CN106700723A - Gravure environment-friendly water-based gold-sand printing ink as well as preparation method and application of gravure environment-friendly water-based gold-sand printing ink - Google Patents
Gravure environment-friendly water-based gold-sand printing ink as well as preparation method and application of gravure environment-friendly water-based gold-sand printing ink Download PDFInfo
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- CN106700723A CN106700723A CN201611013434.0A CN201611013434A CN106700723A CN 106700723 A CN106700723 A CN 106700723A CN 201611013434 A CN201611013434 A CN 201611013434A CN 106700723 A CN106700723 A CN 106700723A
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- C—CHEMISTRY; METALLURGY
- C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
- C09D—COATING COMPOSITIONS, e.g. PAINTS, VARNISHES OR LACQUERS; FILLING PASTES; CHEMICAL PAINT OR INK REMOVERS; INKS; CORRECTING FLUIDS; WOODSTAINS; PASTES OR SOLIDS FOR COLOURING OR PRINTING; USE OF MATERIALS THEREFOR
- C09D11/00—Inks
- C09D11/02—Printing inks
- C09D11/10—Printing inks based on artificial resins
- C09D11/102—Printing inks based on artificial resins containing macromolecular compounds obtained by reactions other than those only involving unsaturated carbon-to-carbon bonds
- C09D11/104—Polyesters
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- C—CHEMISTRY; METALLURGY
- C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
- C09D—COATING COMPOSITIONS, e.g. PAINTS, VARNISHES OR LACQUERS; FILLING PASTES; CHEMICAL PAINT OR INK REMOVERS; INKS; CORRECTING FLUIDS; WOODSTAINS; PASTES OR SOLIDS FOR COLOURING OR PRINTING; USE OF MATERIALS THEREFOR
- C09D11/00—Inks
- C09D11/02—Printing inks
- C09D11/03—Printing inks characterised by features other than the chemical nature of the binder
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- Engineering & Computer Science (AREA)
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Abstract
The invention discloses gravure environment-friendly water-based gold-sand printing ink for silver card paper and glass paper. The gravure environment-friendly water-based gold-sand printing ink is prepared from the following components in percentage by weight: 40 percent to 50 percent of water-based polyester resin, 4 percent to 10 percent of directionally arranged wax paste, 4 percent to 10 percent of absolute ethyl alcohol, 4 percent to 10 percent of de-ionized water, 3 percent to 4.5 percent of a water-based mildew preventive, 0.1 percent to 0.5 percent of a water-based preservative, 0.5 percent to 1.5 percent of a water-based de-foaming agent, 1 percent to 2 percent of a water-based thickener, 0.5 percent to 1.5 percent of an anti-sedimentation agent, 0.5 percent to 1.5 percent of a flatting agent and 20 percent to 30 percent of gold sand. The single-component gravure environment-friendly water-based gold-sand printing ink prepared by the invention has the characteristics of good flowability, good printing adaptability, rapid drying speed, bright color and the like and is suitable for printing other types of paper sheets including the glass paper, the silver card paper and the like.
Description
Technical field
The present invention relates to technical field of ink, in particular it relates to use gravure on a kind of silver foil, cellophane material
Environment-friendly type aqueous gold sand ink.
Background technology
Gravure ink on the market is predominantly solvent type, and substantial amounts of organic solvent is all contained in its composition, in construction
Substantial amounts of organic solvent volatile emission is had in air, environment is polluted, be unfavorable for environmental protection, especially benzene kind solvent is not
Beneficial to the healthy of operating personnel.The present invention uses water-based system, and without esters, ketone, benzene kind solvent, volatile dry is fast,
Do not remained after dry, odorlessness, beneficial to high-speed intaglio printing, without the need for addition plasticiser（Phthalate）, heavy metal free.
Main is that golden light sand effect is good, and bright-colored, colour saturation is high, if being solidified with UV types can cause the ultraviolet light cannot to penetrate bottom
Layer, causes not do problem.
