CN106589563A - Easy-to-weld environment-friendly asphalt-based waterproof material - Google Patents
Easy-to-weld environment-friendly asphalt-based waterproof material Download PDFInfo
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- CN106589563A CN106589563A CN201611002139.5A CN201611002139A CN106589563A CN 106589563 A CN106589563 A CN 106589563A CN 201611002139 A CN201611002139 A CN 201611002139A CN 106589563 A CN106589563 A CN 106589563A
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- C08L—COMPOSITIONS OF MACROMOLECULAR COMPOUNDS
- C08L23/00—Compositions of homopolymers or copolymers of unsaturated aliphatic hydrocarbons having only one carbon-to-carbon double bond; Compositions of derivatives of such polymers
- C08L23/02—Compositions of homopolymers or copolymers of unsaturated aliphatic hydrocarbons having only one carbon-to-carbon double bond; Compositions of derivatives of such polymers not modified by chemical after-treatment
- C08L23/04—Homopolymers or copolymers of ethene
- C08L23/08—Copolymers of ethene
- C08L23/0846—Copolymers of ethene with unsaturated hydrocarbons containing other atoms than carbon or hydrogen atoms
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- C08J—WORKING-UP; GENERAL PROCESSES OF COMPOUNDING; AFTER-TREATMENT NOT COVERED BY SUBCLASSES C08B, C08C, C08F, C08G or C08H
- C08J9/00—Working-up of macromolecular substances to porous or cellular articles or materials; After-treatment thereof
- C08J9/04—Working-up of macromolecular substances to porous or cellular articles or materials; After-treatment thereof using blowing gases generated by a previously added blowing agent
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- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08J—WORKING-UP; GENERAL PROCESSES OF COMPOUNDING; AFTER-TREATMENT NOT COVERED BY SUBCLASSES C08B, C08C, C08F, C08G or C08H
- C08J9/00—Working-up of macromolecular substances to porous or cellular articles or materials; After-treatment thereof
- C08J9/04—Working-up of macromolecular substances to porous or cellular articles or materials; After-treatment thereof using blowing gases generated by a previously added blowing agent
- C08J9/06—Working-up of macromolecular substances to porous or cellular articles or materials; After-treatment thereof using blowing gases generated by a previously added blowing agent by a chemical blowing agent
- C08J9/08—Working-up of macromolecular substances to porous or cellular articles or materials; After-treatment thereof using blowing gases generated by a previously added blowing agent by a chemical blowing agent developing carbon dioxide
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- C—CHEMISTRY; METALLURGY
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- C08J—WORKING-UP; GENERAL PROCESSES OF COMPOUNDING; AFTER-TREATMENT NOT COVERED BY SUBCLASSES C08B, C08C, C08F, C08G or C08H
- C08J2203/00—Foams characterized by the expanding agent
- C08J2203/02—CO2-releasing, e.g. NaHCO3 and citric acid
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- C08J2323/00—Characterised by the use of homopolymers or copolymers of unsaturated aliphatic hydrocarbons having only one carbon-to-carbon double bond; Derivatives of such polymers
- C08J2323/02—Characterised by the use of homopolymers or copolymers of unsaturated aliphatic hydrocarbons having only one carbon-to-carbon double bond; Derivatives of such polymers not modified by chemical after treatment
- C08J2323/04—Homopolymers or copolymers of ethene
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- C08J2453/00—Characterised by the use of block copolymers containing at least one sequence of a polymer obtained by reactions only involving carbon-to-carbon unsaturated bonds; Derivatives of such polymers
- C08J2453/02—Characterised by the use of block copolymers containing at least one sequence of a polymer obtained by reactions only involving carbon-to-carbon unsaturated bonds; Derivatives of such polymers of vinyl aromatic monomers and conjugated dienes
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- C08L2201/00—Properties
- C08L2201/02—Flame or fire retardant/resistant
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- C08L2203/00—Applications
- C08L2203/14—Applications used for foams
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- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08L—COMPOSITIONS OF MACROMOLECULAR COMPOUNDS
- C08L2205/00—Polymer mixtures characterised by other features
- C08L2205/03—Polymer mixtures characterised by other features containing three or more polymers in a blend
- C08L2205/035—Polymer mixtures characterised by other features containing three or more polymers in a blend containing four or more polymers in a blend
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Abstract
The invention discloses an easy-to-weld environment-friendly asphalt-based waterproof material, which consists of the following materials in part by weight: 40 to 60 parts of SBS powder, 30 to 50 parts of sodium nitrite, 40 to 60 parts of magnesium chloride, 20 to 40 parts of polyvinyl chloride, 20 to 40 parts of polystyrene, 15 to 25 parts of No.90 asphalt, 100 to 150 parts of EVA particles, 20 to 30 parts of dimethyl fumarate, 30 to 40 parts of polyurethane, 15 to 25 parts of foaming agent, 25 to 35 parts of magnesium hypophosphite, 40 to 60 parts of activated calcium carbonate, 30 to 50 parts of acrylic emulsion, 20 to 40 parts of nanoscale ZSM-5 zeolite molecular sieve powder and 100 to 150 parts of water. The elastic property of the waterproof material is good, welding temperature can be effectively decreased, and the compressive strength is high.
