CN106622093B - Combined type baffling revolving bed mass transfer and consersion unit - Google Patents

Combined type baffling revolving bed mass transfer and consersion unit Download PDF

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Publication number
CN106622093B
CN106622093B CN201710012625.3A CN201710012625A CN106622093B CN 106622093 B CN106622093 B CN 106622093B CN 201710012625 A CN201710012625 A CN 201710012625A CN 106622093 B CN106622093 B CN 106622093B
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upper plate
liquid
baffle upper
gas
chin spoiler
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CN106622093A (en
Inventor
焦纬洲
刘有智
杨鹏飞
祁贵生
袁志国
张巧玲
栗秀萍
申红艳
高璟
罗莹
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North University of China
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North University of China
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    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J19/00—Chemical, physical or physico-chemical processes in general; Their relevant apparatus
    • B01J19/28—Moving reactors, e.g. rotary drums
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01D—SEPARATION
    • B01D53/00—Separation of gases or vapours; Recovering vapours of volatile solvents from gases; Chemical or biological purification of waste gases, e.g. engine exhaust gases, smoke, fumes, flue gases, aerosols
    • B01D53/14—Separation of gases or vapours; Recovering vapours of volatile solvents from gases; Chemical or biological purification of waste gases, e.g. engine exhaust gases, smoke, fumes, flue gases, aerosols by absorption
    • B01D53/1456—Removing acid components
    • B01D53/1468—Removing hydrogen sulfide
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01D—SEPARATION
    • B01D53/00—Separation of gases or vapours; Recovering vapours of volatile solvents from gases; Chemical or biological purification of waste gases, e.g. engine exhaust gases, smoke, fumes, flue gases, aerosols
    • B01D53/14—Separation of gases or vapours; Recovering vapours of volatile solvents from gases; Chemical or biological purification of waste gases, e.g. engine exhaust gases, smoke, fumes, flue gases, aerosols by absorption
    • B01D53/18—Absorbing units; Liquid distributors therefor
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01D—SEPARATION
    • B01D53/00—Separation of gases or vapours; Recovering vapours of volatile solvents from gases; Chemical or biological purification of waste gases, e.g. engine exhaust gases, smoke, fumes, flue gases, aerosols
    • B01D53/14—Separation of gases or vapours; Recovering vapours of volatile solvents from gases; Chemical or biological purification of waste gases, e.g. engine exhaust gases, smoke, fumes, flue gases, aerosols by absorption
    • B01D53/18—Absorbing units; Liquid distributors therefor
    • B01D53/185—Liquid distributors
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01D—SEPARATION
    • B01D53/00—Separation of gases or vapours; Recovering vapours of volatile solvents from gases; Chemical or biological purification of waste gases, e.g. engine exhaust gases, smoke, fumes, flue gases, aerosols
    • B01D53/34—Chemical or biological purification of waste gases
    • B01D53/46—Removing components of defined structure
    • B01D53/48—Sulfur compounds
    • B01D53/52—Hydrogen sulfide
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01D—SEPARATION
    • B01D53/00—Separation of gases or vapours; Recovering vapours of volatile solvents from gases; Chemical or biological purification of waste gases, e.g. engine exhaust gases, smoke, fumes, flue gases, aerosols
    • B01D53/34—Chemical or biological purification of waste gases
    • B01D53/74—General processes for purification of waste gases; Apparatus or devices specially adapted therefor
    • B01D53/77—Liquid phase processes
    • B01D53/78—Liquid phase processes with gas-liquid contact
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J10/00—Chemical processes in general for reacting liquid with gaseous media other than in the presence of solid particles, or apparatus specially adapted therefor
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J19/00—Chemical, physical or physico-chemical processes in general; Their relevant apparatus
    • B01J19/0053—Details of the reactor
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J19/00—Chemical, physical or physico-chemical processes in general; Their relevant apparatus
