CN106639248A - Light VCP floor and preparation method thereof - Google Patents
Light VCP floor and preparation method thereof Download PDFInfo
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- CN106639248A CN106639248A CN201610981586.3A CN201610981586A CN106639248A CN 106639248 A CN106639248 A CN 106639248A CN 201610981586 A CN201610981586 A CN 201610981586A CN 106639248 A CN106639248 A CN 106639248A
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- vcp
- pvc
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- calcium carbonate
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- E—FIXED CONSTRUCTIONS
- E04—BUILDING
- E04F—FINISHING WORK ON BUILDINGS, e.g. STAIRS, FLOORS
- E04F15/00—Flooring
- E04F15/02—Flooring or floor layers composed of a number of similar elements
- E04F15/10—Flooring or floor layers composed of a number of similar elements of other materials, e.g. fibrous or chipped materials, organic plastics, magnesite tiles, hardboard, or with a top layer of other materials
- E04F15/105—Flooring or floor layers composed of a number of similar elements of other materials, e.g. fibrous or chipped materials, organic plastics, magnesite tiles, hardboard, or with a top layer of other materials of organic plastics with or without reinforcements or filling materials
-
- E—FIXED CONSTRUCTIONS
- E04—BUILDING
- E04F—FINISHING WORK ON BUILDINGS, e.g. STAIRS, FLOORS
- E04F15/00—Flooring
- E04F15/02—Flooring or floor layers composed of a number of similar elements
- E04F15/10—Flooring or floor layers composed of a number of similar elements of other materials, e.g. fibrous or chipped materials, organic plastics, magnesite tiles, hardboard, or with a top layer of other materials
- E04F15/107—Flooring or floor layers composed of a number of similar elements of other materials, e.g. fibrous or chipped materials, organic plastics, magnesite tiles, hardboard, or with a top layer of other materials composed of several layers, e.g. sandwich panels
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- Engineering & Computer Science (AREA)
- Architecture (AREA)
- Civil Engineering (AREA)
- Structural Engineering (AREA)
- Floor Finish (AREA)
Abstract
The invention relates to a composite floor, in particular to a light VCP floor and a preparation method thereof. The light VCP floor is composited by a color film, an abrasion-resistant layer and a VCP base material from top to bottom. The main component of the abrasion-resistant layer is chlorinated polyethylene. The abrasion-resistant layer comprises the raw materials, by mass, of 64%-75% of the chlorinated polyethylene, 15%-20% of environment-friendly plasticizers, 3%-4% of environment-friendly stabilizers and 7%-12% of light calcium carbonate. The VCP base material comprises the raw materials, by mass, of 32%-36% of polyvinyl chloride, 53%-59% of composite calcium carbonate, 3%-4% of environment-friendly stabilizers, 0.8%-1.5% of lubricants, 0.5%-1% of foaming agents and 4%-5% of processing agents. According to the light VCP floor, a PVC base material is not needed, the overall density is 0.95 g/cm<3> or so, installation is simple and convenient, and transportation cost is low.
Description
Technical field
The present invention relates to a kind of composite floor board, more particularly to a kind of lightweight VCP floor and preparation method thereof.
Background technology
VCP floors in the market are mainly by groups such as wearing layer, color film, PVC base, VCP base materials, backing materials
Into global density is in 1.3-1.4g/cm3Between, processor is miscellaneous, and production VCP floors first have to produce PVC base, then with
Wearing layer, color film carry out hot Combined Processing, then carry out surface UV, punching molding, fit, cold pressing, cutting, operation of slotting, entirely
Time, manpower and the resource consumed by production process all compares many, and complex procedures cause the yield rate of production link to reduce;Due to
Current VCP floors belong to multilamellar and meet floor, therefore, also undesirable in terms of THICKNESS CONTROL, the accumulation between each level is public
Difference often exceeds critical field, and general deviation is between 0.15-0.25mm;Further, since current VCP floors top section
It is to be made up of for material of main part PVC, and upper strata layer of PVC, further through heat treatment destressing, the heat shrink rate on upper strata is than lower floor VCP
Little many of the shrinkage factor of base material, so floor is during use, heating warpage situation is than more serious.
The content of the invention
In order to solve the defect pointed out in prior art, the present invention provides a kind of lightweight VCP floor, and which has easily spelling
Connect, density is low, process is simple the advantages of.