The content of the invention
It is described recessed it is contemplated that overcoming the defect of prior art, there is provided a kind of aqueous environment-friendly type gravure gold sand ink
Print golden bright-colored after environment-friendly type aqueous gold sand ink solidification, substantially, hand touches that sand sense is strong, adhesive force is good, stream to sand streak effect
Levelling is good, without plasticiser（Phthalate）, heavy metal free, environmental protection, quick-drying, VOCs indexs comply fully with domestic standard.
Decorative ink requirement can be met.
Preparation method another object of the present invention is to provide the environment-friendly type aqueous gold sand ink of the gravure.
Application another object of the present invention is to provide the environment-friendly type aqueous gold sand ink of the gravure.
Goal of the invention of the invention is achieved by the following technical programs：
A kind of environment-friendly type aqueous gold sand ink of gravure, including following components in percentage by weight：
Aqueous polyester resin 40%-50%
Align wax liquor 4%-10%
Absolute ethyl alcohol 4%-10%
Deionized water 4%-10%
Water mildow-proof agent 3%-4.5%
Waterborne preservative 0.1 ~ 0.5%
Aqueous defoamer 0.5%-1.5%
Water-based thickener 1 ~ 2%
Anti-settling agent 0.5 ~ 1.5%
Levelling agent 0.5 ~ 1.5%
Golden light sand 20 ~ 30%
Deionized water complements to 100%.
The present invention is matrix resin from waterborne polyester, can assign the environment-friendly type aqueous gold sand ink of gravure and preferably align effect
Really, good adhesive force and drying property；Aligning wax liquor can improve the aligning property of ink, and resistance to scraping, slipping is prevented
Adhesive；Water mildow-proof preservative can ensure that water-based ink, will not be during storage in storage and dried stability
It is putrid and deteriorated, mildew long after drying and forming-film.Water-based thickener can ensure the application property of ink during production printing, be conducive at a high speed
Printing.The addition of anti-settling agent, improves the anti-settling property of ink, it is ensured that golden light sand will not be precipitated when ink prints, it is ensured that print
Foaming and levelling when the addition of the uniformity of brushing effects, defoamer and levelling agent prevents high speed printing is bad, improves levelling speed
Degree, beneficial to high speed printing, the golden light sand of Gao Fenliang is added, and improves the covering of ink, and power of painting reaches high speed printing needs
Tinting strength, tinting power.
Preferably, the waterborne polyester is modified water-soluble polyester resin.It is highly preferred that the aqueous modified polyester resin is
The water-soluble particular polyesters resin K700 of Guangzhou Luo Chi trade Co., Ltds.
Preferably, the wax liquor that aligns is for aqueous oxidic polyethylene wax liquor, it is highly preferred that the aqueous poly- second of oxidation
Alkene wax emulsion is the SXFCJ-121 oxidic polyethylenes dispersion pastel of Guangzhou Ya Ben trade Co., Ltds.
Preferably, the water mildow-proof agent is heterocyclic compound mould inhibitor.
Preferably, the waterborne preservative is polycyclic ketone mixture preservative.
Preferably, the water-based thickener is association type acrylic acid alkali swollen thickener.
Preferably, the anti-settling agent is aqueous bentonite；The defoamer is organic silicon emulsion；The levelling agent is water
Dissolubility organic silicon；The golden light sand is cat gold titanium pearl essence.
The preparation method of the environment-friendly type aqueous gold sand ink of gravure, comprises the following steps：
S1. aqueous polyester resin is added, low whipping speed is to add aqueous defoamer, water under 600~800 revs/min of rotating speed
Property thickener, anti-settling agent aligns wax liquor, and stirring 20~30 minutes is complete to dissolving；
S2. in semi-finished product add water mildow-proof agent, waterborne preservative, levelling agent, be well mixed, mixing speed be 400~
600 revs/min, stir 5~15 minutes；
S3. add golden light sand, improve rotating speed to 600~800 revs/min, stir 20~30 minutes, to stirring；
S4. absolute ethyl alcohol is added, deionized water controls mixing speed for 400~600 revs/min, stirs 10 ~ 20 minutes,
Filtered and packaged with 80 mesh filter screens after stirring.
