CN106667802A - Composition for solubilizing natural vegetable oil and fat, application of composition and cosmetic prepared from composition - Google Patents
Composition for solubilizing natural vegetable oil and fat, application of composition and cosmetic prepared from composition Download PDFInfo
- Publication number
- CN106667802A CN106667802A CN201611069148.6A CN201611069148A CN106667802A CN 106667802 A CN106667802 A CN 106667802A CN 201611069148 A CN201611069148 A CN 201611069148A CN 106667802 A CN106667802 A CN 106667802A
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- CN
- China
- Prior art keywords
- alcohol
- natural plant
- oil
- compositionss
- plant grease
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- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
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Classifications
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/92—Oils, fats or waxes; Derivatives thereof, e.g. hydrogenation products thereof
- A61K8/922—Oils, fats or waxes; Derivatives thereof, e.g. hydrogenation products thereof of vegetable origin
-
- A—HUMAN NECESSITIES
- A23—FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
- A23D—EDIBLE OILS OR FATS, e.g. MARGARINES, SHORTENINGS, COOKING OILS
- A23D9/00—Other edible oils or fats, e.g. shortenings, cooking oils
- A23D9/007—Other edible oils or fats, e.g. shortenings, cooking oils characterised by ingredients other than fatty acid triglycerides
-
- A—HUMAN NECESSITIES
- A23—FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
- A23D—EDIBLE OILS OR FATS, e.g. MARGARINES, SHORTENINGS, COOKING OILS
- A23D9/00—Other edible oils or fats, e.g. shortenings, cooking oils
- A23D9/02—Other edible oils or fats, e.g. shortenings, cooking oils characterised by the production or working-up
- A23D9/04—Working-up
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/30—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
- A61K8/33—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing oxygen
- A61K8/34—Alcohols
- A61K8/342—Alcohols having more than seven atoms in an unbroken chain
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/72—Cosmetics or similar toiletry preparations characterised by the composition containing organic macromolecular compounds
- A61K8/84—Cosmetics or similar toiletry preparations characterised by the composition containing organic macromolecular compounds obtained by reactions otherwise than those involving only carbon-carbon unsaturated bonds
- A61K8/86—Polyethers
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
- A61Q19/00—Preparations for care of the skin
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K2800/00—Properties of cosmetic compositions or active ingredients thereof or formulation aids used therein and process related aspects
- A61K2800/40—Chemical, physico-chemical or functional or structural properties of particular ingredients
- A61K2800/49—Solubiliser, Solubilising system
Abstract
The invention discloses a composition for solubilizing natural vegetable oil and fat, application of the composition and a cosmetic prepared from the composition. The composition is prepared from the following components: the natural vegetable oil and fat, higher alcohols, a low polymerization degree nonionic surfactant with a PEG structure, a high polymerization degree nonionic surfactant with a PEG structure and lower alcohols, wherein the weight ratio of vitamin E or derivatives thereof, the higher alcohols, the low polymerization degree nonionic surfactant with the PEG structure, the high polymerization degree nonionic surfactant with the PEG structure and the lower alcohols is 1:(1-3):(2-5):(2-5):(60-120). The composition for solubilizing natural vegetable oil and fat, prepared and obtained in the invention, is applied to low-alcohol or alcohol-free aqueous cosmetics such as lotions, essences and masks, can effectively promote skin effective constituents such as natural oil and fat to be dissolved in water, and can supplement oil to skin and increase the moisture of skin, so that the composition is low in skin sticky feeling and little in stimulation, is applicable to most aqueous systems, and does not influence the stability of the systems.
Description
Technical field
The present invention relates to cosmetic field, the compositionss of more particularly to a kind of solubilized natural plant grease and its application and by
Its cosmetics for preparing.
Background technology
With the improvement of people's living standards, cosmetics have come into huge numbers of families, and people need to high-quality cosmetic
Ask increasingly serious.Due to needing, may require that some oils and fatss, active matter, essence, preservative are added in selection in water-based system sometimes
Deng oil soluble material.But, under general case, these lipophilic components are difficult to dissolve in formula system, it is impossible to form homogeneous.Cause
This, solubilizing agent just serves vital effect in this kind of cosmetics, and solubilizing agent can help lipophilic component to be dissolved in water
In, and form the homogeneous system of transparent and homogeneous.
