CN106578011A - Solid fruit and vegetable fresh keeping agent containing purple perilla essential oil - Google Patents

Solid fruit and vegetable fresh keeping agent containing purple perilla essential oil Download PDF

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Publication number
CN106578011A
CN106578011A CN201610993606.9A CN201610993606A CN106578011A CN 106578011 A CN106578011 A CN 106578011A CN 201610993606 A CN201610993606 A CN 201610993606A CN 106578011 A CN106578011 A CN 106578011A
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CN
China
Prior art keywords
quintessence oil
keeping agent
vegetable fresh
agent containing
fresh
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Pending
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CN201610993606.9A
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Chinese (zh)
Inventor
茅林春
苑佳佳
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Zhejiang University ZJU
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Zhejiang University ZJU
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Priority to CN201610993606.9A priority Critical patent/CN106578011A/en
Publication of CN106578011A publication Critical patent/CN106578011A/en
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    • AHUMAN NECESSITIES
    • A23FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
    • A23BPRESERVING, e.g. BY CANNING, MEAT, FISH, EGGS, FRUIT, VEGETABLES, EDIBLE SEEDS; CHEMICAL RIPENING OF FRUIT OR VEGETABLES; THE PRESERVED, RIPENED, OR CANNED PRODUCTS
    • A23B7/00Preservation or chemical ripening of fruit or vegetables
    • A23B7/14Preserving or ripening with chemicals not covered by groups A23B7/08 or A23B7/10
    • A23B7/153Preserving or ripening with chemicals not covered by groups A23B7/08 or A23B7/10 in the form of liquids or solids
    • A23B7/154Organic compounds; Microorganisms; Enzymes
    • AHUMAN NECESSITIES
    • A23FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
    • A23VINDEXING SCHEME RELATING TO FOODS, FOODSTUFFS OR NON-ALCOHOLIC BEVERAGES AND LACTIC OR PROPIONIC ACID BACTERIA USED IN FOODSTUFFS OR FOOD PREPARATION
    • A23V2002/00Food compositions, function of food ingredients or processes for food or foodstuffs

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  • Life Sciences & Earth Sciences (AREA)
  • Chemical & Material Sciences (AREA)
  • Engineering & Computer Science (AREA)
  • Microbiology (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • General Chemical & Material Sciences (AREA)
  • Wood Science & Technology (AREA)
  • Zoology (AREA)
  • Food Science & Technology (AREA)
  • Polymers & Plastics (AREA)
  • Medicines Containing Plant Substances (AREA)
  • Preparation Of Fruits And Vegetables (AREA)

Abstract

The invention discloses a solid fruit and vegetable fresh keeping agent containing purple perilla essential oil. The solid fruit and vegetable fresh keeping agent is prepared from the following raw material components in parts by weight: 40-60 parts of cyclodextrin, 1-4 parts of microcrystalline cellulose, 1-4 parts of calcium stearate, and 0.5-1 part of the purple perilla essential oil. According to the solid fruit and vegetable fresh keeping agent disclosed by the invention, the purple perilla essential oil is packed in solid materials, the using method is simple and convenient, and when the solid fruit and vegetable fresh keeping agent is exposed to air, effective components can be slowly released; and the fresh-keeping time of fruits and vegetables can be obviously prolonged, and the quality, the appearance and the like of the fruits and vegetables can be guaranteed.

