CN107418682A - A kind of unmanned plane special lube - Google Patents

A kind of unmanned plane special lube Download PDF

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Publication number
CN107418682A
CN107418682A CN201710660895.5A CN201710660895A CN107418682A CN 107418682 A CN107418682 A CN 107418682A CN 201710660895 A CN201710660895 A CN 201710660895A CN 107418682 A CN107418682 A CN 107418682A
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Prior art keywords
additive
unmanned plane
oil
components
alhpa olefin
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CN201710660895.5A
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Chinese (zh)
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CN107418682B (en
Inventor
王红光
孙风成
王雄斌
孙海明
李鲁涛
孟宪雨
朱美华
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Yantai East Thermal Power Co.,Ltd.
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YANTAI HENGBANG CHEMICAL CO Ltd
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Publication of CN107418682A publication Critical patent/CN107418682A/en
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    • C—CHEMISTRY; METALLURGY
    • C10—PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
    • C10M—LUBRICATING COMPOSITIONS; USE OF CHEMICAL SUBSTANCES EITHER ALONE OR AS LUBRICATING INGREDIENTS IN A LUBRICATING COMPOSITION
    • C10M169/00—Lubricating compositions characterised by containing as components a mixture of at least two types of ingredient selected from base-materials, thickeners or additives, covered by the preceding groups, each of these compounds being essential
    • C10M169/04—Mixtures of base-materials and additives
    • C10M169/048—Mixtures of base-materials and additives the additives being a mixture of compounds of unknown or incompletely defined constitution, non-macromolecular and macromolecular compounds
    • C—CHEMISTRY; METALLURGY
    • C10—PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
    • C10M—LUBRICATING COMPOSITIONS; USE OF CHEMICAL SUBSTANCES EITHER ALONE OR AS LUBRICATING INGREDIENTS IN A LUBRICATING COMPOSITION
    • C10M2201/00—Inorganic compounds or elements as ingredients in lubricant compositions
    • C10M2201/04—Elements
    • C10M2201/041—Carbon; Graphite; Carbon black
    • C—CHEMISTRY; METALLURGY
    • C10—PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
    • C10M—LUBRICATING COMPOSITIONS; USE OF CHEMICAL SUBSTANCES EITHER ALONE OR AS LUBRICATING INGREDIENTS IN A LUBRICATING COMPOSITION
    • C10M2205/00—Organic macromolecular hydrocarbon compounds or fractions, whether or not modified by oxidation as ingredients in lubricant compositions
    • C10M2205/02—Organic macromolecular hydrocarbon compounds or fractions, whether or not modified by oxidation as ingredients in lubricant compositions containing acyclic monomers
    • C10M2205/0206—Organic macromolecular hydrocarbon compounds or fractions, whether or not modified by oxidation as ingredients in lubricant compositions containing acyclic monomers used as base material
    • C—CHEMISTRY; METALLURGY
    • C10—PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
    • C10M—LUBRICATING COMPOSITIONS; USE OF CHEMICAL SUBSTANCES EITHER ALONE OR AS LUBRICATING INGREDIENTS IN A LUBRICATING COMPOSITION
    • C10M2209/00—Organic macromolecular compounds containing oxygen as ingredients in lubricant compositions
    • C10M2209/10—Macromolecular compoundss obtained otherwise than by reactions only involving carbon-to-carbon unsaturated bonds
    • C10M2209/102—Polyesters
    • C10M2209/1023—Polyesters used as base material
    • C—CHEMISTRY; METALLURGY
    • C10—PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
    • C10M—LUBRICATING COMPOSITIONS; USE OF CHEMICAL SUBSTANCES EITHER ALONE OR AS LUBRICATING INGREDIENTS IN A LUBRICATING COMPOSITION
    • C10M2217/00—Organic macromolecular compounds containing nitrogen as ingredients in lubricant compositions
    • C10M2217/06—Macromolecular compounds obtained by functionalisation op polymers with a nitrogen containing compound
    • C—CHEMISTRY; METALLURGY
    • C10—PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
