CN106726648A - A kind of nano photo-catalytic tooth whitening gel - Google Patents
A kind of nano photo-catalytic tooth whitening gel Download PDFInfo
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- CN106726648A CN106726648A CN201710049629.9A CN201710049629A CN106726648A CN 106726648 A CN106726648 A CN 106726648A CN 201710049629 A CN201710049629 A CN 201710049629A CN 106726648 A CN106726648 A CN 106726648A
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- mass parts
- whitening
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/19—Cosmetics or similar toiletry preparations characterised by the composition containing inorganic ingredients
- A61K8/29—Titanium; Compounds thereof
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/02—Cosmetics or similar toiletry preparations characterised by special physical form
- A61K8/04—Dispersions; Emulsions
- A61K8/042—Gels
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/19—Cosmetics or similar toiletry preparations characterised by the composition containing inorganic ingredients
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/19—Cosmetics or similar toiletry preparations characterised by the composition containing inorganic ingredients
- A61K8/22—Peroxides; Oxygen; Ozone
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/19—Cosmetics or similar toiletry preparations characterised by the composition containing inorganic ingredients
- A61K8/25—Silicon; Compounds thereof
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/19—Cosmetics or similar toiletry preparations characterised by the composition containing inorganic ingredients
- A61K8/27—Zinc; Compounds thereof
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/19—Cosmetics or similar toiletry preparations characterised by the composition containing inorganic ingredients
- A61K8/28—Zirconium; Compounds thereof
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/72—Cosmetics or similar toiletry preparations characterised by the composition containing organic macromolecular compounds
- A61K8/81—Cosmetics or similar toiletry preparations characterised by the composition containing organic macromolecular compounds obtained by reactions involving only carbon-to-carbon unsaturated bonds
- A61K8/8141—Compositions of homopolymers or copolymers of compounds having one or more unsaturated aliphatic radicals, each having only one carbon-to-carbon double bond, and at least one being terminated by only one carboxyl radical, or of salts, anhydrides, esters, amides, imides or nitriles thereof; Compositions of derivatives of such polymers
- A61K8/8147—Homopolymers or copolymers of acids; Metal or ammonium salts thereof, e.g. crotonic acid, (meth)acrylic acid; Compositions of derivatives of such polymers
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
- A61Q11/00—Preparations for care of the teeth, of the oral cavity or of dentures; Dentifrices, e.g. toothpastes; Mouth rinses
Abstract
The invention belongs to daily use chemicals manufacture field, it is related to a kind of nano photo-catalytic tooth whitening gel.The gel includes following component:The gel of 1 50 mass parts, the surfactant of 0.05 0.5 mass parts, the NMF of 3.3 10 mass parts, the sweetener of 0.01 0.15 mass parts, the deionized water of 20 80 mass parts, the spices of 0.02 0.5 mass parts, the preservative of 0.02 0.18 mass parts, the desensitizer of 0.1 0.5 mass parts, the conditioning agent of 0.1 0.5 mass parts, the whitening factor of 8.8 20 mass parts;The whitening factor is made up of the photocatalyst of 5 10 mass parts, the peracid water element of 3.3 10 mass parts.The gel has high permeability, in can penetrating into the aperture of dentine, the effect of quick whitening;Organic compound and inorganic matter in the pigment of oxidation Decomposition dental surface and oral cavity, destroy the cell membrane of bacterium and the protein of solidification virus, bacterium and decomposing organic matter can be killed, with extremely strong sterilizing oral, except halitosis, tooth-whitening function.Ordinary toothpaste can be played a part of to be beyond one's reach oral cleaning and tooth-whitening.
Description
Technical field
The invention belongs to daily use chemicals manufacture field, it is related to a kind of nano photo-catalytic tooth whitening gel.
Background technology
Traditional tooth whitening gel be a kind of Hydrogenperoxide gel its it is main into composition be high-strength hydrogen peroxide, urea
Carbomer gel.Oxidisability by hydrogen peroxide carrys out bleaching teeth, and oral cavity is glued because high-strength hydrogen peroxide is corrosive
Film is damaged.Influence is healthy.It is photocatalyst and the medical peroxidating of low concentration that the invention of this formula is specifically added the whitening factor
Hydrogen.With nanometer grade silica gel carrier or Carbomer carrier, ultraviolet light or the illumination of far red light or visible ray is coordinated to reach
To safe and efficient U.S. tooth function.Clearly, typically tooth whiteness will rise one to this formula whitening effect after using seven times
Level.