Description
Technical field
The present invention relates to a kind of environment-friendly type asphalt base waterproofing material of easy welding.
Background technology
Waterproof material is a kind of new high-grade waterproof material for growing up in recent years, is mainly used in water conservancy, civil engineering work
Basal plane water-proofing treatment in journey.Waterproof material includes and constitutes the synthetic resin sheet material of its tire basic unit, is compound in above-mentioned tire basic unit
The separating film layer of the adhesive formed by modified pitch and laminating surface of pressure-sensitive adhesive on one or both sides；In production process
In rolling storage or transport.During use, material is spread out and peels off separating film layer, bonded with engineering basal plane by adhesive phase, it is real
The function of existing water-proofing treatment.But there is following defect in the material for being used at present：First, after permanent storage or piling up transport,
Because extruding result in the deformation of material, when launching to use, to be difficult to nature smooth for laying, it is necessary to by means of external force in longer time
It is interior to realize paving, especially construct at low ambient temperatures, be more difficult to be completed in a relatively short time waterproof material material
The laying of material；Second, hot melting temperature o'clock is at 450 DEG C or so, the welding procedure between sheet material is difficult.
The content of the invention
In view of this, it is to solve the technical problem in background technology, the present invention provides a kind of environment-friendly type Colophonium of easy welding
Base waterproof material.
The present invention is adopted the following technical scheme that：
A kind of environment-friendly type asphalt base waterproofing material of easy welding, including the raw material of following parts by weight proportioning：SBS powder 40-60
Part, sodium nitrite 30-50 parts, magnesium chloride 40-60 parts, polrvinyl chloride 20-40 parts, polystyrene 20-40 parts, 90# Colophonium 15-25
Part, EVA granule 100-150 parts, dimethyl fumarate 20-30 parts, polyurethane 30-40 parts, foaming agent 15-25 parts, magnesium hypophosphite
25-35 parts, activated Calcium carbonate 40-60 parts, acrylic emulsion 30-50 parts, nanoscale ZSM-5 zeolite molecular sieve powder 20-40 part,
Water 100-150 parts.Particularly, in the present invention, EVA granules refer to ethylene-vinyl acetate copolymer granule, and SBS powder refers to benzene second
Alkene-butadiene-styrene block copolymer powder.
Further, including the raw material of following parts by weight proportioning：50 parts of SBS powder, 40 parts of sodium nitrite, magnesium chloride 50
Part, 30 parts of polrvinyl chloride, 30 parts of polystyrene, 20 parts of 90# Colophoniumes, 125 parts of EVA granules, 25 parts of dimethyl fumarate, polyurethane
35 parts, 20 parts of foaming agent, 30 parts of magnesium hypophosphite, 50 parts of activated Calcium carbonate, 40 parts of acrylic emulsion, nanoscale ZSM-5 zeolite point
Son 30 parts of powder of sieve, 125 parts of water.