The invention also discloses application of the environment-friendly type aqueous gold sand ink of the gravure on silver foil, glassine paper.Especially
Ground, the environment-friendly type aqueous gold sand ink of gravure of the present invention is applied to cigarette contracted payment paperboard, glassine paper.
Compared with prior art, the present invention has the advantages that：
1）The present invention is matrix resin from waterborne polyester, can assign the environment-friendly type aqueous gold sand ink of gravure and preferably align
Effect, good adhesive force and drying property；
2）Aligning wax liquor can improve the resistance to scraping of ink, slipping, adhesion inhibiting properties；
3）Water mildow-proof preservative can ensure water-based ink in storage and dried stability, will not be rotten during storage
Lose rotten, mildew long after drying and forming-film；
4）Water-based thickener can ensure the application property of ink during production printing, be conducive to high speed printing.The addition of anti-settling agent, carries
The anti-settling property of ink high, it is ensured that golden light sand will not be precipitated when ink prints, it is ensured that the uniformity of printing effect；
5）Foaming and levelling when the addition of defoamer and levelling agent prevents high speed printing is bad, levelling speed is improved, beneficial to height
Print duplication brush；
6）The golden light sand of Gao Fenliang is added, and improves the covering of ink, power of painting, and reaches the tinting strength, tinting power of high speed printing needs.
Specific embodiment
Following examples and the raw materials used model of comparative example are as follows：
Aqueous modified polyester resin is the water-soluble particular polyesters resin K700 of Guangzhou Luo Chi trade Co., Ltds.
It is aqueous to align the SXFCJ-121 oxidic polyethylenes dispersion pasty state that wax liquor is Guangzhou Ya Ben trade Co., Ltds
Thing.
Waterborne preservative is the MB-11 of De Qian companies.
Water mildow-proof agent is the MB-16 of De Qian companies.
Aqueous defoamer is the 0506 of De Qian companies.
Golden light sand is the KW-307 of Kun Wei companies.
What other did not specialized model is ordinary commercial products.
Embodiment 1
S1. 40 kilograms of aqueous polyester resin is added, low whipping speed is to add aqueous defoamer under 600 revs/min of rotating speed
0.5 kilogram, 1 kilogram of water-based thickener, 0.5 kilogram of anti-settling agent aligns 10 kilograms of wax liquor, and stirring 30 minutes is to having dissolved
Entirely；
S2. 3 kilograms of water mildow-proof agent is added in semi-finished product, 0.5 kilogram of waterborne preservative, 0.5 kilogram of levelling agent, stirring is mixed
Close uniform, mixing speed is 400 revs/min, is stirred 15 minutes；
S3. add 30 kilograms of golden light sand, improve rotating speed to 800 revs/min, stir 20 minutes, to stirring；
S4. 4 kilograms of absolute ethyl alcohol is added, 10 kilograms of deionized water controls mixing speed for 600 revs/min, stirs 10 points
Clock, is filtered and packaged after stirring with 80 mesh filter screens.
Embodiment 2
S1. 45 kilograms of aqueous polyester resin is added, low whipping speed is to add aqueous defoamer under 700 revs/min of rotating speed
1.5 kilograms, 1.5 kilograms of water-based thickener, 1.5 kilograms of anti-settling agent aligns 7 kilograms of wax liquor, and stirring 25 minutes is to having dissolved
Entirely；
S2. 4 kilograms of water mildow-proof agent is added in semi-finished product, 0.3 kilogram of waterborne preservative, 1.5 kilograms of levelling agent, stirring is mixed
Close uniform, mixing speed is 500 revs/min, is stirred 10 minutes；
S3. add 20 kilograms of golden light sand, improve rotating speed to 700 revs/min, stir 15 minutes, to stirring；
S4. 10 kilograms of absolute ethyl alcohol is added, 7.7 kilograms of deionized water controls mixing speed for 500 revs/min, stirring 15
Minute, filtered and packaged with 80 mesh filter screens after stirring.