The technical solution adopted for the present invention to solve the technical problems is:
A kind of lightweight VCP floor, the lightweight VCP floor are to be composited by color film, wearing layer, VCP base materials from top to bottom,
The main component of wearing layer is chlorinated polyethylene, and the raw material composition of wearing layer includes by percentage to the quality:Chlorinated polyethylene 64-
75%, environment-friendly plasticizer 15-20%, stabilizer 3-4%, precipitated calcium carbonate 7-12%;The raw material of VCP base materials is constituted with matter
Amount percentages include:Polrvinyl chloride 32-36%, composite calcium carbonate 53-59%, stabilizer 3-4%, lubricant 0.8-
1.5%, foaming agent 0.5-1%, processing aid 4-5%.The composite calcium carbonate is the mixed of precipitated calcium carbonate and ground calcium carbonate
The content of compound, wherein ground calcium carbonate is 55-75%.The optimum weight ratio of precipitated calcium carbonate and ground calcium carbonate is 3:7.
Preferably, the thickness of wearing layer is 0.1-0.6mm, the thickness of color film is 0.07mm, and the thickness of VCP base materials is 4-
5mm。
Preferably, the main component of the color film of printing is PVC, its raw material composition includes by percentage to the quality:PVC 97-
98%, Calcium Carbonate 1-2%, stabilizer 0.5-1%, processing aid 0.5-1%.
A kind of preparation method on described lightweight VCP floor, the method include layer of PVC processing, the processing of VCP base materials, laminating,
Cold pressing, surface UV processes and slot operation, mainly comprise the following steps:Wearing layer and the color film of printing make layer of PVC by heat is compound, and heat is multiple
The temperature of conjunction is 120-150 DEG C, minute time 10-20;Then by layer of PVC and VCP base material cold moudlings, temperature 23-25 DEG C, when
Between 12-36h.
Preferably, the method comprises the steps:
1st, the processing of layer of PVC:The wearing layer for preparing and the color film of printing are overlayed in the carrier of vulcanizing press, temperature
120-150 DEG C of degree setting, the demoulding after heat compound 10-20 minutes, the heat for completing wearing layer with the color film of printing are combined;
2nd, VCP base materials processing:Polrvinyl chloride, composite calcium carbonate, stabilizer, foaming agent are put in proportion mixed at a high speed
Close cylinder to be stirred, rotating speed 700-800 turns/min, and minute time 12-15, temperature is discarded to cooling when reaching 110-115 DEG C and stirs
Cylinder is mixed, 60 ± 5 DEG C are cooled to, and lubricant and processing aid is added through Screw Extrusion slice;
3rd, fit:After VCP base material completion of processing, constant temperature stands and carries out bonding process later in 24 hours, makes layer of PVC and VCP
Base material is fitted;
4th, cold pressing:Be immediately placed in after the completion of laminating cold press fit again it is strong to increase the laminating of layer of PVC and VCP base materials
Degree, cold pressing pressure 5-7MPa, temperature 23-25 DEG C, 12-36 hours of colding pressing;
5th, surface UV process;
6th, slot.
Preferably, heat is combined when making layer of PVC, the compound temperature of heat is 135-150 DEG C, minute time 16-18.
Compared with prior art, lightweight VCP floor of the invention has advantages below:
1st, lightweight VCP floor of the invention is mainly made up of wearing layer, color film, VCP base materials, and global density is in 0.95g/
cm3Left and right, greatly reduces mass area ratio, reduces also reducing cost of transportation while mass area ratio, is installing
The labor intensity of installation personnel is also reduced during floor;
2nd, when lightweight VCP floor is produced, PVC base need not be produced, wearing layer and color film can be carried out into heat directly multiple
Conjunction is processed, and hot recombination time is 10-15 minutes, is compared current VCP floors upper strata PVC heat recombination times and is reduced 60-75%,
The labor intensity of heat compound personnel is also mitigated while reducing energy consumption improve production efficiency, because the layer of PVC on VCP floors at present
The density of base material is 1.85g/cm3, the lightweight VCP floor of the present invention is without the need for PVC base;
3rd, directly need not carry out fitting after heat is compound, cold pressing treatment, UV process is carried out to surface again after colding pressing, then
Carry out cutting, slot, during this, save the operation of heat treatment destressing, and the operation of surface UV process is placed on and colds pressing it
Afterwards, the destruction when fitting, colding pressing to surface UV coating layer can be avoided, makes the glossiness and scratch resistance intensity of floor surface more preferable;
4th, as the composition structure on lightweight VCP floor is relatively simple, level is fewer, thus for gross thickness control ratio compared with
Ideal, maximum deviation are less than 0.07mm so that splicing floors are more smooth.
