CN106580737A - Skin-cleaning mousse composition and preparation method thereof - Google Patents

Abstract

The invention discloses a skin-cleaning mousse composition and a preparation method thereof. The composition is prepared by compounding laureth-1 phosphate and trehalose, which serve as foaming stabilization additives, wherein the additive amount of laureth-1 phosphate is 1-15% and the additive amount of trehalose is 1-10%. According to the skin-cleaning mousse composition and the preparation method, laureth-1 phosphate and trehalose are rationally compounded and added to a skin-cleaning cosmetic; by adopting an aerosol form, generated foams have Q elasticity effects like eggs, and the unique feeling is that aerosol skin-cleaning cosmetics in the market do not have; and therefore, the skin-cleaning mousse composition has uniqueness and novelty, has better attraction to consumers, brings unique and novel usage experience for the consumers, and can achieve balance of foam and cleaning effects and mild and good skin feeling.

Description

A kind of clean skin mouse compositions and preparation method thereof

【Technical field】

The present invention relates to a kind of clean skin mouse compositions and preparation method thereof, belong to cosmetic technical field.

【Background technology】

Skin is the border limitans existed between human body and external environment condition, maintains the cleaning of skin particularly significant with health. The sebum and horny layer of skin surface comes off and its oxidation Decomposition thing (dirt), or coherent cosmetics therewith Residue be all it is unstable, can with the oxygen in air or other deposition molecules reaction.When sunlight is exposed to, or on skin With the presence of antibacterial, it may occur that various physical chemistry or biochemical reaction, some materials that may injure skin are formed.Thus, Even healthy skin, skin clean are also essential.The purpose of clean skin product is to remove the dirt on skin, makes skin clear It is refreshing, help to maintain skin normal physiological condition.

Most commercial skin-cleaning cosmetics all surfactants containing higher concentration, are applied together with water, are cleaned completely Foam was produced all before clean.From in terms of physical chemistry viewpoint, although the quality and quantity of foam is not directly closed with cleaning function System, but abundant and fine and smooth foam is the reusable key factor of consumer.And easily rinse and with rear skin sense be evaluate The important factor of skin-cleaning cosmetics.Therefore the main challenge of the acceptable skin-cleaning cosmetics of developing target market is foam to be reached and clear Clean effect and the balance good to skin mildness and happy skin sense.

Skin-cleaning cosmetics dosage form on existing market is various, and aerial fog type skin-cleaning cosmetics are instant by pressing pump head, energy Abundant foam is produced, it is easy to use, increasingly liked by consumer.Existing aerial fog type clean skin product is nothing more than can produce Fine and closely woven abundant foam, has no special feature in sense of touch.

【The content of the invention】

The invention aims to overcome the deficiencies in the prior art, there is provided one kind can be prepared and be touched with Q bullets as egg The clean skin mouse compositions of sense.

It is a further object of the present invention to provide a kind of preparation method of above-mentioned clean skin mouse compositions.

The present invention for achieving the above object, is employed the following technical solutions：

A kind of clean skin mouse compositions, it is characterised in that sent out using -1 phosphate ester of laureth and trehalose compounding conduct Bubble stabilization additives.

The addition of -1 phosphate ester of laureth in the present invention is 1-15%, and the addition of the trehalose is 1- 10%.

A kind of clean skin mouse compositions of the present invention, it is characterised in that specifically include following weight percentage component：

A phases：Polyhydric alcohol 1-10%

Thickening agent 0.1-2%

Deionized water adds to 100%

B phases：Surfactant 10-30%

C phases：- 1 phosphate ester 1-15% of laureth

Trehalose 1-10%

D phases：PH adjusting agent adjusts pH to 5.5-7.5

Preservative qs

Appropriate essence

E phases：Propellant 4-8%.

The percentage by weight of above each component is with whole system total amount as radix.

By the compounding mixture for adding -1 phosphate ester of laureth and trehalose, can substantially increase the elasticity of foam, Prepare foam Q bullet effects.One of them -1 phosphate ester of component laureth is the phosphate ester for connecing epoxy, and monoester content is high, Its feature is safe, foaming abundancy.In flushing process, dermal sensation is moistened, and washes rear skin sense well, is particularly suited for clean Skin cosmetics.In product development process, it has been found that add -1 phosphate ester of laureth dramatically increase the elasticity of foam And fine and closely woven property, so that the mousse for producing has the elasticity of the Q bullets such as egg.If substituting lauryl alcohol with other surfaces activating agent to gather - 1 phosphate ester of ether, then the mousse elasticity for producing are substantially poor even without elasticity.- 1 phosphate ester of laureth is providing foam There is in elastic and fine and closely woven property its unique advantage.

