CN106620795A - Nanoscale air purifying agent and preparation method thereof - Google Patents

Nanoscale air purifying agent and preparation method thereof Download PDF

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Publication number
CN106620795A
CN106620795A CN201611173403.1A CN201611173403A CN106620795A CN 106620795 A CN106620795 A CN 106620795A CN 201611173403 A CN201611173403 A CN 201611173403A CN 106620795 A CN106620795 A CN 106620795A
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CN
China
Prior art keywords
parts
nano
nanometer
titanium dioxide
air purifying
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CN201611173403.1A
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Chinese (zh)
Inventor
钟雄军
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Qinzhou Science And Technology Development Center
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Qinzhou Science And Technology Development Center
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Priority to CN201611173403.1A priority Critical patent/CN106620795A/en
Publication of CN106620795A publication Critical patent/CN106620795A/en
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    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61LMETHODS OR APPARATUS FOR STERILISING MATERIALS OR OBJECTS IN GENERAL; DISINFECTION, STERILISATION OR DEODORISATION OF AIR; CHEMICAL ASPECTS OF BANDAGES, DRESSINGS, ABSORBENT PADS OR SURGICAL ARTICLES; MATERIALS FOR BANDAGES, DRESSINGS, ABSORBENT PADS OR SURGICAL ARTICLES
    • A61L9/00Disinfection, sterilisation or deodorisation of air
    • A61L9/01Deodorant compositions
    • A61L9/014Deodorant compositions containing sorbent material, e.g. activated carbon
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61LMETHODS OR APPARATUS FOR STERILISING MATERIALS OR OBJECTS IN GENERAL; DISINFECTION, STERILISATION OR DEODORISATION OF AIR; CHEMICAL ASPECTS OF BANDAGES, DRESSINGS, ABSORBENT PADS OR SURGICAL ARTICLES; MATERIALS FOR BANDAGES, DRESSINGS, ABSORBENT PADS OR SURGICAL ARTICLES
    • A61L9/00Disinfection, sterilisation or deodorisation of air
    • A61L9/01Deodorant compositions
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01DSEPARATION
    • B01D53/00Separation of gases or vapours; Recovering vapours of volatile solvents from gases; Chemical or biological purification of waste gases, e.g. engine exhaust gases, smoke, fumes, flue gases, aerosols
    • B01D53/02Separation of gases or vapours; Recovering vapours of volatile solvents from gases; Chemical or biological purification of waste gases, e.g. engine exhaust gases, smoke, fumes, flue gases, aerosols by adsorption, e.g. preparative gas chromatography

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  • Health & Medical Sciences (AREA)
  • Chemical & Material Sciences (AREA)
  • Engineering & Computer Science (AREA)
  • Animal Behavior & Ethology (AREA)
  • General Health & Medical Sciences (AREA)
  • Public Health (AREA)
  • Veterinary Medicine (AREA)
  • Life Sciences & Earth Sciences (AREA)
  • Epidemiology (AREA)
  • Materials Engineering (AREA)
  • Analytical Chemistry (AREA)
  • General Chemical & Material Sciences (AREA)
  • Oil, Petroleum & Natural Gas (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • Catalysts (AREA)
  • Exhaust Gas Treatment By Means Of Catalyst (AREA)

Abstract

The invention discloses a nanoscale air purifying agent and a preparation method thereof. The contains the following components in parts by mass: 7-9 parts of nano-titanium dioxide, 2-4 parts of anatase type nano-titanium dioxide, 7-9 parts of hydrochloric acid, 4-6 parts of nano-silicon dioxide, 1-2 parts of a synergistic agent, 4-6 parts of nano-silver, 3-5 parts of nano-sulfur dioxide, 7-9 parts of benzene dichloride, 1-2 parts of an activating agent, 5-7 parts of activated carbon, 4-6 parts of modified zeolite and 40-50 parts of distilled water. The nanoscale air purifying agent is good in stability and high in adsorption rate, and the preparation method is simple; and by utilizing a combined formula of nano-titanium dioxide, nano-silicon dioxide and nano-sulfur dioxide, harmful gases in indoor air can be effectively removed, bacteria in air can be killed, the air can be purified, and the indoor air can be refreshed.

