CN106701258A - Railway track screw anti-rusting lubricating grease and preparation method thereof - Google Patents
Railway track screw anti-rusting lubricating grease and preparation method thereof Download PDFInfo
- Publication number
- CN106701258A CN106701258A CN201611135043.6A CN201611135043A CN106701258A CN 106701258 A CN106701258 A CN 106701258A CN 201611135043 A CN201611135043 A CN 201611135043A CN 106701258 A CN106701258 A CN 106701258A
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- CN
- China
- Prior art keywords
- lubricating grease
- rusting
- track screw
- weight portions
- oil
- Prior art date
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Classifications
-
- C—CHEMISTRY; METALLURGY
- C10—PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
- C10M—LUBRICATING COMPOSITIONS; USE OF CHEMICAL SUBSTANCES EITHER ALONE OR AS LUBRICATING INGREDIENTS IN A LUBRICATING COMPOSITION
- C10M169/00—Lubricating compositions characterised by containing as components a mixture of at least two types of ingredient selected from base-materials, thickeners or additives, covered by the preceding groups, each of these compounds being essential
-
- C—CHEMISTRY; METALLURGY
- C10—PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
- C10M—LUBRICATING COMPOSITIONS; USE OF CHEMICAL SUBSTANCES EITHER ALONE OR AS LUBRICATING INGREDIENTS IN A LUBRICATING COMPOSITION
- C10M2201/00—Inorganic compounds or elements as ingredients in lubricant compositions
- C10M2201/06—Metal compounds
- C10M2201/062—Oxides; Hydroxides; Carbonates or bicarbonates
-
- C—CHEMISTRY; METALLURGY
- C10—PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
- C10M—LUBRICATING COMPOSITIONS; USE OF CHEMICAL SUBSTANCES EITHER ALONE OR AS LUBRICATING INGREDIENTS IN A LUBRICATING COMPOSITION
- C10M2203/00—Organic non-macromolecular hydrocarbon compounds and hydrocarbon fractions as ingredients in lubricant compositions
- C10M2203/10—Petroleum or coal fractions, e.g. tars, solvents, bitumen
-
- C—CHEMISTRY; METALLURGY
- C10—PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
- C10M—LUBRICATING COMPOSITIONS; USE OF CHEMICAL SUBSTANCES EITHER ALONE OR AS LUBRICATING INGREDIENTS IN A LUBRICATING COMPOSITION
- C10M2205/00—Organic macromolecular hydrocarbon compounds or fractions, whether or not modified by oxidation as ingredients in lubricant compositions
- C10M2205/02—Organic macromolecular hydrocarbon compounds or fractions, whether or not modified by oxidation as ingredients in lubricant compositions containing acyclic monomers
- C10M2205/0206—Organic macromolecular hydrocarbon compounds or fractions, whether or not modified by oxidation as ingredients in lubricant compositions containing acyclic monomers used as base material
-
- C—CHEMISTRY; METALLURGY
- C10—PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
- C10M—LUBRICATING COMPOSITIONS; USE OF CHEMICAL SUBSTANCES EITHER ALONE OR AS LUBRICATING INGREDIENTS IN A LUBRICATING COMPOSITION
- C10M2207/00—Organic non-macromolecular hydrocarbon compounds containing hydrogen, carbon and oxygen as ingredients in lubricant compositions
- C10M2207/10—Carboxylix acids; Neutral salts thereof
- C10M2207/12—Carboxylix acids; Neutral salts thereof having carboxyl groups bound to acyclic or cycloaliphatic carbon atoms
- C10M2207/125—Carboxylix acids; Neutral salts thereof having carboxyl groups bound to acyclic or cycloaliphatic carbon atoms having hydrocarbon chains of eight up to twenty-nine carbon atoms, i.e. fatty acids
- C10M2207/127—Carboxylix acids; Neutral salts thereof having carboxyl groups bound to acyclic or cycloaliphatic carbon atoms having hydrocarbon chains of eight up to twenty-nine carbon atoms, i.e. fatty acids polycarboxylic
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- C—CHEMISTRY; METALLURGY
- C10—PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
- C10M—LUBRICATING COMPOSITIONS; USE OF CHEMICAL SUBSTANCES EITHER ALONE OR AS LUBRICATING INGREDIENTS IN A LUBRICATING COMPOSITION
- C10M2207/00—Organic non-macromolecular hydrocarbon compounds containing hydrogen, carbon and oxygen as ingredients in lubricant compositions
