CN106626651A - Production process for laminating and coating adhesive film - Google Patents

Production process for laminating and coating adhesive film Download PDF

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Publication number
CN106626651A
CN106626651A CN201611085061.8A CN201611085061A CN106626651A CN 106626651 A CN106626651 A CN 106626651A CN 201611085061 A CN201611085061 A CN 201611085061A CN 106626651 A CN106626651 A CN 106626651A
Authority
CN
China
Prior art keywords
eva
emaa
10min
laminating
adhesive film
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Pending
Application number
CN201611085061.8A
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Chinese (zh)
Inventor
崔九峰
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
TIANJIN SUNRAY PLASTIC PRODUCT CO Ltd
Original Assignee
TIANJIN SUNRAY PLASTIC PRODUCT CO Ltd
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by TIANJIN SUNRAY PLASTIC PRODUCT CO Ltd filed Critical TIANJIN SUNRAY PLASTIC PRODUCT CO Ltd
Priority to CN201611085061.8A priority Critical patent/CN106626651A/en
Publication of CN106626651A publication Critical patent/CN106626651A/en
Pending legal-status Critical Current

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Classifications

    • BPERFORMING OPERATIONS; TRANSPORTING
    • B32LAYERED PRODUCTS
    • B32BLAYERED PRODUCTS, i.e. PRODUCTS BUILT-UP OF STRATA OF FLAT OR NON-FLAT, e.g. CELLULAR OR HONEYCOMB, FORM
    • B32B27/00Layered products comprising a layer of synthetic resin
    • B32B27/06Layered products comprising a layer of synthetic resin as the main or only constituent of a layer, which is next to another layer of the same or of a different material
    • B32B27/08Layered products comprising a layer of synthetic resin as the main or only constituent of a layer, which is next to another layer of the same or of a different material of synthetic resin
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B32LAYERED PRODUCTS
    • B32BLAYERED PRODUCTS, i.e. PRODUCTS BUILT-UP OF STRATA OF FLAT OR NON-FLAT, e.g. CELLULAR OR HONEYCOMB, FORM
    • B32B27/00Layered products comprising a layer of synthetic resin
    • B32B27/30Layered products comprising a layer of synthetic resin comprising vinyl (co)polymers; comprising acrylic (co)polymers
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B32LAYERED PRODUCTS
    • B32BLAYERED PRODUCTS, i.e. PRODUCTS BUILT-UP OF STRATA OF FLAT OR NON-FLAT, e.g. CELLULAR OR HONEYCOMB, FORM
    • B32B27/00Layered products comprising a layer of synthetic resin
    • B32B27/30Layered products comprising a layer of synthetic resin comprising vinyl (co)polymers; comprising acrylic (co)polymers
    • B32B27/306Layered products comprising a layer of synthetic resin comprising vinyl (co)polymers; comprising acrylic (co)polymers comprising vinyl acetate or vinyl alcohol (co)polymers

Abstract

The invention relates to a production process for a laminating and coating adhesive film. The production process comprises the following steps: firstly, preparing master match; adopting EMAA (Ethylene Methacrylic Acid) of which a melt index at the temperature of 190DEG C is 0.5 to 5g/10min as a master batch base material, adopting polymeric paraffin as a dispersing agent, and extruding by adopting a twin-screw extruder; secondly, uniformly mixing EVA (Ethylene-Vinyl Acetate) resin with a coupling agent, wherein a melt index of the EVA resin at the temperature of 190DEG C is 5 to 15g/10min; thirdly, generating the laminating and coating adhesive film by adopting a three-layer co-extrusion casting film forming technique, wherein two sides of the laminating and coating adhesive film are EMAA resin, the middle of the laminating and coating adhesive film is the EVA resin, the extrusion temperature of an EMAA screw is 90 to 130DEG C, and the extrusion temperature of an EVA screw is controlled at 60 to 90DEG C; fourthly, carrying out embossing forming; controlling the water temperature of a rubber roller of embossing forming equipment to be 8 to 12DEG C, wherein the rubber roller is made of an integrated silica gel material, the hardness is controlled at 60 to 80A, the grained roughness of the rubber roller is 14 to 18 meshes, the water temperature of a steel roller is controlled at 40 to 50DEG C, and the depth of patterns is 0.06 to 0.15mm.