Description

A kind of solid type fruit and vegetable fresh-keeping agent containing Fructus Perillae quintessence oil
Technical field
The present invention relates to a kind of fruit and vegetable fresh-keeping agent, more particularly to a kind of solid type fruit and vegetable fresh-keeping agent containing Fructus Perillae quintessence oil.
Background technology
It is the mankind rich in nutritional labelings such as substantial amounts of vitamin, organic acid, mineral element and antioxidant in fruit and vegerable Important component part in diet structure.However, fruit and vegerable are in postharvest storage transportation, infecting, breathing due to pathogen It is easily caused with the reason such as aging and rots so that fresh fruit of vegetables quality decline, brings about great losses.It is reported that, developed country Having 15%~25% fresh fruit of vegetables causes the phenomenon such as rotten in storage transportation because postharvest handling is improper.
Folium Perillae(Perilla frutescensL. Britt.), also known as red Soviet Union, Fructus Perillae, common perilla, ancient name is weak, is lip Mesh, Labiatae, Perilla annual herb plant, have the kind of more than one thousand years in Asian countries such as China, Japan, Korea, India Plant history.Its stem, leaf, seed can all be used as medicine, eat, and be one of 60 kinds of dietotherapeutic articles that ministry of Health of China is announced in the first batch. Fructus Perillae quintessence oil has the various biological function such as antibacterial, antiinflammatory, antioxidation.Research discovery, the perillaldehyde and lemon in Fructus Perillae quintessence oil Lemon alkene has synergism, can effectively suppress the growth of putrefaction bacteria.
Existing patent " efficient fresh-keeping method of Fructus Fragariae Ananssae fresh fruit "(Application number:201510299275.4)Add in fresh-keeping liquid Folium Perillae distillate, then Fructus Fragariae Ananssae is soaked in fresh-keeping liquid drain storage after 20-30 min.Though the method can reduce adopting for Fructus Fragariae Ananssae After rot, but workload is larger when operating, and fresh-keeping liquid easily makes fruit surface color change.Additionally, Folium Perillae distillation The antibacterial effect of liquid is not so good as Folium Perillae leaf essential oil.
The content of the invention
It is an object of the invention to provide a kind of solid type fruit and vegetable fresh-keeping agent containing Fructus Perillae quintessence oil, using the anti-of Fructus Perillae quintessence oil Bacterium effect, the problems such as solving fruit and vegerable and harvest later putrid and deteriorated.Meanwhile, tablet form is made, slow releasing function can be played, no It is more convenient when only using, and overcome the use defect of liquidpreservatives.
The technical solution adopted for the present invention to solve the technical problems is:
A kind of solid type fruit and vegetable fresh-keeping agent containing Fructus Perillae quintessence oil, by weight, is made up of following material composition:Cyclodextrin 40- 60 parts, Microcrystalline Cellulose 1-4 part, calcium stearate 1-4 parts, Fructus Perillae quintessence oil 0.5-1 parts.
Preferably, the Fructus Perillae quintessence oil is made by the steps and obtains:
(1)Fresh Folium Perillae blade is placed in in thermostatic drying chamber 60 DEG C and is dried 12h, 120 mesh sieves are crossed after crushing, obtain Folium Perillae Powder;Fresh Folium Perillae blade is to pluck from the Folium Perillae plant that Folium Perillae seedling age is 70 days or so.
(2)According to solid-liquid ratio 1g:The amount of 6mL adds Folium Perillae powder and distilled water, 2.1 h is soaked, using vapor distillation Method extracts 5.6 h, and with petroleum ether extraction Folium Perillae leaf essential oil crude extract is obtained.
(3)Fructus Perillae quintessence oil crude extract is blown down through nitrogen and removes petroleum ether, obtain Fructus Perillae quintessence oil.
A kind of preparation method of the solid type fruit and vegetable fresh-keeping agent containing Fructus Perillae quintessence oil, uniformly mixes each raw material according to formula ratio 20 min, plus water-wet, tablet is made in mixing, pelletize, drying after tabletting.The solid type fruit and vegetable fresh-keeping agent shape is not limited to In lamellar, or granule or other shapes.
Preferably, the piece weight of tablet is 1.0 ± 0.1 g.
Preferably, the solid type fruit and vegetable fresh-keeping agent is applied to fruits and vegetables harvests later anti-corrosive fresh-keeping, to tie up Hold the Post-harvest quality of fruits and vegetables.
The invention has the beneficial effects as follows:Fructus Perillae quintessence oil is inhibited to various fruit and vegerable putrefaction bacteria in the present invention, and pacifies Atoxic, makes low raw-material cost.Cyclodextrin inwall cavity, quintessence oil can be embedded wherein, delay the volatilization of quintessence oil, so as to Reach the purpose of slow release;Microcrystalline Cellulose, calcium stearate are conducive to various raw materials to be bonded into granule and compression molding.The present invention Obtained solid type fruit and vegetable fresh-keeping agent, Fructus Perillae quintessence oil is wrapped in solid material, and using method is simple and easy, is exposed to sky Effective ingredient can be slowly discharged in gas, the preserving fruit and vegetable utilizing time can be obviously prolonged, it is ensured that quality, outward appearance of fruit and vegerable etc..This It is bright simple to operate, can be had a good application prospect with large-scale production.
Specific embodiment
Below by specific embodiment, technical scheme is described in further detail.
In the present invention, if not refering in particular to, the raw material for being adopted and equipment etc. are commercially available or commonly used in the art. Method in following embodiments, if no special instructions, is the conventional method of this area.
Embodiment 1
The g of cyclodextrin 40, the g of Microcrystalline Cellulose 1, the g of calcium stearate 1, the g of Fructus Perillae quintessence oil 0.5 are taken, by the uniformly mixing 20 of each raw material Min, adds 12 g water, mixes, and makes wet grain.The wet grain of gained is placed in into 60 DEG C of h of drying 1 in baking oven and obtains dry particl, by dry Grain is pressed into the above-mentioned fruit and vegetable fresh-keeping agent containing Fructus Perillae quintessence oil, and piece weight is 1.0 ± 0.1 g.First banana is put into into plastics fresh-keeping In bag, then put into above-mentioned fruit and vegetable fresh-keeping agent(Add 1 antistaling agent per 10 kilograms of Fructus Musaes), and avoid antistaling agent straight with fruit as far as possible Contact, then seals freshness protection package, after depositing 25 days at 15 DEG C, rotting rate< 5%.
Embodiment 2
The g of cyclodextrin 50, the g of Microcrystalline Cellulose 2, the g of calcium stearate 2, the g of Folium Perillae leaf essential oil 0.8 are taken, by the uniformly mixing 20 of each raw material Min, adds 15 g water, mixes, and makes wet grain.The wet grain of gained is placed in in baking oven 60 DEG C it is dried 1h and obtains dry particl, will dry Grain is pressed into the above-mentioned fruit and vegetable fresh-keeping agent containing Folium Perillae leaf essential oil, and piece weight is 1.0 ± 0.1 g.Gained fruit and vegetable fresh-keeping agent is added and is wrapped In pack, vacuum sealed package is carried out, 10 per bag.First Fructus Vitis viniferae is put in fact in plastics freshness protection package, then puts into above-mentioned fruit and vegerable and protected Fresh dose(Add 2 antistaling agents per 10 kilograms of Fructus Vitis viniferaes), and the directly contact of antistaling agent and fruit is avoided as far as possible, then seal fresh-keeping Bag, after depositing 60 days at 5 DEG C, rotting rate< 3%.
Embodiment 3
The g of cyclodextrin 60, the g of Microcrystalline Cellulose 4, the g of calcium stearate 4, the g of Folium Perillae leaf essential oil 1 are taken, by the uniformly mixing 20 of each raw material Min, adds appropriate 18g water, mixes, and makes wet grain.The wet grain of gained is placed in in baking oven 60 DEG C it is dried 1h and obtains dry particl, will be dry Granule is pressed into the above-mentioned fruit and vegetable fresh-keeping agent containing Folium Perillae leaf essential oil, and piece weight is 1.0 ± 0.1 g.Gained fruit and vegetable fresh-keeping agent is added In packaging bag, vacuum sealed package is carried out, 10 per bag.First strawberry fruit is put in plastics freshness protection package, then puts into above-mentioned fruit Vegetable antistaling agent(Add 2 antistaling agents per 10 kilograms of Fructus Fragariae Ananssaes), and the directly contact of antistaling agent and fruit is avoided as far as possible, then sealing is protected Fresh bag, after depositing 20 days at 2 DEG C, rotting rate<5%.
Embodiment described above is one kind preferably scheme of the present invention, not makees any pro forma to the present invention Limit, also have other variants and remodeling on the premise of without departing from the technical scheme described in claim.

