CN106590843A - Precision stainless steel band cold-rolling rolling oil - Google Patents
Precision stainless steel band cold-rolling rolling oil Download PDFInfo
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- CN106590843A CN106590843A CN201611081123.8A CN201611081123A CN106590843A CN 106590843 A CN106590843 A CN 106590843A CN 201611081123 A CN201611081123 A CN 201611081123A CN 106590843 A CN106590843 A CN 106590843A
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- stainless steel
- rolling
- rolling oil
- steel band
- cold rolling
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- C—CHEMISTRY; METALLURGY
- C10—PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
- C10M—LUBRICATING COMPOSITIONS; USE OF CHEMICAL SUBSTANCES EITHER ALONE OR AS LUBRICATING INGREDIENTS IN A LUBRICATING COMPOSITION
- C10M167/00—Lubricating compositions characterised by the additive being a mixture of a macromolecular compound, a non-macromolecular compound and a compound of unknown or incompletely defined constitution, each of these compounds being essential
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- C10M—LUBRICATING COMPOSITIONS; USE OF CHEMICAL SUBSTANCES EITHER ALONE OR AS LUBRICATING INGREDIENTS IN A LUBRICATING COMPOSITION
- C10M2205/00—Organic macromolecular hydrocarbon compounds or fractions, whether or not modified by oxidation as ingredients in lubricant compositions
- C10M2205/02—Organic macromolecular hydrocarbon compounds or fractions, whether or not modified by oxidation as ingredients in lubricant compositions containing acyclic monomers
- C10M2205/026—Butene
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- C10M2205/00—Organic macromolecular hydrocarbon compounds or fractions, whether or not modified by oxidation as ingredients in lubricant compositions
- C10M2205/16—Paraffin waxes; Petrolatum, e.g. slack wax
- C10M2205/163—Paraffin waxes; Petrolatum, e.g. slack wax used as base material
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- C10M2207/00—Organic non-macromolecular hydrocarbon compounds containing hydrogen, carbon and oxygen as ingredients in lubricant compositions
- C10M2207/02—Hydroxy compounds
- C10M2207/021—Hydroxy compounds having hydroxy groups bound to acyclic or cycloaliphatic carbon atoms
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- C10M2207/00—Organic non-macromolecular hydrocarbon compounds containing hydrogen, carbon and oxygen as ingredients in lubricant compositions
- C10M2207/10—Carboxylix acids; Neutral salts thereof
- C10M2207/12—Carboxylix acids; Neutral salts thereof having carboxyl groups bound to acyclic or cycloaliphatic carbon atoms
- C10M2207/125—Carboxylix acids; Neutral salts thereof having carboxyl groups bound to acyclic or cycloaliphatic carbon atoms having hydrocarbon chains of eight up to twenty-nine carbon atoms, i.e. fatty acids
- C10M2207/126—Carboxylix acids; Neutral salts thereof having carboxyl groups bound to acyclic or cycloaliphatic carbon atoms having hydrocarbon chains of eight up to twenty-nine carbon atoms, i.e. fatty acids monocarboxylic
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- C10M2207/00—Organic non-macromolecular hydrocarbon compounds containing hydrogen, carbon and oxygen as ingredients in lubricant compositions
- C10M2207/28—Esters
- C10M2207/281—Esters of (cyclo)aliphatic monocarboxylic acids
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- C10M2207/00—Organic non-macromolecular hydrocarbon compounds containing hydrogen, carbon and oxygen as ingredients in lubricant compositions
- C10M2207/28—Esters
- C10M2207/283—Esters of polyhydroxy compounds
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- C10M2207/00—Organic non-macromolecular hydrocarbon compounds containing hydrogen, carbon and oxygen as ingredients in lubricant compositions
- C10M2207/28—Esters
- C10M2207/285—Esters of aromatic polycarboxylic acids
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- C10M2209/00—Organic macromolecular compounds containing oxygen as ingredients in lubricant compositions
- C10M2209/02—Macromolecular compounds obtained by reactions only involving carbon-to-carbon unsaturated bonds
- C10M2209/08—Macromolecular compounds obtained by reactions only involving carbon-to-carbon unsaturated bonds containing monomers having an unsaturated radical bound to a carboxyl radical, e.g. acrylate type
- C10M2209/084—Acrylate; Methacrylate
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- C10M2215/00—Organic non-macromolecular compounds containing nitrogen as ingredients in lubricant compositions
- C10M2215/22—Heterocyclic nitrogen compounds
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- C10M2217/00—Organic macromolecular compounds containing nitrogen as ingredients in lubricant compositions
