CN106635351A - Semi-synthetic cutting fluid with lubricating property enhanced by mica powder and preparation method of semi-synthetic cutting fluid - Google Patents

Semi-synthetic cutting fluid with lubricating property enhanced by mica powder and preparation method of semi-synthetic cutting fluid Download PDF

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Publication number
CN106635351A
CN106635351A CN201611114954.0A CN201611114954A CN106635351A CN 106635351 A CN106635351 A CN 106635351A CN 201611114954 A CN201611114954 A CN 201611114954A CN 106635351 A CN106635351 A CN 106635351A
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China
Prior art keywords
parts
cutting fluid
semi
mica powder
synthetic cutting
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CN201611114954.0A
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Chinese (zh)
Inventor
甘海滨
胡帮友
杨维军
叶彬
蒋春阳
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Wuhu Cang Agricultural Equipment Manufacturing Co Ltd
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Wuhu Cang Agricultural Equipment Manufacturing Co Ltd
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Priority to CN201611114954.0A priority Critical patent/CN106635351A/en
Publication of CN106635351A publication Critical patent/CN106635351A/en
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    • C—CHEMISTRY; METALLURGY
    • C10—PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
    • C10M—LUBRICATING COMPOSITIONS; USE OF CHEMICAL SUBSTANCES EITHER ALONE OR AS LUBRICATING INGREDIENTS IN A LUBRICATING COMPOSITION
    • C10M173/00—Lubricating compositions containing more than 10% water
    • C—CHEMISTRY; METALLURGY
    • C10—PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
    • C10M—LUBRICATING COMPOSITIONS; USE OF CHEMICAL SUBSTANCES EITHER ALONE OR AS LUBRICATING INGREDIENTS IN A LUBRICATING COMPOSITION
    • C10M2201/00—Inorganic compounds or elements as ingredients in lubricant compositions
    • C10M2201/06—Metal compounds
    • C10M2201/065—Sulfides; Selenides; Tellurides
    • C10M2201/066—Molybdenum sulfide
    • C—CHEMISTRY; METALLURGY
    • C10—PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
    • C10M—LUBRICATING COMPOSITIONS; USE OF CHEMICAL SUBSTANCES EITHER ALONE OR AS LUBRICATING INGREDIENTS IN A LUBRICATING COMPOSITION
    • C10M2201/00—Inorganic compounds or elements as ingredients in lubricant compositions
    • C10M2201/10—Compounds containing silicon
    • C10M2201/102—Silicates
    • C10M2201/103—Clays; Mica; Zeolites
    • C—CHEMISTRY; METALLURGY
    • C10—PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
    • C10M—LUBRICATING COMPOSITIONS; USE OF CHEMICAL SUBSTANCES EITHER ALONE OR AS LUBRICATING INGREDIENTS IN A LUBRICATING COMPOSITION
    • C10M2205/00—Organic macromolecular hydrocarbon compounds or fractions, whether or not modified by oxidation as ingredients in lubricant compositions
    • C10M2205/18—Natural waxes, e.g. ceresin, ozocerite, bees wax, carnauba; Degras
    • C—CHEMISTRY; METALLURGY
    • C10—PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
    • C10M—LUBRICATING COMPOSITIONS; USE OF CHEMICAL SUBSTANCES EITHER ALONE OR AS LUBRICATING INGREDIENTS IN A LUBRICATING COMPOSITION
    • C10M2207/00—Organic non-macromolecular hydrocarbon compounds containing hydrogen, carbon and oxygen as ingredients in lubricant compositions
    • C10M2207/40—Fatty vegetable or animal oils
    • C—CHEMISTRY; METALLURGY
    • C10—PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
    • C10M—LUBRICATING COMPOSITIONS; USE OF CHEMICAL SUBSTANCES EITHER ALONE OR AS LUBRICATING INGREDIENTS IN A LUBRICATING COMPOSITION
    • C10M2209/00—Organic macromolecular compounds containing oxygen as ingredients in lubricant compositions
    • C10M2209/02—Macromolecular compounds obtained by reactions only involving carbon-to-carbon unsaturated bonds
    • C10M2209/08—Macromolecular compounds obtained by reactions only involving carbon-to-carbon unsaturated bonds containing monomers having an unsaturated radical bound to a carboxyl radical, e.g. acrylate type
    • C10M2209/084—Acrylate; Methacrylate
    • C—CHEMISTRY; METALLURGY
    • C10—PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
    • C10M—LUBRICATING COMPOSITIONS; USE OF CHEMICAL SUBSTANCES EITHER ALONE OR AS LUBRICATING INGREDIENTS IN A LUBRICATING COMPOSITION
    • C10M2209/00—Organic macromolecular compounds containing oxygen as ingredients in lubricant compositions