    • B01J19/32—Packing elements in the form of grids or built-up elements for forming a unit or module inside the apparatus for mass or heat transfer
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J4/00—Feed or outlet devices; Feed or outlet control devices
    • B01J4/001—Feed or outlet devices as such, e.g. feeding tubes
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J2204/00—Aspects relating to feed or outlet devices; Regulating devices for feed or outlet devices
    • B01J2204/002—Aspects relating to feed or outlet devices; Regulating devices for feed or outlet devices the feeding side being of particular interest
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J2219/00—Chemical, physical or physico-chemical processes in general; Their relevant apparatus
    • B01J2219/32—Details relating to packing elements in the form of grids or built-up elements for forming a unit of module inside the apparatus for mass or heat transfer
    • B01J2219/322—Basic shape of the elements
    • B01J2219/32203—Sheets
    • B01J2219/32213—Plurality of essentially parallel sheets
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J2219/00—Chemical, physical or physico-chemical processes in general; Their relevant apparatus
    • B01J2219/32—Details relating to packing elements in the form of grids or built-up elements for forming a unit of module inside the apparatus for mass or heat transfer
    • B01J2219/322—Basic shape of the elements
    • B01J2219/32203—Sheets
    • B01J2219/32224—Sheets characterised by the orientation of the sheet
    • B01J2219/32234—Inclined orientation
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J2219/00—Chemical, physical or physico-chemical processes in general; Their relevant apparatus
    • B01J2219/32—Details relating to packing elements in the form of grids or built-up elements for forming a unit of module inside the apparatus for mass or heat transfer
    • B01J2219/322—Basic shape of the elements
    • B01J2219/32203—Sheets
    • B01J2219/32248—Sheets comprising areas that are raised or sunken from the plane of the sheet
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J2219/00—Chemical, physical or physico-chemical processes in general; Their relevant apparatus
    • B01J2219/32—Details relating to packing elements in the form of grids or built-up elements for forming a unit of module inside the apparatus for mass or heat transfer
    • B01J2219/324—Composition or microstructure of the elements
    • B01J2219/32408—Metal
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J2219/00—Chemical, physical or physico-chemical processes in general; Their relevant apparatus
    • B01J2219/32—Details relating to packing elements in the form of grids or built-up elements for forming a unit of module inside the apparatus for mass or heat transfer
    • B01J2219/324—Composition or microstructure of the elements
    • B01J2219/32483—Plastics

Abstract

The present invention is specially a kind of combined type baffling revolving bed mass transfer and consersion unit, including quiet disk, liquid distribution trough, liquid inlet tube, gas outlet tube, baffle upper plate, chin spoiler, gas inlet tube, Moving plate, rotary shaft, liquid outlet tube and housing, quiet disk and Moving plate are placed in housing, quiet disk is equipped with the different concentric annular baffle upper plate of several diameters, evenly arranged circular aperture is provided on baffle upper plate, Moving plate is equipped with several round table-like chin spoilers with one heart, evenly arranged acanthopore is provided on chin spoiler, baffle upper plate and chin spoiler are staggered, quiet disk is fixedly linked with gas outlet tube, Moving plate is fixedly connected with rotary shaft, rotary shaft one end passes through housing and seals therewith.The present invention is made full use of in rotor radially and axial space, improves gas-liquid situation unevenly distributed, effectively extend gas-liquid contact time, by increasing to gas level of disruption, improve mass transferring in gas phase efficiency by changing the flow path of gas-liquid fluid.

Description

Combined type baffling revolving bed mass transfer and consersion unit
Technical field
The invention belongs to mass transfer, reaction technology field in super gravity field, specially a kind of combined type baffling revolving bed mass transfer With consersion unit.