Claims (5)

1. a kind of solid type fruit and vegetable fresh-keeping agent containing Fructus Perillae quintessence oil, it is characterised in that by weight, by following material composition system Into:Cyclodextrin 40-60 parts, Microcrystalline Cellulose 1-4 part, calcium stearate 1-4 parts, Fructus Perillae quintessence oil 0.5-1 parts.
2. a kind of solid type fruit and vegetable fresh-keeping agent containing Fructus Perillae quintessence oil according to claim 1, it is characterised in that the Folium Perillae Quintessence oil is made by the steps and obtains:
(1)Fresh Folium Perillae blade is placed in in thermostatic drying chamber 60 DEG C and is dried 12h, 120 mesh sieves are crossed after crushing, obtain Folium Perillae Powder;
(2)According to solid-liquid ratio 1g:The amount of 6mL adds Folium Perillae powder and distilled water, soaks 2.1 h, is carried using steam distillation 5.6 h are taken, with petroleum ether extraction Folium Perillae leaf essential oil crude extract is obtained;
(3)Fructus Perillae quintessence oil crude extract is blown down through nitrogen and removes petroleum ether, obtain Fructus Perillae quintessence oil.
3. a kind of preparation method of solid type fruit and vegetable fresh-keeping agent containing Fructus Perillae quintessence oil according to claim 1, its feature exists In, each raw material is uniformly mixed 20 min, plus water-wet, mixing, pelletize, drying according to formula ratio, tablet is made after tabletting.
4. a kind of solid type fruit and vegetable fresh-keeping agent containing Fructus Perillae quintessence oil according to claim 3, it is characterised in that the piece of tablet Weight is 1.0 ± 0.1 g.
5. a kind of solid type fruit and vegetable fresh-keeping agent containing Fructus Perillae quintessence oil according to claim 1, it is characterised in that the solid Type fruit and vegetable fresh-keeping agent is applied to fruits and vegetables and harvests later anti-corrosive fresh-keeping, to maintain the Post-harvest quality of fruits and vegetables.
CN201610993606.9A 2016-11-11 2016-11-11 Solid fruit and vegetable fresh keeping agent containing purple perilla essential oil Pending CN106578011A (en)

