CN106631654A - 化合物合成装置及方法 - Google Patents
化合物合成装置及方法 Download PDFInfo
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- CN106631654A CN106631654A CN201611149036.1A CN201611149036A CN106631654A CN 106631654 A CN106631654 A CN 106631654A CN 201611149036 A CN201611149036 A CN 201611149036A CN 106631654 A CN106631654 A CN 106631654A
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- synthesizer
- benzene
- hydrocarbon
- carbide
- magnetic valve
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- 230000015572 biosynthetic process Effects 0.000 title claims abstract description 67
- 238000003786 synthesis reaction Methods 0.000 title claims abstract description 67
- 150000001875 compounds Chemical class 0.000 title claims abstract description 34
- 238000000034 method Methods 0.000 title claims abstract description 27
- UHOVQNZJYSORNB-UHFFFAOYSA-N Benzene Chemical compound C1=CC=CC=C1 UHOVQNZJYSORNB-UHFFFAOYSA-N 0.000 claims abstract description 209
- 229930195733 hydrocarbon Natural products 0.000 claims abstract description 51
- 150000002430 hydrocarbons Chemical class 0.000 claims abstract description 50
- 239000004215 Carbon black (E152) Substances 0.000 claims abstract description 49
- 230000002194 synthesizing effect Effects 0.000 claims abstract description 8
- OAKJQQAXSVQMHS-UHFFFAOYSA-N Hydrazine Chemical compound NN OAKJQQAXSVQMHS-UHFFFAOYSA-N 0.000 claims description 60
- CURLTUGMZLYLDI-UHFFFAOYSA-N Carbon dioxide Chemical compound O=C=O CURLTUGMZLYLDI-UHFFFAOYSA-N 0.000 claims description 52
- 229910002092 carbon dioxide Inorganic materials 0.000 claims description 27
- 239000001569 carbon dioxide Substances 0.000 claims description 24
- 238000001816 cooling Methods 0.000 claims description 21
- 238000006243 chemical reaction Methods 0.000 claims description 20
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 claims description 19
- HSFWRNGVRCDJHI-UHFFFAOYSA-N alpha-acetylene Natural products C#C HSFWRNGVRCDJHI-UHFFFAOYSA-N 0.000 claims description 14
- 239000003153 chemical reaction reagent Substances 0.000 claims description 14
- 125000002534 ethynyl group Chemical group [H]C#C* 0.000 claims description 12
- 238000001308 synthesis method Methods 0.000 claims description 4
- 230000005611 electricity Effects 0.000 claims description 3
- 238000011068 loading method Methods 0.000 claims description 2
- 238000012360 testing method Methods 0.000 claims description 2
- 238000001514 detection method Methods 0.000 abstract description 6
- 150000001722 carbon compounds Chemical class 0.000 abstract description 4
- 229960004424 carbon dioxide Drugs 0.000 description 22
- 239000007789 gas Substances 0.000 description 16
- 230000008569 process Effects 0.000 description 10
- TXLQIRALKZAWHN-UHFFFAOYSA-N dilithium carbanide Chemical compound [Li+].[Li+].[CH3-].[CH3-] TXLQIRALKZAWHN-UHFFFAOYSA-N 0.000 description 9
- 241001465754 Metazoa Species 0.000 description 7
- IJGRMHOSHXDMSA-UHFFFAOYSA-N Atomic nitrogen Chemical compound N#N IJGRMHOSHXDMSA-UHFFFAOYSA-N 0.000 description 5
- 229910052799 carbon Inorganic materials 0.000 description 5
- 238000002360 preparation method Methods 0.000 description 5
- 238000000746 purification Methods 0.000 description 5
- 239000000126 substance Substances 0.000 description 5
- 229910011140 Li2C2 Inorganic materials 0.000 description 4
