CN106591006A - Quick cleaning agent for eggs and preparation method thereof - Google Patents
Quick cleaning agent for eggs and preparation method thereof Download PDFInfo
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- CN106591006A CN106591006A CN201610901732.7A CN201610901732A CN106591006A CN 106591006 A CN106591006 A CN 106591006A CN 201610901732 A CN201610901732 A CN 201610901732A CN 106591006 A CN106591006 A CN 106591006A
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- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
- C11D1/00—Detergent compositions based essentially on surface-active compounds; Use of these compounds as a detergent
- C11D1/66—Non-ionic compounds
- C11D1/72—Ethers of polyoxyalkylene glycols
-
- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
- C11D3/00—Other compounding ingredients of detergent compositions covered in group C11D1/00
- C11D3/02—Inorganic compounds ; Elemental compounds
- C11D3/12—Water-insoluble compounds
-
- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
- C11D3/00—Other compounding ingredients of detergent compositions covered in group C11D1/00
- C11D3/02—Inorganic compounds ; Elemental compounds
- C11D3/12—Water-insoluble compounds
- C11D3/124—Silicon containing, e.g. silica, silex, quartz or glass beads
- C11D3/1246—Silicates, e.g. diatomaceous earth
- C11D3/1253—Layer silicates, e.g. talcum, kaolin, clay, bentonite, smectite, montmorillonite, hectorite or attapulgite
-
- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
- C11D3/00—Other compounding ingredients of detergent compositions covered in group C11D1/00
- C11D3/16—Organic compounds
- C11D3/20—Organic compounds containing oxygen
- C11D3/22—Carbohydrates or derivatives thereof
- C11D3/222—Natural or synthetic polysaccharides, e.g. cellulose, starch, gum, alginic acid or cyclodextrin
-
- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
- C11D3/00—Other compounding ingredients of detergent compositions covered in group C11D1/00
- C11D3/16—Organic compounds
- C11D3/37—Polymers
- C11D3/3746—Macromolecular compounds obtained by reactions only involving carbon-to-carbon unsaturated bonds
- C11D3/3753—Polyvinylalcohol; Ethers or esters thereof
-
- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
- C11D3/00—Other compounding ingredients of detergent compositions covered in group C11D1/00
- C11D3/16—Organic compounds
- C11D3/37—Polymers
- C11D3/3746—Macromolecular compounds obtained by reactions only involving carbon-to-carbon unsaturated bonds
- C11D3/3757—(Co)polymerised carboxylic acids, -anhydrides, -esters in solid and liquid compositions
- C11D3/3765—(Co)polymerised carboxylic acids, -anhydrides, -esters in solid and liquid compositions in liquid compositions
-
- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
- C11D3/00—Other compounding ingredients of detergent compositions covered in group C11D1/00
- C11D3/16—Organic compounds
- C11D3/38—Products with no well-defined composition, e.g. natural products
- C11D3/382—Vegetable products, e.g. soya meal, wood flour, sawdust
-
- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
- C11D3/00—Other compounding ingredients of detergent compositions covered in group C11D1/00
- C11D3/48—Medical, disinfecting agents, disinfecting, antibacterial, germicidal or antimicrobial compositions
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- Chemical & Material Sciences (AREA)
- Life Sciences & Earth Sciences (AREA)
- Wood Science & Technology (AREA)
- Engineering & Computer Science (AREA)
- Organic Chemistry (AREA)
- Oil, Petroleum & Natural Gas (AREA)
- Chemical Kinetics & Catalysis (AREA)
- Inorganic Chemistry (AREA)
- Health & Medical Sciences (AREA)
- Molecular Biology (AREA)
- Emergency Medicine (AREA)
- Medicines Containing Plant Substances (AREA)
- Meat, Egg Or Seafood Products (AREA)
Abstract
Relating to the technical field of livestock breeding industry, the invention discloses a quick cleaning agent for eggs and a preparation method thereof. The quick cleaning agent is prepared from the following raw materials by weight: 15-20 parts of dry wheat straw powder, 10-15 parts of bamboo powder, 8-12 parts of activated clay, 6-9 parts of polyvinyl alcohol resin, 4-8 parts of acrylic macroporous adsorption resin, 3-6 parts of polyethylene oxide, 3-6 parts of lotus leaf powder, 3-6 parts of pine needle meal, 2-4 parts of rice wine lees, 2-4 parts of sesbania gum, 2-4 parts of glutinous rice flour, 1-2 parts of hydrogenated palm oil, 1-2 parts of asbestos wool, 0.5-1 part of litsea cubeba oil, 0.5-1 part of citionella oil, 0.5-1 part of bone black, and 100-150 parts of water. The cleaning agent for eggs prepared by the method provided by the invention quickly cleans dirt attached to the egg surfaces by means of wetting, adsorption and flocculation, has high cleaning efficiency, consumes short time, and is conducive to reducing the amount of labor. At the same time, sterilization treatment is carried out on egg surfaces to prevent bacterial reproduction from affecting egg quality.