    • C10M2209/12—Polysaccharides, e.g. cellulose, biopolymers
    • C—CHEMISTRY; METALLURGY
    • C10—PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
    • C10M—LUBRICATING COMPOSITIONS; USE OF CHEMICAL SUBSTANCES EITHER ALONE OR AS LUBRICATING INGREDIENTS IN A LUBRICATING COMPOSITION
    • C10M2215/00—Organic non-macromolecular compounds containing nitrogen as ingredients in lubricant compositions
    • C10M2215/02—Amines, e.g. polyalkylene polyamines; Quaternary amines
    • C—CHEMISTRY; METALLURGY
    • C10—PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
    • C10M—LUBRICATING COMPOSITIONS; USE OF CHEMICAL SUBSTANCES EITHER ALONE OR AS LUBRICATING INGREDIENTS IN A LUBRICATING COMPOSITION
    • C10M2219/00—Organic non-macromolecular compounds containing sulfur, selenium or tellurium as ingredients in lubricant compositions
    • C10M2219/04—Organic non-macromolecular compounds containing sulfur, selenium or tellurium as ingredients in lubricant compositions containing sulfur-to-oxygen bonds, i.e. sulfones, sulfoxides
    • C10M2219/044—Sulfonic acids, Derivatives thereof, e.g. neutral salts
    • C—CHEMISTRY; METALLURGY
    • C10—PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
    • C10M—LUBRICATING COMPOSITIONS; USE OF CHEMICAL SUBSTANCES EITHER ALONE OR AS LUBRICATING INGREDIENTS IN A LUBRICATING COMPOSITION
    • C10M2227/00—Organic non-macromolecular compounds containing atoms of elements not provided for in groups C10M2203/00, C10M2207/00, C10M2211/00, C10M2215/00, C10M2219/00 or C10M2223/00 as ingredients in lubricant compositions
    • C10M2227/06—Organic compounds derived from inorganic acids or metal salts
    • C10M2227/061—Esters derived from boron
    • C—CHEMISTRY; METALLURGY
    • C10—PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
    • C10M—LUBRICATING COMPOSITIONS; USE OF CHEMICAL SUBSTANCES EITHER ALONE OR AS LUBRICATING INGREDIENTS IN A LUBRICATING COMPOSITION
    • C10M2229/00—Organic macromolecular compounds containing atoms of elements not provided for in groups C10M2205/00, C10M2209/00, C10M2213/00, C10M2217/00, C10M2221/00 or C10M2225/00 as ingredients in lubricant compositions
    • C10M2229/04—Siloxanes with specific structure
    • C10M2229/041—Siloxanes with specific structure containing aliphatic substituents
    • C—CHEMISTRY; METALLURGY
    • C10—PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
    • C10N—INDEXING SCHEME ASSOCIATED WITH SUBCLASS C10M RELATING TO LUBRICATING COMPOSITIONS
    • C10N2030/00—Specified physical or chemical properties which is improved by the additive characterising the lubricating composition, e.g. multifunctional additives
    • C10N2030/06—Oiliness; Film-strength; Anti-wear; Resistance to extreme pressure
    • C—CHEMISTRY; METALLURGY
    • C10—PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
    • C10N—INDEXING SCHEME ASSOCIATED WITH SUBCLASS C10M RELATING TO LUBRICATING COMPOSITIONS
    • C10N2030/00—Specified physical or chemical properties which is improved by the additive characterising the lubricating composition, e.g. multifunctional additives
    • C10N2030/12—Inhibition of corrosion, e.g. anti-rust agents or anti-corrosives
    • C—CHEMISTRY; METALLURGY
    • C10—PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
    • C10N—INDEXING SCHEME ASSOCIATED WITH SUBCLASS C10M RELATING TO LUBRICATING COMPOSITIONS
    • C10N2030/00—Specified physical or chemical properties which is improved by the additive characterising the lubricating composition, e.g. multifunctional additives
    • C10N2030/16—Antiseptic; (micro) biocidal or bactericidal
    • C—CHEMISTRY; METALLURGY
    • C10—PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
    • C10N—INDEXING SCHEME ASSOCIATED WITH SUBCLASS C10M RELATING TO LUBRICATING COMPOSITIONS
    • C10N2030/00—Specified physical or chemical properties which is improved by the additive characterising the lubricating composition, e.g. multifunctional additives
    • C10N2030/64—Environmental friendly compositions
    • C—CHEMISTRY; METALLURGY
    • C10—PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
    • C10N—INDEXING SCHEME ASSOCIATED WITH SUBCLASS C10M RELATING TO LUBRICATING COMPOSITIONS
    • C10N2040/00—Specified use or application for which the lubricating composition is intended
    • C10N2040/20—Metal working
    • C10N2040/22—Metal working with essential removal of material, e.g. cutting, grinding or drilling

