CN106630822B - A kind of preparation method of concrete prefabricated board - Google Patents

A kind of preparation method of concrete prefabricated board Download PDF

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Publication number
CN106630822B
CN106630822B CN201611022746.8A CN201611022746A CN106630822B CN 106630822 B CN106630822 B CN 106630822B CN 201611022746 A CN201611022746 A CN 201611022746A CN 106630822 B CN106630822 B CN 106630822B
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washing liquid
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CN106630822A (en
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黎万新
张秋红
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Xinjiang relongda Renewable Resources Technology Co., Ltd.
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Xinjiang Longda Building Materials Ltd Co
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    • CCHEMISTRY; METALLURGY
    • C04CEMENTS; CONCRETE; ARTIFICIAL STONE; CERAMICS; REFRACTORIES
    • C04BLIME, MAGNESIA; SLAG; CEMENTS; COMPOSITIONS THEREOF, e.g. MORTARS, CONCRETE OR LIKE BUILDING MATERIALS; ARTIFICIAL STONE; CERAMICS; REFRACTORIES; TREATMENT OF NATURAL STONE
    • C04B28/00Compositions of mortars, concrete or artificial stone, containing inorganic binders or the reaction product of an inorganic and an organic binder, e.g. polycarboxylate cements
    • C04B28/02Compositions of mortars, concrete or artificial stone, containing inorganic binders or the reaction product of an inorganic and an organic binder, e.g. polycarboxylate cements containing hydraulic cements other than calcium sulfates
    • C04B28/04Portland cements
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B28WORKING CEMENT, CLAY, OR STONE
    • B28BSHAPING CLAY OR OTHER CERAMIC COMPOSITIONS; SHAPING SLAG; SHAPING MIXTURES CONTAINING CEMENTITIOUS MATERIAL, e.g. PLASTER
    • B28B1/00Producing shaped prefabricated articles from the material
    • B28B1/08Producing shaped prefabricated articles from the material by vibrating or jolting
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B28WORKING CEMENT, CLAY, OR STONE
    • B28BSHAPING CLAY OR OTHER CERAMIC COMPOSITIONS; SHAPING SLAG; SHAPING MIXTURES CONTAINING CEMENTITIOUS MATERIAL, e.g. PLASTER
    • B28B11/00Apparatus or processes for treating or working the shaped or preshaped articles
    • B28B11/24Apparatus or processes for treating or working the shaped or preshaped articles for curing, setting or hardening
    • B28B11/245Curing concrete articles
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B28WORKING CEMENT, CLAY, OR STONE
    • B28BSHAPING CLAY OR OTHER CERAMIC COMPOSITIONS; SHAPING SLAG; SHAPING MIXTURES CONTAINING CEMENTITIOUS MATERIAL, e.g. PLASTER
    • B28B7/00Moulds; Cores; Mandrels
    • B28B7/38Treating surfaces of moulds, cores, or mandrels to prevent sticking
    • B28B7/384Treating agents
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B28WORKING CEMENT, CLAY, OR STONE
    • B28BSHAPING CLAY OR OTHER CERAMIC COMPOSITIONS; SHAPING SLAG; SHAPING MIXTURES CONTAINING CEMENTITIOUS MATERIAL, e.g. PLASTER
    • B28B7/00Moulds; Cores; Mandrels
    • B28B7/38Treating surfaces of moulds, cores, or mandrels to prevent sticking
    • B28B7/388Treating surfaces of moulds, cores, or mandrels to prevent sticking with liquid material, e.g. lubricating
    • CCHEMISTRY; METALLURGY
    • C10PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
    • C10MLUBRICATING COMPOSITIONS; USE OF CHEMICAL SUBSTANCES EITHER ALONE OR AS LUBRICATING INGREDIENTS IN A LUBRICATING COMPOSITION
    • C10M173/00Lubricating compositions containing more than 10% water
    • CCHEMISTRY; METALLURGY
    • C04CEMENTS; CONCRETE; ARTIFICIAL STONE; CERAMICS; REFRACTORIES
    • C04BLIME, MAGNESIA; SLAG; CEMENTS; COMPOSITIONS THEREOF, e.g. MORTARS, CONCRETE OR LIKE BUILDING MATERIALS; ARTIFICIAL STONE; CERAMICS; REFRACTORIES; TREATMENT OF NATURAL STONE
    • C04B2201/00Mortars, concrete or artificial stone characterised by specific physical values
    • C04B2201/20Mortars, concrete or artificial stone characterised by specific physical values for the density
    • CCHEMISTRY; METALLURGY
    • C04CEMENTS; CONCRETE; ARTIFICIAL STONE; CERAMICS; REFRACTORIES
    • C04BLIME, MAGNESIA; SLAG; CEMENTS; COMPOSITIONS THEREOF, e.g. MORTARS, CONCRETE OR LIKE BUILDING MATERIALS; ARTIFICIAL STONE; CERAMICS; REFRACTORIES; TREATMENT OF NATURAL STONE
    • C04B2201/00Mortars, concrete or artificial stone characterised by specific physical values
    • C04B2201/50Mortars, concrete or artificial stone characterised by specific physical values for the mechanical strength
    • CCHEMISTRY; METALLURGY
    • C10PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
    • C10MLUBRICATING COMPOSITIONS; USE OF CHEMICAL SUBSTANCES EITHER ALONE OR AS LUBRICATING INGREDIENTS IN A LUBRICATING COMPOSITION
    • C10M2201/00Inorganic compounds or elements as ingredients in lubricant compositions
    • C10M2201/08Inorganic acids or salts thereof
    • C10M2201/082Inorganic acids or salts thereof containing nitrogen
    • C10M2201/083Inorganic acids or salts thereof containing nitrogen nitrites
    • CCHEMISTRY; METALLURGY
    • C10PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
    • C10MLUBRICATING COMPOSITIONS; USE OF CHEMICAL SUBSTANCES EITHER ALONE OR AS LUBRICATING INGREDIENTS IN A LUBRICATING COMPOSITION
    • C10M2201/00Inorganic compounds or elements as ingredients in lubricant compositions
    • C10M2201/087Boron oxides, acids or salts
    • CCHEMISTRY; METALLURGY
    • C10PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
    • C10MLUBRICATING COMPOSITIONS; USE OF CHEMICAL SUBSTANCES EITHER ALONE OR AS LUBRICATING INGREDIENTS IN A LUBRICATING COMPOSITION
    • C10M2215/00Organic non-macromolecular compounds containing nitrogen as ingredients in lubricant compositions
    • C10M2215/02Amines, e.g. polyalkylene polyamines; Quaternary amines
    • C10M2215/04Amines, e.g. polyalkylene polyamines; Quaternary amines having amino groups bound to acyclic or cycloaliphatic carbon atoms
    • C10M2215/042Amines, e.g. polyalkylene polyamines; Quaternary amines having amino groups bound to acyclic or cycloaliphatic carbon atoms containing hydroxy groups; Alkoxylated derivatives thereof
    • CCHEMISTRY; METALLURGY
    • C10PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
    • C10NINDEXING SCHEME ASSOCIATED WITH SUBCLASS C10M RELATING TO LUBRICATING COMPOSITIONS
    • C10N2040/00Specified use or application for which the lubricating composition is intended
    • C10N2040/36Release agents or mold release agents

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  • Chemical & Material Sciences (AREA)
  • Engineering & Computer Science (AREA)
  • Ceramic Engineering (AREA)
  • Mechanical Engineering (AREA)
  • Manufacturing & Machinery (AREA)
  • Structural Engineering (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • Organic Chemistry (AREA)
  • Oil, Petroleum & Natural Gas (AREA)
  • General Chemical & Material Sciences (AREA)
  • Inorganic Chemistry (AREA)
  • Materials Engineering (AREA)
  • Fire-Extinguishing Compositions (AREA)
  • Curing Cements, Concrete, And Artificial Stone (AREA)
  • Road Paving Structures (AREA)
  • Processing Of Solid Wastes (AREA)

Abstract

The invention discloses a kind of preparation methods of concrete partition, the cement of 27~33 parts by weight, the flyash of 3~8 parts by weight, the clinker of 40~45 parts by weight and the aerated blocks particle of 18~22 parts by weight are added in the water of 20~35 parts by weight, stir 2~5min, 0.1~0.2 parts by weight complex accelerator is added later, 2~3min is stirred, the complex accelerator is anhydrous sodium sulphate and sodium chloride according to 1:0.8~1.2 ratio mixing;The raw material mixed is cast in later in the mold of spraying release agent, vibrates, be closed flat green body and cover cover board, stands 6~8h demoulding discharging after heating 3~5h.Compared with prior art, the features such as present invention has preparation method simple, shortens demoulding time, reduces labor intensity of workers.