Description

A kind of lamination Tu applies the production technology of bonding film
Technical field
The present invention relates to a kind of lamination Tu applies the production technology of bonding film.
Background technology
Automobile polishing disk, wool disk, sponge disc was originally all uncontrollable with hot melt adhesive water bonding nylon and wool.Existing layer Pressure Tu is applied typically with hot melt adhesive or glue, time-consuming during production, and function of glue coating is uncontrollable.Therefore, one kind is produced Can solve the problem that function of glue coating uneven, the bad control of personnel and cumbersome problem, control raw material mobility and into The uncontrollable scheme of film, replacement glue solution wool, the deposited bonding film of the lamination Tu of sponge and nylon bonded technology seem and particularly must Will.
The content of the invention
The present invention provides a kind of heat used in replacing lamination Tu to apply to solve technical problem present in known technology Melt the production technology of the deposited bonding film of the lamination Tu of glue or glue, solve the technical problem of wool, sponge and nylon bonded aspect, Lift adhesion efficiency, ensure the effect of bonding.
The present invention is adopted the technical scheme that to solve technical problem present in known technology:One kind lamination Tu applies viscous The production technology of rubber alloy piece is comprised the following steps, and the step of (1) prepares master batch, melt index exists when master batch base material adopts 190 DEG C The EMAA of 0.5g/10min-5g/10min, using macromolecule wax dispersant, double screw extruder extrusion are made;(2) by EVA resin The step of being well mixed with coupling agent, EVA resin at 190 DEG C melt index in 5-15g/10min;(3) using three-layer co-extruded The step of casting film-forming Process Production lamination Tu applies bonding film, both sides be EMAA resins, it is middle be EVA resin, EMAA screw rods Extrusion temperature is 90 DEG C -130 DEG C, and EVA Screw Extrusions temperature control is at 60 DEG C -90 DEG C;(4) the step of embossing shaping, embosses into At 8 DEG C -12 DEG C, rubber roll is integral type silica gel material for the rubber roll water temperature control of type equipment, and soft durometer is controlled in 60-80A, rubber roll sand Mesh rugosity is the mesh of 14 mesh -18;The control of steel rider water temperature at 40 DEG C -50 DEG C, pattern depth 0.06mm-0.15mm.
Advantages of the present invention and good effect are:The invention provides a kind of lamination Tu applies the production technology of bonding film, Bonding film is applied there is provided the lamination Tu of a kind of replacement hot melt adhesive or glue, wool, sponge and nylon bonded aspect is solved Technical problem, improves adhesion efficiency, ensure that the effect of bonding.
Preferably:Macromolecule wax described in step (1) be chosen for the one kind in Tissuemat E, EVA waxes, copolymerization ester type waxes or It is various.
Preferably:Coupling agent described in step (2) is chosen for aminopropyl trimethoxysilane, aminopropyltriethoxy dimethoxy Base silane, aminopropyl triethoxysilane, aminoethylaminopropyl trimethoxy silane, aminoethylaminopropyl triethoxysilane, Aminoethylaminopropyl methyl dimethoxysilane, vinyltrimethoxy silane, VTES, methacryl One or more in epoxide trimethoxy silane.
Specific embodiment
For the content of the invention, feature and effect of the present invention can be further appreciated that, following examples detailed description is hereby lifted as follows:
EMAA is ethene-unsaturated ester copolymer, is ethene-(methyl) zinc acrylate resin also known as sarin (SURLYN) resin Salt, sodium salt, lithium salts plasma key condensate, really a kind of modified poly ethylene.
Embodiment 1:
(1) the step of preparing master batch, melt index is adopted in the EMAA of 1.5g/10min when master batch base material adopts 190 DEG C Macromolecule wax makees dispersant, double screw extruder extrusion;
(2) the step of EVA resin and coupling agent being well mixed, EVA resin at 190 DEG C melt index in 6g/ 10min;
(3) using three-layer co-extruded casting film-forming Process Production lamination Tu apply bonding film the step of, both sides be EMAA resins, Centre is EVA resin, and EMAA Screw Extrusions temperature is 95 DEG C, and EVA Screw Extrusions temperature control is at 65 DEG C;
(4) the step of embossing shaping, embosses the rubber roll water temperature control of former at 9 DEG C, and rubber roll is integral type silica gel material Matter, in 65A, rubber roll Grains rugosity is 15 mesh for soft durometer control;The control of steel rider water temperature at 45 DEG C, pattern depth 0.09mm.
Wherein, the macromolecule wax described in step (1) is chosen for Tissuemat E;Coupling agent described in step (2) is chosen For aminoethylaminopropyl trimethoxy silane.
Embodiment 2:
(1) the step of preparing master batch, melt index is adopted in the EMAA of 3.5g/10min when master batch base material adopts 190 DEG C Macromolecule wax makees dispersant, double screw extruder extrusion;
(2) the step of EVA resin and coupling agent being well mixed, EVA resin at 190 DEG C melt index in 10g/ 10min;
(3) using three-layer co-extruded casting film-forming Process Production lamination Tu apply bonding film the step of, both sides be EMAA resins, Centre is EVA resin, and EMAA Screw Extrusions temperature is 100 DEG C, and EVA Screw Extrusions temperature control is at 75 DEG C;
(4) the step of embossing shaping, embosses the rubber roll water temperature control of former at 10 DEG C, and rubber roll is integral type silica gel material Matter, in 75A, rubber roll Grains rugosity is 16 mesh for soft durometer control;The control of steel rider water temperature at 48 DEG C, pattern depth 0.10mm.
Wherein, the macromolecule wax described in step (1) is chosen for Tissuemat E;Coupling agent described in step (2) is chosen For aminopropyl trimethoxysilane.
Embodiment 3:
(1) the step of preparing master batch, melt index is adopted in the EMAA of 4.5g/10min when master batch base material adopts 190 DEG C Macromolecule wax makees dispersant, double screw extruder extrusion;
(2) the step of EVA resin and coupling agent being well mixed, EVA resin at 190 DEG C melt index in 14g/ 10min;
(3) using three-layer co-extruded casting film-forming Process Production lamination Tu apply bonding film the step of, both sides be EMAA resins, Centre is EVA resin, and EMAA Screw Extrusions temperature is 120 DEG C, and EVA Screw Extrusions temperature control is at 90 DEG C;
(4) the step of embossing shaping, embosses the rubber roll water temperature control of former at 11 DEG C, and rubber roll is integral type silica gel material Matter, in 80A, rubber roll Grains rugosity is 17 mesh for soft durometer control;The control of steel rider water temperature at 50 DEG C, pattern depth 0.15mm.
Wherein, the macromolecule wax described in step (1) is chosen for EVA waxes;Coupling agent described in step (2) is chosen for second Thiazolinyl triethoxysilane.