Background technology
High-gravity technology is one of typical chemical process reinforcement technique, greatly enhance gas-liquid mass transfer, heat transfer with it is anti- Answer process.In high-gravity rotating bed, liquid is formed surface area greatly and constantly updated by high-speed rotating filler shearing-crushing Drop, brin and liquid film, contacted with the gas across filler, enhance the microcosmic mixing of gas-liquid, make mass tranfer coefficient improve 1~ 2 orders of magnitude have many advantages, such as that liquid flooding is high, residence time of material is short.It is high-gravity rotating bed to be applied to by development for many years Rectifying, prepares the processes such as nano material, dedusting at desulfurization, becomes one of the effective way of chemical process reinforcing.
It is high-gravity rotating bed it is small be one of its advantage, but the flow of gas-liquid is also limited in certain space, connect The tactile time is short, does not utilize mass transport process.During existing major part is high-gravity rotating bed, gas-liquid is unevenly distributed so that gas not with Liquid contact will overflow, and influence mass-transfer efficiency, be only capable of strengthening mass transfer in liquid phase process, and since gas is draged by filler friction The effect of power, as solid rotation in rotor, gas phase interface cannot quickly update, but also mass transferring in gas phase is less efficient.
Invention content
The present invention is unevenly distributed and for gas-liquid existing in existing design since gas is by filler frictional drag Effect gas phase interface cannot quickly be updated caused by mass-transfer efficiency low problem, provide a kind of combined type baffling Revolving bed mass transfer and consersion unit.
The present invention adopts the following technical scheme that realization：Combined type baffling revolving bed mass transfer and consersion unit, including quiet disk, Liquid distribution trough, liquid inlet tube, gas outlet tube, baffle upper plate, chin spoiler, gas inlet tube, Moving plate, rotary shaft, liquid Body outlet and housing, it is characterised in that：Quiet disk and Moving plate are placed in housing, and quiet disk is equipped with different concentric of several diameters Cyclic annular baffle upper plate, evenly arranged circular aperture is provided on baffle upper plate, and Moving plate is equipped with several round table-like lower water conservancy diversion with one heart Plate is provided with evenly arranged acanthopore on chin spoiler, and baffle upper plate and chin spoiler are staggered, and quiet disk is consolidated with gas outlet tube Fixed to be connected, Moving plate is fixedly connected with rotary shaft, and rotary shaft one end passes through housing and seals therewith, and acanthopore includes logical on chin spoiler Hole and through-hole top edge perpendicular to chin spoiler or relative to the acclivitous hangnail of chin spoiler.
The gas inlet tube and liquid outlet tube is set on housing, and liquid distribution trough is connected with liquid inlet tube, Liquid inlet tube is arranged in gas outlet tube.
The baffle upper plate material is stainless steel or polypropylene plastics, and chin spoiler material is stainless steel or polypropylene plastics Material.
The baffle upper plate is equally spaced, adjacent baffle upper plate spacing d1It is the 1/12~1/10 of Moving plate length D, on Deflector height d3For adjacent baffle upper plate spacing d12.4~3 times, baffle upper plate and Moving plate spacing d4For adjacent baffle upper plate Spacing d11/7~1/5.
The chin spoiler is equally spaced, and the angle theta between chin spoiler and Moving plate is 45o~75o, chin spoiler Top and baffle upper plate top spacing d2For adjacent baffle upper plate spacing d11/8~1/6.
Circular aperture aperture is 1~2mm on the baffle upper plate, and pitch of holes is 1.5~2.5mm.
The acanthopore is rectangular evenly distributed on chin spoiler, and through-hole aperture is 1~2mm, pitch of holes for 1.5~ 2.5mm。
The liquid distribution trough is cylindrical shape, and surrounding is disposed with 6 groups of circle pores from top to bottom, and every group includes 7 Pore, pore aperture are 0.4~0.5mm.
Compared with prior art, it is an advantage of the invention that：By changing the flow path of gas-liquid fluid, rotor is made full use of Interior radial direction and axial space improve gas-liquid situation unevenly distributed, effectively extend gas-liquid contact time；Meanwhile pass through increase To gas level of disruption, mass transferring in gas phase efficiency is improved.
