CN106667802B - A kind of composition and its application and cosmetics prepared therefrom of solubilising natural plant grease - Google Patents
A kind of composition and its application and cosmetics prepared therefrom of solubilising natural plant grease Download PDFInfo
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- CN106667802B CN106667802B CN201611069148.6A CN201611069148A CN106667802B CN 106667802 B CN106667802 B CN 106667802B CN 201611069148 A CN201611069148 A CN 201611069148A CN 106667802 B CN106667802 B CN 106667802B
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- natural plant
- alcohol
- composition
- oil
- polymerization degree
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Classifications
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/92—Oils, fats or waxes; Derivatives thereof, e.g. hydrogenation products thereof
- A61K8/922—Oils, fats or waxes; Derivatives thereof, e.g. hydrogenation products thereof of vegetable origin
-
- A—HUMAN NECESSITIES
- A23—FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
- A23D—EDIBLE OILS OR FATS, e.g. MARGARINES, SHORTENINGS, COOKING OILS
- A23D9/00—Other edible oils or fats, e.g. shortenings, cooking oils
- A23D9/007—Other edible oils or fats, e.g. shortenings, cooking oils characterised by ingredients other than fatty acid triglycerides
-
- A—HUMAN NECESSITIES
- A23—FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
- A23D—EDIBLE OILS OR FATS, e.g. MARGARINES, SHORTENINGS, COOKING OILS
- A23D9/00—Other edible oils or fats, e.g. shortenings, cooking oils
- A23D9/02—Other edible oils or fats, e.g. shortenings, cooking oils characterised by the production or working-up
- A23D9/04—Working-up
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/30—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
- A61K8/33—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing oxygen
- A61K8/34—Alcohols
- A61K8/342—Alcohols having more than seven atoms in an unbroken chain
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/72—Cosmetics or similar toiletry preparations characterised by the composition containing organic macromolecular compounds
- A61K8/84—Cosmetics or similar toiletry preparations characterised by the composition containing organic macromolecular compounds obtained by reactions otherwise than those involving only carbon-carbon unsaturated bonds
- A61K8/86—Polyethers
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
- A61Q19/00—Preparations for care of the skin
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K2800/00—Properties of cosmetic compositions or active ingredients thereof or formulation aids used therein and process related aspects
- A61K2800/40—Chemical, physico-chemical or functional or structural properties of particular ingredients
- A61K2800/49—Solubiliser, Solubilising system
Abstract
The invention discloses a kind of composition and its application and cosmetics prepared therefrom of solubilized natural plant grease, component is included：Natural plant grease, higher alcohol, low polymerization degree carry PEG structures nonionic surfactant and lower alcohol with PEG structures nonionic surfactant, high polymerization degree, wherein, vitamin E or derivatives thereof：Higher alcohol：Low polymerization degree carries PEG structure nonionic surfactants：High polymerization degree carries PEG structure nonionic surfactants：The weight ratio of lower alcohol is 1：1‑3：2‑5：2‑5：60‑120.The composition for the solubilized natural plant grease that the present invention is prepared, applied to toner, Essence, the low alcohol such as facial mask, without in alcohol aqua cosmetics, it can effectively facilitate that the skin active ingredient such as natural oil is soluble in water, oil can be supplemented to skin, increases the moist degree of skin, skin sticks that soapy feeling is low, irritation is small, will not have an impact suitable for most of aqua system, and to system stability.
Description
Technical field
The present invention relates to cosmetic field, the composition of more particularly to a kind of solubilized natural plant grease and its application and by
Its cosmetics prepared.
Background technology
As the improvement of people's living standards, cosmetics have come into huge numbers of families, makeup of the people to high quality needs
Ask increasingly serious.Due to needing, it may require that some greases, active matter, essence, preservative are added in selection in water-based system sometimes
Deng oil soluble material.But under general case, these lipophilic components are difficult to dissolve in formula system, it is impossible to are formed homogeneous.Cause
This, solubilizer just plays the role of vital in this kind of cosmetics, and solubilizer can help lipophilic component to be dissolved in water
In, and form the homogeneous system of transparent and homogeneous.