There is tooth blackening, flavescence and mainly divide exogenous and two kinds of endogenous in people.Exogenous master is by bacterial plaque, daily
Pigment deposition causes in food in diet, and endogenous is normally due to be deposited on dentine medicine tetracycline, drink in tooth growth course
What the fluorine in water excessively caused.And the method for tooth-whitening is exactly two kinds:One is to dispel exogenous stain on the tooth surface, and two is to dispel tooth
Pigment in essence, the former and need to use whitening agent oxidation Decomposition stain on the tooth surface, traditional whitening is by the friction in toothpaste
Agent brushes teeth to rub off the pigment on surface, and effect is undesirable.Pigment particularly in dentine is difficult to remove.
The content of the invention
Therefore, the technical problems to be solved by the invention are to overcome tooth whitening gel effect in the prior art to pay no attention to
Think, the pigment in dentine is difficult to the bottleneck for removing, so as to propose the nano photo-catalytic tooth of a kind of oral cleaning and tooth-whitening
Tooth whitening gelatin.
In order to solve the above technical problems, the invention discloses a kind of nano photo-catalytic tooth whitening gel, the gel bag
Include following component:The gel of 1-50 mass parts, the surfactant of 0.05-0.5 mass parts, the moisturizing of 3.3-10 mass parts
Agent, the sweetener of 0.01-0.15 mass parts, the deionized water of 20-80 mass parts, the spices of 0.02-0.5 mass parts, 0.02-
The preservative of 0.18 mass parts, the desensitizer of 0.1-0.5 mass parts, the conditioning agent of 0.1-0.5 mass parts, 8.8-20 mass parts
The whitening factor;
The whitening factor is made up of the photocatalyst of 5-10 mass parts, the peracid water element of 3.3-10 mass parts.
Preferably, the photocatalyst is TiO2、ZrO2、ZnO、Fe2O3、SrTiO3、SiO2, platinum, in Lao, Palladium at least one
Kind.
Preferably, the peracid water element is H2O2。
Preferably, the gel is the one kind in Carbomer or nano silicon.
Preferably, the Carbomer is 1-2 mass parts, is the one kind in polyvinylpyrrolidone, poloxamer.
Preferably, the silica is 30-50 mass parts.
Preferably, the surfactant is N- sodium N-lauroyl sarcosinates, lauryl sodium sulfate, laureth
At least one in sulphur, acid esters sodium, AEO.
Preferably, the conditioning agent is in NaOH, potassium hydroxide, triethanolamine, aminomethyl propyl alcohol, polyalcohol
It is at least one;The desensitizer is at least one in sodium fluoride, potassium nitrate, strontium fluoride.
Preferably, the NMF is glycerine, polyethylene glycol, propane diols, sorbierite, Aceonon 300 MO, phosphinylidyne
At least one in amine;The preservative be Sodium Benzoate, p-hydroxybenzoate, chloreresol, methyl hydroxybenzoate, Nipasol,
At least one in thimerosal;The sweetener is at least one in xylitol, saccharin sodium;The spices is lactic acid peppermint
At least one at least one, peach class, mango class in ester, orange flavor, strawberry flavor, peach spices, mango spices.
The invention also discloses the preparation method of gel described in any one, methods described is as follows:By the solidifying of respective quality part
Jelly, surfactant, sweetener, NMF, water, spices, conditioning agent, desensitizer, the whitening factor, preservative, be dissolved in from
Sub- water is simultaneously stirred, and obtains the gel.
Above-mentioned technical proposal of the invention has advantages below compared to existing technology:Gel of the present invention has high oozing
Permeability, can be penetrated into the aperture of dentine, and hydrogen peroxide is decomposed and produces Strong oxdiative thing to promote color in dental surface and deep layer
Element tissue is disintegrated rapidly, the effect of so as to play quick whitening;It is various in the oxidable pigment for decomposing dental surface and oral cavity to have
Machine compound and part inorganic matter, can destroy the cell membrane of bacterium and the protein of solidification virus, and can kill bacterium and decomposition has
Organic pollutants, with extremely strong sterilizing oral, except halitosis, tooth-whitening function.Photocatalyst when itself receives illumination except that can produce
Raw oxidation also promotes effective decomposition of hydrogen peroxide simultaneously, and the HO2- for producing more oxidabilities superpower, HO2- is continuous
Oxidize away pigment, ordinary toothpaste can be played a part of and be beyond one's reach oral cleaning and tooth-whitening;With great city
Field prospect and economic worth.
