CN106675865A - Dioscorea-cirrhosa-extract-containing handmade soap - Google Patents
Dioscorea-cirrhosa-extract-containing handmade soap Download PDFInfo
- Publication number
- CN106675865A CN106675865A CN201611256655.0A CN201611256655A CN106675865A CN 106675865 A CN106675865 A CN 106675865A CN 201611256655 A CN201611256655 A CN 201611256655A CN 106675865 A CN106675865 A CN 106675865A
- Authority
- CN
- China
- Prior art keywords
- extract
- dioscorea
- cirrhosa
- rhizoma dioscoreae
- dioscoreae cirrhosae
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Pending
Links
Classifications
-
- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
- C11D9/00—Compositions of detergents based essentially on soap
- C11D9/02—Compositions of detergents based essentially on soap on alkali or ammonium soaps
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
- A61Q19/00—Preparations for care of the skin
- A61Q19/02—Preparations for care of the skin for chemically bleaching or whitening the skin
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
- A61Q19/00—Preparations for care of the skin
- A61Q19/10—Washing or bathing preparations
-
- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
- C11D9/00—Compositions of detergents based essentially on soap
- C11D9/04—Compositions of detergents based essentially on soap containing compounding ingredients other than soaps
- C11D9/22—Organic compounds, e.g. vitamins
- C11D9/38—Products in which the composition is not well defined
Abstract
The invention mainly relates to a preparation method of dioscorea-cirrhosa-extract-containing handmade soap. The method comprises the following steps: putting dioscorea cirrhosa residues into a vacuum drying oven, drying for several hours, pulverizing by a high speed pulverizer, passing through a 50-mesh screen to obtain dioscorea cirrhosa powder, and preserving in a normal-temperature dry environment for later use; putting certain amounts of dioscorea cirrhosa powder and sodium sulfite into a round-bottom beaker; adding a certain amount of water, putting the round-bottom beaker into an ultrasonic generator, setting the ultrasonic frequency and ultrasonic time, filtering under reduced pressure to obtain a tannin extract, adding a certain amount of ethanol into the extract, uniformly mixing, centrifugating at high speed, and collecting the supernate to obtain a purified dioscorea cirrhosa tannin extract; and proportionally stirring the purified dioscorea cirrhosa extract and deionized water uniformly, adding the oil phase, and stirring uniformly, thereby obtaining the dioscorea-cirrhosa-extract-containing handmade soap. The dioscorea-cirrhosa-extract-containing handmade soap can clean and whiten the skin, and has the characteristics of accessible raw materials and simple technique.
Description
Technical field
The invention belongs to daily wash protector for collar domain, more particularly, to a kind of handmade soap containing dye yam extract and its preparation side
Method.
Background technology
The color of skin is mainly determined that melanic generation is the melanocyte under action of ultraviolet radiation by melanin content
Interior L-Tyrosine Jing tyrosinase catalysis synthesis.Tannin can absorb ultraviolet, again can tryrosinase and catalase always
Activity, can also make melanin reduction-decolor, moreover it is possible to effective Scavenger of ROS, therefore in cosmetics addition containing tanning matter tool
There is white-skinned face function.
Tannin contains compared with polyphenol hydroxyl as a kind of polyphenols, wide material sources, molecular structure, can pass through with protein
Hyarogen-bonding is combined, and is conducive to introducing charged group（Nitrogen-containing group, sulfate group）, its B ring contains ortho position phenolic hydroxyl group, energy
Enough and complexing of metal ion forms stable five-membered ring complex.
There is a national non-material cultural heritage-watered gauze in Shunde area, its complex manufacturing technology, will to environment
Ask high, raw material is Rhizoma Dioscoreae Cirrhosae, squeezes the juice using Rhizoma Dioscoreae Cirrhosae and carry out tie dyeing to silk, subsequently the outdoor accumulation of discarded Rhizoma Dioscoreae Cirrhosae slag, Jing air-dries laggard
Row burning disposal, not only wastes a large amount of Rhizoma Dioscoreae Cirrhosae resources during it, and destruction is caused to local environment.Because of discarded Rhizoma Dioscoreae Cirrhosae residue
Middle tannin content is higher, and Rhizoma Dioscoreae Cirrhosae tannin is poly original cyanidin, number-average molecular weight 4800 or so, the degree of polymerization 16.To solve fragrant cloud
The Rhizoma Dioscoreae Cirrhosae slag de-referencing problem that yarn production brings, using Rhizoma Dioscoreae Cirrhosae slag tannin is extracted, and its extract is used to prepare natural handmade soap product,
Make handmade soap that not only there is stronger dirt-removing power, also with white-skinned face function, make handmade soap that there is higher cost performance.
The content of the invention
The purpose of the present invention is not enough for prior art, develop a kind of process is simple, with white-skinned face function containing Rhizoma Dioscoreae Cirrhosae
The handmade soap of extract.