Solubilizing agent composition is mainly based on nonionic surfactant and anion surfactant on market.By some
Nonpolar Low grease carries out solubilising, and generally requiring the high nonionic table of a large amount of HLB values and living carries out solubilising, but by natural plants
The nonpolar high oils and fatss of oils and fatss such as Jojoba oil, olive oil in water solubilising to transparent, it is to be difficult to make the preparations such as cosmetic water
Realize, its often using substantial amounts of high polymerization degree nonionic surfactant, but solution be also difficult to it is transparent, it is impossible to ensure skin
Skin osmotic absorption.Additionally, using the nonionic surfactant of a large amount of high polymerization degrees, glutinous soapy feeling and stimulation can be caused to skin
Property.
The content of the invention
In order to overcome the shortcoming and deficiency of prior art presence, the primary and foremost purpose of the present invention is that offer one kind solubilising is natural
The compositionss of Vegetable oil lipoprotein, said composition is applied in water system cosmetics, can make solution solubilising to transparent, and the glutinous soapy feeling of skin
Low, zest is little.
The present invention is achieved by the following technical solutions：
A kind of compositionss of solubilized natural plant grease, comprising component：Natural plant grease, higher alcohol, low polymerization degree band
There are PEG structure nonionic surfactants, high polymerization degree with PEG structures nonionic surfactant and lower alcohol, wherein, day
Right Vegetable oil lipoprotein：Higher alcohol：Low polymerization degree carries PEG structure nonionic surfactants：High polymerization degree with PEG structures it is non-from
Sub- surfactant：The weight ratio of lower alcohol is 1：1-3：2-5：2-5：60-120.
The present invention not selects tween according to HLB value, but by being conceived to the polarity of water, oil components
The technical method found with the PEG degree of polymerization of nonionic surfactant.Oil components are natural plant grease, are nonpolar
Oil.However, the polarity highest of water, high polymerization degree is soluble in water with PEG structure nonionic surfactants, but can not be dissolved in
Oil.Low polymerization degree of the present invention by addition positioned at the rwo intermediate polarity carries PEG structures nonionic surfactant and height
Level alcohol so as to become both materials compatible.Additionally, being located at water and high polymerization degree with PEG structure nonionic tables plus polarity
Lower alcohol between the activating agent of face, make oil components in water can solubilising to transparent.From the point of view of the chemical constitution of higher alcohol, its alkane
The end of base carries hydroxyl, and polarity is high in oil components.Polarity bit of the low polymerization degree with PEG structure nonionic surfactants
In higher alcohol and high polymerization degree between the nonionic surfactant with PEG structures, both are all solvable.The present invention is by research
Higher alcohol, low polymerization degree are lived with PEG structure nonionic surfactants, high polymerization degree with PEG structures non-ionic surface
Property agent and lower alcohol be combined with oil components, and the amount of each component is controlled in certain proportion so as to into
For water and the intermediate polarity connectionist of oil components, can be by the small dispersion of oil components and solubilising is to transparent.
PEG structure nonionic surfactants, high polymerization degree are carried according to natural plant grease, higher alcohol, low polymerization degree
With the polar relationship between PEG structures nonionic surfactant and lower alcohol, respective ratio is selected to be 1：1-3：2-5：2-
5：60-120.If low polymerization degree and high polymerization degree are very few with PEG structure nonionic surfactants, higher alcohol is excessive, that
Polarity of the high polymerization degree with PEG structure nonionic surfactants with the polarities match of water, but can not be soluble in height
It is so as to there is lamination or even muddy in level alcohol.If low polymerization degree and high polymerization degree carry PEG structure non-ionic surfaces
Activating agent is excessive, and higher alcohol is very few, then polarity of the low polymerization degree with PEG structure nonionic surfactants can not with it is senior
Alcohol polarities match, also occurs corresponding layering, or even muddy.
Used as further preferred version of the invention, the compositionss of solubilized natural plant grease of the present invention are natural
Vegetable oil lipoprotein：Higher alcohol：Low polymerization degree carries PEG structure nonionic surfactants：High polymerization degree carries PEG structure nonionics
Surfactant：The weight ratio of lower alcohol is 1：2：3-4：3-4：80-100.
Wherein, the natural plant grease is selected from Jojoba oil, olive oil, Petiolus Trachycarpi oil, Oleum Vitis viniferae, Oleum Helianthi, red
One or more in flower seed oil, soybean oil, palm-kernel oil, shea butter, Oleum Ricini.
