CN106700949A - Multifunctional polishing paste and preparation method and usage method thereof - Google Patents
Multifunctional polishing paste and preparation method and usage method thereof Download PDFInfo
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- CN106700949A CN106700949A CN201611210288.0A CN201611210288A CN106700949A CN 106700949 A CN106700949 A CN 106700949A CN 201611210288 A CN201611210288 A CN 201611210288A CN 106700949 A CN106700949 A CN 106700949A
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- C—CHEMISTRY; METALLURGY
- C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
- C09G—POLISHING COMPOSITIONS; SKI WAXES
- C09G1/00—Polishing compositions
- C09G1/06—Other polishing compositions
- C09G1/14—Other polishing compositions based on non-waxy substances
- C09G1/18—Other polishing compositions based on non-waxy substances on other substances
Abstract
The invention discloses a multifunctional polishing past, and the multifunctional polishing paste comprises the following ingredients part by weight: 10-14 parts of methyl adipoyl chloride, 1-2 parts of 7-chloro-4-oxyquinoline-3- carboxylic acid, 2-4 parts of DiMethyl-n-octylchlorosilane, 13-16 parts of wood vinegar, 5-7 parts of trisodium hydrogen 3-carboxylato-2,3-dideoxy-1-hydroxypropane-1,2,3-tricarboxylate, 10-14 parts of EDTA, 3-6 parts of monothioglycerol, 5-7 parts of lycidyl acrylare, and 190-200 parts of water. The polishing paste has powerful functions, not only can effectively prevent workpieces from rusting, improve luster of the workpiece, remove oil, soften the surface of the workpiece to accelerate the grinding effect, also has long storage time, oxidation and precipitation in the process of storage are not prone to happening, and the polishing paste has higher quality.
Description
Technical field
The invention belongs to buffing compound manufacture field, and in particular to a kind of Multifunctional mill photo etching and preparation method thereof and user
Method.
Background technology
Polishing is by the special polishing wheel for being stained with abrasive material（Or band）Rotation, with the process of cutting metal piece surface.
Polishing can remove the various gross imperfections such as burr, corrosion, cut, overlap, weld seam, sand holes, the oxide skin of piece surface, to improve
The flatness and electroplating quality of part.Polishing can once be polished and several times according to piece surface state and quality requirement height
Polishing, Part Surface Roughness Ra values are up to 0.4 μm after polishing, and oil abrasion effect is more preferable.Polishing is applied to processes all metal materials
Material and part nonmetallic materials.Polishing effect depends primarily on the characteristic of abrasive material, the quality of abrasive material, the rigid toughness of polishing wheel and
The rotary speed of wheel shaft.Now with flourishing for machinery industry, polishing is essential in mechanical processing process one
Technique, presently commercially available buffing compound, unitary function is only capable of being provided during polishing the effect of lubrication, therefore grinded
Product quality is poor, surface oxidation it is more serious.
The content of the invention
In order to solve the deficiencies in the prior art, the present invention provides a kind of Multifunctional mill photo etching and preparation method thereof and user
Method.
The present invention is achieved by the following technical solutions.
A kind of Multifunctional mill photo etching, is made up of the component of following weight portion：The chloro- 4- hydroxyls of 10-14 parts of methyl Adipoyl Chloride, 7-
Pungent silane 2-4 parts of 1-2 parts of base quinoline-3-carboxylic acid, Chlorodimethyl, pyrolkigneous liquid 13-16 parts, 5-7 parts of isocitric acid trisodium salt,
EDTA10-14 parts, thioglycerol 3-6 parts, 5-7 parts, water 190-200 parts of acrylic acid glycerine ether-ether.