Handmade soap is prepared in the present invention using dye yam extract to comprise the following steps：
（1）Rhizoma Dioscoreae Cirrhosae slag is put to vacuum drying oven uniform temperature is set, powder is carried out using high speed disintegrator after some hours of drying
It is broken, to cross 50 mesh sieves and obtain Rhizoma Dioscoreae Cirrhosae powder, normal temperature drying environment is saved backup.Take a certain amount of Rhizoma Dioscoreae Cirrhosae powder and sodium sulfite is put to circle
Bottom beaker,.Add and be placed in after a certain amount of water in ultrasonic generator, supersonic frequency and ultrasonic time are set, Jing after filtration under diminished pressure,
Tanning extract is obtained, quantitative ethanol is added in extract, high speed centrifugation after mix homogeneously collects the potato that supernatant obtains purification
Liang tanning extracts.
（2）Configure a certain amount of alkali liquor.Weigh a certain amount of American Avocado Tree oil, Oleum Cocois, Oleum Vitis viniferae and purification Rhizoma Dioscoreae Cirrhosae tannin
Extract, stirs, and oil phase and water are mutually warming up to uniform temperature, and alkali liquor is poured into after oil phase, certain hour is stirred, by soap
Liquid is transferred to the solidification of mould Temperature fall.
Handmade soap containing dye yam extract of the present invention, has whitening effect simultaneously with process is simple.
Specific embodiment
With reference to specific embodiment, the invention will be further described
A kind of utilization dye yam extract of embodiment 1 is modified and prepares the preparation of tannin surfactant and comprise the following steps：
（1）Rhizoma Dioscoreae Cirrhosae slag is put to vacuum drying oven temperature 50 C is set, be dried after 48h and crushed using high speed disintegrator, mistake
50 mesh sieves obtain Rhizoma Dioscoreae Cirrhosae powder, and normal temperature drying environment is saved backup.The sodium sulfite for taking 20g Rhizoma Dioscoreae Cirrhosaes powder and 1g is put to round bottom burning
Cup,.Add and be placed in after a certain amount of water in ultrasonic generator, setting supersonic frequency is 40kHZ, Jing after filtration under diminished pressure, obtains tannin
Extract, in extract ethanol is added（V extracts：V ethanol=1：2）, 3500rpm centrifugations 20min, collects after mix homogeneously
Supernatant obtains the Rhizoma Dioscoreae Cirrhosae tanning extract of purification.
（2）By weight：10 ~ 20 parts of American Avocado Tree oil, 10 ~ 20 parts of Oleum Cocois, 5 ~ 10 parts of Oleum Vitis viniferae and purification Rhizoma Dioscoreae Cirrhosae list
Peaceful 10 ~ 20 parts of extract, the heating that stirs rises high-temperature to 50 55 °C, while adding ionized water to configure a certain amount of alkali liquor
The heating that stirs rises high-temperature to 50 55 °C, alkali liquor is poured slowly into oil phase, high-speed stirred is uniform, and soap lye is turned
Move to the solidification of mould Temperature fall.
Embodiment 2
By weight：20 parts of American Avocado Tree oil, 15 parts of Oleum Cocois, 5 ~ 10 parts of Oleum Vitis viniferae, 5 ~ 10 parts of argan oil and purification
20 parts of Rhizoma Dioscoreae Cirrhosae tanning extract, the heating that stirs rises high-temperature to 50 55 °C, while adding ionized water configuration a certain amount of
Alkali liquor stirs heating liter high-temperature to 50 55 °C, alkali liquor is poured slowly into oil phase, high-speed stirred is uniform, by soap
Liquid is transferred to the solidification of mould Temperature fall.
Claims (3)
1. Rhizoma Dioscoreae Cirrhosae slag is put to vacuum drying oven and uniform temperature is set, powder is carried out using high speed disintegrator after some hours of drying
It is broken, to cross 50 mesh sieves and obtain Rhizoma Dioscoreae Cirrhosae powder, normal temperature drying environment is saved backup, and takes a certain amount of Rhizoma Dioscoreae Cirrhosae powder and sodium sulfite is put to circle
Bottom beaker, adds and is placed in ultrasonic generator after a certain amount of water, arranges supersonic frequency and ultrasonic time, Jing after filtration under diminished pressure,
Tanning extract is obtained, quantitative ethanol is added in extract, high speed centrifugation after mix homogeneously collects the potato that supernatant obtains purification
Liang tanning extracts；A certain amount of alkali liquor is configured, a certain amount of American Avocado Tree oil, Oleum Cocois, Oleum Vitis viniferae and purification Rhizoma Dioscoreae Cirrhosae list is weighed
Peaceful extract, stirs, and oil phase and water are mutually warming up to uniform temperature, and alkali liquor is poured into after oil phase, stirs certain hour, will
Soap lye is transferred to the solidification of mould Temperature fall.
2. the preparation method according to claim 1, it is characterised in that Rhizoma Dioscoreae Cirrhosae tanning extract is 1 with proportion of ethanol：2.