Wherein, the higher alcohol is in octyl dodecanol, isooctadecanol, myristyl alcohol, lauryl alcohol, hexyldecanol or oleyl alcohol
One or more, preferably octyl dodecanol, isooctadecanol or oleyl alcohol.
Wherein, the degree of polymerization of the high polymerization degree with PEG structure nonionic surfactants is 30-80, is chosen in particular from
Polyoxyethylene fatty glyceride type, polyoxyethylene hardened castor oil fatty acid ester type, polyoxyethylene hardened castor oil type, PCA are different
Stearate polyoxyethylene hardened castor oil type, polyoxyethylene fatty acid type, polyoxyethylene sorbitol type, polyoxyethylene alkyl ether
One or more in type, one kind in preferred oleth -50, Cremophor RH40 or PEG-60 castor oil hydrogenated or
It is several.
Wherein, the degree of polymerization of the low polymerization degree with PEG structure nonionic surfactants is 6-20, is chosen in particular from gathering
Oxygen ethylene fatty acid glycerine type, polyoxyethylene hardened castor oil fatty acid ester type, polyoxyethylene hardened castor oil type, PCA are different hard
Fat acid ester polyoxyethylene hardened castor oil type, polyoxyethylene fatty acid type, polyoxyethylene sorbitol type, polyoxyethylene alkyl ether-type
In one or more, preferred PEG-6 iso stearic acid of glycerine ester, PEG-8 iso stearic acid of glycerine ester or PEG-7 glyceryl cocoates
In one or more.
Wherein, the lower alcohol for C2-C9 alcohol apoplexy due to endogenous wind one or more, preferably glycerol, Propylene Glycol, butanediol, different
One or more in pentanediol, hexanediol, 1,2- pentanediols, ethohexadiol, ethohexadiol, dipropylene glycol or diglycerol.
The preparation method of the compositionss of the above-mentioned a kind of solubilized natural plant grease of the present invention is by natural plant grease, height
Level alcohol, low polymerization degree carry PEG structure nonionic surfactants with PEG structure nonionic surfactants, high polymerization degree
With lower alcohol in proportion at 80 DEG C, it is dissolved by stirring, reach solubilizing effect.
Present invention also offers the compositionss of above-mentioned solubilized natural plant grease are in cosmetics, food or health product
Using.
Present invention also offers a kind of cosmetics, the compositionss comprising above-mentioned solubilized natural plant grease.
Preferably, the addition of the compositionss of the solubilized natural plant grease is the 5- of whole cosmetics gross mass
15%.
In the compositionss of the solubilized natural plant grease of the invention described above, not damaging in the range of effect of the present invention,
The composition that generally may be fitted in cosmetics can be arbitrarily coordinated to prepare cosmetics.This any condition include preservative,
Wetting agent, UV absorbent, antioxidant, Ph regulators etc..Its consumption is the conventional amount used for preparing cosmetics.
The present invention compared with prior art, has the advantages that：
(1) present invention by higher alcohol, low polymerization degree by carrying PEG structure nonionic surfactants, high polymerization degree band
There are PEG structures nonionic surfactant and lower alcohol to be combined with oil components, and the amount of each component is controlled one
In fixed proportion, the compositionss of the solubilized natural plant grease for preparing are applied to astringent, essence, facial film etc.
Low alcohol, without alcohol water preparation cosmetics in, it is soluble in water to effectively facilitate the skin effective ingredient such as natural plant grease, can give skin
Supplement oil, increase the moist degree of skin；
(2) non-ionic surface containing PEG structures used in the compositionss of solubilized natural plant grease prepared by the present invention
Activating agent consumption is few, and the glutinous soapy feeling of skin is low, zest is little, it is adaptable to most of water preparation system, and system stability is not had
Affect；
(3) preparation method of the present invention is simple to operate, easily realizes, prepared cosmetics cost performance is high, low cost.
Specific embodiment
The present invention is further illustrated below by specific embodiment, following examples are the present invention preferably embodiment party
Formula, but embodiments of the present invention are not limited by following embodiments.
Raw material of the present invention derives from commercial products.
Performance test methods：
The method of testing of appearance transparence stability：
Take transparent toner/smoothing toner, be placed in 40 DEG C deposit 1 month, 25 DEG C of room temperature deposit 1 month, 5 DEG C of low temperature deposit 1 month, it is extensive
It is multiple to observe appearance transparence to room temperature.