Further, including the raw material of following parts by weight proportioning：60 parts of SBS powder, 50 parts of sodium nitrite, magnesium chloride 60
Part, 40 parts of polrvinyl chloride, 40 parts of polystyrene, 25 parts of 90# Colophoniumes, 150 parts of EVA granules, 30 parts of dimethyl fumarate, polyurethane
40 parts, 25 parts of foaming agent, 35 parts of magnesium hypophosphite, 60 parts of activated Calcium carbonate, 50 parts of acrylic emulsion, nanoscale ZSM-5 zeolite point
Son 40 parts of powder of sieve, 150 parts of water.
Further, including the raw material of following parts by weight proportioning：40 parts of SBS powder, 30 parts of sodium nitrite, magnesium chloride 40
Part, 20 parts of polrvinyl chloride, 20 parts of polystyrene, 15 parts of 90# Colophoniumes, 100 parts of EVA granules, 20 parts of dimethyl fumarate, polyurethane
30 parts, 15 parts of foaming agent, 25 parts of magnesium hypophosphite, 40 parts of activated Calcium carbonate, 30 parts of acrylic emulsion, nanoscale ZSM-5 zeolite point
Son 20 parts of powder of sieve, 100 parts of water.
A kind of preparation method of the environment-friendly type asphalt base waterproofing material of easy welding, comprises the following steps：
1）50 parts of SBS powder, 50 parts of activated Calcium carbonate, nanoscale ZSM-5 zeolite molecular sieve powder are extracted by optimal number proportioning
30 parts, throwing in carries out grinding on flour mill, and rotating speed is 300r/min, grinding time 2h, and control temperature is at 25 DEG C；
2）Toward step 1）In mixed-powder be warming up to 890 DEG C, obtain intensification mixed-powder；
3）By step 2）Mixed-powder put in dore furnace, temperature is risen to into 950 DEG C, be incubated 30 minutes, be cooled to 25 afterwards
DEG C, add 40 parts of sodium nitrite, 50 parts of magnesium chloride, 30 parts of polrvinyl chloride, 30 parts of polystyrene, 125 parts of water to obtain mixing oar；
4）To take 20 parts of 90# Colophoniumes, 125 parts of EVA granules, 25 parts of dimethyl fumarate, 35 parts of polyurethane, 30 parts of magnesium hypophosphite,
40 parts of acrylic emulsion, after stirring 30 minutes, maintains temperature at 30 DEG C, adds 20 parts of foaming agent, obtain mixture；
5）By step 4）In mixture be passed through steam 2h, stand for standby use；
6）By step 3）With step 5) mix and put centrifuge into, rotating speed is 500r/min, and the time is 1h；
7）By step 6）In mixture pour in mould, you can obtain waterproof material.
The present invention is by adding hot acrylic emulsion, nontoxic, non-stimulated, harmless, meets environmental requirement, with excellent
Different gloss, elastic recovery properties are good；90# Colophoniumes are added, flame resistance is good, high temperature performance is stable, thermal insulation is heat-insulated, with preferable
Durability, with magnesium hypophosphite compound synergistic, significantly reduce material welding temperature；Add nanoscale ZSM-5 zeolite point
Son sieve powder, it is lightweight, it is capable of the fracture tensile strength and resistance to chemical attack ability of reinforcing material.
Material of the present invention has good elastic recovery capability, is launching to recover flat in 5 minutes as Jing crimps are latter
Exhibition, and docile property can be laid good according to the conversion of formation level because gesture is converted, it is to avoid because formation level it is asynchronous with waterproof material
And produce the generation that waterproof material local stress deformation even braking effect water resistance changes situation；The hot melt of material of the present invention
Temperature is low, easy welding procedure, on the premise of ensureing that welding effect is superior, compares welding temperature compared with common material low at most
100 DEG C, greatly save the energy consumption of welding equipment；Material of the present invention has fracture tensile strength height, fracture elongation big, tear
The performance of intensity height, resistance to chemical attack etc., can be widely used in the underground waterproof engineerings such as tunnel, culvert, subway.