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Cited By (4)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN107494719A (en) * 2017-09-18 2017-12-22 重庆市碾盘生态农业开发有限责任公司 The ventilative edible preserving fruit and vegetable utilizing film forming agent of one kind
CN108546590A (en) * 2018-04-20 2018-09-18 湖南农业大学 Application process of Fructus Perillae quintessence oil during citrus storage at normal temperature
CN108967520A (en) * 2018-05-24 2018-12-11 中北大学 A kind of preparation method and applications of Fructus Perillae quintessence oil micro-capsule
CN111213710A (en) * 2019-12-02 2020-06-02 浙江工商大学 Green-keeping preservative for broccoli and using method thereof

Citations (7)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN101602982A (en) * 2008-06-11 2009-12-16 湖北中烟工业有限责任公司 The step-by-step extracting method of purple perilla and extract obtained application in cigarette
CN101700009A (en) * 2009-11-05 2010-05-05 国家农产品保鲜工程技术研究中心(天津) Mustard essential oil biofungicide
CN102424770A (en) * 2011-10-10 2012-04-25 江苏兴野食品有限公司 Extraction technology of perilla frutescens essential oil
CN103478232A (en) * 2013-09-23 2014-01-01 浙江省农业科学院 Carvacrol slow release preservative and preparation method thereof
CN104824137A (en) * 2015-06-03 2015-08-12 铜陵新梦想农牧科技有限公司 Efficient preservation method of fresh strawberries
CN105001989A (en) * 2015-07-27 2015-10-28 河南红枫种苗股份有限公司 Euonymus japonicus essential oil and preparing method and application thereof
CN105123905A (en) * 2015-09-15 2015-12-09 齐鲁工业大学 Method for inhibiting potato sprouting

Patent Citations (7)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN101602982A (en) * 2008-06-11 2009-12-16 湖北中烟工业有限责任公司 The step-by-step extracting method of purple perilla and extract obtained application in cigarette
CN101700009A (en) * 2009-11-05 2010-05-05 国家农产品保鲜工程技术研究中心(天津) Mustard essential oil biofungicide
CN102424770A (en) * 2011-10-10 2012-04-25 江苏兴野食品有限公司 Extraction technology of perilla frutescens essential oil
CN103478232A (en) * 2013-09-23 2014-01-01 浙江省农业科学院 Carvacrol slow release preservative and preparation method thereof
CN104824137A (en) * 2015-06-03 2015-08-12 铜陵新梦想农牧科技有限公司 Efficient preservation method of fresh strawberries
CN105001989A (en) * 2015-07-27 2015-10-28 河南红枫种苗股份有限公司 Euonymus japonicus essential oil and preparing method and application thereof
CN105123905A (en) * 2015-09-15 2015-12-09 齐鲁工业大学 Method for inhibiting potato sprouting

Cited By (5)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN107494719A (en) * 2017-09-18 2017-12-22 重庆市碾盘生态农业开发有限责任公司 The ventilative edible preserving fruit and vegetable utilizing film forming agent of one kind
CN108546590A (en) * 2018-04-20 2018-09-18 湖南农业大学 Application process of Fructus Perillae quintessence oil during citrus storage at normal temperature
CN108967520A (en) * 2018-05-24 2018-12-11 中北大学 A kind of preparation method and applications of Fructus Perillae quintessence oil micro-capsule
CN111213710A (en) * 2019-12-02 2020-06-02 浙江工商大学 Green-keeping preservative for broccoli and using method thereof
CN111213710B (en) * 2019-12-02 2022-08-12 浙江工商大学 Green-keeping preservative for broccoli and using method thereof

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Application publication date: 20170426