Specific embodiment
Embodiment 1 is present embodiment discloses a kind of Buccodental whitening gelatin, and the gel component is as follows:8 mass parts
Photocatalyst TIO2, the peracid water element of 7 mass parts, 40 mass parts go from water, the nano silicon of 37 mass parts, 0.3 matter
Measure the laureth sodium sulfovinate, the phosphoamide H of 7 mass parts of part2NCONH2(CO(NH2)2), the poly- second two of 1.5 mass parts
Alcohol, the xylitol of 0.13 mass parts, the orange flavor of 0.25 mass parts, the Sodium Benzoate of 0.5 mass parts, the nitre of 0.3 mass parts
The strontium fluoride of sour potassium, 0.3 mass parts.The cleannes of this implementation whitening gelatin are 94%, remove stain degree 92%.
Embodiment 2 is present embodiment discloses a kind of Buccodental whitening gelatin, and the gel component is as follows:5 mass parts
Photocatalyst TIO2, the peracid water element of 7 mass parts, 48 mass parts go from water, the nano silicon of 50 mass parts, 0.05 matter
Measure the laureth sodium sulfovinate, the phosphoamide H of 7 mass parts of part2NCONH2(CO(NH2)2), the polyethylene glycol of 1 mass parts,
The xylitol of 0.15 mass parts, the orange flavor of 0.02 mass parts, the Sodium Benzoate of 0.5 mass parts, the nitric acid of 0.1 mass parts
The strontium fluoride of potassium, 0.5 mass parts.The cleannes of this implementation whitening gelatin are 93%, remove stain degree 91%.
Embodiment 3 is present embodiment discloses a kind of Buccodental whitening gelatin, and the gel component is as follows:10 mass parts
Photocatalyst TIO2, the peracid water element of 3.3 mass parts, 80 mass parts are gone from water, the Carbomer of 1 mass parts, 1.5 mass parts
Polyvinylpyrrolidone, the poloxamer of 1 mass parts, the laureth sodium sulfovinate of 0.00.5 mass parts, 3.3 mass parts
Phosphoamide H2NCONH2(CO(NH2)2), the polyethylene glycol of 2 mass parts, the xylitol of 0.1 mass parts, 0.5 mass parts strawberry it is fragrant
Material, the NaOH of 0.1 mass parts, the potassium nitrate of 0.5 mass parts, the strontium fluoride of 0.1 mass parts.This implementation whitening gelatin
Cleannes be 90%, remove stain degree 90%.
Embodiment 4 is present embodiment discloses a kind of Buccodental whitening gelatin, and the gel component is as follows:5 mass parts
Photocatalyst TIO2, the peracid water element of 10 mass parts, 20 mass parts are gone from water, the Carbomer of 1.5 mass parts, 1 mass parts
Polyvinylpyrrolidone, the poloxamer of 1.5 mass parts, the laureth sodium sulfovinate of 0.05 mass parts, 10 mass parts
Phosphoamide H2NCONH2(CO(NH2)2), the polyethylene glycol of 1 mass parts, the xylitol of 0.15 mass parts, the strawberry of 0.02 mass parts
Spices, the NaOH of 0.5 mass parts, the potassium nitrate of 0.1 mass parts, the strontium fluoride of 0.5 mass parts.This implementation whitening is coagulated
The cleannes of glue are 91%, remove stain degree 91%.
The present embodiment also discloses the preparation technology of the gel, comprises the following steps that:
By the gel of respective quality part, surfactant, sweetener, NMF, water, spices, conditioning agent, desensitizer,
The whitening factor, preservative, are dissolved in deionized water and stir, and obtain the gel.