- C10M2207/10—Carboxylix acids; Neutral salts thereof
- C10M2207/12—Carboxylix acids; Neutral salts thereof having carboxyl groups bound to acyclic or cycloaliphatic carbon atoms
- C10M2207/125—Carboxylix acids; Neutral salts thereof having carboxyl groups bound to acyclic or cycloaliphatic carbon atoms having hydrocarbon chains of eight up to twenty-nine carbon atoms, i.e. fatty acids
- C10M2207/128—Carboxylix acids; Neutral salts thereof having carboxyl groups bound to acyclic or cycloaliphatic carbon atoms having hydrocarbon chains of eight up to twenty-nine carbon atoms, i.e. fatty acids containing hydroxy groups; Ethers thereof
-
- C—CHEMISTRY; METALLURGY
- C10—PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
- C10M—LUBRICATING COMPOSITIONS; USE OF CHEMICAL SUBSTANCES EITHER ALONE OR AS LUBRICATING INGREDIENTS IN A LUBRICATING COMPOSITION
- C10M2215/00—Organic non-macromolecular compounds containing nitrogen as ingredients in lubricant compositions
- C10M2215/02—Amines, e.g. polyalkylene polyamines; Quaternary amines
- C10M2215/06—Amines, e.g. polyalkylene polyamines; Quaternary amines having amino groups bound to carbon atoms of six-membered aromatic rings
- C10M2215/064—Di- and triaryl amines
-
- C—CHEMISTRY; METALLURGY
- C10—PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
- C10M—LUBRICATING COMPOSITIONS; USE OF CHEMICAL SUBSTANCES EITHER ALONE OR AS LUBRICATING INGREDIENTS IN A LUBRICATING COMPOSITION
- C10M2223/00—Organic non-macromolecular compounds containing phosphorus as ingredients in lubricant compositions
- C10M2223/02—Organic non-macromolecular compounds containing phosphorus as ingredients in lubricant compositions having no phosphorus-to-carbon bonds
- C10M2223/04—Phosphate esters
-
- C—CHEMISTRY; METALLURGY
- C10—PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
- C10N—INDEXING SCHEME ASSOCIATED WITH SUBCLASS C10M RELATING TO LUBRICATING COMPOSITIONS
- C10N2030/00—Specified physical or chemical properties which is improved by the additive characterising the lubricating composition, e.g. multifunctional additives
- C10N2030/08—Resistance to extreme temperature
-
- C—CHEMISTRY; METALLURGY
- C10—PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
- C10N—INDEXING SCHEME ASSOCIATED WITH SUBCLASS C10M RELATING TO LUBRICATING COMPOSITIONS
- C10N2030/00—Specified physical or chemical properties which is improved by the additive characterising the lubricating composition, e.g. multifunctional additives
- C10N2030/12—Inhibition of corrosion, e.g. anti-rust agents or anti-corrosives
Landscapes
- Chemical & Material Sciences (AREA)
- Chemical Kinetics & Catalysis (AREA)
- General Chemical & Material Sciences (AREA)
- Oil, Petroleum & Natural Gas (AREA)
- Organic Chemistry (AREA)
- Lubricants (AREA)
Abstract
The invention discloses railway track screw anti-rusting lubricating grease and a preparation method thereof, and belongs to the technical field of special lubricating grease. According to the technical scheme of the invention, the railway track screw anti-rusting lubricating grease is prepared from the following raw materials in percentage by weight: 70-85% of base oil, 10-20% of a densifier, 3-4% of an additive and 2-6% of asphalt oil. The invention further specifically discloses a preparation method of the railway track screw anti-rusting lubricating grease. The lubricating grease disclosed by the invention is special railway track screw anti-rusting lubricating grease, the base oil of which the low-temperature property can be up to minus 50 DEG C is densified by using the densifier, namely, fatty acid lithium composite soap, and together with an anti-corrosion agent, an antioxidant and a pour point depressant, an excellent anti-rusting property and a relatively wide temperature use range of the lubricating grease can be ensured, and due to the added asphalt oil, the adhesion property of the lubricating grease can be improved, meanwhile as the asphalt oil has a very good air insulating property, a very good anti-rusting function can be achieved for screws.