3. the preparation method according to claim 1, it is characterised in that use raw material from Rhizoma Dioscoreae Cirrhosae slag or Rhizoma Dioscoreae Cirrhosae.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201611256655.0A CN106675865A (en) | 2016-12-30 | 2016-12-30 | Dioscorea-cirrhosa-extract-containing handmade soap |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201611256655.0A CN106675865A (en) | 2016-12-30 | 2016-12-30 | Dioscorea-cirrhosa-extract-containing handmade soap |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| CN106675865A true CN106675865A (en) | 2017-05-17 |
Family
ID=58873483
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN201611256655.0A Pending CN106675865A (en) | 2016-12-30 | 2016-12-30 | Dioscorea-cirrhosa-extract-containing handmade soap |
Country Status (1)
| Country | Link |
|---|---|
| CN (1) | CN106675865A (en) |
Citations (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN1379033A (en) * | 2001-03-30 | 2002-11-13 | 住建产业株式会社 | Method of producing tannin and its application |
| CN101613646A (en) * | 2009-08-05 | 2009-12-30 | 五峰赤诚生物科技有限公司 | A kind of tannin soap and preparation method thereof |
| CN106083946A (en) * | 2016-06-07 | 2016-11-09 | 华南理工大学 | A kind of process extracting tannin from dye yam |
-
2016
- 2016-12-30 CN CN201611256655.0A patent/CN106675865A/en active Pending
Patent Citations (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN1379033A (en) * | 2001-03-30 | 2002-11-13 | 住建产业株式会社 | Method of producing tannin and its application |
| CN101613646A (en) * | 2009-08-05 | 2009-12-30 | 五峰赤诚生物科技有限公司 | A kind of tannin soap and preparation method thereof |
| CN106083946A (en) * | 2016-06-07 | 2016-11-09 | 华南理工大学 | A kind of process extracting tannin from dye yam |
Non-Patent Citations (1)
| Title |
|---|
| 熊晓燕等: ""从薯莨中提取单宁的最佳工艺条件研究"", 《广东工业大学学报》 * |
Similar Documents
| Publication | Publication Date | Title |
|---|---|---|
| CN103205310A (en) | Method for sequentially extracting tea saponin and tea seed oil from oil-tea camellia seeds | |
| CN104004592B (en) | A kind of method simultaneously extracting essential oil and pectin from fresh peel of Citrus reticulata Blanco | |
| CN102210472A (en) | Method for extracting flavone compounds from granatum | |
| CN102824294A (en) | Hair-loss-preventing shampoo and preparation method thereof | |
| CN104629902A (en) | Method for extracting maize germ oil assisted by ethyl alcohol and steam explosion | |
| CN103725032A (en) | Preparation method and application of natural lotus receptacle pigment | |
| CN105708919B (en) | The extracting method of polyphenol and flavones in a kind of Black Box Tracing | |
| CN101921344A (en) | Method for extracting polysaccharides from Lilium Brownii | |
| CN102824291A (en) | Dandruff-removing and itching-relieving shampoo and preparation method thereof | |
| CN108611897A (en) | A method of extraction fruits and vegetables residue prepares levelling agent | |
| CN106675865A (en) | Dioscorea-cirrhosa-extract-containing handmade soap | |
| CN105998792A (en) | Method for extracting general flavones from chequer-shaped indocalamus leaves | |
| CN103239513B (en) | Production technology of prepared fleeceflower root | |
| CN102406582A (en) | Natural hair dye composition and preparation method thereof | |
| CN103468747A (en) | Method for preparing vaccinium bracteatum thunb leaf pigment through enzymic method | |
| CN103536495A (en) | Preparation method of grape seed procyanidin sun cream | |
| CN108587818B (en) | Peony seed oil antibacterial skin care soap and preparation method thereof | |
| CN102836103A (en) | Bamboo charcoal facial cleanser | |
| CN106137843A (en) | Wild Hibisci Mutabilis cosmetic water and preparation method thereof | |
| CN102836102A (en) | Method for preparing bamboo charcoal facial cleanser | |
| CN105064076A (en) | Method for dyeing cotton fabric by use of nutshell pigment | |
| CN111184759A (en) | Preparation method of total saponins of phyllanthus emblica | |
| CN102366368A (en) | Gynostemma pentaphylla shampoo | |
| CN104327131A (en) | Method for extracting punicalagin from pomegranate peel | |
| CN106592213A (en) | Modified tannin antibacterial finishing agent prepared from diosorea cirrhosa extract solution |
Legal Events
| Date | Code | Title | Description |
|---|---|---|---|
| PB01 | Publication | ||
| PB01 | Publication | ||
| SE01 | Entry into force of request for substantive examination | ||
| SE01 | Entry into force of request for substantive examination | ||
| WD01 | Invention patent application deemed withdrawn after publication | ||
| WD01 | Invention patent application deemed withdrawn after publication |
Application publication date: 20170517 |