Specific embodiment
Below by specific embodiment, technical scheme is described in further detail.It should be appreciated that this
Bright enforcement is not limited to the following examples, and any pro forma flexible and/or change made to the present invention will all fall
Enter the scope of the present invention.
In the present invention, if not refering in particular to, all of part, percentage ratio are unit of weight, the equipment for being adopted and raw material etc.
It is commercially available or commonly used in the art.Method in following embodiments, if no special instructions, is the normal of this area
Rule method.
Raw material sources:
Environment-friendly plasticizer, purchased from Zhejiang Wei Bo Chemical Industry Science Co., Ltd;
Stabilizer, purchased from plastic cement company limited of Linan Holley;
Precipitated calcium carbonate, purchased from Jiangxi Guang Yuan chemical industry Co., Ltd;
Composite calcium carbonate, purchased from Jiangxi Guang Yuan chemical industry Co., Ltd;
Foaming agent, purchased from Mai Jisen composites company limited of city of Kunshan;
Lubricant, purchased from Mai Jisen composites company limited of city of Kunshan;
Processing aid, purchased from Mai Jisen composites company limited of city of Kunshan.
Embodiment 1-3:
The preparation method on lightweight VCP floor include layer of PVC processing, VCP base materials process, fit, colding pressing, surface UV process and
Fluting operation, it is specific as follows:
1st, the processing of layer of PVC:The wearing layer for preparing and the color film of printing are overlayed flat board sulfur by mainly hot Compound Machining
In the carrier of change machine, temperature sets 120-150 DEG C, the demoulding after heat compound 10-20 minutes, completes wearing layer with the color film of printing
Heat is compound, use to be fit.Wherein, the thickness of wearing layer is 0.5mm, and the thickness of color film is 0.07mm.
The preparation of wearing layer:The formula of wearing layer is shown in Table 1, each raw material is put into homogenizer and is mixed, and 1500 turns of rotating speed/
, to planet machine, by the mixing discharging of planet machine to open mixing roller, temperature control is at 180-200 DEG C, then passes through for the blanking of min, 5-6 minute
5 roller rolling out films, are embossed process after slice, wearing layer is made in finally winding.
2nd, VCP base materials processing:Polrvinyl chloride, composite calcium carbonate, stabilizer, foaming agent are put in proportion mixed at a high speed
Close cylinder and be stirred 12-15 minutes, rotating speed 700-800 turns/min, and temperature is discarded to cooling and stirring cylinder when reaching 110-115 DEG C,
60 DEG C are cooled to by 25 DEG C of circulating chilled waters, lubricant and processing aid is added through Screw Extrusion slice, the thickness of slice and
Size can select the mould of different size, but corresponding with the size of layer of PVC.The formula of VCP base materials is shown in Table 1, VCP base materials
Thickness be 4mm.
Table 1
Composite calcium carbonate described in table 1 is that precipitated calcium carbonate and ground calcium carbonate weight ratio are 3:7 mixture.
3rd, fit:After VCP base material completion of processing, constant temperature stands and carries out bonding process later in 24 hours, makes layer of PVC and VCP
Base material is fitted, and laminating is carried out using the PUR of polyurethane compositions.
4th, cold pressing:Be immediately placed in after the completion of laminating cold press fit again it is strong to increase the laminating of layer of PVC and VCP base materials
Degree, cold pressing pressure 5-7MPa, temperature 23-25 DEG C, 12-36 hours of colding pressing.
5th, surface UV process:Surface UV process is carried out after colding pressing, according to the gross thickness of product, adjustment UV rubber rolls and steel rod it
Between height, make the glossiness on layer of PVC surface reach the requirement of user, gloss range is typically between 3-20 °.
6th, slot:According to the requirement of user, corresponding button-type is selected.
Embodiment 4:
The preparation method on lightweight VCP floor include layer of PVC processing, VCP base materials process, fit, colding pressing, surface UV process and
Fluting operation, it is specific as follows:
1st, the processing of layer of PVC:The wearing layer for preparing and the color film of printing are overlayed flat board sulfur by mainly hot Compound Machining
In the carrier of change machine, temperature sets 130 DEG C, the demoulding after heat is compound 15 minutes, and the heat for completing wearing layer with the color film of printing is combined,
Use to be fit.Wherein, the thickness of wearing layer is 0.3mm, and the thickness of color film is 0.07mm.