- C10M2217/06—Macromolecular compounds obtained by functionalisation op polymers with a nitrogen containing compound
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- C10M2219/00—Organic non-macromolecular compounds containing sulfur, selenium or tellurium as ingredients in lubricant compositions
- C10M2219/02—Sulfur-containing compounds obtained by sulfurisation with sulfur or sulfur-containing compounds
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- C10M2219/00—Organic non-macromolecular compounds containing sulfur, selenium or tellurium as ingredients in lubricant compositions
- C10M2219/04—Organic non-macromolecular compounds containing sulfur, selenium or tellurium as ingredients in lubricant compositions containing sulfur-to-oxygen bonds, i.e. sulfones, sulfoxides
- C10M2219/044—Sulfonic acids, Derivatives thereof, e.g. neutral salts
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- C10M2219/00—Organic non-macromolecular compounds containing sulfur, selenium or tellurium as ingredients in lubricant compositions
- C10M2219/06—Thio-acids; Thiocyanates; Derivatives thereof
- C10M2219/062—Thio-acids; Thiocyanates; Derivatives thereof having carbon-to-sulfur double bonds
- C10M2219/066—Thiocarbamic type compounds
- C10M2219/068—Thiocarbamate metal salts
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- C10M2223/00—Organic non-macromolecular compounds containing phosphorus as ingredients in lubricant compositions
- C10M2223/02—Organic non-macromolecular compounds containing phosphorus as ingredients in lubricant compositions having no phosphorus-to-carbon bonds
- C10M2223/04—Phosphate esters
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- C10M2227/00—Organic non-macromolecular compounds containing atoms of elements not provided for in groups C10M2203/00, C10M2207/00, C10M2211/00, C10M2215/00, C10M2219/00 or C10M2223/00 as ingredients in lubricant compositions
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- C10N—INDEXING SCHEME ASSOCIATED WITH SUBCLASS C10M RELATING TO LUBRICATING COMPOSITIONS
- C10N2030/00—Specified physical or chemical properties which is improved by the additive characterising the lubricating composition, e.g. multifunctional additives
- C10N2030/04—Detergent property or dispersant property
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- C10N2030/00—Specified physical or chemical properties which is improved by the additive characterising the lubricating composition, e.g. multifunctional additives
- C10N2030/06—Oiliness; Film-strength; Anti-wear; Resistance to extreme pressure
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- C10N2030/00—Specified physical or chemical properties which is improved by the additive characterising the lubricating composition, e.g. multifunctional additives
- C10N2030/10—Inhibition of oxidation, e.g. anti-oxidants
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- C10N2030/00—Specified physical or chemical properties which is improved by the additive characterising the lubricating composition, e.g. multifunctional additives
- C10N2030/50—Emission or smoke controlling properties
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- C10N2040/00—Specified use or application for which the lubricating composition is intended
- C10N2040/20—Metal working
- C10N2040/24—Metal working without essential removal of material, e.g. forming, gorging, drawing, pressing, stamping, rolling or extruding; Punching metal
Abstract
The invention relates to the field of environmental protection, in particular to precision stainless steel band cold-rolling rolling oil. The precision stainless steel band cold-rolling rolling oil is prepared from, by mass, 0.5-2% of cooling agent, 0.5-3% of anti-wear reagent at extreme pressure, 5-10% of lubricant, 0.2-1% of purification dispersant, 1-3% of penetrant, 0.2-1% of smoke resisting agent, 0.1-0.5% of antioxidant and the balance basic oil. The lubricating material is especially suitable for a 1,450mm offset eight-roller or multi-roller reversible stainless steel calendering unit with the strict requirement for lubricating performance, a special extreme pressure lubricating system is established and combined with the cooling control technology, the smoke control technology and the service life control technology, it is achieved that the rolling oil can be recycled for a long time, no waste liquid is generated basically, the production environment in a workshop is remarkably improved, the service life of rollers is prolonged, and rolling pressing force is reduced. The comprehensive board surface quality of finished products can be greatly improved through excellent extreme pressure lubricating performance and annealing detergence, and the requirements of stainless steel sheet surfaces with the 2B and BA high-precision grades or above can be met.