Specific embodiment
Embodiment 1：
A kind of waterproof material, including the raw material of following parts by weight proportioning：40 parts of SBS powder, 30 parts of sodium nitrite, magnesium chloride 40
Part, 20 parts of polrvinyl chloride, 20 parts of polystyrene, 15 parts of 90# Colophoniumes, 100 parts of EVA granules, 20 parts of dimethyl fumarate, polyurethane
30 parts, 15 parts of foaming agent, 25 parts of magnesium hypophosphite, 40 parts of activated Calcium carbonate, 30 parts of acrylic emulsion, nanoscale ZSM-5 zeolite point
Son 20 parts of powder of sieve, 100 parts of water, foaming agent can be the wherein sheets of Calcium Carbonate, magnesium carbonate, sodium bicarbonate, sodium silicate, carborundum
The foaming agent for being used of embodiment is Calcium Carbonate.
A kind of preparation method of waterproof material, comprises the following steps：
1）40 parts of SBS powder, 40 parts of activated Calcium carbonate, nanoscale ZSM-5 zeolite molecular sieve powder are extracted by optimal number proportioning
20 parts, throwing in carries out grinding on flour mill, and rotating speed is 300r/min, grinding time 2h, and control temperature is at 25 DEG C；
2）Toward step 1）In mixed-powder be warming up to 890 DEG C, obtain intensification mixed-powder；
3）By step 2）Mixed-powder put in dore furnace, temperature is risen to into 950 DEG C, be incubated 30 minutes, be cooled to 25 afterwards
DEG C, add 30 parts of sodium nitrite, 40 parts of magnesium chloride, 20 parts of polrvinyl chloride, 20 parts of polystyrene, 100 parts of water to obtain mixing oar；
4）To take 15 parts of 90# Colophoniumes, 100 parts of EVA granules, 20 parts of dimethyl fumarate, 30 parts of polyurethane, 25 parts of magnesium hypophosphite,
30 parts of acrylic emulsion, after stirring 30 minutes, maintains temperature at 30 DEG C, adds 15 parts of foaming agent, obtain mixture；
5）By step 4）In mixture be passed through steam 2h, stand for standby use；
6）By step 3）With step 5) mix and put centrifuge into, rotating speed is 500r/min, and the time is 1h；
7）By step 6）In mixture pour in mould, you can obtain waterproof material.
Embodiment 2：
A kind of waterproof material, including the raw material of following parts by weight proportioning：50 parts of SBS powder, 40 parts of sodium nitrite, magnesium chloride 50
Part, 30 parts of polrvinyl chloride, 30 parts of polystyrene, 20 parts of 90# Colophoniumes, 125 parts of EVA granules, 25 parts of dimethyl fumarate, polyurethane
35 parts, 20 parts of foaming agent, 30 parts of magnesium hypophosphite, 50 parts of activated Calcium carbonate, 40 parts of acrylic emulsion, nanoscale ZSM-5 zeolite point
Son 30 parts of powder of sieve, 125 parts of water, foaming agent can be the wherein sheets of Calcium Carbonate, magnesium carbonate, sodium bicarbonate, sodium silicate, carborundum
The foaming agent for being used of embodiment is magnesium carbonate.
A kind of preparation method of waterproof material, comprises the following steps：
1）50 parts of SBS powder, 50 parts of activated Calcium carbonate, nanoscale ZSM-5 zeolite molecular sieve powder are extracted by optimal number proportioning
30 parts, throwing in carries out grinding on flour mill, and rotating speed is 300r/min, grinding time 2h, and control temperature is at 25 DEG C；
2）Toward step 1）In mixed-powder be warming up to 890 DEG C, obtain intensification mixed-powder；
3）By step 2）Mixed-powder put in dore furnace, temperature is risen to into 950 DEG C, be incubated 30 minutes, be cooled to 25 afterwards
DEG C, add 40 parts of sodium nitrite, 50 parts of magnesium chloride, 30 parts of polrvinyl chloride, 30 parts of polystyrene, 125 parts of water to obtain mixing oar；
4）To take 20 parts of 90# Colophoniumes, 125 parts of EVA granules, 25 parts of dimethyl fumarate, 35 parts of polyurethane, 30 parts of magnesium hypophosphite,
40 parts of acrylic emulsion, after stirring 30 minutes, maintains temperature at 30 DEG C, adds 20 parts of foaming agent, obtain mixture；
5）By step 4）In mixture be passed through steam 2h, stand for standby use；
6）By step 3）With step 5) mix and put centrifuge into, rotating speed is 500r/min, and the time is 1h；
7）By step 6）In mixture pour in mould, you can obtain waterproof material.