The preparation of wearing layer:The formula of wearing layer is shown in Table 1, each raw material is put into homogenizer and is mixed, and 1500 turns of rotating speed/
, to planet machine, by the mixing discharging of planet machine to open mixing roller, temperature control is at 180-200 DEG C, then passes through for the blanking of min, 5-6 minute
5 roller rolling out films, are embossed process after slice, wearing layer is made in finally winding.
2nd, VCP base materials processing:Polrvinyl chloride, composite calcium carbonate, stabilizer, foaming agent are put in proportion mixed at a high speed
Close cylinder to be stirred 15 minutes, 700 turns/min of rotating speed, temperature are discarded to cooling and stirring cylinder when reaching 115 DEG C, by 25 DEG C of cold water
Circulating cooling adds lubricant and processing aid through Screw Extrusion slice to 60 DEG C, and the thickness and size of slice can be selected
The mould of different size, but it is corresponding with the size of layer of PVC.The formula of VCP base materials is shown in Table 1.The thickness of VCP base materials is 4mm.
3rd, fit:After VCP base material completion of processing, constant temperature stands and carries out bonding process later in 24 hours, makes layer of PVC and VCP
Base material is fitted, and laminating is carried out using the PUR of polyurethane compositions.
4th, cold pressing:Be immediately placed in after the completion of laminating cold press fit again it is strong to increase the laminating of layer of PVC and VCP base materials
Degree, cold pressing pressure 5MPa, 25 DEG C of temperature are colded pressing 24 hours.
5th, surface UV process:Surface UV process is carried out after colding pressing, according to the gross thickness of product, adjustment UV rubber rolls and steel rod it
Between height, make the glossiness on layer of PVC surface reach the requirement of user, gloss range is typically between 3-20 °.
6th, slot:According to the requirement of user, corresponding button-type is selected.
Embodiment 5:
The preparation method on lightweight VCP floor include layer of PVC processing, VCP base materials process, fit, colding pressing, surface UV process and
Fluting operation, it is specific as follows:
1st, the processing of layer of PVC:The wearing layer for preparing and the color film of printing are overlayed flat board sulfur by mainly hot Compound Machining
In the carrier of change machine, temperature sets 145 DEG C, the demoulding after heat is compound 18 minutes, and the heat for completing wearing layer with the color film of printing is combined,
Use to be fit.Wherein, the thickness of wearing layer is 0.35mm, and the thickness of color film is 0.07mm.
The preparation of wearing layer:The formula of wearing layer is shown in Table 1, each raw material is put into homogenizer and is mixed, and 1500 turns of rotating speed/
, to planet machine, by the mixing discharging of planet machine to open mixing roller, temperature control is at 180-200 DEG C, then passes through for the blanking of min, 5-6 minute
5 roller rolling out films, are embossed process after slice, wearing layer is made in finally winding.
2nd, VCP base materials processing:Polrvinyl chloride, composite calcium carbonate, stabilizer, foaming agent are put in proportion mixed at a high speed
Close cylinder to be stirred 12 minutes, 800 turns/min of rotating speed, temperature are discarded to cooling and stirring cylinder when reaching 110 DEG C, by 25 DEG C of cold water
Circulating cooling adds lubricant and processing aid through Screw Extrusion slice to 60 DEG C, and the thickness and size of slice can be selected
The mould of different size, but it is corresponding with the size of layer of PVC.The formula of VCP base materials is shown in Table 1.The thickness of VCP base materials is 5mm.
3rd, fit:After VCP base material completion of processing, constant temperature stands and carries out bonding process later in 24 hours, makes layer of PVC and VCP
Base material is fitted, and laminating is carried out using the PUR of polyurethane compositions.
4th, cold pressing:Be immediately placed in after the completion of laminating cold press fit again it is strong to increase the laminating of layer of PVC and VCP base materials
Degree, cold pressing pressure 7MPa, 23 DEG C of temperature are colded pressing 36 hours.
5th, surface UV process:Surface UV process is carried out after colding pressing, according to the gross thickness of product, adjustment UV rubber rolls and steel rod it
Between height, make the glossiness on layer of PVC surface reach the requirement of user, gloss range is typically between 3-20 °.
