 18%, NMF 12%, preservative 0.7% and water 38.3%.
3. nursing type hairspray according to claim 1 and 2, it is characterised in that described film forming agent is by maltose
With shitosan in mass ratio 2:3 compositions.
4. nursing type hairspray according to claim 1 and 2, it is characterised in that described conditioner is double cocounut oil
Alkane acyl ethyl-hydroxyethyl ester quat.
5. nursing type hairspray according to claim 1 and 2, it is characterised in that Suo Shu treatment oil composition is fibroin
Peptide.
6. nursing type hairspray according to claim 1 and 2, it is characterised in that described NMF is by alginic acid
Sodium and trimethylglycine in mass ratio 2:3 compositions.
7. nursing type hairspray according to claim 1 and 2, it is characterised in that described preservative is benzene oxygen second
Alcohol.
8. the preparation method of the nursing type hairspray according to claim any one of 1-7, it is characterised in that including with
Lower step：
S1, weigh raw material according to mass percent；
In S2, film forming agent, conditioner, are treated with oil composition and water addition emulsification pot, 70-80 DEG C is warming up to, stirred, homogeneous
10-20min；
S3, it is cooled to 40-50 DEG C, adds NMF, stirs, homogeneous 5-10min；
S4, continue to be down to room temperature, add preservative, stir, obtain final product.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201611209674.8A CN106726666A (en) | 2016-12-23 | 2016-12-23 | A kind of nursing type hairspray and preparation method thereof |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201611209674.8A CN106726666A (en) | 2016-12-23 | 2016-12-23 | A kind of nursing type hairspray and preparation method thereof |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| CN106726666A true CN106726666A (en) | 2017-05-31 |
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ID=58920389
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN201611209674.8A Pending CN106726666A (en) | 2016-12-23 | 2016-12-23 | A kind of nursing type hairspray and preparation method thereof |
Country Status (1)
| Country | Link |
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| CN (1) | CN106726666A (en) |
Cited By (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN112022742A (en) * | 2020-08-12 | 2020-12-04 | 澳宝化妆品（惠州）有限公司 | Transparent and high-stability hair styling composition and preparation method thereof |
Citations (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN102138873A (en) * | 2010-01-29 | 2011-08-03 | 上海华银日用品有限公司 | Jelly water and preparation method thereof |
-
2016
- 2016-12-23 CN CN201611209674.8A patent/CN106726666A/en active Pending
Patent Citations (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN102138873A (en) * | 2010-01-29 | 2011-08-03 | 上海华银日用品有限公司 | Jelly water and preparation method thereof |
Cited By (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN112022742A (en) * | 2020-08-12 | 2020-12-04 | 澳宝化妆品（惠州）有限公司 | Transparent and high-stability hair styling composition and preparation method thereof |
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Application publication date: 20170531 |