Description

A kind of nanometer air purifying agent and preparation method thereof
Technical field
The present invention relates to technical field of air purification, in particular to a kind of nanometer air purifying agent and its preparation side Method.
Background technology
At present, in house decoration, very Considering Environmental is fitted up.But environmental protection is fitted up and is not equal to and prevent completely nuisance The residual of matter, after house decoration, the deenergized period of toxic gas, the residence time was long typically all in 3-15 in finishing material, danger Evil property is very big.Pernicious gas in order to eliminate finishing, occur in that on the market it is many using spray, apply, cover, the method such as dilution Scavenger, eliminating smell agent etc., are mostly industrial chemicals, and using rear pernicious gas residual can not be eliminated, and can also produce secondary pollution. Ozonization, anion generator have suppression bacterial virus growth, remove peculiar smell, the effect of clean air, but are helpless to eliminate Original polluter in air.
The content of the invention
The invention provides a kind of nanometer air purifying agent and preparation method thereof, preparation method of the present invention is simple, stable Property it is good, adsorption rate is high;Using the combination formula of nano titanium oxide, nano silicon and nanometer titanium dioxide sulphur, Neng Gouyou Effect removes the pernicious gas in room air, and can kill the bacterium in air, purify air, keep the clear of room air Newly.
For achieving the above object, the present invention provides following technical scheme:
A kind of nanometer air purifying agent and preparation method thereof, is made up of following mass fraction formula components:Nano-silica Change titanium 7-9 parts, nanometer anatase titania 2-4 parts, hydrochloric acid 7-9 parts, nano silicon 4-6 parts, synergist 1-2 parts, receive Rice silver 4-6 parts, nanometer titanium dioxide sulphur 3-5 parts, dichlorobenzene 7-9 parts, activator 1-2 parts, activated carbon 5-7 parts, modified zeolite 4-6 Part, distilled water 40-50 parts.
Further:It is made up of following mass fraction formula components:7 parts of nano titanium oxide, nanometer anatase titania 2 Part, 7 parts of hydrochloric acid, 4 parts of nano silicon, 1 part of synergist, 4 parts of Nano Silver, 3 parts of nanometer titanium dioxide sulphur, 7 parts of dichlorobenzene, swash 1 part of agent living, 5 parts of activated carbon, 4 parts of modified zeolite, 40 parts of distilled water.
Further:It is made up of following mass fraction formula components:8 parts of nano titanium oxide, nanometer anatase titania 3 Part, 8 parts of hydrochloric acid, 5 parts of nano silicon, 1.5 parts of synergist, 5 parts of Nano Silver, 4 parts of nanometer titanium dioxide sulphur, 8 parts of dichlorobenzene, 1.5 parts of activator, 6 parts of activated carbon, 5 parts of modified zeolite, 45 parts of distilled water.
Further:It is made up of following mass fraction formula components:9 parts of nano titanium oxide, nanometer anatase titania 4 Part, 9 parts of hydrochloric acid, 6 parts of nano silicon, 2 parts of synergist, 6 parts of Nano Silver, 5 parts of nanometer titanium dioxide sulphur, 9 parts of dichlorobenzene, swash 2 parts of agent living, 7 parts of activated carbon, 6 parts of modified zeolite, 50 parts of distilled water.
Further:Preparation method comprises the steps:
Step one, it is pre-dissolved in kettle first and injects water, water reducer mother liquor, Portland cement are added while stirring, stirs Mix 30 minutes, be configured to the cellulose solution that mass percent is 3% standby;
Step 2, in the second reactor cellulose, Binder Materials, molasses are added to while stirring according to formula rate In excess water;
Step 3, surplus stock is added, formula rate is then pressed in the second reactor and adds step one, stirring 20min, then after stainless steel sieve impurity screening, that is, make.