Embodiment 3：
A kind of waterproof material, including the raw material of following parts by weight proportioning：60 parts of SBS powder, 50 parts of sodium nitrite, magnesium chloride 60
Part, 40 parts of polrvinyl chloride, 40 parts of polystyrene, 25 parts of 90# Colophoniumes, 150 parts of EVA granules, 30 parts of dimethyl fumarate, polyurethane
40 parts, 25 parts of foaming agent, 35 parts of magnesium hypophosphite, 60 parts of activated Calcium carbonate, 50 parts of acrylic emulsion, nanoscale ZSM-5 zeolite point
Son 40 parts of powder of sieve, 150 parts of water, foaming agent can be the wherein sheets of Calcium Carbonate, magnesium carbonate, sodium bicarbonate, sodium silicate, carborundum
The foaming agent for being used of embodiment is sodium silicate.
A kind of preparation method of waterproof material, comprises the following steps：
1）60 parts of SBS powder, 60 parts of activated Calcium carbonate, nanoscale ZSM-5 zeolite molecular sieve powder are extracted by optimal number proportioning
40 parts, throwing in carries out grinding on flour mill, and rotating speed is 300r/min, grinding time 2h, and control temperature is at 25 DEG C；
2）Toward step 1）In mixed-powder be warming up to 890 DEG C, obtain intensification mixed-powder；
3）By step 2）Mixed-powder put in dore furnace, temperature is risen to into 950 DEG C, be incubated 30 minutes, be cooled to 25 afterwards
DEG C, add 50 parts of sodium nitrite, 60 parts of magnesium chloride, 40 parts of polrvinyl chloride, 40 parts of polystyrene, 150 parts of water to obtain mixing oar；
4）To take 25 parts of 90# Colophoniumes, 150 parts of EVA granules, 30 parts of dimethyl fumarate, 40 parts of polyurethane, 35 parts of magnesium hypophosphite,
50 parts of acrylic emulsion, after stirring 30 minutes, maintains temperature at 30 DEG C, adds 25 parts of foaming agent, obtain mixture；
5）By step 4）In mixture be passed through steam 2h, stand for standby use；
6）By step 3）With step 5) mix and put centrifuge into, rotating speed is 500r/min, and the time is 1h；
7）By step 6）In mixture pour in mould, you can obtain waterproof material.
Experimental example：
Experimental subject：100 blocks of sheet materials manufactured by waterproof material of the present invention and 100 blocks of common sheet materials.
Experimental technique：By waterproof material of the present invention manufacture sheet material be experimental group, existing common sheet material as a control group,
By following test, concrete outcome is as shown in the table：
By contrasting to 2 groups of experiments, the waterproof material a kind of of the present invention of the present invention manufactures sheet material and existing common plate
Material compares nontoxic, stretching, bending, comprcssive strength height.
The present invention is by adding hot acrylic emulsion, nontoxic, non-stimulated, harmless, meets environmental requirement, with excellent
Different gloss, elastic recovery properties are good；90# Colophoniumes are added, flame resistance is good, high temperature performance is stable, thermal insulation is heat-insulated, with preferable
Durability, with magnesium hypophosphite compound synergistic, significantly reduce material welding temperature；Add nanoscale ZSM-5 zeolite point
Son sieve powder, it is lightweight, it is capable of the fracture tensile strength and resistance to chemical attack ability of reinforcing material.
The above, the only specific embodiment of the present invention, but protection scope of the present invention is not limited thereto, any
The change or replacement expected without creative work, should all cover within the scope of the present invention.It is not detailed in the present invention
The ins and outs of description can be realized by this area any prior art.
Claims (4)
1. a kind of environment-friendly type asphalt base waterproofing material of easy welding, it is characterised in that including the raw material of following parts by weight proportioning：
SBS powder 40-60 parts, sodium nitrite 30-50 parts, magnesium chloride 40-60 parts, polrvinyl chloride 20-40 parts, polystyrene 20-40 parts,
90# Colophonium 15-25 parts, EVA granule 100-150 parts, dimethyl fumarate 20-30 parts, polyurethane 30-40 parts, foaming agent 15-25
Part, magnesium hypophosphite 25-35 parts, activated Calcium carbonate 40-60 parts, acrylic emulsion 30-50 parts, nanoscale ZSM-5 zeolite molecular sieve
Powder 20-40 parts, water 100-150 parts.