The method of testing of the particle diameter of vitamin and its derivant：Tested using LS900 type laser particle size analyzers, surveyed
Examination scope：0.05~500 μm；Input mode：Wet method, circular sample feeder and static sample pond；Repeatability error：<3%；Test
Time：1-2 minutes；Standalone probe unit number：53；Light source category：Helium-neon laser, power：2.0mW, wavelength：0.6328μm；Work
Make environment：Temperature：5-35 DEG C, humidity：＜ 85%.
Transmittance method of testing：Using ultraviolet-uisible spectrophotometer UV1000, Exposure Metering：Single beam；Wave-length coverage:
190.0~1100.0nm；Spectral bandwidth:2nm；Transmittance ranges:0~200%T；Range of absorbency:- 0.3~3Abs；Light source:
Deuterium lamp, halogen tungsten lamp；Dispersion element:Grating, 1200L/mm；Detector:Silicon photo diode；Use environment temperature:5 DEG C~35 DEG C；
Use environment relative humidity:≤ 85%.
The preparation of the compositionss of solubilized natural plant grease：
By the formula of table 1, by natural plant grease, higher alcohol, low polymerization degree with PEG structure nonionic surfactants,
High polymerization degree in proportion at 80 DEG C, dissolves it, i.e., with PEG structures nonionic surfactant and lower alcohol by stirring
The compositionss of solubilized natural plant grease are obtained.
Table 1：The composition (weight portion) of the compositionss of solubilized natural plant grease
Continued 1
Embodiment 1-13 and comparative example 1-5：
By the formula of table 2, by compositionss, preservative, the pure water of solubilized natural plant grease obtained above according to certain
At 40 DEG C, stirring is mixed with and obtains transparent toner/smoothing toner ratio, tests its performance, and results of property is as shown in table 2：
The composition and the performance test results (%) of embodiment 1-13 of table 2 and the transparent toner/smoothing toner of comparative example 1-5
Continued 2：
The present invention can be seen that by the result of the embodiment of table 2 and comparative example higher alcohol, low polymerization degree are carried into PEG structures
Nonionic surfactant, high polymerization degree are carried out with PEG structures nonionic surfactant and lower alcohol and oil components
Combination, and the amount of each component is controlled in certain proportion, the compositionss of the solubilized natural plant grease for preparing,
In being applied to toner/smoothing toner, it is soluble in water to effectively facilitate the skin effective ingredient such as natural plant grease, can solubilising to transparent.
Claims (10)
1. a kind of compositionss of solubilized natural plant grease, it is characterised in that comprising component：It is natural plant grease, higher alcohol, low
The degree of polymerization is with PEG structure nonionic surfactants, high polymerization degree with PEG structures nonionic surfactant and rudimentary
Alcohol, wherein, natural plant grease：Higher alcohol：Low polymerization degree carries PEG structure nonionic surfactants：High polymerization degree is carried
PEG structure nonionic surfactants：The weight ratio of lower alcohol is 1：1-3：2-5：2-5：60-120, preferably 1：1：3-4：3-
4：80-100.
2. compositionss of solubilized natural plant grease according to claim 1, it is characterised in that the natural plant grease
Selected from Jojoba oil, olive oil, Petiolus Trachycarpi oil, Oleum Vitis viniferae, Oleum Helianthi, safflower oil, soybean oil, palm-kernel oil, Butyrospermum Parkii
One or more in oil, Oleum Ricini.
3. compositionss of solubilized natural plant grease according to claim 1, it is characterised in that the higher alcohol is octyl group
One or more in lauryl alcohol, isooctadecanol, myristyl alcohol, lauryl alcohol, hexyldecanol or oleyl alcohol, preferably octyl group 12
One or more in alcohol, isooctadecanol or oleyl alcohol.
4. compositionss of solubilized natural plant grease according to claim 1, it is characterised in that the high polymerization degree is carried
The degree of polymerization of PEG structure nonionic surfactants is 30-80, is chosen in particular from polyoxyethylene fatty glyceride type, Polyethylene oxide
Hardened castor oil fatty acid ester type, polyoxyethylene hardened castor oil type, PCA isostearate polyoxyethylene hardened castor oil types,
One or more in polyoxyethylene fatty acid type, polyoxyethylene sorbitol type, polyoxyethylene alkyl ether-type, preferred oleyl alcohol gathers
One or more in ether -50, Cremophor RH40 or PEG-60 castor oil hydrogenated.