Another component trehalose is a kind of natural saccharide, is present in many desert plants, is formed when plant is withered One layer of vitreous substrate, protects its internal structure, until rainwater comes, plant can miraculously play " dead " and demutation.In a large number Research with practice have shown that, trehalose can effectively protect epidermis cell membrane structure, activating cell, nurse one's health skin, make skin be good for It is Kang Ziran, flexible.Epidermis cell under the environment such as high temperature, high and cold, dry, intensive ultraviolet radiation easily dries out and makes Skin damage, trehalose can form one layer of special protecting film in cell surface layer in this case, keep the original battalion of skin Support and moisture, it is to avoid skin sunburn and melanin deposition, be effective against skin ageing phenomenon；The mucus separated out from film can be gentle Glycerin, makes bright skin jade-like stone, gloss, tender.Be experimentally confirmed, trehalose added in clean skin product, can make to wash rear skin Skin is tender to moisten not tight, produces happy skin sense.In product development process, it has been found that add Sargassum in clean skin product Sugar, can increase the stability of foam, make foamed elastic maintain the longer time.

In product development process, it has been found that only in skin-cleaning cosmetics add -1 phosphate ester of laureth or Trehalose, the Q elasticity of produced foam are not ideal enough, individually add -1 phosphate ester foamed elastic of laureth good but strong Degree and stability are poor, and elasticity is held time short, and individually adds trehalose, and foamed elastic is poor but intensity and good stability, and adds After entering both, the elasticity of foam, intensity and stability can reach preferably requirement.It is therefore believed that both collocation tools There is Synergistic, the effect of foam Q bullets such as egg can be prepared.The combination of -1 phosphate ester of laureth and trehalose Characteristic for the present invention is combined.

Preferably, the addition of -1 phosphate ester of laureth of the present invention is 5-8%, and the addition of the trehalose is 3- 6%.

It is further preferred that -1 phosphate ester of laureth is 1-2 with the addition mass ratio of trehalose：1.

One or more in polyhydric alcohol preferably glycerine, Propylene Glycol, Sorbitol, butanediol in the present invention.

Thickening agent in the present invention is preferably one or more in carbomer, HANSHENGJIAO, cellulose.

Surfactant in the present invention can be anion surfactant, amphoteric surfactant, non-ionic surface One or more in activating agent, the good surfactant of preferred mildness, to improve the safety of product.

PH adjusting agent in the present invention can be the one kind in potassium hydroxide, sodium hydroxide, triethanolamine.

Propellant in the present invention is one or more in propane, butane, iso-butane, dimethyl ether and its homologue.

A kind of above-mentioned clean skin mouse compositions, it is characterised in that comprise the following steps：

A, A phase components are mixed and stirred for being warmed up to 80 DEG C, are uniformly dissolved；

B, addition B phases, C phase components are mixed and stirred for being uniformly dissolved, and start cooling；

C, 45 DEG C are cooled to, add D phase components, stir

D, material body produced above is poured in aerosol container in proportion, set up valve, pour into E phase components in proportion i.e. Can.

Compared with prior art, the present invention has the following advantages：

The present invention is rationally compounded with two component of trehalose by -1 phosphate ester of laureth, is added to clean skin and is made up In product, using aerosol-type, make the foam of generation that there is the Q bullets effect such as egg, its unique sense of touch is aerosol on the market Not available for type skin-cleaning cosmetics, unique and novelty has bigger captivation to consumer, gives consumer's band Carry out unique novel experience, while reaching, foam and cleaning effectiveness are good with gentle to skin and happy skin sense to put down Weighing apparatus.

Product of the present invention will not produce anaphylaxiss to user, using safety.

【Specific embodiment】

Further more detailed description is done to the present invention below by way of specific embodiment.

The each component mass percentage content of embodiment 1-5 is as shown in table 1：

Table 1：

The preparation method of embodiment 1-5 is：

A, A phase components are mixed and stirred for being warmed up to 80 DEG C, are uniformly dissolved；

B, addition B phases, C phase components are mixed and stirred for being uniformly dissolved, and start cooling；

C, 45 DEG C are cooled to, add D phase components, stir

D, material body produced above is poured in aerosol container in proportion, set up valve, pour into E phase components in proportion i.e. Can.

The preparation method of comparative example 1-2 is ibid.

Embodiment 1-5 is tested with comparative example 1-2, test effect is with foam back highly representing foamed elastic Size, the bigger explanation elasticity of foam back height are better, and the less explanation elasticity of foam back height is poorer.By following test number According to understanding, 1,2,3,4,5 foamed elastic effect of embodiment is substantially better than comparative example 1 and 2, illustrate -1 phosphate ester of laureth and Trehalose compounding use effect is significantly better than exclusive use.

