CN106634887A - Production method for anti-sloughing lubricating solid polyalcohol used for drilling fluid - Google Patents
Production method for anti-sloughing lubricating solid polyalcohol used for drilling fluid Download PDFInfo
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- CN106634887A CN106634887A CN201611257417.1A CN201611257417A CN106634887A CN 106634887 A CN106634887 A CN 106634887A CN 201611257417 A CN201611257417 A CN 201611257417A CN 106634887 A CN106634887 A CN 106634887A
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- Prior art keywords
- surfactant
- production method
- polyacrylonitrile
- ammonium salt
- span
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- C—CHEMISTRY; METALLURGY
- C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
- C09K—MATERIALS FOR MISCELLANEOUS APPLICATIONS, NOT PROVIDED FOR ELSEWHERE
- C09K8/00—Compositions for drilling of boreholes or wells; Compositions for treating boreholes or wells, e.g. for completion or for remedial operations
- C09K8/02—Well-drilling compositions
- C09K8/03—Specific additives for general use in well-drilling compositions
- C09K8/035—Organic additives
-
- C—CHEMISTRY; METALLURGY
- C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
- C09K—MATERIALS FOR MISCELLANEOUS APPLICATIONS, NOT PROVIDED FOR ELSEWHERE
- C09K2208/00—Aspects relating to compositions of drilling or well treatment fluids
- C09K2208/12—Swell inhibition, i.e. using additives to drilling or well treatment fluids for inhibiting clay or shale swelling or disintegrating
-
- C—CHEMISTRY; METALLURGY
- C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
- C09K—MATERIALS FOR MISCELLANEOUS APPLICATIONS, NOT PROVIDED FOR ELSEWHERE
- C09K2208/00—Aspects relating to compositions of drilling or well treatment fluids
- C09K2208/34—Lubricant additives
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- Chemical & Material Sciences (AREA)
- Life Sciences & Earth Sciences (AREA)
- General Life Sciences & Earth Sciences (AREA)
- Engineering & Computer Science (AREA)
- Materials Engineering (AREA)
- Organic Chemistry (AREA)
- Curing Cements, Concrete, And Artificial Stone (AREA)
- Degasification And Air Bubble Elimination (AREA)
- Detergent Compositions (AREA)
Abstract
The invention provides a production method for anti-sloughing lubricating solid polyalcohol used for a drilling fluid. The production method is realized by compounding the following six substances: a surfactant PE, sodium lignosulfonate, polyacrylonitrile-ammonium salt, a surfactant L62, a surfactant span 80 and an antifoaming agent xp, wherein the mass ratio of solid materials of the surfactant PE to the sodium lignosulfonate to the polyacrylonitrile-ammonium salt is 1: 1: 1; the mass ratio of liquid materials of the high-purity and high-concentration surfactant L62 to the surfactant span 80 to the antifoaming agent xp is 5: 5: 2; and the mass of the solid materials is 9 times of the mass of the liquid materials. The invention has the following advantages: the production process is simple to operate and facilitates environmental protection; and the product produced by using the method provided by the invention has good dispersity, water solubility and compatibility, is economical and practical, and is convenient to use.
Description
Technical field
The present invention relates to petroleum drilling fluid uses polymerized polyalcohol field, more particularly, to a kind of drilling well
The liquid production method of caving-preventing and lubrication solid polymerization alcohol.
Background technology
With constantly carrying out for petroleum exploration and development, now warp-wise deep-well, ultradeep well and Holes of Complicated Wells development, here development
During, occur in that because shale hydration expansion cause bit freezing, blowout, well slough, serious bit wear a series of problems, such as, very
To causing well to be scrapped, oil-gas Layer heavy damage can cause very big economic loss.
Drilling fluid polymerized polyalcohol has excellent inhibition, lubricity and borehole wall stability, and its cloud point spread is in brill
Be conducive to recognizing during well, find and reservoir protec-tion.Liquid drilling fluid polymeric alcohol is packed special, handling trouble, addition
In-convenience in use, the shortcomings of the term of validity is short.In the past solid polymerization alcohol mainly had based on oxirane, expoxy propane, polyglycereol etc.
Material is wanted, is formed by high temperature polymerization, complex manufacturing, easily caused environmental pollution, high cost, product and easily bond, effectively
The shortcomings of phase is short.
The content of the invention
It is an object of the invention to solve the deficiencies in the prior art, and a kind of drilling fluid is provided and is used
The production method of caving-preventing and lubrication solid polymerization alcohol.