Description
Technical field
The present invention relates to field of environment protection, more particularly to a kind of precise stainless steel strip cold rolling oil.
Background technology
With constantly advancing for modern society, the living standard of people especially material conditions there occurs it is earth-shaking
Change, stainless steel products applied more and more widely because of superperformances such as corrosion-resistant, high temperature resistance, intensity height, surface finenesses
In fields such as kitchen appliance, communications and transportation, medical treatment, building industries, stainless steel products already become in people's daily life can not or
One of scarce primary article.For China's stainless steel industry is than European and American developed countries, starting and development are relatively later；Reform
After opening, with the fast development of national economy, stainless steel products is just from original defence and military industry entry ordinary people
Daily life.Last century the nineties start, and China's stainless steel industry is presented fast-developing trend, and integrated demand is far above complete
Ball average level.
According to statistics, China's stainless steel crude steel yield in 2014 increases by 14.27% to 2169.2 ten thousand ton on a year-on-year basis, accounts for global product
Amount 50%.The actual demand of huge market capacity and rapid growth so that new stainless-steel cold-rolling enterprise constantly goes into operation, one
Large quantities of medium-sized and small enterprises are able to exist and develop.These corporate bosses will, 750mm four-roller reversible with 450mm four-rollers be reversible, 850 four-rollers
Or inclined eight roller it is reversible, 900mm four-rollers are reversible, inclined eight rollers of 1450mm and multiple roll（Such as 12 rollers, 16 rollers, 18 rollers, 20 rollers）
It is reversible to wait based on the reversible type of unit, rolled material is mainly with 200,300 be with 400 be based on；Inclined eight rollers of wherein 1450mm
It is and the reversible unit speed of multiple roll is fast, drafts big, high in machining efficiency and excellent performance but also harsh to lubricating requirement.Add again
Rapidoprint upstream source is relative complex and extensive, and quality is uneven, and overall processing difficulty is larger.At present, domestic stainless steel
Cold rolling processing is main using Process of Emulsifying Oil For Rolling and to be aided with to be added dropwise by the way of vegetable oil and carries out technological lubrication, and vegetable oil can not be circulated and made
With and cleaning difference be easily attached on plate face, finished products detergency is poor, easily produce macula lutea, and poor surface smoothness causes not
Rust steel enterprise product overall market competitiveness is low.Meanwhile, the service life of rolling emulsion is short, and enterprise typically about 6 months is thorough
Bottom is changed, and generates substantial amounts of Process of Emulsifying Oil For Rolling waste liquid, and waste liquid is difficult, somewhat expensive, and produces secondary pollution, with state
The policy of family's energy-conserving and environment-protective runs in the opposite direction.
With the surplus of recent year stainless steel industry production capacity, the competition between stainless steel enterprises, market pair are exacerbated
Finished product plate shape, surface quality propose higher and higher requirement.Simultaneously as stainless-steel cold-rolling technology continuous ripe and sending out
Exhibition, the cold rolling importance with lubriation material increasingly obtains the consistent accreditation of industry personnel, is farthest to improve product matter
Amount, the comprehensive market competitiveness of further enterprise and the strategy of quickening Promoting Enterprise clean manufacturing, mostly to suitable for state
The lubriation material of interior stainless-steel cold-rolling technique proposes new expectation.