It is specific as follows：
（1）Baffle upper plate and chin spoiler it is radially equidistant from be fixed on quiet disk and Moving plate, gas is radially by outer Inwardly successively alternately through baffle upper plate and chin spoiler, liquid then radially from inside to outside successively alternately through chin spoiler and Baffle upper plate.Liquid enters liquid distribution trough after the pore of 0.4mm sprays, and forms the larger spraying of specific surface area, effectively Ground increases gas-liquid interface area, enhances the gas-liquid mass transfer effect of equipment.
（2）After spray impingement to the chin spoiler with acanthopore, under the influence of centrifugal force, liquid is in acanthopore and deflector Upper to form thin liquid film rather than laminar flow is formed on deflector, partially liq impinges upon next baffle upper plate across acanthopore, greatly Part is flowed along chin spoiler, increases the gas liquid interfacial area on each chin spoiler；Meanwhile gas can be by acanthopore Liquid film is blown brokenly, draws thinner by liquid film, and there are angles, liquid between chin spoiler and Moving plate under the influence of centrifugal force, to pass through Acanthopore forms liquid film in the outside of chin spoiler, increases the surface utilisation of gas liquid interfacial area and deflector.
（4）In centrifugal field, gas is constantly sheared when by fluid channel between acanthopore and upper chin spoiler And dispersion, counter current contacting between the channel formed with liquid in deflector, occur strong mixing, the interaction between gas-liquid Enhancing, the enhancing of gas phase less turbulence, mass transferring in gas phase process are strengthened.
（5）Filling filler is not needed to, reduces the cost of manufacture of device, reduces operation energy consumption, and rotator inertia is shown It writes and reduces, operation stability is improved, can long-time continuous operation.
Description of the drawings
Fig. 1 is combined type baffling revolving bed structure diagram;
Fig. 2 is liquid distribution trough structure expanded view;
Fig. 3 positions baffle upper plate side view;
Fig. 4 is chin spoiler side view.
In figure：The quiet disks of 1-, 2- liquid distribution troughs, 3- liquid inlet tubes, 4- gas outlet tubes, 5- baffle upper plates are led under 6- Flowing plate, 7- gas inlet tubes, 8- Moving plates, 9- acanthopores, 10- rotary shafts, 11- liquid outlet tubes, 12- housings.
Specific embodiment
The specific embodiment of the present invention is most further illustrated with reference to attached drawing.
As shown in Figure 1, a kind of combined type baffling revolving bed mass transfer and consersion unit, including quiet disk 1, liquid distribution trough 2, liquid Body inlet tube 3, gas outlet tube 4, baffle upper plate 5, chin spoiler 6, gas inlet tube 7, Moving plate 8, rotary shaft 10, liquid outlet Pipe 11 and housing 12, it is characterised in that：Quiet disk 1 and Moving plate 8 are placed in housing, and quiet disk 1 is equipped with different same of several diameters Deflector 5 in the heart, Moving plate 8 are equipped with several concentric round platform chin spoilers 6, and baffle upper plate 5 and chin spoiler 6 are staggered, quiet Disk 1 is fixedly linked with gas outlet tube 4, and Moving plate 8 is fixedly connected with rotary shaft 10, and 10 one end of rotary shaft passes through housing 12 and therewith Sealing.Gas inlet tube 7 and liquid outlet tube 11 are provided on housing 12, liquid distribution trough 2 connects with liquid inlet tube 3, liquid Inlet tube 3 is arranged in gas outlet tube 4.Mass transfer, reaction detailed process are：Gas enters from gas feed 7, in rotor according to It is secondary by chin spoiler 6 and baffle upper plate 5, limited by water conservancy diversion board channel, in the multiple action of acanthopore 9 and upper chin spoiler Under, less turbulence greatly enhances；Liquid enter in liquid distribution trough 2 after after pore sprays, it is larger to form specific surface area Spraying 6 on spray impingement to chin spoiler, forms very thin liquid film, is flowed up along chin spoiler 6, by acanthopore and upper Fluid channel strikes with tiny drop is formed on foraminate baffle upper plate 5, under gravity between chin spoiler It drops on Moving plate 8, is then thrown on the chin spoiler 6 with acanthopore again and forms very thin liquid film, so go down repeatedly； Counter current contacting between the channel that gas and liquid are formed in deflector, occurs strong mixing, and the interaction between gas-liquid increases By force, gas phase less turbulence enhances, and mass transferring in gas phase process is strengthened.Finally, gas is flowed out from gas vent 4, and liquid is by liquid 11 outflow of outlet, completes mass transfer, reaction process.