Claims (3)

1. a kind of lamination Tu applies the production technology of bonding film, it is characterized in that:Comprise the following steps,
(1) the step of preparing master batch, master batch base material adopt 190 DEG C when melt index 0.5g/10min-5g/10min EMAA, Dispersant, double screw extruder extrusion are made using macromolecule wax;
(2) the step of EVA resin and coupling agent being well mixed, EVA resin at 190 DEG C melt index in 5-15g/10min;
(3) the step of applying bonding film using three-layer co-extruded casting film-forming Process Production lamination Tu, both sides are EMAA resins, centre For EVA resin, EMAA Screw Extrusions temperature is 90 DEG C -130 DEG C, and EVA Screw Extrusions temperature control is at 60 DEG C -90 DEG C;
(4) the step of embossing shaping, embosses the rubber roll water temperature control of former at 8 DEG C -12 DEG C, and rubber roll is integral type silica gel material Matter, in 60-80A, rubber roll Grains rugosity is the mesh of 14 mesh -18 for soft durometer control;The control of steel rider water temperature at 40 DEG C -50 DEG C, decorative pattern depth Degree 0.06mm-0.15mm.
2. lamination Tu as claimed in claim 1 applies the production technology of bonding film, it is characterised in that:Described in step (1) Macromolecule wax is chosen for one or more in Tissuemat E, EVA waxes, copolymerization ester type waxes.
3. lamination Tu as claimed in claim 1 applies the production technology of bonding film, it is characterised in that:It is characterized in that:Step (2) coupling agent described in is chosen for aminopropyl trimethoxysilane, aminopropyltriethoxy dimethoxysilane, the ethoxy of aminopropyl three Base silane, aminoethylaminopropyl trimethoxy silane, aminoethylaminopropyl triethoxysilane, aminoethylaminopropyl methyl dimethoxy In TMOS, vinyltrimethoxy silane, VTES, methacryloxy trimethoxy silane One or more.
CN201611085061.8A 2016-12-01 2016-12-01 Production process for laminating and coating adhesive film Pending CN106626651A (en)