Description
Technical field：
The present invention relates to livestock culture industry technical field, and in particular to a kind of egg fast cleaning agent and preparation method thereof.
Background technology：
Egg is the byproduct that raiser produces while chicken class is cultivated, and is that raiser increases income.After picking up
Egg need the once purged sale that could case, being otherwise attached to the excrement of eggshell surface will affect egg quality.Tradition
Cleaning way is wiped using washing or rag, and washes water consumption greatly, and it is attached on eggshell to need high pressure washing effectively to remove
The dirt, has the shortcomings that waste water resource；Rag wiping there is cleaning speed slowly and rag needs fixed time cleaning, otherwise can
Dirt under wiping is sticked to again on other eggs.Further, since contain a large amount of bacteriums in excrement, only can not be thorough by washing
Bottom is removed, if the bacterium amount reproduction being attached on egg, it will cause egg necrosis, is received so as to reduce the economic of raiser
Enter and affect the normal of consumer to eat.
The content of the invention：
The technical problem to be solved is to provide that a kind of cleaning efficiency is high, bactericidal effect is good and safety in utilization
High egg fast cleaning agent and preparation method thereof.
The technical problem to be solved is realized using following technical scheme：
A kind of egg fast cleaning agent, is made up of the raw material of following parts by weight：
Wheat Straw dry powder 15-20 parts, bamboo powder 10-15 part, atlapulgite 8-12 parts, polyvinyl alcohol resin 6-9 parts, acrylic acid
Macroporous absorbent resin 4-8 parts, polyethylene glycol oxide 3-6 parts, lotus leaf powder 3-6 parts, pine needle meal 3-6 parts, rice wine grain 2-4 part, sesbania gum
2-4 parts, glutinous rice flour 2-4 parts, HPO 1-2 parts, asbestos wool 1-2 parts, litsea citrate oil 0.5-1 parts, citronella oil 0.5-1 parts,
Bone black 0.5-1 parts, water 100-150 parts.
Using front through modification, its processing method is the acroleic acid macroporous adsorption resin：By 12-15 part acrylic acid
Macroporous absorbent resin is added in 30-40 part hexamethylenes, and 15-30min is stood after being uniformly dispersed, and adds 2-3 part pregelatinized starch
With 0.5-1 part N hydroxymethyl acrylamides, microwave treatment 3- under microwave frequency 2450MHz, power 700W is sufficiently mixed
5min, microwave is immediately placed in -5-0 DEG C of environment after terminating and cools down 2-3h, is then heated to reflux state insulation mixing 5-
10min, and 1-2 parts bipentaerythrite and 2-3 part 10wt% saleratus solutions are added, continue to be incubated backflow mixing 10-15min,
Subsequently cooled with the speed of 10-15 DEG C/min under ice-water bath, add 3-5 part 5wt% dilute after temperature is down to 30-35 DEG C
Hydrochloric acid solution, the insulation mixing 15-30min at 30-35 DEG C, gained mixture is sent in vacuum drier, Jing after being fully dried
Washing 2-3 time, is most dried 8-12h at 75-80 DEG C, obtains final product modified acroleic acid macroporous adsorption resin particle.