The content of the invention
In order to overcome the shortcoming and deficiency of above-mentioned prior art, the primary and foremost purpose of the present invention is to provide a kind of environmental protection, length
Life-span, high-performance stainless steel cold rolling oil.The ROLLING OIL is particularly well-suited to inclined eight rollers or many of the 1450mm high to lubricating requirement
The reversible stainless steel re-entrant trough profiled steel sheeting of roller, with excellent lubricity, wear resistence, antioxidant and cooling, is obviously improved cold rolling finished product
Surface smoothness, while improve production operation environment, can realize being recycled for a long time, during stainless-steel cold-rolling substantially without
Waste oil is produced.
The technical problem to be solved is achieved by the following technical programs：
A kind of precise stainless steel strip cold rolling oil, the component comprising following quality percentage meter：0.5 ~ 2% cooling agent, 0.5 ~ 3 %
Extreme pressure anti-wear additives, 5 ~ 10 % lubricants, 0.2 ~ 1 % detergent-dispersant additives, 1 ~ 3 % bleeding agents, 0.2 ~ 1 % antifume agents, 0.1 ~ 0.5
% antioxidant, and it is supplemented to 100% with base oil.
Further, described cooling agent is in polymethacrylates, ethylene-propylene copolymer, polyisobutene, poly alpha olefin
At least one.
Further, described extreme pressure anti-wear additives are in organic-molybdenum, C12-C18 stearic acid, fatty alcohol modified phosphate
It is at least one.
Further, described base oil is in two classes hydrogenation paraffin base oil, three classes hydrogenation paraffin base oil
At least one,
Further, 40 DEG C of kinematic viscosity of the base oil are 7 ~ 13mm2/s。
Further, described lubricant is 12/tetradecyl alchohol oleate, pentaerythritol ester, Ethylhexyl stearate, tristearin
Acid butyl ester, phthalic acid ester, palmitate, sulfuration succinate, at least one of dioctyl adipate.
Further, described detergent-dispersant additive is succimide type, polyisobutylene succinic acid ester, polyisobutene fourth two
Acid imide, base number calcium mahogany sulfonate, base number calcium sulfenyl phenolate, alkylsalicylate, thio-phosphonates and the poly- isobutyl of sulphur phosphatization
One or more of alkene barium salt.
Further, described bleeding agent is at least one in Laurocapram, C14-C16 fatty alcohols, certainly, its
The GSK-588 of his product such as Gauss can also realize the present invention.
Further, described antioxidant is at least one in sulfenyl phenolate, thiocarbamic acid copper.
The antifume agent of the present invention can adopt the speciality polymer polymer A DDCO ADDTAC of Lubrizol Corp..
Application of the above-mentioned stainless-steel cold-rolling ROLLING OIL in inclined eight rollers of 1450mm or the reversible stainless steel re-entrant trough profiled steel sheeting of multiple roll.
The preparation method of ROLLING OIL of the present invention is：
1st, antifume agent and cooling agent are added in a certain amount of base oil, is heated to 60 DEG C ~ 70 DEG C or so, and stir constant temperature
60min, makes cooling agent and antifume agent spread apart completely in base oil；
2nd, base oil temperature control is added thereto the antifume agent after being dissolved with base oil and cooling agent at 20 DEG C ~ 50 DEG C,
Antiwear additive, lubricant, antioxidant, bleeding agent are sequentially added under stirring to be added in reactor, is stirred to being well mixed, and clarify
It is transparent, obtain stainless-steel cold-rolling ROLLING OIL.
The present invention has the advantages that：
The optimized combination of currently preferred each additive, the stainless-steel cold-rolling ROLLING OIL of acquisition has excellent combination property,
Inventive formulation system combines the process characteristic of inclined eight rollers of 1450mm or the reversible stainless steel re-entrant trough profiled steel sheeting of multiple roll, and using innovation
Cooling Control Technology, infiltration technology and lubricating system, the moment amount of heat for making rolling zone taken away in time, is greatly reduced and rolls
Roller thermal stress deformation, reduces roller consumption, extends work roll cooling birthday noodle；By smog control technology, oil consumption, Er Qiegai are not only reduced
The operating environment of Shan Liao factories；System is recycled to set up the long-life by preferred antioxidant, detergent-dispersant additive, base oil；
By preferred antiwear additive, base oil, lubricant, while reaching the technological lubrication requirement of guarantee stainless-steel cold-rolling, significantly reduce
Rolling depressing force consumes with roller, and annealing cleanness is excellent, and plate face comprehensive quality is high, can meet more than 2B, BA high accuracy grade
Stainless sheet steel plate face is required.