    • C10M—LUBRICATING COMPOSITIONS; USE OF CHEMICAL SUBSTANCES EITHER ALONE OR AS LUBRICATING INGREDIENTS IN A LUBRICATING COMPOSITION
    • C10M2219/00—Organic non-macromolecular compounds containing sulfur, selenium or tellurium as ingredients in lubricant compositions
    • C10M2219/02—Sulfur-containing compounds obtained by sulfurisation with sulfur or sulfur-containing compounds
    • C—CHEMISTRY; METALLURGY
    • C10—PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
    • C10M—LUBRICATING COMPOSITIONS; USE OF CHEMICAL SUBSTANCES EITHER ALONE OR AS LUBRICATING INGREDIENTS IN A LUBRICATING COMPOSITION
    • C10M2219/00—Organic non-macromolecular compounds containing sulfur, selenium or tellurium as ingredients in lubricant compositions
    • C10M2219/04—Organic non-macromolecular compounds containing sulfur, selenium or tellurium as ingredients in lubricant compositions containing sulfur-to-oxygen bonds, i.e. sulfones, sulfoxides
    • C10M2219/044—Sulfonic acids, Derivatives thereof, e.g. neutral salts
    • C—CHEMISTRY; METALLURGY
    • C10—PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
    • C10M—LUBRICATING COMPOSITIONS; USE OF CHEMICAL SUBSTANCES EITHER ALONE OR AS LUBRICATING INGREDIENTS IN A LUBRICATING COMPOSITION
    • C10M2219/00—Organic non-macromolecular compounds containing sulfur, selenium or tellurium as ingredients in lubricant compositions
    • C10M2219/06—Thio-acids; Thiocyanates; Derivatives thereof
    • C10M2219/062—Thio-acids; Thiocyanates; Derivatives thereof having carbon-to-sulfur double bonds
    • C—CHEMISTRY; METALLURGY
    • C10—PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
    • C10M—LUBRICATING COMPOSITIONS; USE OF CHEMICAL SUBSTANCES EITHER ALONE OR AS LUBRICATING INGREDIENTS IN A LUBRICATING COMPOSITION
    • C10M2223/00—Organic non-macromolecular compounds containing phosphorus as ingredients in lubricant compositions
    • C10M2223/02—Organic non-macromolecular compounds containing phosphorus as ingredients in lubricant compositions having no phosphorus-to-carbon bonds
    • C10M2223/04—Phosphate esters
    • C10M2223/045—Metal containing thio derivatives
    • C—CHEMISTRY; METALLURGY
    • C10—PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
    • C10N—INDEXING SCHEME ASSOCIATED WITH SUBCLASS C10M RELATING TO LUBRICATING COMPOSITIONS
    • C10N2010/00—Metal present as such or in compounds
    • C10N2010/04—Groups 2 or 12
    • C—CHEMISTRY; METALLURGY
    • C10—PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
    • C10N—INDEXING SCHEME ASSOCIATED WITH SUBCLASS C10M RELATING TO LUBRICATING COMPOSITIONS
    • C10N2030/00—Specified physical or chemical properties which is improved by the additive characterising the lubricating composition, e.g. multifunctional additives
    • C10N2030/06—Oiliness; Film-strength; Anti-wear; Resistance to extreme pressure
    • C—CHEMISTRY; METALLURGY
    • C10—PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
    • C10N—INDEXING SCHEME ASSOCIATED WITH SUBCLASS C10M RELATING TO LUBRICATING COMPOSITIONS
    • C10N2030/00—Specified physical or chemical properties which is improved by the additive characterising the lubricating composition, e.g. multifunctional additives
    • C10N2030/08—Resistance to extreme temperature
    • C—CHEMISTRY; METALLURGY
    • C10—PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
    • C10N—INDEXING SCHEME ASSOCIATED WITH SUBCLASS C10M RELATING TO LUBRICATING COMPOSITIONS
    • C10N2030/00—Specified physical or chemical properties which is improved by the additive characterising the lubricating composition, e.g. multifunctional additives
    • C10N2030/10—Inhibition of oxidation, e.g. anti-oxidants
    • C—CHEMISTRY; METALLURGY
    • C10—PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
    • C10N—INDEXING SCHEME ASSOCIATED WITH SUBCLASS C10M RELATING TO LUBRICATING COMPOSITIONS
    • C10N2030/00—Specified physical or chemical properties which is improved by the additive characterising the lubricating composition, e.g. multifunctional additives
    • C10N2030/18—Anti-foaming property