6th, slot:According to the requirement of user, corresponding button-type is selected.
Data Detection is carried out to lightweight VCP flooring product obtained in the present invention, 2 are the results are shown in Table.
2 properties of product data of table
Embodiment described above is one kind preferably scheme of the present invention, not the present invention is made any pro forma
Limit, also have other variants and remodeling on the premise of without departing from the technical scheme described in claim.
Claims (6)
1. a kind of lightweight VCP floor, it is characterised in that:The lightweight VCP floor be by color film, wearing layer, VCP base materials from top to bottom
It is composited, the main component of wearing layer is chlorinated polyethylene, the raw material composition of wearing layer includes by percentage to the quality:Chlorination
Polyethylene 64-75%, environment-friendly plasticizer 15-20%, stabilizer 3-4%, precipitated calcium carbonate 7-12%;The raw material group of VCP base materials
Into including by percentage to the quality:Polrvinyl chloride 32-36%, composite calcium carbonate 53-59%, stabilizer 3-4%, lubricant
0.8-1.5%, foaming agent 0.5-1%, processing aid 4-5%, the composite calcium carbonate are the mixed of precipitated calcium carbonate and ground calcium carbonate
The content of compound, wherein ground calcium carbonate is 55-75%.
2. lightweight VCP floor according to claim 1, it is characterised in that:The thickness of wearing layer be 0.1-0.6mm, color film
Thickness be 0.07 mm, the thickness of VCP base materials is 4-5mm.
3. lightweight VCP floor according to claim 1 and 2, it is characterised in that:The main component of the color film of printing is PVC, its
Raw material composition includes by percentage to the quality:PVC 97-98%, Calcium Carbonate 1-2%, stabilizer 0.5-1%, processing aid 0.5-1%.
4. the preparation method on the lightweight VCP floor described in a kind of claim 1, it is characterised in that the method include layer of PVC processing,
VCP base materials are processed, are fitted, colding pressing, surface UV is processed and operation of slotting, and are mainly comprised the following steps:Wearing layer and the color film of printing are by warm
Compound to make layer of PVC, the compound temperature of heat is 120-150 DEG C, minute time 10-20;Then layer of PVC and VCP base materials are colded pressing
Molding, temperature 23-25 DEG C, time 12-36h.
5. the preparation method on lightweight VCP floor according to claim 4, it is characterised in that the method comprises the steps:
1st, the processing of layer of PVC:The wearing layer for preparing and the color film of printing are overlayed in the carrier of vulcanizing press, temperature sets
Determine 120-150 DEG C, the demoulding after heat compound 10-20 minutes, the heat for wearing layer being completed with the color film of printing are combined;
2nd, VCP base materials processing:Polrvinyl chloride, composite calcium carbonate, stabilizer, foaming agent are put into into mixed at high speed cylinder in proportion
It is stirred, rotating speed 700-800 turns/min, minute time 12-15, temperature are discarded to cooling and stirring cylinder when reaching 110-115 DEG C,
60 ± 5 DEG C are cooled to, and lubricant and processing aid are added through Screw Extrusion slice;
3rd, fit:After VCP base material completion of processing, constant temperature stands and carries out bonding process later in 24 hours, makes layer of PVC and VCP base materials
Laminating;
4th, cold pressing:It is immediately placed in cold press to be fitted to increase the laminating intensity of layer of PVC and VCP base materials again after the completion of laminating, it is cold
Pressure pressure 5-7MPa, temperature 23-25 DEG C, 12-36 hours of colding pressing;
5th, surface UV process;
6th, slot.
6. the preparation method on lightweight VCP floor according to claim 4, it is characterised in that:Heat is combined when making layer of PVC,
The compound temperature of heat is 135-150 DEG C, minute time 16-18.
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WO2019237224A1 (en) * | 2018-06-11 | 2019-12-19 | 明和科技(唐山)股份有限公司 | Mute decorative material and preparation method therefor and use thereof |
CN114161801A (en) * | 2021-12-14 | 2022-03-11 | 苏州宏昌包装材料有限公司 | Composite packaging material with excellent oxygen and moisture permeability and preparation method thereof |
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CN107082982A (en) * | 2017-05-10 | 2017-08-22 | 安徽森泰木塑集团股份有限公司 | A kind of online three rollers laminating big flooring method of belt lock catch |
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