As the further scheme of invention, a kind of preparation method of Multifunctional mill photo etching, including following operating procedure：
（1）The pyrolkigneous liquid that 0.2-0.3 times of its weight weighs is added to acrylic acid glycerine ether-ether, is then stirred using the rotating speed of 500r/min
After mixing 15min, then thioglycerol is added thereto to, it is standby after continuation stirring 10min；Acrylic acid glycerine ether-ether has more strong
Excitant, after itself and pyrolkigneous liquid and thioglycerol are mixed, can effectively lift its stability, prevent it in the mistake for preparing
Volatilize pollution surrounding air, the security performance of lifting polishing liquid, and pyrolkigneous liquid, thioglycerol and acrylic acid glycerine ether-ether in journey
Synergy, can effectively lift the antioxygenic property of polishing liquid, prevent mechanical part during polishing, due to high temperature hair
Raw oxidation；
（2）After by methyl Adipoyl Chloride, 7- chloro-4-hydroxyls quinoline-3-carboxylic acid, the pungent silane mixture of Chlorodimethyl, it is added thereto to
Remaining pyrolkigneous liquid, after stirring 20min using the rotating speed of 400r/min, then using standby after ultrasonically treated 15min；By mixed liquor
After ultrasonically treated, can significantly increase the synergistic action effect between mixed liquor so that it has excellent antirust, decontamination
Ability, and it can also effectively improve the glossiness of workpiece surface after polishing；
（3）Isocitric acid trisodium salt, EDTA are added to the water, 55 DEG C are heated water to, step is then added thereto to（1）Gained
Mixed liquor, step（2）Gained mixed liquor, after the rotating speed stirring 40min of 600r/min, prepared buffing compound；Isocitric acid three
Sodium salt and EDTA act synergistically, and can play the effective effect for softening workpiece surface, reduce the loss of grinding tool and accelerate iron filings
Come off, prevent its workpiece surface remaining influence polish effect.
As the further scheme of invention, a kind of application method of Multifunctional mill photo etching, by buffing compound and water with 1:50-60
Weight than mixing after, using the rotating speed stirring 30min of 400r/min after, be added thereto to 0.01-0.03 times of polishing liquid weight
The sodium chloride of weight, continues to stir 5min, and polishing liquid is obtained；Sodium chloride has preferable demulsification, can effectively lift solution
Homogeneity so that active ingredient in buffing compound can be uniformly dispersed in liquid is polished.
Beneficial effect：Obtained buffing compound of the invention, it is powerful, the corrosion of workpiece can not only be effectively prevented, improve
The gloss of workpiece, go to degrease, soften workpiece surface to accelerate the effect of grinding, and also with storage time more long, no
Easily during storage, there is oxidation and generation deposited phenomenon, with quality higher.
Specific embodiment
In order that those skilled in the art can be further understood that feature of the invention and technology contents, referring to following has
Close detailed description of the invention.
Embodiment 1
A kind of Multifunctional mill photo etching, is made up of the component of following weight portion：10 parts of methyl Adipoyl Chloride, 7- chloro-4-hydroxyls quinoline-
2 parts of the pungent silane of 1 part of 3- carboxylic acids, Chlorodimethyl, 13 parts of pyrolkigneous liquid, 5 parts of isocitric acid trisodium salt, EDTA10 parts, thioglycerol 3
Part, 5 parts of acrylic acid glycerine ether-ether, 190 parts of water.
As the further scheme of invention, a kind of preparation method of Multifunctional mill photo etching, including following operating procedure：
（1）0.2 times of pyrolkigneous liquid of weight of its weight is added to acrylic acid glycerine ether-ether, is then stirred using the rotating speed of 500r/min
After 15min, then thioglycerol is added thereto to, it is standby after continuation stirring 10min；
（2）After by methyl Adipoyl Chloride, 7- chloro-4-hydroxyls quinoline-3-carboxylic acid, the pungent silane mixture of Chlorodimethyl, it is added thereto to
Remaining pyrolkigneous liquid, after stirring 20min using the rotating speed of 400r/min, then using standby after ultrasonically treated 15min；
（3）Isocitric acid trisodium salt, EDTA are added to the water, 55 DEG C are heated water to, step is then added thereto to（1）Gained
Mixed liquor, step（2）Gained mixed liquor, after the rotating speed stirring 40min of 600r/min, prepared buffing compound.
As the further scheme of invention, a kind of application method of Multifunctional mill photo etching, by buffing compound and water with 1:50
After weight is than mixing, after stirring 30min using the rotating speed of 400r/min, it is added thereto to polish liquid 0.01 times of chlorination of weight of weight
Sodium, continues to stir 5min, and polishing liquid is obtained.