Description

A kind of preparation method of concrete prefabricated board
Technical field
The present invention relates to a kind of preparation methods of concrete prefabricated board.
Background technique
China is a big coal country, using coal as power generation substantially fuel.The energy industry stable development in China, power generation Ability annual growth is 7.3%, and the rapid development of power industry brings sharply increasing for clinker and flyash discharge capacity, is fired The clinker and flyash total amount that coal steam power plant is discharged every year increase year by year.Flyash is under catching in the flue gas after coal combustion The fine ash come, main oxides group become:SiO2, Al2O3, FeO, Fe2O3, CaO, TiO2 etc..Place is not added in a large amount of flyash Reason will generate fugitive dust, pollute atmosphere;Silt up if being discharged into water system and will cause river, and toxic chemical substance therein can also be right Human body and biology cause damages.
China is the per capita limited country of resource reserve again, the comprehensive utilization of flyash and clinker, change give up into Treasured turns bane into boon, it has also become an important techno-economic policy in economic construction of China is to solve China's power generation environment It pollutes, contradictory important means and one of the task of the faced solution of power generation between resource shortage.By exploitation, powder Coal ash is widely used building each department such as work, building materials, water conservancy.
With economic construction, construction industry is phased out the use of common brick, and serious waste resource is understood in the production of common brick, and The pollution that will cause environment, the characteristic without sustainable development.Therefore, construction industry starts largely to use concrete product, It is mainly reflected in concrete prefabricated material, concrete prefabricated material has the following advantages that:One, modularized production, root may be implemented According to needing to produce different products, is transported later to scene, installed at the scene;Two, the construction period of building is improved, Different plate can be produced in advance according to construction requirements, it is time saving and energy saving to install at the scene;Three, with sustainable development May, clinker and flyash belong to industrial waste, turn waste into wealth, circular economy.
But at present concrete prefabricated board manufacturing enterprise problem is encountered that, demoulding time is longer, and general demoulding time is 10~12 hours, a mould can only be gone out within one day, production efficiency is lower, and worker-hours are also very long.From preparation raw material, pour It builds demoulding to the end to discharge, the entire duty cycle at least needs 13 hours, and not only labor intensity of workers is big, but also production efficiency It is low.
Therefore, a kind of preparation method is simple, shortens demoulding time, reduces the system of the concrete prefabricated board of labor intensity of workers Preparation Method is suggested.
Summary of the invention
The present invention provides a kind of preparation method is simple, shorten demoulding time, the concrete for reducing labor intensity of workers is pre- The preparation method of making sheet.
A kind of preparation method of concrete prefabricated board, it is characterised in that include the following steps:
A, raw material mixes:The cement of 27~33 parts by weight, the powder of 3~8 parts by weight are added in the water of 20~35 parts by weight The aerated blocks particle of coal ash, the clinker of 40~45 parts by weight and 18~22 parts by weight stirs 2~5min, and addition 0.1 later~ 0.2 parts by weight complex accelerator, stirs 2~3min, and the complex accelerator is anhydrous sodium sulphate and sodium chloride according to 1:0.8~1.2 Ratio mixing;
B, mold is poured:In mould surface spraying release agent, the raw material that a step mixes later is poured into mold, is opened Dynamic vibration device, vibrates 10~30s, is closed flat green body, covers cover board;
C, heating is stood:Start heating device, temperature is 30~48 DEG C, 3~5h of heating time;
D, demoulding discharging:6~8h demoulding discharging after heating;
Above-mentioned release agent is prepared using following methods:
A, the used oil of 30~35 parts by weight is added in the water of 65~70 parts by weight, opens heating device, temperature is 90℃;
B, the emulsifier of 0.26~0.64 parts by weight is added, and continues 20~35min of stirring, the emulsifier be PO-10, At least one of Span -60 or polyvinyl lactam;
C, be reduced to after room temperature be added the borax of 0.6~1.0 parts by weight, the sodium nitrite of 0.2~0.3 parts by weight and 1~ The triethanolamine of 1.5 parts by weight;
D, it is 7~9 that stearic acid or sodium hydroxide adjusting pH value, which is added,;
E, after standing 3~7 days, the dish washing liquid solution of 10~20 parts by weight and the diesel oil of 3~8 parts by weight is added, it is described to wash Clean essence solution is dish washing liquid and water according to weight ratio 1:The mixed solution that 3~7 ratio is mixed with.
Above-mentioned cement is ordinary portland cement.
Above-mentioned clinker is the clinker of loss on ignition≤5%.
Above-mentioned flyash is greater than three-level, the flyash of loss on ignition≤5%.
Above-mentioned aerated blocks particle is the particle of partial size 0.5mm~10mm.
Above-mentioned used oil is that motor vehicle used discarded machine oil.
Above-mentioned dish washing liquid is common liq dish washing liquid.
Above-mentioned diesel oil is one of 0# diesel oil, -10# diesel oil either -35# diesel oil.
The method for preparing concrete prefabricated board by this method can mitigate mitigation finished weight, mitigate surface density extremely 75-80kg/m2.And can demould in advance, improve production efficiency, it is most important that, the concrete prefabricated board produced it is strong Degree can achieve national standard.2 hours demoulding strengths are increased to 2.5~2.8MPa from zero.Demoulding strength reaches after 12 hours To 4.0~5.0MPa.