- 230000008901 benefit Effects 0.000 description 4
- 238000010438 heat treatment Methods 0.000 description 4
- 239000007788 liquid Substances 0.000 description 4
- 239000000463 material Substances 0.000 description 4
- 238000007789 sealing Methods 0.000 description 4
- OKTJSMMVPCPJKN-UHFFFAOYSA-N Carbon Chemical compound [C] OKTJSMMVPCPJKN-UHFFFAOYSA-N 0.000 description 3
- -1 Hydrogen compound Chemical class 0.000 description 3
- 229910001873 dinitrogen Inorganic materials 0.000 description 3
- 239000001257 hydrogen Substances 0.000 description 3
- 229910052739 hydrogen Inorganic materials 0.000 description 3
- 238000004519 manufacturing process Methods 0.000 description 3
- 238000002203 pretreatment Methods 0.000 description 3
- 150000001721 carbon Chemical group 0.000 description 2
- 239000003638 chemical reducing agent Substances 0.000 description 2
- 239000003795 chemical substances by application Substances 0.000 description 2
- 239000000498 cooling water Substances 0.000 description 2
- 238000013461 design Methods 0.000 description 2
- 238000005516 engineering process Methods 0.000 description 2
- 239000012530 fluid Substances 0.000 description 2
- 230000006870 function Effects 0.000 description 2
- 229910052744 lithium Inorganic materials 0.000 description 2
- 238000001556 precipitation Methods 0.000 description 2
- 239000002994 raw material Substances 0.000 description 2
- 230000029058 respiratory gaseous exchange Effects 0.000 description 2
- 239000010935 stainless steel Substances 0.000 description 2
- 229910001220 stainless steel Inorganic materials 0.000 description 2
- OKTJSMMVPCPJKN-IGMARMGPSA-N Carbon-12 Chemical compound [12C] OKTJSMMVPCPJKN-IGMARMGPSA-N 0.000 description 1
- OKTJSMMVPCPJKN-NJFSPNSNSA-N Carbon-14 Chemical compound [14C] OKTJSMMVPCPJKN-NJFSPNSNSA-N 0.000 description 1
- FUJCRWPEOMXPAD-UHFFFAOYSA-N Li2O Inorganic materials [Li+].[Li+].[O-2] FUJCRWPEOMXPAD-UHFFFAOYSA-N 0.000 description 1
- 229910000617 Mangalloy Inorganic materials 0.000 description 1
- 229910000792 Monel Inorganic materials 0.000 description 1
- 229910000831 Steel Inorganic materials 0.000 description 1
- QCWXUUIWCKQGHC-UHFFFAOYSA-N Zirconium Chemical compound [Zr] QCWXUUIWCKQGHC-UHFFFAOYSA-N 0.000 description 1
- QFGIVKNKFPCKAW-UHFFFAOYSA-N [Mn].[C] Chemical compound [Mn].[C] QFGIVKNKFPCKAW-UHFFFAOYSA-N 0.000 description 1
- 238000010521 absorption reaction Methods 0.000 description 1
- 238000007259 addition reaction Methods 0.000 description 1
- 229910045601 alloy Inorganic materials 0.000 description 1
- 239000000956 alloy Substances 0.000 description 1
- 238000000429 assembly Methods 0.000 description 1
- 230000000712 assembly Effects 0.000 description 1
- WAKZZMMCDILMEF-UHFFFAOYSA-H barium(2+);diphosphate Chemical compound [Ba+2].[Ba+2].[Ba+2].[O-]P([O-])([O-])=O.[O-]P([O-])([O-])=O WAKZZMMCDILMEF-UHFFFAOYSA-H 0.000 description 1
- 230000009286 beneficial effect Effects 0.000 description 1
- 230000005540 biological transmission Effects 0.000 description 1
- 229910002090 carbon oxide Inorganic materials 0.000 description 1
- 238000003763 carbonization Methods 0.000 description 1
- JJWKPURADFRFRB-UHFFFAOYSA-N carbonyl sulfide Chemical compound O=C=S JJWKPURADFRFRB-UHFFFAOYSA-N 0.000 description 1
- 239000003054 catalyst Substances 0.000 description 1