Embodiment 2
A kind of Multifunctional mill photo etching, is made up of the component of following weight portion：12 parts of methyl Adipoyl Chloride, 7- chloro-4-hydroxyls quinoline-
3 parts of the pungent silane of 1 part of 3- carboxylic acids, Chlorodimethyl, 15 parts of pyrolkigneous liquid, 6 parts of isocitric acid trisodium salt, EDTA12 parts, thioglycerol 5
Part, 6 parts of acrylic acid glycerine ether-ether, 195 parts of water.
As the further scheme of invention, a kind of preparation method of Multifunctional mill photo etching, including following operating procedure：
（1）0.2 times of pyrolkigneous liquid of weight of its weight is added to acrylic acid glycerine ether-ether, is then stirred using the rotating speed of 500r/min
After 15min, then thioglycerol is added thereto to, it is standby after continuation stirring 10min；
（2）After by methyl Adipoyl Chloride, 7- chloro-4-hydroxyls quinoline-3-carboxylic acid, the pungent silane mixture of Chlorodimethyl, it is added thereto to
Remaining pyrolkigneous liquid, after stirring 20min using the rotating speed of 400r/min, then using standby after ultrasonically treated 15min；
（3）Isocitric acid trisodium salt, EDTA are added to the water, 55 DEG C are heated water to, step is then added thereto to（1）Gained
Mixed liquor, step（2）Gained mixed liquor, after the rotating speed stirring 40min of 600r/min, prepared buffing compound.
As the further scheme of invention, a kind of application method of Multifunctional mill photo etching, by buffing compound and water with 1:55
After weight is than mixing, after stirring 30min using the rotating speed of 400r/min, it is added thereto to polish liquid 0.02 times of chlorination of weight of weight
Sodium, continues to stir 5min, and polishing liquid is obtained.
Embodiment 3
A kind of Multifunctional mill photo etching, is made up of the component of following weight portion：14 parts of methyl Adipoyl Chloride, 7- chloro-4-hydroxyls quinoline-
4 parts of the pungent silane of 2 parts of 3- carboxylic acids, Chlorodimethyl, 16 parts of pyrolkigneous liquid, 7 parts of isocitric acid trisodium salt, 14 parts of EDTA, thioglycerol 6
Part, 7 parts of acrylic acid glycerine ether-ether, 200 parts of water.
As the further scheme of invention, a kind of preparation method of Multifunctional mill photo etching, including following operating procedure：
（1）0.3 times of pyrolkigneous liquid of weight of its weight is added to acrylic acid glycerine ether-ether, is then stirred using the rotating speed of 500r/min
After 15min, then thioglycerol is added thereto to, it is standby after continuation stirring 10min；
（2）After by methyl Adipoyl Chloride, 7- chloro-4-hydroxyls quinoline-3-carboxylic acid, the pungent silane mixture of Chlorodimethyl, it is added thereto to
Remaining pyrolkigneous liquid, after stirring 20min using the rotating speed of 400r/min, then using standby after ultrasonically treated 15min；
（3）Isocitric acid trisodium salt, EDTA are added to the water, 55 DEG C are heated water to, step is then added thereto to（1）Gained
Mixed liquor, step（2）Gained mixed liquor, after the rotating speed stirring 40min of 600r/min, prepared buffing compound.
As the further scheme of invention, a kind of application method of Multifunctional mill photo etching, by buffing compound and water with 1:60
After weight is than mixing, after stirring 30min using the rotating speed of 400r/min, it is added thereto to polish liquid 0.03 times of chlorination of weight of weight
Sodium, continues to stir 5min, and polishing liquid is obtained.
Application Example：The machinery plant of Ma ' anshan City one, grinding tool is changed once for average every 2 months on grinding machine, later
Using the polishing liquid provided in embodiment 1, under identical working strength, grinding tool is changed once for average every 4 months, and is ground
The workpiece surface for coming is more smooth, and glossiness is higher, and decay resistance and oxidation resistent susceptibility are more superior, and obtained mill
In the one-year age of photo etching storage, macroscopic impurity generation is not found.
Claims (3)
1. a kind of Multifunctional mill photo etching, it is characterised in that be made up of the component of following weight portion：10-14 parts of methyl Adipoyl Chloride,
Pungent silane 2-4 parts of 1-2 parts of 7- chloro-4-hydroxyl quinoline-3-carboxylic acids, Chlorodimethyl, pyrolkigneous liquid 13-16 parts, isocitric acid trisodium salt
5-7 parts, EDTA10-14 parts, thioglycerol 3-6 parts, 5-7 parts, water 190-200 parts of acrylic acid glycerine ether-ether.