Acroleic acid macroporous adsorption resin not only strengthens its adsorption capacity by above-mentioned modification so as to effectively adsorb attached
The dirt on egg, so as to accelerate cleaning speed；And can improve its hydrophobicity so as to adsorb and rely on after dirt gravity
Sedimentation, so as to be beneficial to wastewater treatment.
A kind of preparation method of egg fast cleaning agent, comprises the steps：
(1) polyvinyl alcohol resin and polyethylene glycol oxide are added in water, and is heated to reflux state insulation mixing 15-
30min, adds sesbania gum, glutinous rice flour and HPO, continues the insulation mixing 10-15min that flows back, and obtains final product material I；
(2) asbestos wool and bone black are added in atlapulgite, 80-85 DEG C is first heated to, mixing 10-15min is follow-up for insulation
Continuous heating, insulation mixing 5-10min, then naturally cools to room temperature after temperature reaches 110-115 DEG C, adds litsea citrate oil
And citronella oil, it is sufficiently mixed and 3-5h is stood in 0-5 DEG C of environment, obtain final product material II；
(3) Wheat Straw dry powder, bamboo powder, pine needle meal and rice wine grain, gained mixture is added to proceed to ball mill in material I
In, fineness is milled to less than 0.1mm, acroleic acid macroporous adsorption resin and lotus leaf powder are eventually adding, it is sufficiently mixed uniform.
The invention has the beneficial effects as follows：The made egg cleaning agent of the present invention is by wetting, absorption and flocculation mode come quick
The dirt of cleaning egg surface attachment, cleaning efficiency is high, and the used time is short, is conducive to the amount of lightening one's labor；Egg surface is carried out simultaneously
Sterilization processing, prevents bacterial reproduction and affects egg quality；And the cleaning agent will not produce any adverse effect, Jing to eggshell
Egg after the cleaning agent cleaning is only rinsed after once being dried with water and cased, and suitable for duck's egg, goose egg or other birds
The Rapid Cleaning of egg.
Specific embodiment：
In order that technological means, creation characteristic, reached purpose and effect that the present invention is realized are easy to understand, tie below
Specific embodiment is closed, the present invention is expanded on further.
Embodiment 1
(1) 6 parts of polyvinyl alcohol resins and 3 parts of polyethylene glycol oxides are added in 150 parts of water, and is heated to reflux state insulation
Mixing 20min, adds 2 parts of sesbania gums, 2 parts of glutinous rice flours and 1 part of HPO, continues the insulation mixing 10min that flows back, and obtains final product
Material I；
(2) 1 part of asbestos wool and 0.5 part of bone black are added in 10 parts of atlapulgites, 80-85 DEG C is first heated to, insulation mixing
Continue to heat after 10min, insulation mixing 10min, then naturally cools to room temperature after temperature reaches 110-115 DEG C, adds
0.5 portion of litsea citrate oil and 0.5 part of citronella oil, are sufficiently mixed and 5h are stood in 0-5 DEG C of environment, obtain final product material II；
(3) 15 parts of Wheat Straw dry powder, 10 parts of bamboo powders, 3 parts of pine needle meals and 2 parts of rice wine grains, gained mixing are added in material I
Thing is proceeded in ball mill, is milled to fineness less than 0.1mm, is eventually adding 4 parts of acroleic acid macroporous adsorption resins and 3 parts of lotus leaf powders,
It is sufficiently mixed uniform.