Landscapes

  • Chemical & Material Sciences (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • General Chemical & Material Sciences (AREA)
  • Oil, Petroleum & Natural Gas (AREA)
  • Organic Chemistry (AREA)
  • Lubricants (AREA)

Abstract

The invention provides a kind of unmanned plane special lube, including following components in percentage by weight：Base oil and additive, oily 8 21% based on the addition of additive, the base oil includes three kinds of components：Small viscosity polymerize alhpa olefin 70 80%, polyester 10 15%, and big viscosity polymerize alhpa olefin 5 20%；The additive includes eight kinds of components：The pungent salt 1 3% of the double octyl group alkalescence of sulphur phosphorus, the more succimides 3 6% of polyisobutene, sulfurized alkylphenol calcium 1 3%, hyperalkaline sulfoacid calcium 1 3%, aminothio ester 2% 4%, oil-soluble graphene 0.001 0.005%, complex type antioxidant 0.3 1%, composite anti-foam agent 0.001 0.002%, organic-molybdenum 0.1 0.3%.The present invention has excellent antifriction resistance to elevated temperatures, splendid viscosity temperature characteristic, good antifoam property and Oxidation Stability, can adapt to the of short duration oil-break lubrication of unmanned plane, safety and environmental protection.

Description

A kind of unmanned plane special lube
Technical field
The invention belongs to chemical technology field, relates in particular to a kind of unmanned plane special lube.
Background technology
Unmanned plane can realize higher maneuvering flight ability, can under various flight attitudes reliably working, This can bear bigger maneuvering flight load with regard to all parts of inevitable requirement unmanned plane, meet under various flying conditions Requirement, this also inevitable requirement Unmanned Aerial Vehicle Powerplants lubricating system have bear than there is man-machine more high maneuver flight load And the ability of more harsh flight attitude.Unmanned plane is substantially using there is man-machine existing lubricating oil to be lubricated at present, still Unmanned plane has bigger maneuvering flight load, more stringent flight attitude requires, more due to its special adaptability design Prolonged instantaneous oil-break.Current substitute has man-machine engine oil, in these cases, does not reach good protection It is required that the especially oil-break of longer time, easily causes abrasion.
The content of the invention
The invention provides a kind of unmanned plane special lube, solves the lubricating oil in background technology to unmanned plane up to not The shortcomings that to more preferable protection and easily causing abrasion in oil-break.
The technical proposal of the invention is realized in this way：A kind of unmanned plane special lube, including following percentage by weight Component：Base oil and additive, oily 8-21%, the base oil include three kinds of components based on the addition of additive：It is small Viscosity polymerize alhpa olefin 70-80%, polyester 10-15%, big viscosity polymerization alhpa olefin 5-20%；The additive includes eight kinds of components： The sulphur phosphorus pungent salt 1-3% of double octyl groups alkalescence, polyisobutene more succimide 3-6%, sulfurized alkylphenol calcium 1-3%, hyperalkaline sulfoacid calcium 1-3%, aminothio ester 2%-4%, oil-soluble graphene 0.001-0.005%, complex type antioxidant 0.3-1%, composite anti-foam agent 0.001-0.002%, organic-molybdenum 0.1-0.3%；
Preferably, including following components in percentage by weight：Base oil and additive, it is oily based on the addition of additive 14.8045%, the base oil includes three kinds of components：Small viscosity polymerize alhpa olefin 75%, polyester 12%, and big viscosity polymerize alhpa olefin 13%；The additive includes eight kinds of components：The pungent salt 2% of the double octyl group alkalescence of sulphur phosphorus, the more succimides 5% of polyisobutene, vulcanizes alkane Base phenol calcium 2%, hyperalkaline sulfoacid calcium 2%, aminothio ester 3%, oil-soluble graphene 0.003%, complex type antioxidant 0.6% are compound Anti-foaming agent 0.0015%, organic-molybdenum 0.2%；