Embodiment effect:Embodiment 1 and 2 is by two kinds of whitening factors photocatalyst (nano titanium oxide) of addition in gel
With peracid water element (hydrogen peroxide) of low concentration, synthesize whitening gelatin agent, gel has the slow release whitening factor to act on.It is made
It is that low mass parts of dense hydrogen peroxide 3.3 have high permeability with mechanism, in can penetrating into the aperture of dentine, peroxidating
Hydrogen decomposes pigment tissue in producing Strong oxdiative thing to promote dental surface and deep layer disintegrates rapidly, so as to play the work(of quick whitening
Effect.Other photocatalyst (Nano titanium dioxide) ultramicron receive ultraviolet or far infrared that wavelength is below 388nm,
During the irradiation of visible ray, similar photosynthetic light-catalyzed reaction can be produced, excite generation electricity inside it due to absorbing luminous energy
Sub- hole pair, i.e. photo-generated carrier, then move to rapidly its surface and activate adsorbed oxygen and moisture, produce oxidation
The very competent free hydroxy (OH) of activity and superoxide anion O2, active oxygen (HO2.H2O2), with very strong photooxidation
Change restoring function light life group, the energy of these light life groups, the high temperature equivalent to 3600K, with very strong oxidisability.
Various organic compounds and part inorganic matter in the oxidable pigment for decomposing dental surface and oral cavity, can destroy the cell membrane of bacterium
With solidification virus protein, bacterium and decomposing organic pollutant can be killed, organic pollution resolve into it is free of contamination go from
Sub- water (H2) and carbon dioxide (CO O2), thus with extremely strong sterilizing oral, except halitosis, tooth-whitening function.Photocatalyst except
Oxidation can be produced also to promote effective decomposition of hydrogen peroxide simultaneously when itself is by illumination, produces more oxidabilities to surpass
Strong HO2-,HO2- pigment is constantly oxidized away, both whitening factors combine can be played ordinary toothpaste and be beyond one's reach
The effect of oral cleaning and tooth-whitening.
Obviously, above-described embodiment is only intended to clearly illustrate example, and not to the restriction of implementation method.It is right
For those of ordinary skill in the art, can also make on the basis of the above description other multi-forms change or
Change.There is no need and unable to be exhaustive to all of implementation method.And the obvious change thus extended out or
Among changing still in the protection domain of the invention.
Claims (10)
1. a kind of nano photo-catalytic tooth whitening gel, it is characterised in that the gel includes following component:1-50 mass parts
Gel, the surfactant of 0.05-0.5 mass parts, the NMF of 3.3-10 mass parts, the sweet taste of 0.01-0.15 mass parts
Agent, the deionized water of 20-80 mass parts, the spices of 0.02-0.5 mass parts, the preservative of 0.02-0.18 mass parts, 0.1-0.5
The desensitizer of mass parts, the conditioning agent of 0.1-0.5 mass parts, the whitening factor of 8.8-20 mass parts;
The whitening factor is made up of the photocatalyst of 5-10 mass parts, the peracid water element of 3.3-10 mass parts.
2. whitening gelatin as claimed in claim 1, it is characterised in that the photocatalyst is TiO2、ZrO2、ZnO、Fe2O3、
SrTiO3、SiO2, platinum, at least one in Lao, Palladium.
3. whitening gelatin as claimed in claim 2, it is characterised in that the peracid water element is H2O2。
4. whitening gelatin as claimed in claim 3, it is characterised in that during the gel is Carbomer or nano silicon
One kind.
5. whitening gelatin as claimed in claim 4, it is characterised in that the Carbomer content is 1-2 mass parts, is polyethylene
One kind in pyrrolidones, poloxamer.
6. whitening gelatin as claimed in claim 4, it is characterised in that the silica is 30-50 mass parts.
7. the whitening gelatin as described in claim any one of 1-6, it is characterised in that the surfactant is N- lauroyls
At least one in sodium sarcosinate, lauryl sodium sulfate, laureth sulphur, acid esters sodium, AEO.
8. whitening gelatin as claimed in claim 7, it is characterised in that the conditioning agent is NaOH, potassium hydroxide, three second
At least one in hydramine, aminomethyl propyl alcohol, polyalcohol;The desensitizer be sodium fluoride, potassium nitrate, strontium fluoride at least
It is a kind of.