2. the environment-friendly type asphalt base waterproofing material for easily welding as claimed in claim 1, it is characterised in that including following weight portion
The raw material of number proportioning：50 parts of SBS powder, 40 parts of sodium nitrite, 50 parts of magnesium chloride, 30 parts of polrvinyl chloride, 30 parts of polystyrene,
20 parts of 90# Colophoniumes, 125 parts of EVA granules, 25 parts of dimethyl fumarate, 35 parts of polyurethane, 20 parts of foaming agent, 30 parts of magnesium hypophosphite,
50 parts of activated Calcium carbonate, 40 parts of acrylic emulsion, 30 parts of nanoscale ZSM-5 zeolite molecular sieve powder, 125 parts of water.
3. the environment-friendly type asphalt base waterproofing material for easily welding as claimed in claim 1, it is characterised in that including following weight portion
The raw material of number proportioning：60 parts of SBS powder, 50 parts of sodium nitrite, 60 parts of magnesium chloride, 40 parts of polrvinyl chloride, 40 parts of polystyrene,
25 parts of 90# Colophoniumes, 150 parts of EVA granules, 30 parts of dimethyl fumarate, 40 parts of polyurethane, 25 parts of foaming agent, 35 parts of magnesium hypophosphite,
60 parts of activated Calcium carbonate, 50 parts of acrylic emulsion, 40 parts of nanoscale ZSM-5 zeolite molecular sieve powder, 150 parts of water.
4. the environment-friendly type asphalt base waterproofing material for easily welding as claimed in claim 1, it is characterised in that including following weight portion
The raw material of number proportioning：40 parts of SBS powder, 30 parts of sodium nitrite, 40 parts of magnesium chloride, 20 parts of polrvinyl chloride, 20 parts of polystyrene,
15 parts of 90# Colophoniumes, 100 parts of EVA granules, 20 parts of dimethyl fumarate, 30 parts of polyurethane, 15 parts of foaming agent, 25 parts of magnesium hypophosphite,
40 parts of activated Calcium carbonate, 30 parts of acrylic emulsion, 20 parts of nanoscale ZSM-5 zeolite molecular sieve powder, 100 parts of water.
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| CN108250771A (en) * | 2017-12-04 | 2018-07-06 | 杭州睿琦化工科技有限公司 | Road modified asphalt |
| CN109385104A (en) * | 2017-08-10 | 2019-02-26 | 常州利尔德通新材料科技有限公司 | A kind of preparation method and applications of warm mix environmentally-friendly asphalt fire retardant |
| CN109796751A (en) * | 2019-02-18 | 2019-05-24 | 苏州复之恒新材料科技有限公司 | A kind of preparation method of polyurethane/nano zeolite elastic composite |
| EP3656831A1 (en) * | 2018-11-26 | 2020-05-27 | Aladdin Manufactuing Corporation | Composition and flooring product comprising such composition |
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Cited By (5)
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| CN109385104A (en) * | 2017-08-10 | 2019-02-26 | 常州利尔德通新材料科技有限公司 | A kind of preparation method and applications of warm mix environmentally-friendly asphalt fire retardant |
| CN108250771A (en) * | 2017-12-04 | 2018-07-06 | 杭州睿琦化工科技有限公司 | Road modified asphalt |
| EP3656831A1 (en) * | 2018-11-26 | 2020-05-27 | Aladdin Manufactuing Corporation | Composition and flooring product comprising such composition |
| EP3887064A4 (en) * | 2018-11-26 | 2022-09-14 | Aladdin Manufacturing Corporation | Composition and flooring product comprising such composition |
| CN109796751A (en) * | 2019-02-18 | 2019-05-24 | 苏州复之恒新材料科技有限公司 | A kind of preparation method of polyurethane/nano zeolite elastic composite |
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Application publication date: 20170426 |