Specific embodiment
Embodiment 1:A kind of preparation method of concrete prefabricated board, it is characterised in that include the following steps:
A, raw material mixes:The cement of 27 parts by weight, the flyash of 3 parts by weight, 40 weight are added in the water of 20 parts by weight The clinker of part and the aerated blocks particle of 18 parts by weight, stir 2min, and 0.1 parts by weight complex accelerator is added later, stir 2min, The complex accelerator is anhydrous sodium sulphate and sodium chloride according to 1:0.8 ratio mixing;Above-mentioned cement is ordinary portland cement;On State the clinker that clinker is loss on ignition 0.8%;Above-mentioned flyash is greater than three-level, the flyash of loss on ignition 1%;Above-mentioned aerated blocks Particle is the particle of partial size 0.5mm;
B, mold is poured:In mould surface spraying release agent, the raw material mixed is poured into prefabricated board die, is started Vibration device vibrates 23s, is closed flat green body, covers cover board;
C, heating is stood:Start heating device, temperature is 39 DEG C, heating time 4.1h;
D, demoulding discharging:7.1h demoulding discharging after heating;
Above-mentioned release agent is prepared using following methods:
A, the used oil of 30.9 parts by weight is added in the water of 69.2 parts by weight, opens heating device, temperature 90 ℃;
B, the emulsifier of 0.46 parts by weight is added, and continues to stir 33min, the emulsifier is PO-10 and Span -60;
C, the borax of 0.88 parts by weight, the sodium nitrite of 0.26 parts by weight and 1.33 parts by weight are added after being reduced to room temperature Triethanolamine;
D, it is 8.4 that stearic acid or sodium hydroxide adjusting pH value, which is added,;
E, after standing 4 days, the dish washing liquid solution of 18 parts by weight and the diesel oil of 4.5 parts by weight, the dish washing liquid solution is added It is dish washing liquid and water according to weight ratio 1:The mixed solution that 6.8 ratio is mixed with.
Above-mentioned used oil is that motor vehicle used discarded machine oil.
Above-mentioned dish washing liquid is common liq dish washing liquid.
Above-mentioned diesel oil is -10# diesel oil.
By test:2 hours demoulding strengths are increased to 2.5MPa from zero.Demoulding strength reaches after 12 hours 4.0MPa。
Embodiment 2:A kind of preparation method of concrete prefabricated board, it is characterised in that include the following steps:
A, raw material mixes:The cement of 27.6 parts by weight, the flyash of 3.9 parts by weight, 43 are added in the water of 27 parts by weight The aerated blocks particle of the clinker of parts by weight and 18.6 parts by weight stirs 2.7min, 0.15 parts by weight complex accelerator is added later, 2.6min is stirred, the complex accelerator is anhydrous sodium sulphate and sodium chloride according to 1:0.9 ratio mixing;Above-mentioned cement is ordinary silicon Acid salt cement;Above-mentioned clinker is the clinker of loss on ignition 2%;Above-mentioned flyash is greater than three-level, the flyash of loss on ignition 1.5%; Above-mentioned aerated blocks particle is the particle of partial size 3.5mm;
B, mold is poured:In mould surface spraying release agent, the raw material mixed is poured into prefabricated board die, is started Vibration device vibrates 27s, is closed flat green body, covers cover board;
C, heating is stood:Start heating device, temperature is 31 DEG C, heating time 4.8h;
D, demoulding discharging:6.7h demoulding discharging after heating;
Above-mentioned release agent is prepared using following methods:
A, the used oil of 34.5 parts by weight is added in the water of 66.5 parts by weight, opens heating device, temperature 90 ℃;
B, the emulsifier of 0.56 parts by weight is added, and continues to stir 24min, the emulsifier is PO-10 and polyethylene acyl Amine;
C, the borax of 0.93 parts by weight, the sodium nitrite of 0.23 parts by weight and 1.42 parts by weight are added after being reduced to room temperature Triethanolamine;
D, it is 7.1 that stearic acid or sodium hydroxide adjusting pH value, which is added,;
E, after standing 3.5 days, the dish washing liquid solution of 14 parts by weight and the diesel oil of 3.6 parts by weight is added, the dish washing liquid is molten Liquid is dish washing liquid and water according to weight ratio 1:The mixed solution that 5.5 ratio is mixed with.
Above-mentioned used oil is that motor vehicle used discarded machine oil.
Above-mentioned dish washing liquid is common liq dish washing liquid.
Above-mentioned diesel oil is 0# diesel oil.
By test:2 hours demoulding strengths are increased to 2.55MPa from zero.Demoulding strength reaches after 12 hours 4.2MPa。
Embodiment 3:A kind of preparation method of concrete prefabricated board, it is characterised in that include the following steps:
A, raw material mixes:The cement of 28.4 parts by weight, the flyash of 6.3 amount parts, 41.8 are added in the water of 34 parts by weight The aerated blocks particle of the clinker of parts by weight and 19 parts by weight stirs 2.2min, 0.13 parts by weight complex accelerator is added later, stirs 2.2min is mixed, the complex accelerator is anhydrous sodium sulphate and sodium chloride according to 1:0.86 ratio mixing;Above-mentioned cement is ordinary silicon Acid salt cement;Above-mentioned clinker is the clinker of loss on ignition 1.3%;Above-mentioned flyash is greater than three-level, the fine coal of loss on ignition 1.8% Ash;Above-mentioned aerated blocks particle is the particle of partial size 1.5mm;
B, mold is poured:In mould surface spraying release agent, the raw material mixed is poured into prefabricated board die, is started Vibration device vibrates 21s, is closed flat green body, covers cover board;
C, heating is stood:Start heating device, temperature is 42 DEG C, heating time 3.3h;
D, demoulding discharging:6.2h demoulding discharging after heating;
Above-mentioned release agent is prepared using following methods:
A, the used oil of 34.2 parts by weight is added in the water of 68.9 parts by weight, opens heating device, temperature 90 ℃;
B, the emulsifier of 0.38 parts by weight is added, and continues to stir 26min, the emulsifier is polyvinyl lactam;
C, the borax of 0.7 parts by weight, the sodium nitrite of 0.23 parts by weight and 1.39 parts by weight are added after being reduced to room temperature Triethanolamine;
D, it is 7.6 that stearic acid or sodium hydroxide adjusting pH value, which is added,;
E, after standing 4.3 days, the dish washing liquid solution of 11 parts by weight and the diesel oil of 4.2 parts by weight is added, the dish washing liquid is molten Liquid is dish washing liquid and water according to weight ratio 1:The mixed solution that 6.5 ratio is mixed with.
Above-mentioned used oil is that motor vehicle used discarded machine oil.
Above-mentioned dish washing liquid is common liq dish washing liquid.
Above-mentioned diesel oil is -10# diesel oil.
By test:2 hours demoulding strengths are increased to 2.59MPa from zero.Demoulding strength reaches after 12 hours 4.3MPa。
Embodiment 4:A kind of preparation method of concrete prefabricated board, it is characterised in that include the following steps:
A, raw material mixes:Be added in the water of 21 parts by weight the cement of 27.3 parts by weight, the flyash of 4.5 parts by weight, The aerated blocks particle of the clinker of 43.9 parts by weight and 18.3 parts by weight stirs 2.9min, 0.17 parts by weight compound morning is added later Strong agent, stirs 2.9min, and the complex accelerator is anhydrous sodium sulphate and sodium chloride according to 1:0.96 ratio mixing;Above-mentioned cement is Ordinary portland cement;Above-mentioned clinker is the clinker of loss on ignition 1.5%;Above-mentioned flyash be greater than three-level, loss on ignition 2.0% Flyash;Above-mentioned aerated blocks particle is the particle of partial size 5.0mm;
B, mold is poured:In mould surface spraying release agent, the raw material mixed is poured into prefabricated board die, is started Vibration device vibrates 10s, is closed flat green body, covers cover board;
C, heating is stood:Start heating device, temperature is 30 DEG C, heating time 3h;
D, demoulding discharging:6h demoulding discharging after heating;
Above-mentioned release agent is prepared using following methods:
A, the used oil of 30 parts by weight is added in the water of 65 parts by weight, opens heating device, temperature is 90 DEG C;
B, the emulsifier of 0.26 parts by weight is added, and continues to stir 20min, the emulsifier is PO-10;
C, three second that the borax of 0.6 parts by weight, the sodium nitrite of 0.2 parts by weight and 1 parts by weight are added after room temperature are reduced to Hydramine;
D, it is 7 that stearic acid or sodium hydroxide adjusting pH value, which is added,;
E, after standing 3 days, the dish washing liquid solution of 10 parts by weight and the diesel oil of 3 parts by weight is added, the dish washing liquid solution is Dish washing liquid and water are according to weight ratio 1:The mixed solution that 3 ratio is mixed with.