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  • Chemical & Material Sciences (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • General Chemical & Material Sciences (AREA)
  • Oil, Petroleum & Natural Gas (AREA)
  • Organic Chemistry (AREA)
  • Lubricants (AREA)

Abstract

The invention discloses semi-synthetic cutting fluid with the lubricating property enhanced by mica powder and a preparation method of the semi-synthetic cutting fluid. The semi-synthetic cutting fluid is characterized by being prepared from the following raw materials in parts by weight: 2 to 3 parts of mica powder, 15 to 25 parts of organic alkylol amine, 5 to 10 parts of boric acid, 15 to 25 parts of ethanol, 4 to 7 parts of oleic acid, 2 to 3 parts of sodium alginate, 2 to 4 parts of nano-molybdenum disulfide, 5 to 12 parts of sodium dodecyl sulfate, 10 to 20 parts of polyacrylic resin emulsion, 30 to 40 parts of palm oil, 5 to 9 parts of lauric acid, 2 to 3 parts of Span 80, 2 to 3 parts of Tween 80, 5 to 10 parts of paraffine-based oil, 1 to 2 parts of polydimethylsiloxane and 50 to 100 parts of distilled water. According to the semi-synthetic cutting fluid disclosed by the invention, the nano-molybdenum disulfide is dispersed by using the sodium alginate, and the surface of the nano-molybdenum disulfide is enabled to be rich in abundant functional groups; the sodium alginate is added into an additive to realize good compatibility, so that wear resistance, extreme pressure property and stability of the cutting fluid can be improved; by matching with the added mica powder, the lubricating property of the cutting fluid is enhanced.