In the market solubilizer component is mainly based on nonionic surfactant and anion surfactant.By some
Nonpolar Low grease carries out solubilising, generally requires the high nonionic table of a large amount of HLB values and lives and carries out solubilising, but by natural plants
For solubilising to transparent, it is to be difficult to that the preparations such as toner are made to the nonpolar high grease of grease such as jojoba oil, olive oil etc. in water
Realize, it often uses the nonionic surfactant of substantial amounts of high polymerization degree, but solution is also difficult to transparent, can not ensure skin
Skin osmotic absorption.In addition, using the nonionic surfactant of a large amount of high polymerization degrees, glutinous soapy feeling and stimulation can be caused to skin
Property.
The content of the invention
In order to overcome shortcoming and deficiency existing in the prior art, primary and foremost purpose of the invention is to provide a kind of solubilising naturally
The composition of vegetable fat, said composition are applied in water system cosmetics, can make solution solubilising to transparent, and skin sticks soapy feeling
It is low, irritation is small.
The present invention is achieved by the following technical solutions：
A kind of composition of solubilising natural plant grease, includes component：Natural plant grease, higher alcohol, low polymerization degree band
There are PEG structures nonionic surfactant, high polymerization degree to carry PEG structures nonionic surfactant and lower alcohol, wherein, day
Right vegetable fat：Higher alcohol：Low polymerization degree carries PEG structure nonionic surfactants：High polymerization degree with PEG structures it is non-from
Sub- surfactant：The weight ratio of lower alcohol is 1：1-3：2-5：2-5：60-120.
The present invention selects tween not according to HLB value, but by being conceived to the polarity of water, oil components
The technical method found with the PEG degree of polymerization of nonionic surfactant.Oil components are natural plant grease, are nonpolar
Oil.However, the polarity highest of water, high polymerization degree is soluble easily in water with PEG structure nonionic surfactants, cannot but be dissolved in
Oil.The present invention carries PEG structures nonionic surfactant and height by the low polymerization degree added positioned at the rwo intermediate polarity
Level alcohol, becomes both compatible materials.In addition, being located at water plus polarity and high polymerization degree carries PEG structure nonionic tables
Lower alcohol between the activating agent of face, makes oil components in water can be solubilized to transparent.From the point of view of the chemical constitution of higher alcohol, its alkane
The end of base carries hydroxyl, and polarity is high in oil components.Low polymerization degree carries the polarity bit of PEG structure nonionic surfactants
Between the nonionic surfactant of higher alcohol and high polymerization degree with PEG structures, both are all solvable.The present invention passes through research
Higher alcohol, low polymerization degree are lived with PEG structures nonionic surfactant, high polymerization degree with PEG structures non-ionic surface
Property agent and lower alcohol be combined with oil components, and the amount of each component is controlled in certain proportion, make its into
, can be small scattered and solubilized to transparent by oil components for the intermediate polarity connectionist of water and oil components.
According to natural plant grease, higher alcohol, low polymerization degree with PEG structures nonionic surfactant, high polymerization degree
With the polar relationship between PEG structures nonionic surfactant and lower alcohol, respective ratio is selected as 1：1-3：2-5：2-
5：60-120.If low polymerization degree and high polymerization degree are very few with PEG structure nonionic surfactants, higher alcohol is excessive, that
Polarity of the high polymerization degree with PEG structure nonionic surfactants but cannot be soluble in height with the polarities match of water
In level alcohol, so that there is lamination, in addition it is muddy.If low polymerization degree and high polymerization degree carry PEG structure non-ionic surfaces
Activating agent is excessive, and higher alcohol is very few, then low polymerization degree with PEG structure nonionic surfactants polarity cannot with it is advanced
Alcohol polarities match, also occurs corresponding layering, or even muddy.
As the further preferred solution of the present invention, the composition of solubilising natural plant grease of the present invention, naturally
Vegetable fat：Higher alcohol：Low polymerization degree carries PEG structure nonionic surfactants：High polymerization degree carries PEG structure nonionics
Surfactant：The weight ratio of lower alcohol is 1：2：3-4：3-4：80-100.
Wherein, the natural plant grease is selected from jojoba oil, olive oil, palm oil, grape-kernel oil, sunflower oil, red
One or more in flower seed oil, soybean oil, palm-kernel oil, shea butter, castor oil.