As shown in Fig. 2, structure after the expansion of cylindrical shape liquid distribution trough 3, surrounding is asymmetric from top to bottom to be provided with pore, Pore aperture is 0.4~0.5mm, ensures that liquid is uniformly sprayed onto on chin spoiler 6.
As shown in figure 3, baffle upper plate 5 is mounted on quiet disk 1, circular aperture is provided on baffle upper plate 5.
As shown in figure 4, the angle theta between chin spoiler 6 and Moving plate 8 is 45o~75o, acanthopore 9 is provided on chin spoiler 6, Rolled over out on plate in a manner of roll off, acanthopore 9 include through-hole and through-hole top edge perpendicular to chin spoiler or relative to The acclivitous hangnail of chin spoiler, acanthopore 9 are rectangular evenly distributed on chin spoiler 6.
Embodiments of the present invention are described further with reference to specific embodiment.
Embodiment 1：Present device is applied to 2000mg/m3Hydrogen sulfide absorption process.Apparatus structure parameter in experiment For：θ=45o、d1=1/10D、d2=1/7d1、d3=3d1、d4=1/7d1, acanthopore aperture 1.5mm, acanthopore spacing 2mm, circular aperture hole Diameter 1mm, acanthopore spacing 2.5mm, liquid distribution trough pore aperture 0.45mm；Operating parameter is：Liquid-gas ratio is 10L/m3, revolving bed Under the conditions of rotating speed 1000r/min, soda content 12g/L, PDS content 15mg/L, 30 DEG C of temperature, the average removal efficiency of hydrogen sulfide is 96.4%。
Embodiment 2：Present device is applied to 2000mg/m3Hydrogen sulfide absorption process.Apparatus structure parameter in experiment For：θ=60o、d1=1/12D、d2=1/6d1、d3=2.4d1、d4=1/5d1, acanthopore aperture 1mm, acanthopore spacing 2.5mm, circular aperture Aperture 1.5mm, acanthopore spacing 2mm, liquid distribution trough pore aperture 0.4mm；Operating parameter is：Liquid-gas ratio is 10L/m3, rotation Under the conditions of bed rotating speed 1000r/min, soda content 12g/L, PDS content 15mg/L, 30 DEG C of temperature, the average removal efficiency of hydrogen sulfide It is 98.7%.
Embodiment 3：Present device is applied to 2000mg/m3Hydrogen sulfide absorption process.Apparatus structure parameter in experiment For：θ=75o、d1=1/11D、d2=1/8d1、d3=2.7d1、d4=1/6d1, acanthopore aperture 2mm, acanthopore spacing 1.5mm, circular aperture Aperture 2mm, acanthopore spacing 1.5mm, liquid distribution trough pore aperture 0.5mm；Operating parameter is：Liquid-gas ratio is 10L/m3, rotation Under the conditions of bed rotating speed 1000r/min, soda content 12g/L, PDS content 15mg/L, 30 DEG C of temperature, the average removal efficiency of hydrogen sulfide It is 95.3%.
Under same operation parameter, with document（Hydrogen sulfide [J] in gravity Method removing gas, chemical industry progress, 2008,27 （9）：1404-1407）Applied to 2000mg/m3The comparison of hydrogen sulfide absorption process see the table below.