Embodiment 3
S1. 50 kilograms of aqueous polyester resin is added, low whipping speed is to add aqueous defoamer 1 under 800 revs/min of rotating speed
Kilogram, 2 kilograms of water-based thickener, 1 kilogram of anti-settling agent aligns 4 kilograms of wax liquor, and stirring is extremely dissolved complete for 20 minutes；
S2. 4.5 kilograms of water mildow-proof agent is added in semi-finished product, 0.1 kilogram of waterborne preservative, 1 kilogram of levelling agent, stirring is mixed
Close uniform, mixing speed is 600 revs/min, is stirred 5 minutes；
S3. add 25 kilograms of golden light sand, improve rotating speed to 800 revs/min, stir 10 minutes, to stirring；
S4. 7.4 kilograms of absolute ethyl alcohol is added, 4 kilograms of deionized water controls mixing speed for 400 revs/min, stirs 20 points
Clock, is filtered and packaged after stirring with 80 mesh filter screens.
Comparative example 1
S1. water-based acrylic resin is added（The AC-0304JW of Zhuhai Ji Li chemical enterprises Co., Ltd）40 kilograms, in stirring
Speed is that 0.5 kilogram of aqueous defoamer is added under 600 revs/min of rotating speed, 1 kilogram of water-based thickener, 0.5 kilogram of anti-settling agent,
10 kilograms of wax liquor is aligned, stirring is extremely dissolved complete for 30 minutes；
S2. 3 kilograms of water mildow-proof agent is added in semi-finished product, 0.5 kilogram of waterborne preservative, 0.5 kilogram of levelling agent, stirring is mixed
Close uniform, mixing speed is 400 revs/min, is stirred 15 minutes；
S3. add 30 kilograms of golden light sand, improve rotating speed to 800 revs/min, stir 20 minutes, to stirring；
S4. 4 kilograms of absolute ethyl alcohol is added, 10 kilograms of deionized water controls mixing speed for 600 revs/min, stirs 10 points
Clock, is filtered and packaged after stirring with 80 mesh filter screens.
Comparative example 2
S1 adds 45 kilograms of aqueous polyester resin, and low whipping speed is to add aqueous defoamer 1.5 under 700 revs/min of rotating speed
Kilogram, 1.5 kilograms of water-based thickener, 1.5 kilograms of anti-settling agent, aqueous wax emulsion（Guangzhou Yang Song trade Co., Ltds agency's
TANATEX5441 its chlorinated polypropylene wax emulsions）7 kilograms, stirring is extremely dissolved complete for 25 minutes；
S2. 4 kilograms of water mildow-proof agent is added in semi-finished product, 0.3 kilogram of waterborne preservative, 1.5 kilograms of levelling agent, stirring is mixed
Close uniform, mixing speed is 500 revs/min, is stirred 10 minutes；
S3. add 20 kilograms of golden light sand, improve rotating speed to 700 revs/min, stir 15 minutes, to stirring；
S4. 10 kilograms of absolute ethyl alcohol is added, 7.7 kilograms of deionized water controls mixing speed for 500 revs/min, stirring 15
Minute, filtered and packaged with 80 mesh filter screens after stirring.
Comparative example 3
S1.S1. water-based acrylic resin is added（The AC-0304JW of Zhuhai Ji Li chemical enterprises Co., Ltd）50 kilograms, stirring
Mix 1 kilogram of aqueous defoamer of addition, 2 kilograms of water-based thickener, 1 kilogram of anti-settling agent, water under the rotating speed that speed is 800 revs/min
Property wax emulsion（The TANATEX5441 its chlorinated polypropylene wax emulsions of Guangzhou Yang Song trade Co., Ltds agency）4 kilograms, stirring 20
Minute is complete to dissolving；
S2. 4.5 kilograms of water mildow-proof agent is added in semi-finished product, 0.1 kilogram of waterborne preservative, 1 kilogram of levelling agent, stirring is mixed
Close uniform, mixing speed is 600 revs/min, is stirred 5 minutes；
S3. add 25 kilograms of golden light sand, improve rotating speed to 800 revs/min, stir 10 minutes, to stirring；
S4. 7.4 kilograms of absolute ethyl alcohol is added, 4 kilograms of deionized water controls mixing speed for 400 revs/min, stirs 20 points
Clock, is filtered and packaged after stirring with 80 mesh filter screens.