Above-mentioned used oil is that motor vehicle used discarded machine oil.
Above-mentioned dish washing liquid is common liq dish washing liquid.
Above-mentioned diesel oil is 0# diesel oil.By test:2 hours demoulding strengths are increased to 2.51MPa from zero.After 12 hours Demoulding strength reaches 4.15MPa.
Embodiment 5:A kind of preparation method of concrete prefabricated board, it is characterised in that include the following steps:
A, raw material mixes:The cement of 28 parts by weight, the flyash of 6.6 parts by weight, 40.6 are added in the water of 28 parts by weight The aerated blocks particle of the clinker of parts by weight and 19.5 parts by weight stirs 2.5min, 0.12 parts by weight complex accelerator is added later, 2.1min is stirred, the complex accelerator is anhydrous sodium sulphate and sodium chloride according to 1:1 ratio mixing;Above-mentioned cement is common silicic acid Salt cement;Above-mentioned clinker is the clinker of loss on ignition 2.1%;Above-mentioned flyash is greater than three-level, the flyash of loss on ignition 2.5%; Above-mentioned aerated blocks particle is the particle of partial size 5.5mm;
B, mold is poured:In mould surface spraying release agent, the raw material mixed is poured into prefabricated board die, is started Vibration device vibrates 25s, is closed flat green body, covers cover board;
C, heating is stood:Start heating device, temperature is 37 DEG C, heating time 3.6h;
D, demoulding discharging:7.6h demoulding discharging after heating;
Above-mentioned release agent is prepared using following methods:
A, the used oil of 30.3 parts by weight is added in the water of 69.5 parts by weight, opens heating device, temperature 90 ℃;
B, the emulsifier of 0.44 parts by weight is added, and continues to stir 22min, the emulsifier is Span -60 and polyethylene Amide;
C, the borax of 0.75 parts by weight, the sodium nitrite of 0.22 parts by weight and 1.06 parts by weight are added after being reduced to room temperature Triethanolamine;
D, it is 8.8 that stearic acid or sodium hydroxide adjusting pH value, which is added,;
E, after standing 6.3 days, the dish washing liquid solution of 18.3 parts by weight and the diesel oil of 4.8 parts by weight, the dish washing liquid is added Solution is dish washing liquid and water according to weight ratio 1:The mixed solution that 3.5 ratio is mixed with.
Above-mentioned used oil is that motor vehicle used discarded machine oil.
Above-mentioned dish washing liquid is common liq dish washing liquid.
Above-mentioned diesel oil is -35# diesel oil.
By test:2 hours demoulding strengths are increased to 2.57MPa from zero.Demoulding strength reaches after 12 hours 4.35MPa。
Embodiment 6:A kind of preparation method of concrete prefabricated board, it is characterised in that include the following steps:
A, raw material mixes:Be added in the water of 33 parts by weight the cement of 30.3 parts by weight, the flyash of 5.4 parts by weight, The aerated blocks particle of the clinker of 41.2 parts by weight and 18.5 parts by weight stirs 2.3min, 0.14 parts by weight compound morning is added later Strong agent, stirs 2.7min, and the complex accelerator is anhydrous sodium sulphate and sodium chloride according to 1:1.04 ratio mixing;Above-mentioned cement is Ordinary portland cement;Above-mentioned clinker is the clinker of loss on ignition 2.5%;Above-mentioned flyash be greater than three-level, loss on ignition 2.7% Flyash;Above-mentioned aerated blocks particle is the particle of partial size 2.5mm;
B, mold is poured:In mould surface spraying release agent, the raw material mixed is poured into prefabricated board die, is started Vibration device vibrates 17s, is closed flat green body, covers cover board;
C, heating is stood:Start heating device, temperature is 41 DEG C, heating time 4h;
D, demoulding discharging:7.7h demoulding discharging after heating;
Above-mentioned release agent is prepared using following methods:
A, the used oil of 31.5 parts by weight is added in the water of 69.8 parts by weight, opens heating device, temperature 90 ℃;
B, 0.30 part of emulsifier is added, and continues to stir 21.5min, the emulsifier is Span -60 and polyethylene acyl Amine;
C, the borax of 0.65 parts by weight, the sodium nitrite of 0.21 parts by weight and 1.21 parts by weight are added after being reduced to room temperature Triethanolamine;
D, it is 7.8 that stearic acid or sodium hydroxide adjusting pH value, which is added,;
E, after standing 6.8 days, the dish washing liquid solution of 16 parts by weight and the diesel oil of 5.4 parts by weight is added, the dish washing liquid is molten Liquid is dish washing liquid and water according to weight ratio 1:The mixed solution that 3.8 ratio is mixed with.
Above-mentioned used oil is that motor vehicle used discarded machine oil.
Above-mentioned dish washing liquid is common liq dish washing liquid.
Above-mentioned diesel oil is -35# diesel oil.
By test:2 hours demoulding strengths are increased to 2.53MPa from zero.Demoulding strength reaches after 12 hours 4.25MPa。
Embodiment 7:A kind of preparation method of concrete prefabricated board, it is characterised in that include the following steps:
A, raw material mixes:The cement of 29 parts by weight, the flyash of 4.2 parts by weight, 44.2 are added in the water of 22 parts by weight The aerated blocks particle of the clinker of parts by weight and 19.7 parts by weight stirs 3min, 0.11 parts by weight complex accelerator is added later, stirs 2.4min is mixed, the complex accelerator is anhydrous sodium sulphate and sodium chloride according to 1:0.88 ratio mixing;Above-mentioned cement is ordinary silicon Acid salt cement;Above-mentioned clinker is the clinker of loss on ignition 2.6%;Above-mentioned flyash is greater than three-level, the fine coal of loss on ignition 2.4% Ash;Above-mentioned aerated blocks particle is the particle of partial size 4.5mm;
B, mold is poured:In mould surface spraying release agent, the raw material mixed is poured into prefabricated board die, is started Vibration device vibrates 14s, is closed flat green body, covers cover board;
C, heating is stood:Start heating device, temperature is 33 DEG C, heating time 3.4h;
D, demoulding discharging:6.4h demoulding discharging after heating;
Above-mentioned release agent is prepared using following methods:
A, the used oil of 30.9 parts by weight is added in the water of 69.2 parts by weight, opens heating device, temperature 90 ℃;
B, the emulsifier of 0.46 parts by weight is added, and continues to stir 33min, the emulsifier is PO-10 and Span -60;
C, the borax of 0.88 parts by weight, the sodium nitrite of 0.26 parts by weight and 1.33 parts by weight are added after being reduced to room temperature Triethanolamine;
D, it is 8.4 that stearic acid or sodium hydroxide adjusting pH value, which is added,;
E, after standing 4 days, the dish washing liquid solution of 18 parts by weight and the diesel oil of 4.5 parts by weight, the dish washing liquid solution is added It is dish washing liquid and water according to weight ratio 1:The mixed solution that 6.8 ratio is mixed with.