- 230000008859 change Effects 0.000 description 1
- 239000002131 composite material Substances 0.000 description 1
- 230000008878 coupling Effects 0.000 description 1
- 238000010168 coupling process Methods 0.000 description 1
- 238000005859 coupling reaction Methods 0.000 description 1
- 238000011161 development Methods 0.000 description 1
- XUCJHNOBJLKZNU-UHFFFAOYSA-M dilithium;hydroxide Chemical compound [Li+].[Li+].[OH-] XUCJHNOBJLKZNU-UHFFFAOYSA-M 0.000 description 1
- 238000007599 discharging Methods 0.000 description 1
- 238000001704 evaporation Methods 0.000 description 1
- 230000008020 evaporation Effects 0.000 description 1
- 230000007062 hydrolysis Effects 0.000 description 1
- 238000006460 hydrolysis reaction Methods 0.000 description 1
- 230000006872 improvement Effects 0.000 description 1
- 230000002452 interceptive effect Effects 0.000 description 1
- 230000007246 mechanism Effects 0.000 description 1
- 239000000203 mixture Substances 0.000 description 1
- 238000012986 modification Methods 0.000 description 1
- 230000004048 modification Effects 0.000 description 1
- 229910052757 nitrogen Inorganic materials 0.000 description 1
- 239000005416 organic matter Substances 0.000 description 1
- 238000012856 packing Methods 0.000 description 1
- 230000029553 photosynthesis Effects 0.000 description 1
- 238000010672 photosynthesis Methods 0.000 description 1
- 238000004886 process control Methods 0.000 description 1
- 230000002285 radioactive effect Effects 0.000 description 1
- 239000000376 reactant Substances 0.000 description 1
- 230000008439 repair process Effects 0.000 description 1
- 238000011160 research Methods 0.000 description 1
- 239000010959 steel Substances 0.000 description 1
- 238000003756 stirring Methods 0.000 description 1
- 238000010189 synthetic method Methods 0.000 description 1
- QORWJWZARLRLPR-UHFFFAOYSA-H tricalcium bis(phosphate) Chemical compound [Ca+2].[Ca+2].[Ca+2].[O-]P([O-])([O-])=O.[O-]P([O-])([O-])=O QORWJWZARLRLPR-UHFFFAOYSA-H 0.000 description 1
- 229910000391 tricalcium phosphate Inorganic materials 0.000 description 1
- 229910052726 zirconium Inorganic materials 0.000 description 1
Classifications
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
- C07C2/00—Preparation of hydrocarbons from hydrocarbons containing a smaller number of carbon atoms
- C07C2/02—Preparation of hydrocarbons from hydrocarbons containing a smaller number of carbon atoms by addition between unsaturated hydrocarbons
- C07C2/42—Preparation of hydrocarbons from hydrocarbons containing a smaller number of carbon atoms by addition between unsaturated hydrocarbons homo- or co-oligomerisation with ring formation, not being a Diels-Alder conversion
- C07C2/48—Preparation of hydrocarbons from hydrocarbons containing a smaller number of carbon atoms by addition between unsaturated hydrocarbons homo- or co-oligomerisation with ring formation, not being a Diels-Alder conversion of only hydrocarbons containing a carbon-to-carbon triple bond
Landscapes
- Chemical & Material Sciences (AREA)
- Organic Chemistry (AREA)
- Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
Abstract
Description
Claims (10)
Priority Applications (1)
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CN201611149036.1A CN106631654A (zh) | 2016-12-13 | 2016-12-13 | 化合物合成装置及方法 |