Wherein, the higher alcohol is in octyl dodecanol, isooctadecanol, myristyl alcohol, laruyl alcohol, hexyl decyl alcohol or oleyl alcohol
One or more, be preferably octyl dodecanol, isooctadecanol or oleyl alcohol.
Wherein, the degree of polymerization of the high polymerization degree with PEG structure nonionic surfactants is 30-80, is chosen in particular from
Polyoxyethylene fatty glyceride type, polyoxyethylene hardened castor oil fatty acid ester type, polyoxyethylene hardened castor oil type, PCA are different
Stearate polyoxyethylene hardened castor oil type, polyoxyethylene fatty acid type, polyoxyethylene sorbitol type, polyoxyethylene alkyl ether
One or more in type, preferably oleth -50, Cremophor RH40 or one kind in PEG-60 rilanit specials or
It is several.
Wherein, the degree of polymerization of the low polymerization degree with PEG structure nonionic surfactants is 6-20, is chosen in particular from gathering
Ethylene oxide fatty acid glycerine type, polyoxyethylene hardened castor oil fatty acid ester type, polyoxyethylene hardened castor oil type, PCA are different hard
Resin acid ester polyoxyethylene hardened castor oil type, polyoxyethylene fatty acid type, polyoxyethylene sorbitol type, polyoxyethylene alkyl ether-type
In one or more, preferably PEG-6 iso stearic acid of glycerine ester, PEG-8 iso stearic acid of glycerine ester or PEG-7 glyceryl cocoates
In one or more.
Wherein, the lower alcohol is the one or more in C2-C9 alcohols, is preferably glycerine, propane diols, butanediol, different
One or more in pentanediol, hexylene glycol, 1,2- pentanediols, ethohexadiol, ethohexadiol, dipropylene glycol or diglycerol.
A kind of preparation method of the composition of the above-mentioned solubilized natural plant grease of the present invention is by natural plant grease, height
Level alcohol, low polymerization degree carry PEG structure nonionic surfactants with PEG structures nonionic surfactant, high polymerization degree
With lower alcohol in proportion at 80 DEG C, by stirring to dissolve, reach solubilizing effect.
Composition present invention also offers above-mentioned solubilized natural plant grease is in cosmetics, food or health products
Using.
Present invention also offers a kind of cosmetics, the composition of above-mentioned solubilized natural plant grease is included.
Preferably, the additive amount of the composition of the solubilized natural plant grease is the 5- of whole cosmetics gross mass
15%.
In the composition of the solubilized natural plant grease of the invention described above, within the scope of the effect of the invention,
The component that usually may be fitted in cosmetics can be arbitrarily coordinated to prepare cosmetics.This any condition include preservative,
Moisturizer, ultra-violet absorber, antioxidant, Ph conditioning agents etc..Its dosage is to prepare the conventional amount used of cosmetics.
Compared with prior art, the present invention have the advantages that：
(1) present invention by higher alcohol, low polymerization degree by carrying PEG structures nonionic surfactant, high polymerization degree band
There are PEG structures nonionic surfactant and lower alcohol to be combined with oil components, and the amount of each component is controlled one
In fixed proportion, the composition for the solubilized natural plant grease being prepared, applied to toner, Essence, facial mask etc.
It is low alcohol, soluble in water without the skin active ingredient such as natural plant grease in alcohol aqua cosmetics, can be effectively facilitated, skin can be given
Supplement oil, increase the moist degree of skin；
(2) non-ionic surface of the structure containing PEG used in the composition of solubilized natural plant grease prepared by the present invention
Activating agent dosage is few, and skin sticks that soapy feeling is low, irritation is small, is not had suitable for most of aqua system, and to system stability
Influence；
(3) preparation method of the present invention is easy to operate, easy to implement, and prepared cosmetics are cost-effective, and cost is low.
Embodiment
The present invention is further illustrated below by embodiment, and following embodiments are the preferable embodiment party of the present invention
Formula, but embodiments of the present invention and from the limitation of following embodiments.
Raw material of the present invention derives from commercial products.