Environment-friendly type aqueous gold sand ink prepared by embodiment and comparative example is milky, by prepared environment-friendly type water
Property gold sand ink be coated in gold and silver cardboard material, after hot blast solidification, investigate the performance of environment-friendly type aqueous gold sand ink, its performance
Test result is shown in Table 1.
Method for testing performance is as follows：
Adhesive force：By GB《GB9286-1988》Cross-cut methods test is carried out by film coated surface.
Tinting strength, tinting power：By GB《GB/T 14624.2-2008》Test；
Gold sand arrangement property：Visually
Viscosity：Tested with rotation viscometer；
Gloss：Press《GB/T 13217.2-2009》Test；
Bending：Press《GB T 1731-1993》Paint film flexibility determination method is tested；
It is water-fast：Press《GB T 1733-1993》Paint film water resistance determines the test of Division A League Matches of French Football method；
Resistance to ethanol：By 500 grams/cm of power, 99.6% alcohol rubs one and is back-calculated once back and forth, 2 ~ 3 centimetres of stroke；
Abrasion-resistant：RCA175 gram force friction testings are pressed with paper tape tester；
Solid content：By GB《GB/T 1725-2007》Test；
The testing result of the environment-friendly type aqueous gold sand ink of gravure prepared by the embodiment of table 1 and comparative example
To sum up：Embodiment has visual metal sense strong, aligns, bright-colored feature, and the visual metal sense of comparative example is poor, face
Color is gloomy, blacks, not bright-coloured shortcoming.
Embodiment described above only expresses embodiments of the present invention, and its description is more specific and detailed, but can not
Therefore the limitation to the scope of the claims of the present invention is interpreted as, as long as the skill obtained in the form of equivalent or equivalent transformation
Art scheme, all should be included within the protection domain of the claims in the present invention.
Claims (10)
1. the environment-friendly type aqueous gold sand ink of a kind of gravure, it is characterised in that including following components in percentage by weight：
Aqueous polyester resin 40%-50%
Align wax liquor 4%-10%
Absolute ethyl alcohol 4%-10%
Deionized water 4%-10%
Water mildow-proof agent 3%-4.5%
Waterborne preservative 0.1 ~ 0.5%
Aqueous defoamer 0.5%-1.5%
Water-based thickener 1 ~ 2%
Anti-settling agent 0.5 ~ 1.5%
Levelling agent 0.5 ~ 1.5%
Golden light sand 20 ~ 30%；
Deionized water complements to 100%.
2. the environment-friendly type aqueous gold sand ink of gravure according to claim 1, it is characterised in that the aqueous polyester resin is water
The special modified polyester resin of property.
3. the environment-friendly type aqueous gold sand ink of gravure according to claim 1, it is characterised in that the wax liquor that aligns is for water
Property oxidic polyethylene wax liquor.
4. the environment-friendly type aqueous gold sand ink of gravure according to claim 1, it is characterised in that the water mildow-proof agent is heterocycle
Compound mould inhibitor.
5. the environment-friendly type aqueous gold sand ink of gravure according to claim 1, it is characterised in that the waterborne preservative is ketone
Compound preservative.
6. the environment-friendly type aqueous gold sand ink of gravure according to claim 1, it is characterised in that the aqueous defoamer is poly- silicon
Oxygen alkane emulsion.
7. the environment-friendly type aqueous gold sand ink of gravure according to claim 1, it is characterised in that the water-based thickener is to associate
Type acrylic acid alkali swollen thickener.
8. the environment-friendly type aqueous gold sand ink of gravure according to claim 1, it is characterised in that the anti-settling agent is aqueous swelling
Native anti-settling agent；The levelling agent is organic silicon emulsion levelling agent；The golden light sand is cat gold titanium pearl essence.