The new technical scheme of the present invention is:A kind of drilling fluid production method of caving-preventing and lubrication solid polymerization alcohol, it is described
Production method includes surfactant PE, lignin sulfonic acid sodium salt, polyacrylonitrile-ammonium salt, surfactant L62, surface-active
Agent Span 80, six kinds of material compoundings of defoamer xp are formed, wherein:It is solid material surfactant PE, lignin sulfonic acid sodium salt, poly-
The mass ratio of acrylonitrile-ammonium salt is successively 1:1:1;Liquid material high purity concentrations surfactant L62, surfactant department
The class 80, mass ratio of defoamer xp is successively 5:5:2;Wherein solid material quality is approximately 9 times of liquid material quality.
The step of described production method, is as follows:
(1)Start mixer, surfactant PE is added into mixer, be then followed by adding polyacrylonitrile-ammonium salt and wood
Quality sulfonate sodium, stirs 15-20Min;Then it is uniform respectively to spray high purity concentrations surfactant L62 and surfactant department
Class 80, finally sprays defoamer xp;
(2)Surfactant PE is continuously added, is then followed by adding polyacrylonitrile-ammonium salt and lignin sulfonic acid sodium salt, then
Respectively uniform sprinkling high purity concentrations surfactant L62 and surfactant Span 80, stir 20-40Min;
(3)Whether observation material stirs, sample examination;Blowing is packed.
Described production method is comprised the following steps that:
(1)Start mixer, whether testing equipment works well;150kg surfactant PE are added into mixer, then
150Kg polyacrylonitrile-ammonium salt and 150Kg lignin sulfonic acid sodium salts are subsequently added into, 15Min is stirred;Then respectively uniform sprinkling is high
The pure concentration surface activating agent L62 and each 25kg of surfactant Span 80, finally sprays the defoamer xp of 20kg;
(2)150kg surfactant PE are continuously added, is then followed by adding 150Kg polyacrylonitrile-ammonium salt and 150Kg lignin
Sulfonate sodium;Then it is uniform respectively to spray the high purity concentrations surfactant L62 and each 25kg of surfactant Span 80, stirring
30Min;
(3)Whether observation material stirs, sample examination;Blowing is packed.
The invention has the beneficial effects as follows:The simple in production process operation of the present invention, beneficial to environmental protection;The product for being produced
Good dispersion, good water solubility, compatibility are good, economical and practical, easy to use.
Specific embodiment
A kind of drilling fluid production method of caving-preventing and lubrication solid polymerization alcohol, described production method include surfactant PE,
Lignin sulfonic acid sodium salt, polyacrylonitrile-ammonium salt, surfactant L62, surfactant Span 80, six kinds of materials of defoamer xp
Compounding is formed, wherein:Solid material surfactant PE, lignin sulfonic acid sodium salt, polyacrylonitrile-ammonium salt mass ratio according to
Secondary is 1:1:1;Liquid material high purity concentrations surfactant L62, surfactant Span 80, defoamer xp mass ratio according to
Secondary is 5:5:2;Wherein solid material quality is approximately 9 times of liquid material quality.
The step of described production method, is as follows:
(1)Start mixer, surfactant PE is added into mixer, be then followed by adding polyacrylonitrile-ammonium salt and wood
Quality sulfonate sodium, stirs 15-20Min;Then it is uniform respectively to spray high purity concentrations surfactant L62 and surfactant department
Class 80, finally sprays defoamer xp;
(2)Surfactant PE is continuously added, is then followed by adding polyacrylonitrile-ammonium salt and lignin sulfonic acid sodium salt, then
Respectively uniform sprinkling high purity concentrations surfactant L62 and surfactant Span 80, stir 20-40Min;
(3)Whether observation material stirs, sample examination;Blowing is packed.
Described production method is comprised the following steps that:
(1)Start mixer, whether testing equipment works well;150kg surfactant PE are added into mixer, then
150Kg polyacrylonitrile-ammonium salt and 150Kg lignin sulfonic acid sodium salts are subsequently added into, 15Min is stirred;Then respectively uniform sprinkling is high
The pure concentration surface activating agent L62 and each 25kg of surfactant Span 80, finally sprays the defoamer xp of 20kg;
(2)150kg surfactant PE are continuously added, is then followed by adding 150Kg polyacrylonitrile-ammonium salt and 150Kg lignin
Sulfonate sodium;Then it is uniform respectively to spray the high purity concentrations surfactant L62 and each 25kg of surfactant Span 80, stirring
30Min;
(3)Whether observation material stirs, sample examination;Blowing is packed.
Claims (3)
1. a kind of drilling fluid production method of caving-preventing and lubrication solid polymerization alcohol, it is characterised in that:Described production method includes
Surfactant PE, lignin sulfonic acid sodium salt, polyacrylonitrile-ammonium salt, surfactant L62, surfactant Span 80, disappear
Six kinds of material compoundings of infusion xp are formed, wherein:Solid material surfactant PE, lignin sulfonic acid sodium salt, polyacrylonitrile-ammonium
The mass ratio of salt is successively 1:1:1;Liquid material high purity concentrations surfactant L62, surfactant Span 80, defoamer
The mass ratio of xp is successively 5:5:2;Wherein solid material quality is approximately 9 times of liquid material quality.