Performance test methods：
The test method of appearance transparence stability：
Take transparent smoothing toner, be placed in 40 DEG C store 1 month, 25 DEG C of room temperature store 1 month, 5 DEG C of low temperature store 1 month, it is extensive
Appearance transparence is observed after answering to room temperature.
The test method of the particle diameter of vitamin and its derivative：Tested, surveyed using LS900 type laser particle size analyzers
Try scope：0.05~500 μm；Input mode：Wet method, circular sample feeder and static sample pond；Repeatability error：<3%；Test
Time：1-2 minutes；Standalone probe unit number：53；Light source species：Helium-neon laser, power：2.0mW, wavelength：0.6328μm；Work
Make environment：Temperature：5-35 DEG C, humidity：＜ 85%.
Light transmittance test method：Using ultraviolet-uisible spectrophotometer UV1000, Exposure Metering：Single beam；Wave-length coverage:
190.0~1100.0nm；Spectral bandwidth:2nm；Transmittance ranges:0~200%T；Range of absorbency:- 0.3~3Abs；Light source:
Deuterium lamp, halogen tungsten lamp；Dispersion element:Grating, 1200L/mm；Detector:Silicon photo diode；Use environment temperature:5 DEG C~35 DEG C；
Use environment relative humidity:≤ 85%.
The preparation of the composition of solubilized natural plant grease：
Be formulated by table 1, by natural plant grease, higher alcohol, low polymerization degree with PEG structures nonionic surfactant,
In proportion at 80 DEG C, by stirring to dissolve, i.e., high polymerization degree carries PEG structures nonionic surfactant and lower alcohol
It can obtain the composition of solubilized natural plant grease.
Table 1：The composition (parts by weight) of the composition of solubilized natural plant grease
Continued 1
Embodiment 1-13 and comparative example 1-5：
It is formulated by table 2, by the composition, preservative, pure water of solubilized natural plant grease obtained above according to certain
Ratio is stirred and transparent smoothing toner is prepared at 40 DEG C, tests its performance, and results of property is as shown in table 2：
The composition and performance test result (%) of 2 embodiment 1-13 of table and the transparent smoothing toners of comparative example 1-5
Continued 2：
Higher alcohol, low polymerization degree are carried PEG structures by the present invention it can be seen from the result of 2 embodiment of table and comparative example
Nonionic surfactant, high polymerization degree are carried out with PEG structures nonionic surfactant and lower alcohol and oil components
Combination, and the amount of each component is controlled in certain proportion, the composition for the solubilized natural plant grease being prepared,
Applied to that in smoothing toner, can effectively facilitate, the skin active ingredient such as natural plant grease is soluble in water, can be solubilized to transparent.
Claims (12)
1. a kind of composition of solubilising natural plant grease, it is characterised in that include component：It is natural plant grease, higher alcohol, low
The degree of polymerization carries PEG structures nonionic surfactant, high polymerization degree carries PEG structures nonionic surfactant and rudimentary
Alcohol, wherein, natural plant grease：Higher alcohol：Low polymerization degree carries PEG structure nonionic surfactants：High polymerization degree carries
PEG structure nonionic surfactants：The weight ratio of lower alcohol is 1：1-3：2-5：2-5：60-120;
The higher alcohol be octyl dodecanol, isooctadecanol, myristyl alcohol, laruyl alcohol, hexyl decyl alcohol or oleyl alcohol in one kind or
It is several;
The degree of polymerization of the high polymerization degree with PEG structure nonionic surfactants is 30-80;
The degree of polymerization of the low polymerization degree with PEG structure nonionic surfactants is 6-20;
The lower alcohol is the one or more in C2-C9 alcohols.
2. the composition of solubilising natural plant grease according to claim 1, it is characterised in that natural plant grease：It is high
Level alcohol：Low polymerization degree carries PEG structure nonionic surfactants：High polymerization degree carries PEG structure nonionic surfactants：
The weight ratio of lower alcohol is 1：1：3-4：3-4：80-100.
3. the composition of solubilising natural plant grease according to claim 1, it is characterised in that the natural plant grease
Selected from jojoba oil, olive oil, palm oil, grape-kernel oil, sunflower oil, safflower seed oil, soybean oil, palm-kernel oil, the wooden fruit of breast
One or more in oil, castor oil.