Description
Technical field
The invention belongs to special grease technical field, and in particular to a kind of railroad track screw rust-inhibiting lubricant and its system
Preparation Method.
Background technology
Chinese Railway development speed quickly, will lay new railway every year, and the speed of train is more and more faster, bullet train
Also more and more, with the quickening of speed, the safety of train seems more important.Rail safety is also to ensure train safe operation
Key factor.Railroad track is made from multiple components, and the screw above each member tracks is each portion of connection track
The critical elements of part, it is to ensure the key factor that track is not caused danger that screw does not loosen in a long time.Keep spiral shell
Nail is firm for a long time effectively it is necessary that screw will not be corroded gets rusty.It is special it is therefore desirable to develop railroad track screw antirust
With lubricating grease, above the bolt dedicated for track all parts junction, it is ensured that bolt will not be corroded for a long time.
Chinese Regional is vast, and temperature has a long way to go, and influence of the temperature to lubricating grease is very big, and this requires railroad track spiral shell
There is nail rust-inhibiting lubricant temperature very wide to use scope, it is therefore necessary to which developing one kind had not only had rust-inhibiting lubricant characteristic but also tool
There is the railroad track screw antirust special grease of low temperature grease characteristic.
The content of the invention
Present invention solves the technical problem that a kind of railroad track screw rust-inhibiting lubricant and preparation method thereof is there is provided, should
The screw division position that lubricating grease is used for railroad track ensure that screw, for a long time not by corrosion, the safety of track traffic is ensured with this
Property, while this lubricating grease can be used throughout the country, it is to avoid the limitation that different geographical is used lubricating grease.
The present invention is to solve above-mentioned technical problem to adopt the following technical scheme that, railroad track screw rust-inhibiting lubricant, and it is special
Levy and be that what the raw material matched by following weight percent was prepared from:Base oil 70%-85%, thickening agent 10%-20%, additive
3%-4% and coal tar 2%-6%, wherein base oil be synthesize alkene oil or transformer oil in one or more, thickening agent is ten
The compound soap of dihydroxy aliphatic acid lithium salts and decanedioic acid lithium salts, additive is organic phosphate preservative, phenylenediamine compound resists
Oxidant and poly-alpha-olefin pour depressant.
Further preferably, ten described dihydroxy aliphatic acid lithium salts are lithium 12-hydroxy stearate salt, described preservative
It is fatty acid amide phosphate, described phenylenediamine compound is diphenylamines.
The preparation method of railroad track screw rust-inhibiting lubricant of the present invention, it is characterised in that concretely comprise the following steps:Will
The synthesis alkene oil of 56.2 weight portions is added in saponification kettle, is heated to 80 DEG C to adding 6.3 weight portions in saponification kettle
Ten dihydroxystearic acids, 90 DEG C are warming up to after ten dihydroxystearic acids are completely dissolved, and to being added in saponification kettle, lithium hydroxide is molten
Liquid, the lithium hydroxide solution is prepared from by the lithium hydroxide of 2.9 weight portions and the water of 8.7 weight portions, and continuing to heat up takes off
Water, the decanedioic acid of 4.8 weight portions is added when saponification temperature in the kettle rises to 130 DEG C and 30min is incubated, and end temperature rises to 180
DEG C stop heat up, circulation temperature lowering, shearing, added when saponification temperature in the kettle is down to 150 DEG C 18.8 weight portions synthesis alkene oil,
Add the coal tar of 6 weight portions, added when saponification temperature in the kettle is down to 100 DEG C 0.8 weight portion fatty acid amide phosphate,
The poly alpha olefin of the diphenylamines of 1.2 weight portions and 1 weight portion, shearing, degassing is obtained railroad track screw rust-inhibiting lubricant.