Description

A kind of mica powder strengthens semi-synthetic cutting fluid of lubricity and preparation method thereof
Technical field
The present invention relates to a kind of semi-synthetic cutting fluid, and in particular to a kind of mica powder strengthens the semi-synthetic cutting fluid of lubricity And preparation method thereof.
Background technology
Semi-synthetic metalworking fluid, also known as micro emulsion metalworking fluid, i.e. dilute with water according to a certain percentage, emulsified particles are straight Footpath is less than 1 μm, is applied in the processing industries such as metal cutting, while having the good lubricity of emulsion concurrently and Synthesis liquid is good Cleaning feature, and be a very promising class cutting fluid with suitable extreme pressure property；Semi-synthetic metalworking fluid Main component be lubricating base oil (mineral oil), water, emulsifying agent, antirust agent, extreme pressure anti-wear additives, defoamer, antimildew disinfectant Deng.It is all low than Emulsified Metal Cutting Fluid in terms of emulsifying agent, mineral oil, the content of extreme pressure anti-wear additives.Water base semi-synthetic metal is cut The prospect for cutting liquid is very fine, not only shows excellent and environmentally friendly, easily dilute in the required aspect of performance of metalworking fluid Release, cost is also low than other kinds of metalworking fluid. 
Shi Renzong exists《The preparation research of semi-synthetic cutting fluid》Middle utilization mineral oil, extreme pressure put lubrication prescription be prepared for it is a kind of water base hemizygous Into cutting fluid, but its wear resistence, stability need to be improved.
The content of the invention
Think deeply based on more than, the present invention is intended to provide a kind of wear resistence is high, stability by force, environmentally friendly easily biological-degradable it is hemizygous Into cutting fluid, and preparation method thereof.
The technical problem to be solved is realized using following technical scheme：
A kind of mica powder strengthens the semi-synthetic cutting fluid of lubricity, it is characterised in that be made up of the raw material of following weight portion：
Mica powder 2-3, organic alcohol amine 15-25, boric acid 5-10, ethanol 15-25, oleic acid 4-7, sodium alginate 2-3, nanometer curing Molybdenum 2-4, dodecyl sodium sulfate 5-12, polyacrylic resin emulsion 10-20, palm oil 30-40, laurate 5-9, sorbester p17 2-3, Tween 80 2-3, paraffine base crude oil 5-10, dimethyl silicone polymer 1-2, distilled water 50-100；
The solid content of the polyacrylic resin emulsion is 10-30%.
A kind of described mica powder strengthens the preparation method of the semi-synthetic cutting fluid of lubricity, it is characterised in that be by with Lower step is made：
A. after 5-10 part organic alcohol amine stirring in water bath being heated into 60-80 DEG C, boric acid is added, continues heating stirring 50-100min, Oleic acid is added, continues to react 30-60min, organic boric acid ester antirust EP agent is obtained after cooling；
B. sodium alginate, nano molybdenum disulfide, 3-7 part dodecyl sodium sulfates, 30-60 are added in step a gained additive Ultrasonic vibration 10-30min at DEG C, obtains the additive package containing modified Nano molybdenum bisuphide；
C. palm oil, laurate and remaining organic alcohol amine are reacted into 1-3h at 80-130 DEG C, is generated containing laurate alkanolamine ester Mixing oiliness improver；
D. mica powder is put into ball mill after ball milling, uses ethanol solution ultrasonic disperse, after being dried, with polyacrylic acid tree Fat liquor is sprayed to its surface, is persistently stirred after 10-30min, is dried, and obtains mixture；
E. step b gained additive, distilled water, step c gained are mixed oiliness improver, step d gained mixture, sorbester p17, are told Temperature 80 after mixing and stirring at 30-50 DEG C, add paraffine base crude oil and remaining dodecyl sodium sulfate mixed solution, poly- two Methylsiloxane, stirs.
A kind of described mica powder strengthens the semi-synthetic cutting fluid of lubricity, it is characterised in that using method is by stoste In being added to suitable quantity of water, the dilution of 0.5%-1% is configured to.
The invention has the beneficial effects as follows：The organic boric acid ester of synthesis is a kind of novel environment-friendly additive, nontoxic, extreme pressure profit Slip is good, and has the functions such as antirust, anti-mattress concurrently；Nano molybdenum disulfide, surface is disperseed to contain abundant functional group with sodium alginate, Add it to have good compatibility in additive, such that it is able to improve wearability, the extreme pressure property of cutting fluid；While alginic acid Sodium has the effect of very strong protecting colloid, strong to the emulsifying ability of grease, improves the stability of cutting fluid；By laurate and hydramine Carry out reaction and generate laurate alkanolamine ester, the laurate of generation has anti-corrosion, the function of antibacterial, and biological degradability is good； Sorbester p17 and Tween 80 collocation are used, existing good emulsifying effectiveness, also certain rust-proof effect；Coordinate the mica powder of addition Enhance the lubricity of cutting fluid.
Specific embodiment
The specific embodiment of the present invention is further described with reference to embodiment.
Embodiment
A kind of mica powder strengthens the semi-synthetic cutting fluid of lubricity, it is characterised in that be by the raw material system of following weight portion Into：
Mica powder 3, organic alcohol amine 25, boric acid 10, ethanol 25, oleic acid 7, sodium alginate 3, nano molybdenum disulfide 4, dodecyl sulphur Sour sodium 12, polyacrylic resin emulsion 20, palm oil 40, laurate 9, sorbester p17 3, Tween 80 3, paraffine base crude oil 10, poly- two Methylsiloxane 2, distilled water 100；
The solid content of the polyacrylic resin emulsion is 10-30%.
A kind of described mica powder strengthens the preparation method of the semi-synthetic cutting fluid of lubricity, it is characterised in that be by with Lower step is made：
A. after 5-10 part organic alcohol amine stirring in water bath being heated into 60-80 DEG C, boric acid is added, continues heating stirring 50-100min, Oleic acid is added, continues to react 30-60min, organic boric acid ester antirust EP agent is obtained after cooling；
B. sodium alginate, nano molybdenum disulfide, 3-7 part dodecyl sodium sulfates, 30-60 are added in step a gained additive Ultrasonic vibration 10-30min at DEG C, obtains the additive package containing modified Nano molybdenum bisuphide；
C. palm oil, laurate and remaining organic alcohol amine are reacted into 1-3h at 80-130 DEG C, is generated containing laurate alkanolamine ester Mixing oiliness improver；
D. mica powder is put into ball mill after ball milling, uses ethanol solution ultrasonic disperse, after being dried, with polyacrylic acid tree Fat liquor is sprayed to its surface, is persistently stirred after 10-30min, is dried, and obtains mixture；
E. step b gained additive, distilled water, step c gained are mixed oiliness improver, step d gained mixture, sorbester p17, are told Temperature 80 after mixing and stirring at 30-50 DEG C, add paraffine base crude oil and remaining dodecyl sodium sulfate mixed solution, poly- two Methylsiloxane, stirs.
A kind of described mica powder strengthens the semi-synthetic cutting fluid of lubricity, it is characterised in that using method is by stoste In being added to suitable quantity of water, the dilution of 0.5%-1% is configured to.
The present invention properties of product test data be：Without seizing loadP BValue >=1568N（Extreme pressure property）；Coefficient of friction≤ 0.012。