2. a kind of drilling fluid according to claim 1 production method of caving-preventing and lubrication solid polymerization alcohol, it is characterised in that:
The step of described production method, is as follows:
(1)Start mixer, surfactant PE is added into mixer, be then followed by adding polyacrylonitrile-ammonium salt and wood
Quality sulfonate sodium, stirs 15-20Min;Then it is uniform respectively to spray high purity concentrations surfactant L62 and surfactant department
Class 80, finally sprays defoamer xp;
(2)Surfactant PE is continuously added, is then followed by adding polyacrylonitrile-ammonium salt and lignin sulfonic acid sodium salt, Ran Houfen
High purity concentrations surfactant L62 and surfactant Span 80 are not uniformly sprayed, 20-40Min is stirred;
(3)Whether observation material stirs, sample examination;Blowing is packed.
3. a kind of drilling fluid according to claim 1 production method of caving-preventing and lubrication solid polymerization alcohol, it is characterised in that:
Described production method is comprised the following steps that:
(1)Start mixer, whether testing equipment works well;150kg surfactant PE are added into mixer, then
150Kg polyacrylonitrile-ammonium salt and 150Kg lignin sulfonic acid sodium salts are subsequently added into, 15Min is stirred;Then respectively uniform sprinkling is high
The pure concentration surface activating agent L62 and each 25kg of surfactant Span 80, finally sprays the defoamer xp of 20kg;
(2)150kg surfactant PE are continuously added, is then followed by adding 150Kg polyacrylonitrile-ammonium salt and 150Kg lignin
Sulfonate sodium;Then it is uniform respectively to spray the high purity concentrations surfactant L62 and each 25kg of surfactant Span 80, stirring
30Min;
(3)Whether observation material stirs, sample examination;Blowing is packed.
Priority Applications (1)
Application Number | Priority Date | Filing Date | Title |
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CN201611257417.1A CN106634887A (en) | 2016-12-30 | 2016-12-30 | Production method for anti-sloughing lubricating solid polyalcohol used for drilling fluid |
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CN201611257417.1A CN106634887A (en) | 2016-12-30 | 2016-12-30 | Production method for anti-sloughing lubricating solid polyalcohol used for drilling fluid |
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CN106634887A true CN106634887A (en) | 2017-05-10 |
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CN201611257417.1A Pending CN106634887A (en) | 2016-12-30 | 2016-12-30 | Production method for anti-sloughing lubricating solid polyalcohol used for drilling fluid |
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Cited By (1)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
CN107418529A (en) * | 2017-06-28 | 2017-12-01 | 常州明华运输有限公司 | A kind of anti-caving agent for drilling fluid |
Citations (5)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
CN1775892A (en) * | 2005-11-25 | 2006-05-24 | 王刚 | Polymeric alcohol oil-layer protectant formula and its preparing method |
CN1958713A (en) * | 2006-11-29 | 2007-05-09 | 中国石油大学(北京) | Solid polyalcohol in use for drilling fluid |
CN104341589A (en) * | 2014-10-17 | 2015-02-11 | 北京培康佳业技术发展有限公司 | Solid polyalcohol for oilfield drilling fluid and preparation method and application thereof |
CN104592960A (en) * | 2014-12-31 | 2015-05-06 | 西南石油大学 | Amphoteric potassium-based polyalcohol water-based drilling fluid for drilling shale |
CN105670574A (en) * | 2014-11-21 | 2016-06-15 | 中石化胜利石油工程有限公司钻井工艺研究院 | Drilling fluid ether-amine compound inhibitor and preparation method thereof |
-
2016
- 2016-12-30 CN CN201611257417.1A patent/CN106634887A/en active Pending
Patent Citations (5)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
CN1775892A (en) * | 2005-11-25 | 2006-05-24 | 王刚 | Polymeric alcohol oil-layer protectant formula and its preparing method |
CN1958713A (en) * | 2006-11-29 | 2007-05-09 | 中国石油大学(北京) | Solid polyalcohol in use for drilling fluid |
CN104341589A (en) * | 2014-10-17 | 2015-02-11 | 北京培康佳业技术发展有限公司 | Solid polyalcohol for oilfield drilling fluid and preparation method and application thereof |
CN105670574A (en) * | 2014-11-21 | 2016-06-15 | 中石化胜利石油工程有限公司钻井工艺研究院 | Drilling fluid ether-amine compound inhibitor and preparation method thereof |
CN104592960A (en) * | 2014-12-31 | 2015-05-06 | 西南石油大学 | Amphoteric potassium-based polyalcohol water-based drilling fluid for drilling shale |
Cited By (1)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
CN107418529A (en) * | 2017-06-28 | 2017-12-01 | 常州明华运输有限公司 | A kind of anti-caving agent for drilling fluid |
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