Priority Applications (1)

Application Number Priority Date Filing Date Title
CN201611085061.8A CN106626651A (en) 2016-12-01 2016-12-01 Production process for laminating and coating adhesive film

Applications Claiming Priority (1)

Application Number Priority Date Filing Date Title
CN201611085061.8A CN106626651A (en) 2016-12-01 2016-12-01 Production process for laminating and coating adhesive film

Publications (1)

Publication Number Publication Date
CN106626651A true CN106626651A (en) 2017-05-10

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Cited By (8)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN107400467A (en) * 2017-09-20 2017-11-28 天津三瑞塑胶制品有限公司 A kind of production technology of EVA bathrooms safety door special adhesive
CN107400468A (en) * 2017-09-20 2017-11-28 天津三瑞塑胶制品有限公司 A kind of production technology of EVA self-adhesions protection film
CN107400466A (en) * 2017-09-20 2017-11-28 天津三瑞塑胶制品有限公司 A kind of production technology of ultralow medium-temperature reinforced description film
CN107522935A (en) * 2017-09-20 2017-12-29 天津三瑞塑胶制品有限公司 A kind of production technology of EVA ultraviolet isolatings film
CN107573865A (en) * 2017-09-20 2018-01-12 天津三瑞塑胶制品有限公司 A kind of anti-production technology for pounding film of EVA cross-linking types
CN107602997A (en) * 2017-09-20 2018-01-19 天津三瑞塑胶制品有限公司 A kind of production technology of EVA colored solars film
CN109796911A (en) * 2019-02-22 2019-05-24 天津三瑞塑胶制品有限公司 A kind of production technology of shower house professional film
CN109852292A (en) * 2019-02-02 2019-06-07 天津三瑞塑胶制品有限公司 A kind of production technology of glass plank road special adhesive

Citations (2)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
JP2002067156A (en) * 2000-08-30 2002-03-05 C I Kasei Co Ltd Resin tube for steel pipe lining, its manufacturing method, and lining steel pipe
CN103205212A (en) * 2013-04-27 2013-07-17 汕头市安德利环保科技有限公司 EVA (Ethylene vinyl-acetate) film and manufacturing method thereof

Patent Citations (2)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
JP2002067156A (en) * 2000-08-30 2002-03-05 C I Kasei Co Ltd Resin tube for steel pipe lining, its manufacturing method, and lining steel pipe
CN103205212A (en) * 2013-04-27 2013-07-17 汕头市安德利环保科技有限公司 EVA (Ethylene vinyl-acetate) film and manufacturing method thereof

Cited By (8)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN107400467A (en) * 2017-09-20 2017-11-28 天津三瑞塑胶制品有限公司 A kind of production technology of EVA bathrooms safety door special adhesive
CN107400468A (en) * 2017-09-20 2017-11-28 天津三瑞塑胶制品有限公司 A kind of production technology of EVA self-adhesions protection film
CN107400466A (en) * 2017-09-20 2017-11-28 天津三瑞塑胶制品有限公司 A kind of production technology of ultralow medium-temperature reinforced description film
CN107522935A (en) * 2017-09-20 2017-12-29 天津三瑞塑胶制品有限公司 A kind of production technology of EVA ultraviolet isolatings film
CN107573865A (en) * 2017-09-20 2018-01-12 天津三瑞塑胶制品有限公司 A kind of anti-production technology for pounding film of EVA cross-linking types
CN107602997A (en) * 2017-09-20 2018-01-19 天津三瑞塑胶制品有限公司 A kind of production technology of EVA colored solars film
CN109852292A (en) * 2019-02-02 2019-06-07 天津三瑞塑胶制品有限公司 A kind of production technology of glass plank road special adhesive
CN109796911A (en) * 2019-02-22 2019-05-24 天津三瑞塑胶制品有限公司 A kind of production technology of shower house professional film

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Application publication date: 20170510

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