Claims (3)

1. a kind of mica powder strengthens the semi-synthetic cutting fluid of lubricity, it is characterised in that be made up of the raw material of following weight portion：
Mica powder 2-3, organic alcohol amine 15-25, boric acid 5-10, ethanol 15-25, oleic acid 4-7, sodium alginate 2-3, nanometer curing Molybdenum 2-4, dodecyl sodium sulfate 5-12, polyacrylic resin emulsion 10-20, palm oil 30-40, laurate 5-9, sorbester p17 2-3, Tween 80 2-3, paraffine base crude oil 5-10, dimethyl silicone polymer 1-2, distilled water 50-100；
The solid content of the polyacrylic resin emulsion is 10-30%.
2. a kind of mica powder according to claim 1 strengthens the preparation method of the semi-synthetic cutting fluid of lubricity, its feature It is to be made up of following steps：
A. after 5-10 part organic alcohol amine stirring in water bath being heated into 60-80 DEG C, boric acid is added, continues heating stirring 50-100min, Oleic acid is added, continues to react 30-60min, organic boric acid ester antirust EP agent is obtained after cooling；
B. sodium alginate, nano molybdenum disulfide, 3-7 part dodecyl sodium sulfates, 30-60 are added in step a gained additive Ultrasonic vibration 10-30min at DEG C, obtains the additive package containing modified Nano molybdenum bisuphide；
C. palm oil, laurate and remaining organic alcohol amine are reacted into 1-3h at 80-130 DEG C, is generated containing laurate alkanolamine ester Mixing oiliness improver；
D. mica powder is put into ball mill after ball milling, uses ethanol solution ultrasonic disperse, after being dried, with polyacrylic acid tree Fat liquor is sprayed to its surface, is persistently stirred after 10-30min, is dried, and obtains mixture；
E. step b gained additive, distilled water, step c gained are mixed oiliness improver, step d gained mixture, sorbester p17, are told Temperature 80 after mixing and stirring at 30-50 DEG C, add paraffine base crude oil and remaining dodecyl sodium sulfate mixed solution, poly- two Methylsiloxane, stirs.
3. a kind of mica powder according to claim 1 strengthens the semi-synthetic cutting fluid of lubricity, it is characterised in that user Method is that stoste is added in suitable quantity of water, is configured to the dilution of 0.5%-1%.
CN201611114954.0A 2016-12-07 2016-12-07 Semi-synthetic cutting fluid with lubricating property enhanced by mica powder and preparation method of semi-synthetic cutting fluid Pending CN106635351A (en)

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Cited By (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN112675779A (en) * 2020-12-23 2021-04-20 南通恒润新材料科技有限公司 High-temperature-resistant easy-to-disperse emulsifier and preparation method thereof

Citations (2)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN104277900A (en) * 2014-09-25 2015-01-14 巢湖广丰金属制品有限公司 High-antiwear cutting fluid
CN104789311A (en) * 2015-04-22 2015-07-22 青岛承天伟业机械制造有限公司 Multifunctional cutting liquid

Patent Citations (2)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN104277900A (en) * 2014-09-25 2015-01-14 巢湖广丰金属制品有限公司 High-antiwear cutting fluid
CN104789311A (en) * 2015-04-22 2015-07-22 青岛承天伟业机械制造有限公司 Multifunctional cutting liquid

Non-Patent Citations (2)

* Cited by examiner, † Cited by third party
Title
赵炳桢等: "《现代刀具设计与应用》", 30 September 2014, 国防工业出版社 *
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Cited By (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN112675779A (en) * 2020-12-23 2021-04-20 南通恒润新材料科技有限公司 High-temperature-resistant easy-to-disperse emulsifier and preparation method thereof

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Application publication date: 20170510