The modification of acroleic acid macroporous adsorption resin：15 parts of acroleic acid macroporous adsorption resins are added into 40 parts of hexamethylenes
In, 30min is stood after being uniformly dispersed, 2 parts of pregelatinized starch and 0.5 part of N hydroxymethyl acrylamide are added, after being sufficiently mixed
Microwave treatment 5min under microwave frequency 2450MHz, power 700W, microwave is immediately placed in -5-0 DEG C of environment after terminating and cools down
3h, is then heated to reflux state insulation mixing 10min, and adds 2 parts of bipentaerythrites and 3 parts of 10wt% saleratus solutions,
Continue to be incubated backflow mixing 15min, subsequently cooled with the speed of 10-15 DEG C/min under ice-water bath, treat that temperature is down to 30-
5 parts of 5wt% dilute hydrochloric acid solutions are added after 35 DEG C, the insulation mixing 30min at 30-35 DEG C, gained mixture sends into vacuum drying
In machine, wash 2 times Jing after being fully dried, be most dried 12h at 75-80 DEG C, obtain final product modified acroleic acid macroporous absorption tree
Fat particle.
Embodiment 2
(1) 8 parts of polyvinyl alcohol resins and 5 parts of polyethylene glycol oxides are added in 150 parts of water, and is heated to reflux state insulation
Mixing 20min, adds 2 parts of sesbania gums, 2 parts of glutinous rice flours and 1 part of HPO, continues the insulation mixing 10min that flows back, and obtains final product
Material I；
(2) 1 part of asbestos wool and 0.5 part of bone black are added in 10 parts of atlapulgites, 80-85 DEG C is first heated to, insulation mixing
Continue to heat after 10min, insulation mixing 10min, then naturally cools to room temperature after temperature reaches 110-115 DEG C, adds 1
Part litsea citrate oil and 0.5 part of citronella oil, are sufficiently mixed and 5h are stood in 0-5 DEG C of environment, obtain final product material II；
(3) 20 parts of Wheat Straw dry powder, 10 parts of bamboo powders, 3 parts of pine needle meals and 2 parts of rice wine grains, gained mixing are added in material I
Thing is proceeded in ball mill, is milled to fineness less than 0.1mm, is eventually adding 6 parts of acroleic acid macroporous adsorption resins and 3 parts of lotus leaf powders,
It is sufficiently mixed uniform.
The modification of acroleic acid macroporous adsorption resin：15 parts of acroleic acid macroporous adsorption resins are added into 40 parts of hexamethylenes
In, 30min is stood after being uniformly dispersed, 3 parts of pregelatinized starch and 0.5 part of N hydroxymethyl acrylamide are added, after being sufficiently mixed
Microwave treatment 5min under microwave frequency 2450MHz, power 700W, microwave is immediately placed in -5-0 DEG C of environment after terminating and cools down
3h, is then heated to reflux state insulation mixing 10min, and adds 1 part of bipentaerythrite and 3 parts of 10wt% saleratus solutions,
Continue to be incubated backflow mixing 15min, subsequently cooled with the speed of 10-15 DEG C/min under ice-water bath, treat that temperature is down to 30-
3 parts of 5wt% dilute hydrochloric acid solutions are added after 35 DEG C, the insulation mixing 30min at 30-35 DEG C, gained mixture sends into vacuum drying
In machine, wash 2 times Jing after being fully dried, be most dried 12h at 75-80 DEG C, obtain final product modified acroleic acid macroporous absorption tree
Fat particle.
The general principle and principal character and advantages of the present invention of the present invention has been shown and described above.The technology of the industry
Personnel it should be appreciated that the present invention is not restricted to the described embodiments, the simply explanation described in above-described embodiment and specification this
The principle of invention, without departing from the spirit and scope of the present invention, the present invention also has various changes and modifications, these changes
Change and improvement is both fallen within scope of the claimed invention.The claimed scope of the invention by appending claims and its
Equivalent thereof.
Claims (3)
1. a kind of egg fast cleaning agent, it is characterised in that be made up of the raw material of following parts by weight：Wheat Straw dry powder 15-20
Part, bamboo powder 10-15 part, atlapulgite 8-12 parts, polyvinyl alcohol resin 6-9 parts, acroleic acid macroporous adsorption resin 4-8 parts, polyoxy
Change ethene 3-6 parts, lotus leaf powder 3-6 parts, pine needle meal 3-6 parts, rice wine grain 2-4 part, sesbania gum 2-4 parts, glutinous rice flour 2-4 parts, hydrogenation
Palm oil 1-2 parts, asbestos wool 1-2 parts, litsea citrate oil 0.5-1 parts, citronella oil 0.5-1 parts, bone black 0.5-1 parts, water 100-150
Part.