Obtained lubricating grease of the invention is railroad track screw antirust special grease, multiple using thickening agent aliphatic acid lithium salts
The base oil that soap thickening cryogenic property reaches -50 DEG C is closed, along with anticorrosive, antioxidant and pour-point depressant, it is ensured that lubricating grease
Scope is used with excellent rustless property and temperature wider, the adhesive force that adding coal tar can improve lubricating grease is dripped simultaneously
Blue or green oil has good air exclusion ability, and good antirust function can be played to screw.
Specific embodiment
The above of the invention is described in further details by the following examples, but this should not be interpreted as this
The scope for inventing above-mentioned theme is only limitted to following embodiment, and all technologies realized based on the above of the present invention belong to this hair
Bright scope.
Embodiment
56.2 kilograms of synthesis alkene oil are added in saponification kettle, 80 DEG C is heated to the public affairs of addition 6.3 in saponification kettle
Ten dihydroxystearic acids of jin, are warming up to 90 DEG C, to adding lithium hydroxide in saponification kettle after ten dihydroxystearic acids are completely dissolved
Solution, the lithium hydroxide solution is prepared from by 2.9 kilograms of lithium hydroxides and 8.7 kg of water, continues the dehydration that heats up, and works as soap
Change and 4.8 kilograms of decanedioic acid added when temperature in the kettle rises to 130 DEG C and 30min is incubated, end temperature rises to 180 DEG C to be stopped heating up,
Circulation temperature lowering, shearing adds 18.8 kilograms of synthesis alkene oil when saponification temperature in the kettle is down to 150 DEG C, adds 6 kilograms of pitches
Oil, adds 0.8 kilogram of fatty acid amide phosphate, 1.2 kilograms of diphenylamines and 1 kilogram poly- when saponification temperature in the kettle is down to 100 DEG C
Alpha-olefin, shearing, degassing is obtained railroad track screw rust-inhibiting lubricant.
The present invention utilizes the thick low temperature base oil of compound soap, and adds antioxidant, anticorrosive and pour-point depressant, is subsequently adding
The railroad track screw antirust special grease of coal tar modulation, it is sufficiently low that low temperature base oil ensure that lubricating grease has
Pour point, improved using the high adhesion force of pitch, antioxygenic property and good sealing property track rust-inhibiting lubricant it is attached
Put forth effort, the ability that anti-rain drop erosion and the anti-sun are exposed to the sun.
This kind of use of lubricating grease for convenience, the cone penetration of this lubricating grease is 25 degree 480, is a kind of fluid lubrication
Fat, workman need to only dip in screw toward lubricating grease the inside once can be to use.When usually maintenance, workman only need to be by lubricating grease
Uniformly it is coated on screw.Track bolt using can ensure after this lubricating grease screw for a long time will not by corrosion,
Ensure the safety of track, while facilitating the dismounting of track.
Embodiment above describes general principle of the invention, principal character and advantage, the technical staff of the industry should
Understand, the present invention is not limited to the above embodiments, simply original of the invention is illustrated described in above-described embodiment and specification
Reason, under the scope for not departing from the principle of the invention, various changes and modifications of the present invention are possible, and these changes and improvements each fall within
In the scope of protection of the invention.
Claims (3)
1. railroad track screw rust-inhibiting lubricant, it is characterised in that be that the raw material matched by following weight percent is prepared from:
Base oil 70%-85%, thickening agent 10%-20%, additive 3%-4% and coal tar 2%-6%, wherein base oil for synthesis alkene oil or
One or more in transformer oil, thickening agent is the compound soap of ten dihydroxy aliphatic acid lithium salts and decanedioic acid lithium salts, and additive is
Organic phosphate preservative, phenylenediamine compound antioxidant and poly-alpha-olefin pour depressant.