Specific embodiment
With reference to embodiment, the present invention will be described in detail, and embodiment is only the preferred embodiment of the present invention,
It is not limitation of the invention.
The present invention is prepared according to above-mentioned experimental technique.
Embodiment 1
A kind of precise stainless steel strip cold rolling oil, by the raw material of following percentage by weight：Two classes are hydrogenated with paraffin base oil
88.3%, polymethacrylates 0.5%, polyisobutene 0.5%, organic-molybdenum 1%, C12-C18 stearic acid 1%, fatty alcohol modified phosphoric acid
Ester 0.5%, pentaerythritol ester 2%, Ethylhexyl stearate 1%, phthalic acid ester 1% vulcanize succinate 1%, polyisobutene fourth two
Acid imide 0.3%, base number calcium mahogany sulfonate 0.4%, Laurocapram 0.5%, C14-C16 fatty alcohols 1%, sulfenyl phenolate 0.2%,
Thiocarbamic acid copper 0.3%, ADDCO ADDTAC 0.5%.
Embodiment 2：
A kind of precise stainless steel strip cold rolling oil, by the raw material of following percentage by weight：Three classes are hydrogenated with paraffin base oil
89.3%, polymethacrylates 0.2%, polyisobutene 1%, organic-molybdenum 0.5%, fatty alcohol modified phosphoesterase 30 .5%, pentaerythrite
Ester 3%, Ethylhexyl stearate 1%, phthalic acid ester 1%, vulcanize succinate 1%, polyisobutene succinimide 0.2%, base number
Calcium mahogany sulfonate 0.2%, Laurocapram 1.5%, sulfenyl phenolate 0.2%, thiocarbamic acid copper 0.1%, ADDCO ADDTAC
0.3%。
Embodiment 3：
A kind of precise stainless steel strip cold rolling oil, by the raw material of following percentage by weight：Three classes are hydrogenated with paraffin base oil
85.5%, polymethacrylates 0.2%, polyisobutene 0.4%, C12-C18 stearic acid 0.2%, fatty alcohol modified phosphoesterase 30 .8%,
Pentaerythritol ester 2%, Ethylhexyl stearate 3%, phthalic acid ester 2%, vulcanize succinate 2%, polyisobutene succinimide
0.4%, base number calcium mahogany sulfonate 0.2%, GSK-588 2.1%, sulfenyl phenolate 0.1%, thiocarbamic acid copper 0.4%, ADDCO
ADDTAC 0.7%。
Embodiment 4：
A kind of precise stainless steel strip cold rolling oil, by the raw material of following percentage by weight：Base oil 86.4%, polymethyl
Acid esters 0.2%, polyisobutene 0.4%, organic-molybdenum 0.7%, C12-C18 stearic acid 0.6%, pentaerythritol ester 2%, Ethylhexyl stearate
2%th, phthalic acid ester 2%, sulfuration succinate 2%, polyisobutene succinimide 0.3%, base number calcium mahogany sulfonate 0.5%,
GSK-588 2%, sulfenyl phenolate 0.2%, thiocarbamic acid copper 0.2%, ADDCO ADDTAC 0.5%.
Correlated performance detection is carried out to the product of above example and market same type, testing result is described in table 1 below.