The invention has the beneficial effects as follows:
1st, preparation method of the present invention is simple, good stability, and adsorption rate is high;
2nd, using the combination formula of nano titanium oxide, nano silicon and nanometer titanium dioxide sulphur, can effectively go Except the pernicious gas in room air, and the bacterium in air, purify air can be killed, the pure and fresh of room air is kept.
Specific embodiment
Below in conjunction with the embodiment of the present invention, the technical scheme in the embodiment of the present invention is clearly and completely described, Obviously, described embodiment is only a part of embodiment of the invention, rather than the embodiment of whole.Based in the present invention Embodiment, the every other embodiment that those of ordinary skill in the art are obtained under the premise of creative work is not made, all Belong to the scope of protection of the invention.
Embodiment one:
A kind of nanometer air purifying agent is made up of following mass fraction formula components:Nano titanium oxide 7-9 parts, sharp titanium Type nano titanium oxide 2-4 parts, hydrochloric acid 7-9 parts, nano silicon 4-6 parts, synergist 1-2 parts, Nano Silver 4-6 parts, nanometer Sulfur dioxide 3-5 parts, dichlorobenzene 7-9 parts, activator 1-2 parts, activated carbon 5-7 parts, modified zeolite 4-6 parts, distilled water 40-50 Part.
Embodiment two:
A kind of nanometer air purifying agent is made up of following mass fraction formula components:7 parts of nano titanium oxide, anatase titanium dioxide 2 parts of nano titanium oxide, 7 parts of hydrochloric acid, 4 parts of nano silicon, 1 part of synergist, 4 parts of Nano Silver, 3 parts of nanometer titanium dioxide sulphur, 7 parts of dichlorobenzene, 1 part of activator, 5 parts of activated carbon, 4 parts of modified zeolite, 40 parts of distilled water.
Embodiment three:
A kind of nanometer air purifying agent is made up of following mass fraction formula components:8 parts of nano titanium oxide, anatase titanium dioxide 3 parts of nano titanium oxide, 8 parts of hydrochloric acid, 5 parts of nano silicon, 1.5 parts of synergist, 5 parts of Nano Silver, nanometer titanium dioxide sulphur 4 Part, 8 parts of dichlorobenzene, 1.5 parts of activator, 6 parts of activated carbon, 5 parts of modified zeolite, 45 parts of distilled water.
Example IV:
A kind of nanometer air purifying agent is made up of following mass fraction formula components:9 parts of nano titanium oxide, anatase titanium dioxide 4 parts of nano titanium oxide, 9 parts of hydrochloric acid, 6 parts of nano silicon, 2 parts of synergist, 6 parts of Nano Silver, 5 parts of nanometer titanium dioxide sulphur, 9 parts of dichlorobenzene, 2 parts of activator, 7 parts of activated carbon, 6 parts of modified zeolite, 50 parts of distilled water.
Embodiment five:
A kind of preparation method of nanometer air purifying agent comprises the steps:
Step one, it is pre-dissolved in kettle first and injects water, water reducer mother liquor, Portland cement are added while stirring, stirs Mix 30 minutes, be configured to the cellulose solution that mass percent is 3% standby;
Step 2, in the second reactor cellulose, Binder Materials, molasses are added to while stirring according to formula rate In excess water;
Step 3, surplus stock is added, formula rate is then pressed in the second reactor and adds step one, stirring 20min, then after stainless steel sieve impurity screening, that is, make.
Moreover, it will be appreciated that although this specification is been described by according to embodiment, not each embodiment is only wrapped Containing an independent technical scheme, this narrating mode of specification is only that for clarity those skilled in the art should Using specification as an entirety, the technical scheme in each embodiment can also Jing it is appropriately combined, form those skilled in the art Understandable other embodiment.