Above-mentioned used oil is that motor vehicle used discarded machine oil.
Above-mentioned dish washing liquid is common liq dish washing liquid.
Above-mentioned diesel oil is -10# diesel oil.
By test:2 hours demoulding strengths are increased to 2.6MPa from zero.Demoulding strength reaches after 12 hours 4.5MPa。
Embodiment 8:A kind of preparation method of concrete prefabricated board, it is characterised in that include the following steps:
A, raw material mixes:The cement of 30 parts by weight, the flyash of 5.1 parts by weight, 42.4 are added in the water of 29 parts by weight The aerated blocks particle of the clinker of parts by weight and 20 parts by weight stirs 3.3min, 0.18 parts by weight complex accelerator is added later, stirs 2.8min is mixed, the complex accelerator is anhydrous sodium sulphate and sodium chloride according to 1:1.08 ratio mixing;Above-mentioned cement is ordinary silicon Acid salt cement;Above-mentioned clinker is the clinker of loss on ignition 2.5%;Above-mentioned flyash is greater than three-level, the fine coal of loss on ignition 3.3% Ash;Above-mentioned aerated blocks particle is the particle of partial size 6.0mm;
B, mold is poured:In mould surface spraying release agent, the raw material mixed is poured into prefabricated board die, is started Vibration device vibrates 15s, is closed flat green body, covers cover board;
C, heating is stood:Start heating device, temperature is 35 DEG C, heating time 3.2h;
D, demoulding discharging:7.5h demoulding discharging after heating;
Above-mentioned release agent is prepared using following methods:
A, the used oil of 33 parts by weight is added in the water of 65.3 parts by weight, opens heating device, temperature is 90 DEG C;
B, the emulsifier of 0.62 parts by weight is added, and continues to stir 23min, the emulsifier is PO-10 and polyethylene acyl Amine;
C, the borax of 0.83 parts by weight, the sodium nitrite of 0.24 parts by weight and 1.24 parts by weight are added after being reduced to room temperature Triethanolamine;
D, it is 8.2 that stearic acid or sodium hydroxide adjusting pH value, which is added,;
E, after standing 4.5 days, the dish washing liquid solution of 11.2 parts by weight and the diesel oil of 3.3 parts by weight, the dish washing liquid is added Solution is dish washing liquid and water according to weight ratio 1:The mixed solution that 6.8 ratio is mixed with.
Above-mentioned used oil is that motor vehicle used discarded machine oil.
Above-mentioned dish washing liquid is common liq dish washing liquid.
Above-mentioned diesel oil is -35# diesel oil.
By test:2 hours demoulding strengths are increased to 2.68MPa from zero.Demoulding strength reaches after 12 hours 4.6MPa。
Embodiment 9:A kind of preparation method of concrete prefabricated board, it is characterised in that include the following steps:
A, raw material mixes:The cement of 31 parts by weight, the flyash of 3.3 parts by weight, 40.9 are added in the water of 23 parts by weight The aerated blocks particle of the clinker of parts by weight and 20.4 parts by weight stirs 3.1min, 0.16 parts by weight complex accelerator is added later, 2.2min is stirred, the complex accelerator is anhydrous sodium sulphate and sodium chloride according to 1:1.16 ratio mixing;Above-mentioned cement is common Portland cement;Above-mentioned clinker is the clinker of loss on ignition 3.0%;Above-mentioned flyash is greater than three-level, the fine coal of loss on ignition 4.0% Ash;Above-mentioned aerated blocks particle is the particle of partial size 7.5mm;
B, mold is poured:In mould surface spraying release agent, the raw material mixed is poured into prefabricated board die, is started Vibration device vibrates 20s, is closed flat green body, covers cover board;
C, heating is stood:Start heating device, temperature is 43 DEG C, heating time 3.5h;
D, demoulding discharging:7.4h demoulding discharging after heating;
Above-mentioned release agent is prepared using following methods:
A, the used oil of 31.8 parts by weight is added in the water of 65.6 parts by weight, opens heating device, temperature 90 ℃;
B, the emulsifier of 0.34 parts by weight is added, and continues to stir 27min, the emulsifier is Span -60;
C, the borax of 0.73 parts by weight, the sodium nitrite of 0.22 parts by weight and 1.09 parts by weight are added after being reduced to room temperature Triethanolamine;
D, it is 7.5 that stearic acid or sodium hydroxide adjusting pH value, which is added,;
E, after standing 6.5 days, the dish washing liquid solution of 15.6 parts by weight and the diesel oil of 6.0 parts by weight, the dish washing liquid is added Solution is dish washing liquid and water according to weight ratio 1:The mixed solution that 6 ratio is mixed with.
Above-mentioned used oil is that motor vehicle used discarded machine oil.
Above-mentioned dish washing liquid is common liq dish washing liquid.
Above-mentioned diesel oil is -35# diesel oil.
By test:2 hours demoulding strengths are increased to 2.63MPa from zero.Demoulding strength reaches after 12 hours 4.4MPa。
Embodiment 10:A kind of preparation method of concrete prefabricated board, it is characterised in that include the following steps:
A, raw material mixes:Be added in the water of 30 parts by weight the cement of 31.8 parts by weight, the flyash of 7.5 parts by weight, The aerated blocks particle of the clinker of 43.3 parts by weight and 20.5 parts by weight stirs 3.5min, 0.19 parts by weight compound morning is added later Strong agent, stirs 2.8min, and the complex accelerator is anhydrous sodium sulphate and sodium chloride according to 1:0.84 ratio mixing;Above-mentioned cement is Ordinary portland cement;Above-mentioned clinker is the clinker of loss on ignition 3.6%;Above-mentioned flyash be greater than three-level, loss on ignition 3.6% Flyash;Above-mentioned aerated blocks particle is the particle of partial size 4.0mm;
B, mold is poured:In mould surface spraying release agent, the raw material mixed is poured into prefabricated board die, is started Vibration device vibrates 12s, is closed flat green body, covers cover board;
C, heating is stood:Start heating device, temperature is 32 DEG C, heating time 4.7h;
D, demoulding discharging:7.8h demoulding discharging after heating;
Above-mentioned release agent is prepared using following methods:
A, the used oil of 30~35 parts by weight is added in the water of 65~70 parts by weight, opens heating device, temperature is 90℃;
B, the emulsifier of 0.26~0.64 parts by weight is added, and continues 20~35min of stirring, the emulsifier polyethylene acyl Amine;
C, be reduced to after room temperature be added the borax of 0.6~1.0 parts by weight, the sodium nitrite of 0.2~0.3 parts by weight and 1~ The triethanolamine of 1.5 parts by weight;
D, it is 7~9 that stearic acid or sodium hydroxide adjusting pH value, which is added,;
E, after standing 3~7 days, the dish washing liquid solution of 10~20 parts by weight and the diesel oil of 3~8 parts by weight is added, it is described to wash Clean essence solution is dish washing liquid and water according to weight ratio 1:The mixed solution that 3~7 ratio is mixed with;
Used oil is that motor vehicle used discarded machine oil;Dish washing liquid is common liq dish washing liquid;Above-mentioned diesel oil taste 0# bavin Oil.