The detection project performance table of table 1
It is excellent that the stainless-steel cold-rolling of the present invention rolls oil lubricity, extreme pressure anti-wear, cooling, annealing cleanness and antioxygen property
In market like product.The stainless-steel cold-rolling ROLLING OIL for illustrating the present invention has good extreme pressure and antiwear behavior and excellent lubrication
Performance, can not only meet the lubricating requirement of stainless steel calendering technology, and roller consumption and rolling depressing force can be greatly reduced, greatly
Width improves plate face surface smoothness and comprehensive quality, and the service life of ROLLING OIL is significantly extended in addition, and improves factory
Operating environment.
Embodiment described above only expresses embodiments of the present invention, and its description is more concrete and detailed, but can not
Therefore the restriction to the scope of the claims of the present invention is interpreted as, as long as the skill obtained in the form of equivalent or equivalent transformation
Art scheme, all should fall within the scope and spirit of the invention.
Claims (10)
1. a kind of precise stainless steel strip cold rolling oil, it is characterised in that the component comprising following quality percentage meter：0.5 ~ 2% is cold
But agent, 0.5 ~ 3 % extreme pressure anti-wear additives, 5 ~ 10 % lubricants, 0.2 ~ 1 % detergent-dispersant additives, 1 ~ 3 % bleeding agents, the anti-cigarettes of 0.2 ~ 1 %
Mist agent, 0.1 ~ 0.5 % antioxidant, and it is supplemented to 100% with base oil.
2. stainless steel band cold rolling oil according to claim 1, it is characterised in that：Described cooling agent is poly- methyl-prop
At least one in olefin(e) acid ester, ethylene-propylene copolymer, polyisobutene, poly alpha olefin.
3. stainless steel band cold rolling oil according to claim 1, it is characterised in that：Described extreme pressure anti-wear additives are organic
At least one in molybdenum, C12-C18 stearic acid, fatty alcohol modified phosphate.
4. stainless steel band cold rolling oil according to claim 1, it is characterised in that：Described base oil is two classes hydrogenation
At least one in paraffin base oil, three classes hydrogenation paraffin base oil.
5. stainless steel band cold rolling oil according to claim 4, it is characterised in that：40 DEG C of kinematic viscosity of the base oil
For 7 ~ 13mm2/s。
6. stainless steel band cold rolling oil according to claim 1, it is characterised in that：Described lubricant is 12/ten
Tetrol oleate, pentaerythritol ester, Ethylhexyl stearate, butyl stearate, phthalic acid ester, palmitate, sulfuration fourth two
At least one of acid esters, dioctyl adipate.
7. stainless steel band cold rolling oil according to claim 1, it is characterised in that：Described detergent-dispersant additive is fourth two
Imide-type, polyisobutylene succinic acid ester, polyisobutene succinimide, base number calcium mahogany sulfonate, base number calcium sulfenyl phenolate,
One or more of alkylsalicylate, thio-phosphonates and sulfur phosphorization polyisobutylene titanate salt.
8. stainless steel band cold rolling oil according to claim 1, it is characterised in that：Described bleeding agent is that bay nitrogen is tall and erect
At least one in ketone, C14-C16 fatty alcohols.
9. stainless steel band cold rolling oil according to claim 1, it is characterised in that：Described antioxidant is alkyl monosulfide
At least one in phenol, thiocarbamic acid copper.
10. the stainless-steel cold-rolling ROLLING OIL according to any one of claim 1 ~ 9 is reversible not in inclined eight rollers of 1450mm or multiple roll
The application of rust steel re-entrant trough profiled steel sheeting.
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| CN201611081123.8A CN106590843A (en) | 2016-11-30 | 2016-11-30 | Precision stainless steel band cold-rolling rolling oil |
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| CN112063435A (en) * | 2019-06-10 | 2020-12-11 | 广州加美隆润滑油有限公司 | Cleaning-free stainless steel rolling lubricant |
| CN113462449A (en) * | 2021-06-16 | 2021-10-01 | 广东洁润斯新材料科技有限公司 | Oil product for calendering and drawing copper material by matching with rolling liquid |
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| CN113462449A (en) * | 2021-06-16 | 2021-10-01 | 广东洁润斯新材料科技有限公司 | Oil product for calendering and drawing copper material by matching with rolling liquid |
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Application publication date: 20170426 |