Preferably, the small viscosity polymerization alhpa olefin is PAO4；
Preferably, the big viscosity polymerization alhpa olefin is V600.
Aminothio ester, there is prominent abrasion resistant extreme-pressure performance and good antioxidant effect；
Oil-soluble graphene, abrasion resistance protrude, and form layer protecting film, adapt to of short duration oil-break, save；
Complex type antioxidant, excellent high/low temperature antioxygenic property；
Organic-molybdenum, antifriction is wear-resistant, the effect of lubrication；
The pungent salt of the double octyl groups alkalescence of sulphur phosphorus, has excellent anti-oxidant corrosion resistance, and its heat endurance is especially good, oil-soluble and adds Add agent compatibility good；
Sulfurized alkylphenol calcium, there is good high temperature detergency and very strong acid neutralization capacity, antioxidant-anticorrosive properties, control is lived Fill in apical ring carbon distribution significant effect；
Hyperalkaline sulfoacid calcium, there is excellent high temperature detergency and acid neutralization capacity, and there is rust-preventing characteristic, can effectively reduce engine High temperature deposition thing on part, extend the drain period.
The method for making unmanned plane special lube, comprises the following steps：
（1）, put into reactor polyalphaolefin, the polyester of large and small viscosity, be warming up to 60~70 DEG C, stir 8~10 minutes；
（2）, successively put into the pungent salt of the double octyl groups alkalescence of oiliness improver, sulphur phosphorus, the more succimides of polyisobutene, sulfurized alkylphenol calcium, Hyperalkaline sulfoacid calcium, aminothio ester, complex type antioxidant, composite anti-foam agent, oil-soluble graphene, organic-molybdenum；
60 DEG C~70 DEG C of constant temperature, stir 30 minutes, be changed into finished product after 1 μm of sock filtration.
The beneficial effects of the invention are as follows：The robot special lube of the present invention has excellent antifriction, resistance to elevated temperatures, Splendid viscosity temperature characteristic, good antifoam property and Oxidation Stability, high anti-load-carrying ability, energy-conserving and environment-protective.
Embodiment
For a better understanding and implementation, the invention will be further described below：A kind of unmanned plane special lube, it is accurate Standby polymerization alhpa olefin PAO4 750kg, polyester 100kg, polyalphaolefin V600 150 kg, the sulphur phosphorus pungent salt 20kg of double octyl group alkalescence, gathers Isobutene more succimide 50kg, sulfurized alkylphenol calcium 20kg, hyperalkaline sulfoacid calcium 20kg, the kg of aminothio ester 20, oil are molten Property graphene 0.01 kg, the kg of complex type antioxidant 5, the kg of composite anti-foam agent 0.01；The kg of organic-molybdenum 1.
Preparation method：Put into PAO4 into reactor, polyester, V600, be warming up to 60 DEG C -70 DEG C, stir 10 minutes, then The pungent salt of the double octyl group alkalescence of sulphur phosphorus, the more succimides of polyisobutene, sulfurized alkylphenol calcium, hyperalkaline sulfoacid calcium, ammonia are put into successively Base monothioester, complex type antioxidant, ammonium-phosphate mixture, metal deactivator, composite anti-foam agent, oil-soluble graphene, organic-molybdenum, 60 DEG C -70 DEG C of constant temperature stirs 30 minutes, is changed into finished product after 1 μm of sock filtration.
Quality index
The present invention is due to using oil based on clean type, biodegradable artificial oil, being aided with multifunction additive, having oil product There is excellent antifriction, resistance to elevated temperatures, splendid viscosity temperature characteristic, good antifoam property and Oxidation Stability, pour point is low, energy Enough adapt to the of short duration oil-break lubrication of unmanned plane, safety and environmental protection.