5. compositionss of solubilized natural plant grease according to claim 1, it is characterised in that the low polymerization degree is carried
The degree of polymerization of PEG structure nonionic surfactants is 6-20, is chosen in particular from polyoxyethylene fatty glyceride type, Polyethylene oxide hard
Change Castor Oil Fatty Acid ester type, polyoxyethylene hardened castor oil type, PCA isostearate polyoxyethylene hardened castor oil types, poly-
One or more in oxygen ethylene fatty acid type, polyoxyethylene sorbitol type, polyoxyethylene alkyl ether-type, preferred PEG-6 glycerol
One or more of isostearate, PEG-8 iso stearic acid of glycerine ester or PEG-7 glyceryl cocoates.
6. compositionss of solubilized natural plant grease according to claim 1, it is characterised in that the lower alcohol is C2-
One or more of C9 alcohol apoplexy due to endogenous wind.
7. compositionss of solubilized natural plant grease according to claim 6, it is characterised in that the lower alcohol is sweet
Oil, Propylene Glycol, butanediol, isoprene, hexanediol, 1,2- pentanediols, ethohexadiol, ethohexadiol, dipropylene glycol or double sweet
One or more in oil.
8. the compositionss of the solubilized natural plant grease described in any one of claim 1-7 are in cosmetics, food or health product
Application.
9. a kind of cosmetics, the compositionss comprising the solubilized natural plant grease described in any one of claim 1-7.
10. cosmetics according to claim 9, it is characterised in that the compositionss of the solubilized natural plant grease add
Dosage is the 5-15% of whole cosmetics gross mass.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201611069148.6A CN106667802B (en) | 2016-11-29 | 2016-11-29 | A kind of composition and its application and cosmetics prepared therefrom of solubilising natural plant grease |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201611069148.6A CN106667802B (en) | 2016-11-29 | 2016-11-29 | A kind of composition and its application and cosmetics prepared therefrom of solubilising natural plant grease |
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| Publication Number | Publication Date |
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| CN106667802A true CN106667802A (en) | 2017-05-17 |
| CN106667802B CN106667802B (en) | 2018-04-17 |
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| CN201611069148.6A Active CN106667802B (en) | 2016-11-29 | 2016-11-29 | A kind of composition and its application and cosmetics prepared therefrom of solubilising natural plant grease |
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Cited By (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN109620758A (en) * | 2019-01-04 | 2019-04-16 | 澳宝化妆品（惠州）有限公司 | A kind of bilayer scalp care compositions and preparation method thereof |
| CN112791015A (en) * | 2021-01-25 | 2021-05-14 | 湖北煜韩环境科技有限公司 | Essence solubilizer and preparation method thereof |
Citations (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| JP2004352689A (en) * | 2003-05-30 | 2004-12-16 | Kose Corp | O/w-type emulsion cosmetic |
| CN105997704A (en) * | 2016-06-30 | 2016-10-12 | 赖保全 | Anti-chapping hand cream |
-
2016
- 2016-11-29 CN CN201611069148.6A patent/CN106667802B/en active Active
Patent Citations (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| JP2004352689A (en) * | 2003-05-30 | 2004-12-16 | Kose Corp | O/w-type emulsion cosmetic |
| CN105997704A (en) * | 2016-06-30 | 2016-10-12 | 赖保全 | Anti-chapping hand cream |
Non-Patent Citations (1)
| Title |
|---|
| 广州市花安堂生物科技有限公司: "奢睿男士保湿精华水", 《国产非特殊用途化妆品备案服务平台》 * |
Cited By (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN109620758A (en) * | 2019-01-04 | 2019-04-16 | 澳宝化妆品（惠州）有限公司 | A kind of bilayer scalp care compositions and preparation method thereof |
| CN109620758B (en) * | 2019-01-04 | 2021-11-12 | 澳宝化妆品（惠州）有限公司 | Double-layer scalp care composition and preparation method thereof |
| CN112791015A (en) * | 2021-01-25 | 2021-05-14 | 湖北煜韩环境科技有限公司 | Essence solubilizer and preparation method thereof |
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| Publication number | Publication date |
|---|---|
| CN106667802B (en) | 2018-04-17 |
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