2. the preparation method of the Multifunctional mill photo etching described in a kind of claim 1, it is characterised in that including following operation step
Suddenly：
（1）The pyrolkigneous liquid that 0.2-0.3 times of its weight weighs is added to acrylic acid glycerine ether-ether, is then stirred using the rotating speed of 500r/min
After mixing 15min, then thioglycerol is added thereto to, it is standby after continuation stirring 10min；
（2）After by methyl Adipoyl Chloride, 7- chloro-4-hydroxyls quinoline-3-carboxylic acid, the pungent silane mixture of Chlorodimethyl, it is added thereto to
Remaining pyrolkigneous liquid, after stirring 20min using the rotating speed of 400r/min, then using standby after ultrasonically treated 15min；
（3）Isocitric acid trisodium salt, EDTA are added to the water, 55 DEG C are heated water to, step is then added thereto to（1）Gained
Mixed liquor, step（2）Gained mixed liquor, after the rotating speed stirring 40min of 600r/min, prepared buffing compound.
3. the application method of the Multifunctional mill photo etching described in a kind of claim 1, it is characterised in that by buffing compound and water with 1:
After the weight of 50-60 is than mixing, after stirring 30min using the rotating speed of 400r/min, polishing liquid weight 0.01- is added thereto to
0.03 times of sodium chloride of weight, continues to stir 5min, and polishing liquid is obtained.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201611210288.0A CN106700949A (en) | 2016-12-24 | 2016-12-24 | Multifunctional polishing paste and preparation method and usage method thereof |
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|---|---|---|---|
| CN201611210288.0A CN106700949A (en) | 2016-12-24 | 2016-12-24 | Multifunctional polishing paste and preparation method and usage method thereof |
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| CN106700949A true CN106700949A (en) | 2017-05-24 |
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| CN101255378A (en) * | 2008-04-22 | 2008-09-03 | 大连三达奥克化学股份有限公司 | Automobile clutch diaphragm special-purpose water-based milling liquid and production method |
| CN101323813A (en) * | 2007-06-29 | 2008-12-17 | 大连弘瑞化工有限公司 | Multiple-effect type water-based synthesized cutting solution and preparation thereof |
| CN103555410A (en) * | 2013-11-21 | 2014-02-05 | 李荣福 | Water-based antirust grinding cooling liquid for automobile connecting rod as well as preparation method and application of water-based antirust grinding cooling liquid |
| CN104017636A (en) * | 2014-06-06 | 2014-09-03 | 清华大学 | Water soluble full-alloy metal grinding fluid |
| CN104120010A (en) * | 2014-06-30 | 2014-10-29 | 安徽铖友汽车零部件制造有限公司 | High-property water-based cutting fluid for metal working and preparation method thereof |
| CN104212623A (en) * | 2014-09-03 | 2014-12-17 | 句容金猴机械研究所有限公司 | Mechanical lubricating and cutting agent and preparation method thereof |
-
2016
- 2016-12-24 CN CN201611210288.0A patent/CN106700949A/en active Pending
Patent Citations (6)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN101323813A (en) * | 2007-06-29 | 2008-12-17 | 大连弘瑞化工有限公司 | Multiple-effect type water-based synthesized cutting solution and preparation thereof |
| CN101255378A (en) * | 2008-04-22 | 2008-09-03 | 大连三达奥克化学股份有限公司 | Automobile clutch diaphragm special-purpose water-based milling liquid and production method |
| CN103555410A (en) * | 2013-11-21 | 2014-02-05 | 李荣福 | Water-based antirust grinding cooling liquid for automobile connecting rod as well as preparation method and application of water-based antirust grinding cooling liquid |
| CN104017636A (en) * | 2014-06-06 | 2014-09-03 | 清华大学 | Water soluble full-alloy metal grinding fluid |
| CN104120010A (en) * | 2014-06-30 | 2014-10-29 | 安徽铖友汽车零部件制造有限公司 | High-property water-based cutting fluid for metal working and preparation method thereof |
| CN104212623A (en) * | 2014-09-03 | 2014-12-17 | 句容金猴机械研究所有限公司 | Mechanical lubricating and cutting agent and preparation method thereof |
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Application publication date: 20170524 |