Claims (5)

1. a kind of nanometer air purifying agent, it is characterised in that:It is made up of following mass fraction formula components:
Nano titanium oxide 7-9 parts, nanometer anatase titania 2-4 parts, hydrochloric acid 7-9 parts, nano silicon 4-6 parts, increasing Effect agent 1-2 parts, Nano Silver 4-6 parts, nanometer titanium dioxide sulphur 3-5 parts, dichlorobenzene 7-9 parts, activator 1-2 parts, activated carbon 5-7 Part, modified zeolite 4-6 parts, distilled water 40-50 parts.
2. a kind of nanometer air purifying agent according to claim 1, it is characterised in that:Filled a prescription into by following mass fraction It is grouped into:
7 parts of nano titanium oxide, 2 parts of nanometer anatase titania, 7 parts of hydrochloric acid, 4 parts of nano silicon, 1 part of synergist, 4 parts of Nano Silver, 3 parts of nanometer titanium dioxide sulphur, 7 parts of dichlorobenzene, 1 part of activator, 5 parts of activated carbon, 4 parts of modified zeolite, distilled water 40 parts.
3. a kind of nanometer air purifying agent according to claim 1, it is characterised in that:Filled a prescription into by following mass fraction It is grouped into:
8 parts of nano titanium oxide, 3 parts of nanometer anatase titania, 8 parts of hydrochloric acid, 5 parts of nano silicon, synergist 1.5 Part, 5 parts of Nano Silver, 4 parts of nanometer titanium dioxide sulphur, 8 parts of dichlorobenzene, 1.5 parts of activator, 6 parts of activated carbon, 5 parts of modified zeolite, steaming 45 parts of distilled water.
4. a kind of nanometer air purifying agent according to claim 1, it is characterised in that:Filled a prescription into by following mass fraction It is grouped into:
9 parts of nano titanium oxide, 4 parts of nanometer anatase titania, 9 parts of hydrochloric acid, 6 parts of nano silicon, 2 parts of synergist, 6 parts of Nano Silver, 5 parts of nanometer titanium dioxide sulphur, 9 parts of dichlorobenzene, 2 parts of activator, 7 parts of activated carbon, 6 parts of modified zeolite, distilled water 50 parts.
5. a kind of a kind of preparation method of nanometer air purifying agent according to claim 1, it is characterised in that:Including such as Lower step:
Step one, in parts by weight, weighs nano titanium oxide, nanometer anatase titania, hydrochloric acid, nanometer titanium dioxide Silicon, synergist, Nano Silver, are sequentially placed into ultrasonic wave mixer and are mixed, and obtain raw mixture;Wherein, mixing temperature For 40-60 degree, incorporation time is 0.5-1.5 hours;
Step 2, nanometer titanium dioxide sulphur, dichlorobenzene will be put into above-mentioned ultrasonic wave mixer successively, activator, activated carbon, changed Property zeolite, carry out hybrid reaction, reaction temperature is 40-60 degree, and the reaction time is 0.5-1.5 hours, is subsequently adding distilled water again Secondary to be mixed, last precipitate and separate goes out supernatant and obtains required air cleanser.
CN201611173403.1A 2016-12-19 2016-12-19 Nanoscale air purifying agent and preparation method thereof Pending CN106620795A (en)

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Cited By (2)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN108421405A (en) * 2018-01-31 2018-08-21 盱眙启睿矿业有限公司 A kind of indoor air purification agent and preparation method thereof containing recessed soil
CN108636354A (en) * 2018-06-04 2018-10-12 合肥奇呗数字科技有限公司 A kind of novel air cleanser and its preparation process

Citations (5)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN101044848A (en) * 2007-04-03 2007-10-03 山东农业大学 Nanometer silver antibiotic powder fixed by silk fibroin and preparation method thereof
CZ2006829A3 (en) * 2006-12-27 2008-07-30 CTC AP a. s. Mixed, powder TiOi2-based decontaminant
CN102989308A (en) * 2012-11-28 2013-03-27 欧阳杰 Multifunctional air cleaning agent
CN103120801A (en) * 2011-11-18 2013-05-29 大连得达科技发展有限公司 Nano photocatalyst fragrant air purification agent
CN105771886A (en) * 2015-12-16 2016-07-20 无锡吉进环保科技有限公司 Nanoscale air purifying preparation

Patent Citations (5)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CZ2006829A3 (en) * 2006-12-27 2008-07-30 CTC AP a. s. Mixed, powder TiOi2-based decontaminant
CN101044848A (en) * 2007-04-03 2007-10-03 山东农业大学 Nanometer silver antibiotic powder fixed by silk fibroin and preparation method thereof
CN103120801A (en) * 2011-11-18 2013-05-29 大连得达科技发展有限公司 Nano photocatalyst fragrant air purification agent
CN102989308A (en) * 2012-11-28 2013-03-27 欧阳杰 Multifunctional air cleaning agent
CN105771886A (en) * 2015-12-16 2016-07-20 无锡吉进环保科技有限公司 Nanoscale air purifying preparation

Cited By (2)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN108421405A (en) * 2018-01-31 2018-08-21 盱眙启睿矿业有限公司 A kind of indoor air purification agent and preparation method thereof containing recessed soil
CN108636354A (en) * 2018-06-04 2018-10-12 合肥奇呗数字科技有限公司 A kind of novel air cleanser and its preparation process

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Application publication date: 20170510