2. egg fast cleaning agent according to claim 1, it is characterised in that：The acroleic acid macroporous adsorption resin is used
It is front through modification, its processing method is：12-15 parts acroleic acid macroporous adsorption resin is added in 30-40 part hexamethylenes, point
Uniform rear standing 15-30min is dissipated, 2-3 parts pregelatinized starch and 0.5-1 part N hydroxymethyl acrylamides is added, is sufficiently mixed
Microwave treatment 3-5min under microwave frequency 2450MHz, power 700W, microwave is immediately placed in cold in -5-0 DEG C of environment after terminating
But 2-3h, is then heated to reflux state insulation mixing 5-10min, and adds 1-2 parts bipentaerythrite and 2-3 part 10wt% little
Soda solution, continues to be incubated backflow mixing 10-15min, is subsequently cooled with the speed of 10-15 DEG C/min under ice-water bath,
3-5 part 5wt% dilute hydrochloric acid solutions are added after temperature is down to 30-35 DEG C, insulation mixing 15-30min, gained at 30-35 DEG C
Mixture is sent in vacuum drier, is washed 2-3 time Jing after being fully dried, and is most dried 8-12h at 75-80 DEG C, obtains final product and changes
Acroleic acid macroporous adsorption resin particle after property.
3. a kind of preparation method of egg fast cleaning agent, it is characterised in that comprise the steps：
(1) polyvinyl alcohol resin and polyethylene glycol oxide are added in water, and is heated to reflux state insulation mixing 15-30min, then
Sesbania gum, glutinous rice flour and HPO are added, continues the insulation mixing 10-15min that flows back, obtain final product material I；
(2) asbestos wool and bone black are added in atlapulgite, 80-85 DEG C is first heated to, continues to add after insulation mixing 10-15min
Heat, insulation mixing 5-10min, then naturally cools to room temperature after temperature reaches 110-115 DEG C, adds litsea citrate oil and perfume (or spice)
Thatch oil, is sufficiently mixed and 3-5h is stood in 0-5 DEG C of environment, obtains final product material II；
(3) Wheat Straw dry powder, bamboo powder, pine needle meal and rice wine grain, gained mixture is added to proceed in ball mill in material I, ball
Fineness is milled to less than 0.1mm, acroleic acid macroporous adsorption resin and lotus leaf powder is eventually adding, is sufficiently mixed uniform.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201610901732.7A CN106591006A (en) | 2016-10-18 | 2016-10-18 | Quick cleaning agent for eggs and preparation method thereof |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201610901732.7A CN106591006A (en) | 2016-10-18 | 2016-10-18 | Quick cleaning agent for eggs and preparation method thereof |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| CN106591006A true CN106591006A (en) | 2017-04-26 |
Family
ID=58555887
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN201610901732.7A Pending CN106591006A (en) | 2016-10-18 | 2016-10-18 | Quick cleaning agent for eggs and preparation method thereof |
Country Status (1)
| Country | Link |
|---|---|
| CN (1) | CN106591006A (en) |
Cited By (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN109055034A (en) * | 2018-08-08 | 2018-12-21 | 廖家平 | Liquid detergent |
| CN112266833A (en) * | 2020-10-23 | 2021-01-26 | 郭亮 | Pine leaf environment-friendly enzyme and preparation method thereof |
-
2016
- 2016-10-18 CN CN201610901732.7A patent/CN106591006A/en active Pending
Cited By (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN109055034A (en) * | 2018-08-08 | 2018-12-21 | 廖家平 | Liquid detergent |
| CN112266833A (en) * | 2020-10-23 | 2021-01-26 | 郭亮 | Pine leaf environment-friendly enzyme and preparation method thereof |
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Application publication date: 20170426 |
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