By test:2 hours demoulding strengths are increased to 2.7MPa from zero.Demoulding strength reaches after 12 hours 4.7MPa。
Embodiment 11:A kind of preparation method of concrete prefabricated board, it is characterised in that include the following steps:
A, raw material mixes:Be added in the water of 24 parts by weight the cement of 32.3 parts by weight, the flyash of 4.8 parts by weight, The aerated blocks particle of the clinker of 41.5 parts by weight and 20.1 parts by weight stirs 4min, 0.14 parts by weight composite high-early strength is added later Agent, stirs 2.6min, and the complex accelerator is anhydrous sodium sulphate and sodium chloride according to 1:1.1 ratio mixing;Above-mentioned cement is general Logical portland cement;Above-mentioned clinker is the clinker of loss on ignition 3.3%;Above-mentioned flyash is greater than three-level, the powder of loss on ignition 3.2% Coal ash;Above-mentioned aerated blocks particle is the particle of partial size 2.0mm;
B, mold is poured:In mould surface spraying release agent, the raw material mixed is poured into prefabricated board die, is started Vibration device vibrates 11s, is closed flat green body, covers cover board;
C, heating is stood:Start heating device, temperature is 36 DEG C, heating time 4.3h;
D, demoulding discharging:6.3h demoulding discharging after heating;
Above-mentioned release agent is prepared using following methods:
A, the used oil of 33.6 parts by weight is added in the water of 68 parts by weight, opens heating device, temperature is 90 DEG C;
B, be added 0.32 parts by weight emulsifier, and continue stir 28min, the emulsifier be PO-10, Span -60 and Polyvinyl lactam;
C, the borax of 0.8 parts by weight, the sodium nitrite of 0.27 parts by weight and 1.36 parts by weight are added after being reduced to room temperature Triethanolamine;
D, it is 7.4 that stearic acid or sodium hydroxide adjusting pH value, which is added,;
E, after standing 3.8 days, the dish washing liquid solution of 17.5 parts by weight and the diesel oil of 7.8 parts by weight, the dish washing liquid is added Solution is dish washing liquid and water according to weight ratio 1:The mixed solution that 4.3 ratio is mixed with.
Above-mentioned used oil is that motor vehicle used discarded machine oil.
Above-mentioned dish washing liquid is common liq dish washing liquid.
Above-mentioned diesel oil is -10# diesel oil.
By test:2 hours demoulding strengths are increased to 2.62MPa from zero.Demoulding strength reaches after 12 hours 4.45MPa。
Embodiment 12:A kind of preparation method of concrete prefabricated board, it is characterised in that include the following steps:
A, raw material mixes:Be added in the water of 31 parts by weight the cement of 30.7 parts by weight, the flyash of 6.0 parts by weight, The aerated blocks particle of the clinker of 43.6 parts by weight and 21 parts by weight stirs 3.7min, 0.17 parts by weight composite high-early strength is added later Agent, stirs 2.3min, and the complex accelerator is anhydrous sodium sulphate and sodium chloride according to 1:1.18 ratio mixing;Above-mentioned cement is general Logical portland cement;Above-mentioned clinker is the clinker of loss on ignition 2.4%;Above-mentioned flyash is greater than three-level, the powder of loss on ignition 2.7% Coal ash;Above-mentioned aerated blocks particle is the particle of partial size 6.5mm;
B, mold is poured:In mould surface spraying release agent, the raw material mixed is poured into prefabricated board die, is started Vibration device vibrates 26s, is closed flat green body, covers cover board;
C, heating is stood:Start heating device, temperature is 47 DEG C, heating time 4.5h;
D, demoulding discharging:6.8h demoulding discharging after heating;
Above-mentioned release agent is prepared using following methods:
A, the used oil of 32.1 parts by weight is added in the water of 66.8 parts by weight, opens heating device, temperature 90 ℃;
B, the emulsifier of 0.60 parts by weight is added, and continues to stir 30.5min, the emulsifier is Span -60;
C, the borax of 0.98 parts by weight, the sodium nitrite of 0.21 parts by weight and 1.27 parts by weight are added after being reduced to room temperature Triethanolamine;
D, it is 8.5 that stearic acid or sodium hydroxide adjusting pH value, which is added,;
E, after standing 6.8 days, the dish washing liquid solution of 19 parts by weight and the diesel oil of 6.9 parts by weight is added, the dish washing liquid is molten Liquid is dish washing liquid and water according to weight ratio 1:The mixed solution that 5.8 ratio is mixed with.
Above-mentioned used oil is that motor vehicle used discarded machine oil.
Above-mentioned dish washing liquid is common liq dish washing liquid.
Above-mentioned diesel oil is 0# diesel oil.
By test:2 hours demoulding strengths are increased to 2.65MPa from zero.Demoulding strength reaches after 12 hours 4.55MPa。
Embodiment 13:A kind of preparation method of concrete prefabricated board, it is characterised in that include the following steps:
A, raw material mixes:Be added in the water of 24.5 parts by weight the cement of 31.4 parts by weight, the flyash of 7.8 parts by weight, The aerated blocks particle of the clinker of 44.5 parts by weight and 21.5 parts by weight stirs 4.6min, 0.15 parts by weight compound morning is added later Strong agent, stirs 2.3min, and the complex accelerator is anhydrous sodium sulphate and sodium chloride according to 1:0.84 ratio mixing;Above-mentioned cement is Ordinary portland cement;Above-mentioned clinker is the clinker of loss on ignition 4.0%;Above-mentioned flyash be greater than three-level, loss on ignition 4.3% Flyash;Above-mentioned aerated blocks particle is the particle of partial size 8.5mm;
B, mold is poured:In mould surface spraying release agent, the raw material mixed is poured into prefabricated board die, is started Vibration device vibrates 25s, is closed flat green body, covers cover board;
C, heating is stood:Start heating device, temperature is 34 DEG C, heating time 4.5h;
D, demoulding discharging:7h demoulding discharging after heating;
Above-mentioned release agent is prepared using following methods:
A, the used oil of 34.8 parts by weight is added in the water of 68.3 parts by weight, opens heating device, temperature 90 ℃;
B, the emulsifier of 0.48 parts by weight is added, and continues to stir 25min, the emulsifier is polyvinyl lactam;
C, the borax of 0.68 parts by weight, the sodium nitrite of 0.23 parts by weight and 1.15 parts by weight are added after being reduced to room temperature Triethanolamine;
D, it is 8.3 that stearic acid or sodium hydroxide adjusting pH value, which is added,;
E, after standing 5.7 days, the dish washing liquid solution of 15 parts by weight and the diesel oil of 5.7 parts by weight is added, the dish washing liquid is molten Liquid is dish washing liquid and water according to weight ratio 1:The mixed solution that 6.3 ratio is mixed with.
Above-mentioned used oil is that motor vehicle used discarded machine oil.
Above-mentioned dish washing liquid is common liq dish washing liquid.