Experiment Experiment 1 Experiment 2 Experiment 3 Document
Hydrogen sulfide is averaged removal efficiency 96.40% 98.70% 95.30% 92.40%

Claims (8)

1. a kind of combined type baffling revolving bed mass transfer and consersion unit, including quiet disk（1）, liquid distribution trough（2）, liquid inlet tube （3）, gas outlet tube（4）, baffle upper plate（5）, chin spoiler（6）, gas inlet tube（7）, Moving plate（8）, rotary shaft（10）, liquid Body outlet（11）And housing（12）, it is characterised in that：Quiet disk（1）And Moving plate（8）It is placed in housing, quiet disk（1）It is equipped with The different concentric annular baffle upper plate of several diameters（5）, baffle upper plate（5）On be provided with evenly arranged circular aperture, Moving plate（8） It is equipped with several round table-like chin spoilers with one heart（6）, chin spoiler（6）On be provided with evenly arranged acanthopore（9）, baffle upper plate （5）And chin spoiler（6）It is staggered, quiet disk（1）With gas outlet tube（4）It is fixedly linked, Moving plate（8）With rotary shaft（10）Gu Fixed connection, rotary shaft（10）One end passes through housing（12）And it seals therewith, acanthopore（9）Hanging down including through-hole and through-hole top edge Directly in chin spoiler（6）Or relative to chin spoiler（6）Acclivitous hangnail.
2. combined type baffling revolving bed mass transfer according to claim 1 and consersion unit, it is characterised in that：Gas inlet tube （7）And liquid outlet tube（11）It is set to housing（12）On, liquid distribution trough（2）With liquid inlet tube（3）It is connected, liquid-inlet Pipe（3）It is arranged on gas outlet tube（4）It is interior.
3. combined type baffling revolving bed mass transfer according to claim 1 or 2 and consersion unit, it is characterised in that：Described Baffle upper plate（5）Material be stainless steel or polypropylene plastics, chin spoiler（6）Material is stainless steel or polypropylene plastics.
4. combined type baffling revolving bed mass transfer according to claim 3 and consersion unit, it is characterised in that：Baffle upper plate （5）It is equally spaced, adjacent baffle upper plate（5）Spacing d1For Moving plate（8）The 1/12~1/10 of length D, baffle upper plate（5）Highly d3For adjacent baffle upper plate（5）Spacing d12.4~3 times, baffle upper plate（5）With Moving plate（8）Spacing d4For adjacent baffle upper plate （5）Spacing d11/7~1/5.
5. combined type baffling revolving bed mass transfer according to claim 4 and consersion unit, it is characterised in that：Chin spoiler （6）It is equally spaced, chin spoiler（6）With Moving plate（8）Between angle theta be 45o~75o, chin spoiler（6）Top is with above leading Flowing plate（5）Top spacing d2For adjacent baffle upper plate（5）Spacing d11/8~1/6.
6. combined type baffling revolving bed mass transfer according to claim 5 and consersion unit, it is characterised in that：Baffle upper plate （5）Upper circular aperture aperture is 1~2mm, and pitch of holes is 1.5~2.5mm.
7. combined type baffling revolving bed mass transfer according to claim 1 and consersion unit, it is characterised in that：Acanthopore（9） Rectangular evenly distributed on chin spoiler, through-hole aperture is 1~2mm, and pitch of holes is 1.5~2.5mm.
8. combined type baffling revolving bed mass transfer according to claim 1 or 2 and consersion unit, it is characterised in that：Liquid point Cloth device（3）For cylindrical shape, surrounding is disposed with 6 groups of circle pores from top to bottom, and every group includes 7 pores, and pore aperture is 0.4 ~0.5mm.
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CN112206698B (en) * 2020-09-01 2022-09-30 浙江工业大学 Baffling type super-gravity rotating bed with integrally rotating rotor
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CN114832419B (en) * 2022-03-17 2023-11-14 浙江工业大学 Concentric ring type super-gravity rotating bed and continuous rectifying system
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