Method of testing sees below：

1st, the clean skin of embodiment 1, embodiment 2, embodiment 3, embodiment 4, embodiment 5, comparative example 1, comparative example 2 is made up Product do some testing performance indexes, and its test is as follows：

1) outward appearance：Semi-transparent mucus

2) pH value：5.5-7.5

3) viscosity：5000-10000mpa.s

4) heat-resistant stability investigates (48 DEG C × 24H)：It is qualified

5) resist cold study on the stability (- 15 DEG C × 24H)：It is qualified

2nd, foamed elastic test：

1) method of testing：

Skin-cleaning cosmetics obtained by preparing spray the foam of identical height same volume in the middle of thumb, light with forefinger Flicking is depressed into a half height of original height, then the finger that comes up, record foam back height, calculate restore height with it is original The ratio of height, continuous pressing three times record foam back height after pressing every time, calculate the ratio of recovery height and original height Value.Each example retest three times, averages.

2) test data：

Foam back height	Embodiment 1	Embodiment 2	Embodiment 3	Embodiment 4	Embodiment 5	Comparative example 1	Comparative example 2
								Press for the first time	92%	93%	92%	90%	88%	90%	72%
Press for second	85%	87%	86%	83%	82%	76%	65%
								Third time is pressed	82%	85%	83%	79%	77%	68%	60%

3) test result：

Jing after three pressings, 1 foam back of embodiment height 82%, 2 foam back of embodiment height 85%, embodiment 3 Foam back height 83%, 4 foam back of embodiment height 79%, 5 foam back of embodiment height 77%, 1 foam of comparative example Restore height 68%, 2 foam back of comparative example height 60%.

4) efficiency assessment：

- 1 phosphate ester of laureth and trehalose of different proportion is with the addition of in the product, and its foamed elastic more individually adds Plus -1 phosphate ester of laureth increases 14-17%, more individually adding trehalose increases 22-25%, has the above-mentioned test result can Know, in the present invention, -1 phosphate ester of characteristic compositionss laureth and trehalose possess the effect for substantially increasing foamed elastic, Add the clean skin mousse that this compositions can prepare the Q bullets such as egg in skin-cleaning cosmetics.

3rd, security test：

1) test crowd：

Trial volunteer 105, man 39, female 66, age reckling 17 years old, the maximum 67 years old, mean age 34.76 Year.Dry skin 56, neutral skin 13 and oily skin 36.

2) method of testing：

Tester first drenches face with clear water, will prepare the skin-cleaning cosmetics of gained in centre of the palm ejection about Ovum Coturnicis japonicae size Foam, uniform application were rubbed in face and in the way of looping by one minute, then were cleaned with clear water, and observation whether there is discomfort in 5 minutes Or allergy.

3) test result：

Without allergic phenomena.

From above-mentioned test result, product of the present invention will not produce anaphylaxiss to user, using safety.

Above-described embodiment is only currently preferred case study on implementation, it is impossible to model required for protection of the invention is limited with this Enclose, the replacement of any unsubstantiality that those skilled in the art is done on the basis of the present invention belongs to application claims guarantor The scope of shield.

Claims (7)

1. a kind of clean skin mouse compositions, it is characterised in that using -1 phosphate ester of laureth and trehalose compounding as foaming Stabilization additives.

2. a kind of clean skin mouse compositions according to claim 1, it is characterised in that described -1 phosphoric acid of laureth The addition of ester is 1-15%, and the addition of the trehalose is 1-10%.

3. a kind of clean skin mouse compositions according to claim 1, it is characterised in that specifically include following weight percent and contain Amount component：

4. a kind of clean skin mouse compositions according to claim 1, it is characterised in that described -1 phosphoric acid of laureth The addition of ester is 5-8%, and the addition of the trehalose is 3-6%.

5. a kind of clean skin mouse compositions according to claim 1, it is characterised in that described -1 phosphoric acid of laureth Ester is 1-2 with the addition mass ratio of trehalose：1.

6. a kind of clean skin mouse compositions according to claim 3, it is characterised in that described propellant is propane, fourth One or more in alkane, iso-butane, dimethyl ether and its homologue.

7. clean skin mouse compositions any one of a kind of claim 1-6, it is characterised in that comprise the following steps：

A, A phase components are mixed and stirred for being warmed up to 80 DEG C, are uniformly dissolved；

B, addition B phases, C phase components are mixed and stirred for being uniformly dissolved, and start cooling；

C, 45 DEG C are cooled to, add D phase components, stir

D, material body produced above is poured in aerosol container in proportion, set up valve, pour into E phase components in proportion.