Claims (4)

1. a kind of unmanned plane special lube, it is characterised in that including following components in percentage by weight：Base oil and additive, Oily 8-21% based on the addition of additive, the base oil include three kinds of components：Small viscosity polymerize alhpa olefin 70-80%, Polyester 10-15%, big viscosity polymerization alhpa olefin 5-20%；The additive includes eight kinds of components：The pungent salt 1- of the double octyl group alkalescence of sulphur phosphorus 3%, polyisobutene more succimide 3-6%, sulfurized alkylphenol calcium 1-3%, hyperalkaline sulfoacid calcium 1-3%, aminothio ester 2%- 4%, oil-soluble graphene 0.001-0.005%, complex type antioxidant 0.3-1%, composite anti-foam agent 0.001-0.002%, organic-molybdenum 0.1-0.3%。
2. a kind of unmanned plane special lube as claimed in claim 1, it is characterised in that include the group of following percentage by weight Point：Base oil and additive, oily 14.8045% based on the addition of additive, the base oil includes three kinds of components：It is small Viscosity polymerize alhpa olefin 75%, polyester 12%, and big viscosity polymerize alhpa olefin 13%；The additive includes eight kinds of components：Sulphur phosphorus is double pungent The pungent salt 2% of base alkalescence, the more succimides 5% of polyisobutene, sulfurized alkylphenol calcium 2%, hyperalkaline sulfoacid calcium 2%, aminothio ester 3%, oil-soluble graphene 0.003%, complex type antioxidant 0.6%, composite anti-foam agent 0.0015%, organic-molybdenum 0.2%.
A kind of 3. unmanned plane special lube as claimed in claim 1 or 2, it is characterised in that the small viscosity polymerization alhpa olefin For PAO4.
A kind of 4. unmanned plane special lube as claimed in claim 1 or 2, it is characterised in that the big viscosity polymerization alhpa olefin For V600.
CN201710660895.5A 2017-08-04 2017-08-04 Special lubricating oil for unmanned aerial vehicle Active CN107418682B (en)

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CN107418682B CN107418682B (en) 2020-06-02

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Cited By (3)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN109233960A (en) * 2018-10-26 2019-01-18 辽宁海华科技股份有限公司 A kind of industrial robot precision speed reduction device lubricant oil composite
CN110564479A (en) * 2019-07-15 2019-12-13 四川科地亚石油制品有限公司 Graphene lubricating oil
CN113881482A (en) * 2021-09-24 2022-01-04 亚培烯科技（杭州）有限公司 Gearbox transmission lubricant composition and preparation method and application thereof

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CN106883918A (en) * 2017-04-05 2017-06-23 烟台恒邦化工有限公司 A kind of long-life diesel engine oil of high pressure-charging and preparation method thereof

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Cited By (4)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN109233960A (en) * 2018-10-26 2019-01-18 辽宁海华科技股份有限公司 A kind of industrial robot precision speed reduction device lubricant oil composite
CN109233960B (en) * 2018-10-26 2021-08-20 辽宁海华科技股份有限公司 Lubricating oil composition for precision speed reducer of industrial robot
CN110564479A (en) * 2019-07-15 2019-12-13 四川科地亚石油制品有限公司 Graphene lubricating oil
CN113881482A (en) * 2021-09-24 2022-01-04 亚培烯科技（杭州）有限公司 Gearbox transmission lubricant composition and preparation method and application thereof

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Address after: 264117 beijucheng, Dayao Town, Muping District, Yantai City, Shandong Province

Patentee after: Yantai East Thermal Power Co.,Ltd.

Address before: 264117 beijucheng, Dayao Town, Muping District, Yantai City, Shandong Province

Patentee before: YANTAI HUMON CHEMICAL Co.,Ltd.

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Denomination of invention: A special lubricating oil for UAV

Effective date of registration: 20211115

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