Above-mentioned diesel oil is -35# diesel oil.
By test:2 hours demoulding strengths are increased to 2.76MPa from zero.Demoulding strength reaches after 12 hours 4.8MPa。
Embodiment 14:A kind of preparation method of concrete prefabricated board, it is characterised in that include the following steps:
A, raw material mixes:Be added in the water of 32 parts by weight the cement of 32.6 parts by weight, the flyash of 3.6 parts by weight, The aerated blocks particle of the clinker of 40.3 parts by weight and 21.2 parts by weight stirs 4.1min, 0.12 parts by weight compound morning is added later Strong agent, stirs 2.9min, and the complex accelerator is anhydrous sodium sulphate and sodium chloride according to 1:0.94 ratio mixing;Above-mentioned cement is Ordinary portland cement;Above-mentioned clinker is the clinker of loss on ignition 4.2%;Above-mentioned flyash be greater than three-level, loss on ignition 4.5% Flyash;Above-mentioned aerated blocks particle is the particle of partial size 3.0mm;
B, mold is poured:In mould surface spraying release agent, the raw material mixed is poured into prefabricated board die, is started Vibration device vibrates 18s, is closed flat green body, covers cover board;
C, heating is stood:Start heating device, temperature is 44 DEG C, heating time 4.2h;
D, demoulding discharging:7.2h demoulding discharging after heating;
Above-mentioned release agent is prepared using following methods:
A, the used oil of 33.3 parts by weight is added in the water of 65.9 parts by weight, opens heating device, temperature 90 ℃;
B, the emulsifier of 0.54 parts by weight is added, and continues to stir 32min, the emulsifier is PO-10 and Span -60;
C, the borax of 0.9 parts by weight, the sodium nitrite of 0.29 parts by weight and 1.18 parts by weight are added after being reduced to room temperature Triethanolamine;
D, it is 8.6 that stearic acid or sodium hydroxide adjusting pH value, which is added,;
E, after standing 6 days, the dish washing liquid solution of 17 parts by weight and the diesel oil of 7.5 parts by weight, the dish washing liquid solution is added It is dish washing liquid and water according to weight ratio 1:The mixed solution that 4 ratio is mixed with.
Above-mentioned used oil is that motor vehicle used discarded machine oil.
Above-mentioned dish washing liquid is common liq dish washing liquid.
Above-mentioned diesel oil is 0# diesel oil.
By test:2 hours demoulding strengths are increased to 2.72MPa from zero.Demoulding strength reaches after 12 hours 4.9MPa。
Embodiment 15:A kind of preparation method of concrete prefabricated board, it is characterised in that include the following steps:
A, raw material mixes:The cement of 32 parts by weight, the flyash of 6.9 parts by weight, 42.1 are added in the water of 25 parts by weight The aerated blocks particle of the clinker of parts by weight and 2.09 parts by weight stirs 4.5min, 0.16 parts by weight complex accelerator is added later, 2.7min is stirred, the complex accelerator is anhydrous sodium sulphate and sodium chloride according to 1:0.98 ratio mixing;Above-mentioned cement is common Portland cement;Above-mentioned clinker is the clinker of loss on ignition 4.5%;Above-mentioned flyash is greater than three-level, the fine coal of loss on ignition 3.9% Ash;Above-mentioned aerated blocks particle is the particle of partial size 7.0mm;
B, mold is poured:In mould surface spraying release agent, the raw material mixed is poured into prefabricated board die, is started Vibration device vibrates 24s, is closed flat green body, covers cover board;
C, heating is stood:Start heating device, temperature is 40 DEG C, heating time 3.8h;
D, demoulding discharging:6.5h demoulding discharging after heating;
Above-mentioned release agent is prepared using following methods:
A, the used oil of 34.8 parts by weight is added in the water of 68.3 parts by weight, opens heating device, temperature 90 ℃;
B, the emulsifier of 0.48 parts by weight is added, and continues to stir 25min, the emulsifier is polyvinyl lactam;
C, the borax of 0.68 parts by weight, the sodium nitrite of 0.23 parts by weight and 1.15 parts by weight are added after being reduced to room temperature Triethanolamine;
D, it is 8.3 that stearic acid or sodium hydroxide adjusting pH value, which is added,;
E, after standing 5.7 days, the dish washing liquid solution of 15 parts by weight and the diesel oil of 5.7 parts by weight is added, the dish washing liquid is molten Liquid is dish washing liquid and water according to weight ratio 1:The mixed solution that 6.3 ratio is mixed with.
Above-mentioned used oil is that motor vehicle used discarded machine oil.
Above-mentioned dish washing liquid is common liq dish washing liquid.
Above-mentioned diesel oil is -35# diesel oil.
By test:2 hours demoulding strengths are increased to 2.74MPa from zero.Demoulding strength reaches after 12 hours 4.75MPa。
Embodiment 16:A kind of preparation method of concrete prefabricated board, it is characterised in that include the following steps:
A, raw material mixes:Be added in the water of 32.5 parts by weight the cement of 29.5 parts by weight, the flyash of 5.7 parts by weight, The aerated blocks particle of the clinker of 44.8 parts by weight and 19.4 parts by weight stirs 4.3min, 0.13 parts by weight compound morning is added later Strong agent, stirs 2.4min, and the complex accelerator is anhydrous sodium sulphate and sodium chloride according to 1:1.14 ratio mixing;Above-mentioned cement is Ordinary portland cement;Above-mentioned clinker is the clinker of loss on ignition 4.2%;Above-mentioned flyash be greater than three-level, loss on ignition 4.6% Flyash;Above-mentioned aerated blocks particle is the particle of partial size 8.0mm;
B, mold is poured:In mould surface spraying release agent, the raw material mixed is poured into prefabricated board die, is started Vibration device vibrates 16s, is closed flat green body, covers cover board;
C, heating is stood:Start heating device, temperature is 46 DEG C, heating time 4.6h;
D, demoulding discharging:7.3h demoulding discharging after heating;
Above-mentioned release agent is prepared using following methods:
A, the used oil of 32.7 parts by weight is added in the water of 66.2 parts by weight, opens heating device, temperature 90 ℃;
B, the emulsifier of 0.52 parts by weight is added, and continues to stir 30min, the emulsifier is Span -60;
C, the borax of 0.95 parts by weight, the sodium nitrite of 0.27 parts by weight and 1.12 parts by weight are added after being reduced to room temperature Triethanolamine;
D, it is 8.0 that stearic acid or sodium hydroxide adjusting pH value, which is added,;
E, after standing 3.3 days, the dish washing liquid solution of 16.4 parts by weight and the diesel oil of 6.3 parts by weight, the dish washing liquid is added Solution is dish washing liquid and water according to weight ratio 1:The mixed solution that 4.8 ratio is mixed with.
Above-mentioned used oil is that motor vehicle used discarded machine oil.
Above-mentioned dish washing liquid is common liq dish washing liquid.
Above-mentioned diesel oil is -10# diesel oil.