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CN201611149036.1A CN106631654A (zh) | 2016-12-13 | 2016-12-13 | 化合物合成装置及方法 |
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CN106631654A true CN106631654A (zh) | 2017-05-10 |
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CN201611149036.1A Pending CN106631654A (zh) | 2016-12-13 | 2016-12-13 | 化合物合成装置及方法 |
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Citations (8)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
JP2007047134A (ja) * | 2005-08-05 | 2007-02-22 | Aomoriken Kogyo Gijutsu Kyoiku Shinkokai | 炭素14測定試料の調製方法と装置 |
CN201628644U (zh) * | 2010-03-16 | 2010-11-10 | 中国地质科学院岩溶地质研究所 | 放射性碳测年样品制备系统的集成控制装置 |
CN103135629A (zh) * | 2013-01-30 | 2013-06-05 | 常州大学 | 一种啤酒发酵过程温度控制系统及其方法 |
CN203011761U (zh) * | 2012-09-27 | 2013-06-19 | 南阳理工学院 | 放射性碳测定中合成苯除水纯化装置 |
CN103822811A (zh) * | 2014-02-28 | 2014-05-28 | 中国地质大学(武汉) | 一种测试有机物类样品14c丰度的前处理方法和设备 |
CN105286637A (zh) * | 2015-11-25 | 2016-02-03 | 浙江沁园水处理科技有限公司 | 一种快速制冷的饮水机 |
CN105527142A (zh) * | 2016-01-15 | 2016-04-27 | 中国地质科学院岩溶地质研究所 | 一种放射性碳测年样品制备金属系统 |
CN206529417U (zh) * | 2016-12-13 | 2017-09-29 | 武汉中地依舸科技有限公司 | 化合物合成装置及设备 |
-
2016
- 2016-12-13 CN CN201611149036.1A patent/CN106631654A/zh active Pending
Patent Citations (8)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
JP2007047134A (ja) * | 2005-08-05 | 2007-02-22 | Aomoriken Kogyo Gijutsu Kyoiku Shinkokai | 炭素14測定試料の調製方法と装置 |
CN201628644U (zh) * | 2010-03-16 | 2010-11-10 | 中国地质科学院岩溶地质研究所 | 放射性碳测年样品制备系统的集成控制装置 |
CN203011761U (zh) * | 2012-09-27 | 2013-06-19 | 南阳理工学院 | 放射性碳测定中合成苯除水纯化装置 |
CN103135629A (zh) * | 2013-01-30 | 2013-06-05 | 常州大学 | 一种啤酒发酵过程温度控制系统及其方法 |
CN103822811A (zh) * | 2014-02-28 | 2014-05-28 | 中国地质大学(武汉) | 一种测试有机物类样品14c丰度的前处理方法和设备 |
CN105286637A (zh) * | 2015-11-25 | 2016-02-03 | 浙江沁园水处理科技有限公司 | 一种快速制冷的饮水机 |
CN105527142A (zh) * | 2016-01-15 | 2016-04-27 | 中国地质科学院岩溶地质研究所 | 一种放射性碳测年样品制备金属系统 |
CN206529417U (zh) * | 2016-12-13 | 2017-09-29 | 武汉中地依舸科技有限公司 | 化合物合成装置及设备 |
Non-Patent Citations (3)
Title |
---|
万军伟等: "《同位素水文学理论与实践》", 武汉:中国地质大学出版社, pages: 356 - 75 * |
杨海兰: "环境和生物样品中~3H和~(14)C的测量", no. 03, pages 184 - 188 * |
王华;饶文波;杨学清;应启和;钟云;苏治国;冯玉梅;涂林玲;: "常规碳十四制样系统及其优化", no. 02, pages 129 - 132 * |
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Effective date of registration: 20170622 Address after: 430000, No. 19, Buddha Road, East Lake New Technology Development Zone, Hubei, Wuhan, China Applicant after: WUHAN ZHONGDI YIGE TECHNOLOGY CO.,LTD. Address before: 430000 No. 388 Lu Lu, Hongshan District, Hubei, Wuhan Applicant before: Wuhan in the big asset management Co.,Ltd. Applicant before: Zhang Wei Effective date of registration: 20170622 Address after: 430000 No. 388 Lu Lu, Hongshan District, Hubei, Wuhan Applicant after: Wuhan in the big asset management Co.,Ltd. Applicant after: Zhang Wei Address before: 430000 No. 388 Lu Lu, Hongshan District, Hubei, Wuhan Applicant before: CHINA University OF GEOSCIENCES (WUHAN CITY) Applicant before: Zhang Wei Effective date of registration: 20170622 Address after: 430000 No. 388 Lu Lu, Hongshan District, Hubei, Wuhan Applicant after: CHINA University OF GEOSCIENCES (WUHAN CITY) Applicant after: Zhang Wei Address before: 430000 No. 388 Lu Lu, Hongshan District, Hubei, Wuhan Applicant before: CHINA University OF GEOSCIENCES (WUHAN CITY) |