9. whitening gelatin as claimed in claim 8, it is characterised in that the NMF be glycerine, polyethylene glycol, propane diols,
At least one in sorbierite, Aceonon 300 MO, phosphoamide;The preservative is Sodium Benzoate, P-hydroxybenzoic acid
At least one in ester, chloreresol, methyl hydroxybenzoate, Nipasol, thimerosal;The sweetener is in xylitol, saccharin sodium
It is at least one;The spices be menthyl lactate, orange flavor, strawberry flavor, peach spices, mango spices at least one,
At least one in peach class, mango class.
10. a kind of method for preparing the whitening gelatin as described in claim any one of 1-6, it is characterised in that methods described is:
By the gel of respective quality part, surfactant, sweetener, NMF, water, spices, conditioning agent, desensitizer, the whitening factor,
Preservative, is dissolved in deionized water and stirs, and obtains the gel.
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Cited By (6)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
CN109481069A (en) * | 2018-12-21 | 2019-03-19 | 南京奇迪康生物科技有限公司 | A kind of method of bleaching tooth based on whitening cleansing gel |
CN109998933A (en) * | 2019-03-04 | 2019-07-12 | 西安蓝极医疗电子科技有限公司 | A kind of tooth whitening gel and preparation method thereof, application method |
CN111214307A (en) * | 2020-01-18 | 2020-06-02 | 陈敬 | Tooth-protecting and whitening tooth socket and manufacturing method and using method thereof |
CN111494230A (en) * | 2020-04-30 | 2020-08-07 | 江西师范大学 | Cold light tooth whitening gel, preparation method and application |
CN112274441A (en) * | 2020-11-03 | 2021-01-29 | 成都大学 | Tooth polishing paste with whitening self-repairing function and preparation method and application thereof |
CN115721572A (en) * | 2022-10-27 | 2023-03-03 | 四川大学 | Novel piezoelectric-photocatalytic tooth whitening formula |
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CN1358085A (en) * | 1999-07-02 | 2002-07-10 | 石桥卓郎 | Tooth bleaching compositions and method of bleaching discored tooth |
CN1739482A (en) * | 2005-08-26 | 2006-03-01 | 广州市华之特奥因特种材料科技有限公司 | Photocatalyst beautifying and whitening toothpaste and its prepn process |
CN101703456A (en) * | 2009-12-11 | 2010-05-12 | 江西诚志日化有限公司 | Combined chloranthus glaber whitening gelatin with anti-allergic agent and preparation method thereof |
CN102614090A (en) * | 2012-04-24 | 2012-08-01 | 苏州维蒂卡科技有限公司 | Toothpaste composition |
CN103131556A (en) * | 2013-02-20 | 2013-06-05 | 杨新莲 | Nano-grade photocatalytic/peroxide composite bleaching agent and preparation method thereof |
CN103893021A (en) * | 2012-12-26 | 2014-07-02 | 大连林桥科技有限公司 | A preparing method of photocatalyst whitening toothpaste |
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CN1358085A (en) * | 1999-07-02 | 2002-07-10 | 石桥卓郎 | Tooth bleaching compositions and method of bleaching discored tooth |
CN1739482A (en) * | 2005-08-26 | 2006-03-01 | 广州市华之特奥因特种材料科技有限公司 | Photocatalyst beautifying and whitening toothpaste and its prepn process |
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Cited By (6)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
CN109481069A (en) * | 2018-12-21 | 2019-03-19 | 南京奇迪康生物科技有限公司 | A kind of method of bleaching tooth based on whitening cleansing gel |
CN109998933A (en) * | 2019-03-04 | 2019-07-12 | 西安蓝极医疗电子科技有限公司 | A kind of tooth whitening gel and preparation method thereof, application method |
CN111214307A (en) * | 2020-01-18 | 2020-06-02 | 陈敬 | Tooth-protecting and whitening tooth socket and manufacturing method and using method thereof |
CN111494230A (en) * | 2020-04-30 | 2020-08-07 | 江西师范大学 | Cold light tooth whitening gel, preparation method and application |
CN112274441A (en) * | 2020-11-03 | 2021-01-29 | 成都大学 | Tooth polishing paste with whitening self-repairing function and preparation method and application thereof |
CN115721572A (en) * | 2022-10-27 | 2023-03-03 | 四川大学 | Novel piezoelectric-photocatalytic tooth whitening formula |
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