9. a kind of preparation method of the environment-friendly type aqueous gold sand ink of gravure described in claim 1 to 8 any one, its feature exists
In comprising the following steps：
S1. aqueous polyester resin is added, low whipping speed is to add aqueous defoamer, water under 600~800 revs/min of rotating speed
Property thickener, anti-settling agent aligns wax liquor, and stirring 20~30 minutes is complete to dissolving；
S2. in semi-finished product add water mildow-proof agent, waterborne preservative, levelling agent, be well mixed, mixing speed be 400~
600 revs/min, stir 5~15 minutes；
S3. add golden light sand, improve rotating speed to 600~800 revs/min, stir 20~30 minutes, to stirring；
S4. absolute ethyl alcohol is added, deionized water controls mixing speed for 400~600 revs/min, stirs 10 ~ 20 minutes,
Filtered and packaged with 80 mesh filter screens after stirring.
10. a kind of environment-friendly type aqueous gold sand ink of gravure described in claim 1 to 8 any one is on silver foil, glassine paper
Using.
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| CN201611013434.0A CN106700723A (en) | 2016-11-18 | 2016-11-18 | Gravure environment-friendly water-based gold-sand printing ink as well as preparation method and application of gravure environment-friendly water-based gold-sand printing ink |
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| CN201611013434.0A CN106700723A (en) | 2016-11-18 | 2016-11-18 | Gravure environment-friendly water-based gold-sand printing ink as well as preparation method and application of gravure environment-friendly water-based gold-sand printing ink |
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Cited By (6)
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| CN108624129A (en) * | 2018-05-31 | 2018-10-09 | 厦门欧化实业有限公司 | Fast-drying aqueous ink of a kind of damage resistant environmental protection and its preparation method and application |
| CN108948866A (en) * | 2018-08-07 | 2018-12-07 | 长春吉星印务有限责任公司 | One kind becoming special printing inks and preparation method thereof for the aqueous light of intaglio plate green |
| CN109401427A (en) * | 2018-10-11 | 2019-03-01 | 厦门欧化实业有限公司 | A kind of colored ink and preparation method thereof on packing |
| CN110939011A (en) * | 2018-09-22 | 2020-03-31 | 东莞市锐泽创艺新材料有限公司 | Silver diamond high-flash packaging paper and manufacturing process thereof |
| CN111379191A (en) * | 2018-12-28 | 2020-07-07 | 上海杰易森股份有限公司 | Primer coating for water-based silver cardboard and preparation method thereof |
| CN115093749A (en) * | 2022-07-13 | 2022-09-23 | 中瀚新材料科技有限公司 | Environment-friendly gravure water-based ink and preparation method thereof |
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Cited By (7)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN108624129A (en) * | 2018-05-31 | 2018-10-09 | 厦门欧化实业有限公司 | Fast-drying aqueous ink of a kind of damage resistant environmental protection and its preparation method and application |
| CN108948866A (en) * | 2018-08-07 | 2018-12-07 | 长春吉星印务有限责任公司 | One kind becoming special printing inks and preparation method thereof for the aqueous light of intaglio plate green |
| CN110939011A (en) * | 2018-09-22 | 2020-03-31 | 东莞市锐泽创艺新材料有限公司 | Silver diamond high-flash packaging paper and manufacturing process thereof |
| CN109401427A (en) * | 2018-10-11 | 2019-03-01 | 厦门欧化实业有限公司 | A kind of colored ink and preparation method thereof on packing |
| CN111379191A (en) * | 2018-12-28 | 2020-07-07 | 上海杰易森股份有限公司 | Primer coating for water-based silver cardboard and preparation method thereof |
| CN115093749A (en) * | 2022-07-13 | 2022-09-23 | 中瀚新材料科技有限公司 | Environment-friendly gravure water-based ink and preparation method thereof |
| CN115093749B (en) * | 2022-07-13 | 2023-11-14 | 中瀚新材料科技有限公司 | Environment-friendly gravure water-based ink and preparation method thereof |
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Application publication date: 20170524 |
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