2. railroad track screw rust-inhibiting lubricant according to claim 1, it is characterised in that:Described ten dihydroxy fat
Sour lithium salts is lithium 12-hydroxy stearate salt, and described preservative is fatty acid amide phosphate, and described phenylenediamine compound is
Diphenylamines.
3. a kind of preparation method of railroad track screw rust-inhibiting lubricant, it is characterised in that concretely comprise the following steps:By 56.2 weight portions
Synthesis alkene oil be added in saponification kettle, be heated to 80 DEG C to adding ten dihydroxy of 6.3 weight portions hard in saponification kettle
Resin acid, 90 DEG C are warming up to after ten dihydroxystearic acids are completely dissolved, to adding lithium hydroxide solution in saponification kettle, the hydroxide
Lithium solution is prepared from by the lithium hydroxide of 2.9 weight portions and the water of 8.7 weight portions, continues the dehydration that heats up, when saponification kettle
Interior temperature adds the decanedioic acid of 4.8 weight portions and is incubated 30min when rising to 130 DEG C, end temperature rises to 180 DEG C to be stopped heating up,
Circulation temperature lowering, shearing adds the synthesis alkene oil of 18.8 weight portions when saponification temperature in the kettle is down to 150 DEG C, adds 6 weight
Part coal tar, the fatty acid amide phosphate of 0.8 weight portion, 1.2 weight portions are added when saponification temperature in the kettle is down to 100 DEG C
The poly alpha olefin of diphenylamines and 1 weight portion, shearing, degassing is obtained railroad track screw rust-inhibiting lubricant.
Priority Applications (1)
Application Number | Priority Date | Filing Date | Title |
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CN201611135043.6A CN106701258A (en) | 2016-12-11 | 2016-12-11 | Railway track screw anti-rusting lubricating grease and preparation method thereof |
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Application Number | Priority Date | Filing Date | Title |
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CN201611135043.6A CN106701258A (en) | 2016-12-11 | 2016-12-11 | Railway track screw anti-rusting lubricating grease and preparation method thereof |
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CN106701258A true CN106701258A (en) | 2017-05-24 |
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CN201611135043.6A Pending CN106701258A (en) | 2016-12-11 | 2016-12-11 | Railway track screw anti-rusting lubricating grease and preparation method thereof |
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Citations (4)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
CN1526802A (en) * | 2003-03-04 | 2004-09-08 | 夏位松 | Protective oil and grease |
CN101805656A (en) * | 2009-12-30 | 2010-08-18 | 成都蜀光石油化学有限公司 | Grease used for metal fastener |
CN105132097A (en) * | 2015-08-11 | 2015-12-09 | 新乡市恒星化工有限责任公司 | Preparation method of railway track spike anticorrosive grease |
CN105733753A (en) * | 2014-12-10 | 2016-07-06 | 中国石油天然气股份有限公司 | Lubricating grease composition, and preparation method and application thereof |
-
2016
- 2016-12-11 CN CN201611135043.6A patent/CN106701258A/en active Pending
Patent Citations (4)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
CN1526802A (en) * | 2003-03-04 | 2004-09-08 | 夏位松 | Protective oil and grease |
CN101805656A (en) * | 2009-12-30 | 2010-08-18 | 成都蜀光石油化学有限公司 | Grease used for metal fastener |
CN105733753A (en) * | 2014-12-10 | 2016-07-06 | 中国石油天然气股份有限公司 | Lubricating grease composition, and preparation method and application thereof |
CN105132097A (en) * | 2015-08-11 | 2015-12-09 | 新乡市恒星化工有限责任公司 | Preparation method of railway track spike anticorrosive grease |
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PB01 | Publication | ||
PB01 | Publication | ||
SE01 | Entry into force of request for substantive examination | ||
WD01 | Invention patent application deemed withdrawn after publication | ||
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Application publication date: 20170524 |