By test:2 hours demoulding strengths are increased to 2.69MPa from zero.Demoulding strength reaches after 12 hours 4.65MPa。
Embodiment 17:A kind of preparation method of concrete prefabricated board, it is characterised in that include the following steps:
A, raw material mixes:Be added in the water of 26 parts by weight the cement of 28.8 parts by weight, the flyash of 7.2 parts by weight, The aerated blocks particle of the clinker of 42.7 parts by weight and 2.18 parts by weight stirs 2.5min, 0.12 parts by weight compound morning is added later Strong agent, stirs 4.8min, and the complex accelerator is anhydrous sodium sulphate and sodium chloride according to 1:1.12 ratio mixing;Above-mentioned cement is Ordinary portland cement;Above-mentioned clinker is the clinker of loss on ignition 4.8%;Above-mentioned flyash be greater than three-level, loss on ignition 4.4% Flyash;Above-mentioned aerated blocks particle is the particle of partial size 9.0mm;
B, mold is poured:In mould surface spraying release agent, the raw material mixed is poured into prefabricated board die, is started Vibration device vibrates 22s, is closed flat green body, covers cover board;
C, heating is stood:Start heating device, temperature is 45 DEG C, heating time 3.7h;
D, demoulding discharging:6.6h demoulding discharging after heating;
Above-mentioned release agent is prepared using following methods:
A, the used oil of 31.2 parts by weight is added in the water of 68.6 parts by weight, opens heating device, temperature 90 ℃;
B, the emulsifier of 0.40 parts by weight is added, and continues to stir 21min, the emulsifier is polyvinyl lactam;
C, the borax of 0.63 parts by weight, the sodium nitrite of 0.25 parts by weight and 1.45 parts by weight are added after being reduced to room temperature Triethanolamine;
D, it is 7.2 that stearic acid or sodium hydroxide adjusting pH value, which is added,;
E, after standing 4.8 days, the dish washing liquid solution of 10.5 parts by weight and the diesel oil of 3.9 parts by weight, the dish washing liquid is added Solution is dish washing liquid and water according to weight ratio 1:The mixed solution that 5.3 ratio is mixed with.
Above-mentioned used oil is that motor vehicle used discarded machine oil.
Above-mentioned dish washing liquid is common liq dish washing liquid.
Above-mentioned diesel oil is -10# diesel oil.
By test:2 hours demoulding strengths are increased to 2.78MPa from zero.Demoulding strength reaches after 12 hours 4.85MPa。
Embodiment 18:A kind of preparation method of concrete prefabricated board, it is characterised in that include the following steps:
A, raw material mixes:The cement of 33 parts by weight, the flyash of 8 parts by weight, 45 weight are added in the water of 35 parts by weight The clinker of part and the aerated blocks particle of 22 parts by weight, stir 5min, and 0.2 parts by weight complex accelerator is added later, stir 3min, The complex accelerator is anhydrous sodium sulphate and sodium chloride according to 1:1.2 ratio mixing;Above-mentioned cement is ordinary portland cement;On State the clinker that clinker is loss on ignition 5%;Above-mentioned flyash is greater than three-level, the flyash of loss on ignition 5%;Above-mentioned aerated blocks particle For the particle of partial size 10mm;
B, mold is poured:In mould surface spraying release agent, the raw material mixed is poured into prefabricated board die, is started Vibration device vibrates 30s, is closed flat green body, covers cover board;
C, heating is stood:Start heating device, temperature is 48 DEG C, heating time 5h;
D, demoulding discharging:8h demoulding discharging after heating;
Above-mentioned release agent is prepared using following methods:
A, the used oil of 35 parts by weight is added in the water of 70 parts by weight, opens heating device, temperature is 90 DEG C;
B, the emulsifier of 0.64 parts by weight is added, and continues to stir 35min, the emulsifier is PO-10 and Span -60;
C, the three of the borax of 1.0 parts by weight, the sodium nitrite of 0.3 parts by weight and 1.5 parts by weight are added after being reduced to room temperature Ethanol amine;
D, it is 9 that stearic acid or sodium hydroxide adjusting pH value, which is added,;
E, after standing 7 days, the dish washing liquid solution of 20 parts by weight and the diesel oil of 8 parts by weight is added, the dish washing liquid solution is Dish washing liquid and water are according to weight ratio 1:The mixed solution that 7 ratio is mixed with.
Above-mentioned used oil is that motor vehicle used discarded machine oil.
Above-mentioned dish washing liquid is common liq dish washing liquid.
Above-mentioned diesel oil is -10# diesel oil.
By test:2 hours demoulding strengths are increased to 2.8MPa from zero.Demoulding strength reaches after 12 hours 5.0MPa。

Claims (8)

1. a kind of preparation method of concrete prefabricated board, it is characterised in that include the following steps:
A, raw material mixes:Be added in the water of 20~35 parts by weight the cement of 27~33 parts by weight, 3~8 parts by weight flyash, The aerated blocks particle of the clinker of 40~45 parts by weight and 18~22 parts by weight stirs 2~5min, and 0.1~0.2 weight is added later Part complex accelerator, stirs 2~3min, and the complex accelerator is anhydrous sodium sulphate and sodium chloride according to 1:0.8~1.2 ratio is mixed It closes;
B, mold is poured:In mould surface spraying release agent, the raw material that a step mixes later is poured into mold, starting vibration Dynamic device, vibrates 10~30s, is closed flat green body, covers cover board;
C, heating is stood:Start heating device, temperature is 30~48 DEG C, 3~5h of heating time;
D, demoulding discharging:6~8h demoulding discharging after heating;
Above-mentioned release agent is prepared using following methods:
A, the used oil of 30~35 parts by weight is added in the water of 65~70 parts by weight, opens heating device, temperature is 90 DEG C;
B, the emulsifier of 0.26~0.64 parts by weight is added, and continues 20~35min of stirring, the emulsifier is PO-10, takes charge of Class at least one of -60 or polyvinyl lactam;
C, the borax of 0.6~1.0 parts by weight, the sodium nitrite and 1~1.5 weight of 0.2~0.3 parts by weight is added after being reduced to room temperature Measure the triethanolamine of part;
D, it is 7~9 that stearic acid or sodium hydroxide adjusting pH value, which is added,;
E, after standing 3~7 days, the dish washing liquid solution of 10~20 parts by weight and the diesel oil of 3~8 parts by weight, the dish washing liquid is added Solution is dish washing liquid and water according to weight ratio 1:The mixed solution that 3~7 ratio is mixed with.
2. the preparation method of concrete prefabricated board as described in claim 1, it is characterised in that:Cement is normal silicate water Mud.
3. the preparation method of concrete prefabricated board as described in claim 1, it is characterised in that:Clinker is loss on ignition≤5% Clinker.
4. the preparation method of concrete prefabricated board as described in claim 1, it is characterised in that:Flyash is to burn greater than three-level The flyash of vector≤5%.
5. the preparation method of concrete prefabricated board as described in claim 1, it is characterised in that:Aerated blocks particle is partial size The particle of 0.5mm~10mm.
6. the preparation method of concrete prefabricated board as described in claim 1, it is characterised in that:Used oil is that motor vehicle used Discarded machine oil.
7. the preparation method of concrete prefabricated board as described in claim 1, it is characterised in that:Dish washing liquid is washed clean for common liq Essence.
8. the preparation method of concrete prefabricated board as described in claim 1, it is characterised in that:Diesel oil is 0# diesel oil, -10# bavin Oil either one of -35# diesel oil.
CN201611022746.8A 2016-11-17 2016-11-17 A kind of preparation method of concrete prefabricated board Active CN106630822B (en)

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