4. the composition of solubilising natural plant grease according to claim 1, it is characterised in that the higher alcohol is octyl group
One or more in lauryl alcohol, isooctadecanol or oleyl alcohol.
5. the composition of solubilising natural plant grease according to claim 1, it is characterised in that the high polymerization degree carries
PEG structures nonionic surfactant be selected from polyoxyethylene fatty glyceride type, polyoxyethylene hardened castor oil fatty acid ester type,
Polyoxyethylene hardened castor oil type, PCA isostearate polyoxyethylene hardened castor oils type, polyoxyethylene fatty acid type, polyoxy
One or more in ethene sorb alcohol type, polyoxyethylene alkyl ether-type.
6. the composition of solubilising natural plant grease according to claim 5, it is characterised in that the high polymerization degree carries
PEG structures nonionic surfactant is one in oleth -50, Cremophor RH40 or PEG-60 rilanit specials
Kind is several.
7. the composition of solubilising natural plant grease according to claim 1, it is characterised in that the low polymerization degree carries
PEG structures nonionic surfactant be selected from polyoxyethylene fatty glyceride type, polyoxyethylene hardened castor oil fatty acid ester type,
Polyoxyethylene hardened castor oil type, PCA isostearate polyoxyethylene hardened castor oils type, polyoxyethylene fatty acid type, polyoxy
One or more in ethene sorb alcohol type, polyoxyethylene alkyl ether-type.
8. the composition of solubilising natural plant grease according to claim 7, it is characterised in that the low polymerization degree carries
PEG structures nonionic surfactant is PEG-6 iso stearic acid of glycerine ester, PEG-8 iso stearic acid of glycerine ester or PEG-7 glycerine
The one or more of cocounut oil acid esters.
9. the composition of solubilising natural plant grease according to claim 1, it is characterised in that the lower alcohol is sweet
Oil, propane diols, butanediol, isoprene, hexylene glycol, 1,2- pentanediols, ethohexadiol, ethohexadiol, dipropylene glycol or double sweet
One or more in oil.
10. the composition of claim 1-9 any one of them solubilising natural plant greases is preparing cosmetics, food or health care
Application in product.
11. a kind of cosmetics, include the composition of claim 1-9 any one of them solubilising natural plant greases.
12. cosmetics according to claim 11, it is characterised in that the composition of the solubilising natural plant grease adds
Dosage is the 5-15% of whole cosmetics gross mass.
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| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201611069148.6A CN106667802B (en) | 2016-11-29 | 2016-11-29 | A kind of composition and its application and cosmetics prepared therefrom of solubilising natural plant grease |
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| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201611069148.6A CN106667802B (en) | 2016-11-29 | 2016-11-29 | A kind of composition and its application and cosmetics prepared therefrom of solubilising natural plant grease |
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| CN106667802A CN106667802A (en) | 2017-05-17 |
| CN106667802B true CN106667802B (en) | 2018-04-17 |
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| CN109620758B (en) * | 2019-01-04 | 2021-11-12 | 澳宝化妆品（惠州）有限公司 | Double-layer scalp care composition and preparation method thereof |
| CN112791015B (en) * | 2021-01-25 | 2022-10-04 | 湖北煜韩环境科技有限公司 | Essence solubilizer and preparation method thereof |
Citations (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| JP2004352689A (en) * | 2003-05-30 | 2004-12-16 | Kose Corp | O/w-type emulsion cosmetic |
| CN105997704A (en) * | 2016-06-30 | 2016-10-12 | 赖保全 | Anti-chapping hand cream |
-
2016
- 2016-11-29 CN CN201611069148.6A patent/CN106667802B/en active Active
Patent Citations (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| JP2004352689A (en) * | 2003-05-30 | 2004-12-16 | Kose Corp | O/w-type emulsion cosmetic |
| CN105997704A (en) * | 2016-06-30 | 2016-10-12 | 赖保全 | Anti-chapping hand cream |
Non-Patent Citations (1)
| Title |
|---|
| 奢睿男士保湿精华水;广州市花安堂生物科技有限公司;《国产非特殊用途化妆品备案服务平台》;20160706;第1-2页 * |
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