CN106572689A - Method for manufacturing thickener composition - Google Patents
Method for manufacturing thickener composition Download PDFInfo
- Publication number
- CN106572689A CN106572689A CN201580040375.3A CN201580040375A CN106572689A CN 106572689 A CN106572689 A CN 106572689A CN 201580040375 A CN201580040375 A CN 201580040375A CN 106572689 A CN106572689 A CN 106572689A
- Authority
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- China
- Prior art keywords
- bonding agent
- manufacture method
- agent composition
- gum
- granules
- Prior art date
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- 239000000203 mixture Substances 0.000 title claims abstract description 67
- 238000004519 manufacturing process Methods 0.000 title claims abstract description 55
- 238000000034 method Methods 0.000 title claims abstract description 43
- 239000002562 thickening agent Substances 0.000 title abstract 3
- 239000007788 liquid Substances 0.000 claims abstract description 65
- 229920002907 Guar gum Polymers 0.000 claims abstract description 47
- 235000010417 guar gum Nutrition 0.000 claims abstract description 47
- 239000000665 guar gum Substances 0.000 claims abstract description 47
- 229960002154 guar gum Drugs 0.000 claims abstract description 47
- 239000008187 granular material Substances 0.000 claims abstract description 46
- 235000010491 tara gum Nutrition 0.000 claims abstract description 43
- 239000000213 tara gum Substances 0.000 claims abstract description 43
- 239000007864 aqueous solution Substances 0.000 claims abstract description 41
- 239000011230 binding agent Substances 0.000 claims abstract description 41
- 239000000843 powder Substances 0.000 claims abstract description 37
- 229920001282 polysaccharide Polymers 0.000 claims abstract description 29
- 239000005017 polysaccharide Substances 0.000 claims abstract description 29
- 230000008719 thickening Effects 0.000 claims abstract description 26
- 238000004090 dissolution Methods 0.000 claims abstract description 10
- 150000004676 glycans Chemical class 0.000 claims abstract 2
- 239000007767 bonding agent Substances 0.000 claims description 49
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 claims description 30
- 238000009818 secondary granulation Methods 0.000 claims description 17
- 229920001353 Dextrin Polymers 0.000 claims description 15
- 239000004375 Dextrin Substances 0.000 claims description 15
- 235000019425 dextrin Nutrition 0.000 claims description 15
- 235000005911 diet Nutrition 0.000 claims description 13
- 230000037213 diet Effects 0.000 claims description 13
- 229920001285 xanthan gum Polymers 0.000 claims description 11
- 239000000470 constituent Substances 0.000 claims description 10
- 235000010493 xanthan gum Nutrition 0.000 claims description 10
- 239000000230 xanthan gum Substances 0.000 claims description 10
- 229940082509 xanthan gum Drugs 0.000 claims description 10
- 239000003292 glue Substances 0.000 claims description 5
- 239000003795 chemical substances by application Substances 0.000 claims description 3
- 239000000853 adhesive Substances 0.000 claims description 2
- 230000001070 adhesive effect Effects 0.000 claims description 2
- 150000001720 carbohydrates Chemical class 0.000 claims description 2
- 239000002994 raw material Substances 0.000 abstract description 13
- 239000000243 solution Substances 0.000 abstract description 2
- 238000005507 spraying Methods 0.000 abstract description 2
- 239000006185 dispersion Substances 0.000 abstract 1
- 150000004804 polysaccharides Chemical class 0.000 description 27
- MSXHSNHNTORCAW-GGLLEASOSA-M sodium;(2s,3s,4s,5r,6s)-3,4,5,6-tetrahydroxyoxane-2-carboxylate Chemical compound [Na+].O[C@H]1O[C@H](C([O-])=O)[C@@H](O)[C@H](O)[C@H]1O MSXHSNHNTORCAW-GGLLEASOSA-M 0.000 description 11
- 230000000052 comparative effect Effects 0.000 description 6
- 238000005516 engineering process Methods 0.000 description 5
- WCUXLLCKKVVCTQ-UHFFFAOYSA-M Potassium chloride Chemical compound [Cl-].[K+] WCUXLLCKKVVCTQ-UHFFFAOYSA-M 0.000 description 4
- 229920002472 Starch Polymers 0.000 description 4
- 238000013329 compounding Methods 0.000 description 4
- 239000000463 material Substances 0.000 description 4
- 239000003607 modifier Substances 0.000 description 4
- 238000011084 recovery Methods 0.000 description 4
- 150000003839 salts Chemical group 0.000 description 4
- 235000019698 starch Nutrition 0.000 description 4
- 239000008107 starch Substances 0.000 description 4
- 208000019505 Deglutition disease Diseases 0.000 description 3
- 229920000161 Locust bean gum Polymers 0.000 description 3
- 244000269722 Thea sinensis Species 0.000 description 3
- 235000013305 food Nutrition 0.000 description 3
- 235000011389 fruit/vegetable juice Nutrition 0.000 description 3
- 235000010420 locust bean gum Nutrition 0.000 description 3
- 239000000711 locust bean gum Substances 0.000 description 3
- 239000002245 particle Substances 0.000 description 3
- 238000003756 stirring Methods 0.000 description 3
- 229920001817 Agar Polymers 0.000 description 2
- RGHNJXZEOKUKBD-SQOUGZDYSA-N D-gluconic acid Chemical compound OC[C@@H](O)[C@@H](O)[C@H](O)[C@@H](O)C(O)=O RGHNJXZEOKUKBD-SQOUGZDYSA-N 0.000 description 2
- 229920002683 Glycosaminoglycan Polymers 0.000 description 2
- FAPWRFPIFSIZLT-UHFFFAOYSA-M Sodium chloride Chemical compound [Na+].[Cl-] FAPWRFPIFSIZLT-UHFFFAOYSA-M 0.000 description 2
- 239000008272 agar Substances 0.000 description 2
- 235000010419 agar Nutrition 0.000 description 2
- 239000012752 auxiliary agent Substances 0.000 description 2
- 230000015572 biosynthetic process Effects 0.000 description 2
- 159000000007 calcium salts Chemical class 0.000 description 2
- 230000001055 chewing effect Effects 0.000 description 2
- 150000001875 compounds Chemical class 0.000 description 2
- 238000005469 granulation Methods 0.000 description 2
- 230000003179 granulation Effects 0.000 description 2
- 239000004615 ingredient Substances 0.000 description 2
- 210000003800 pharynx Anatomy 0.000 description 2
- XAEFZNCEHLXOMS-UHFFFAOYSA-M potassium benzoate Chemical compound [K+].[O-]C(=O)C1=CC=CC=C1 XAEFZNCEHLXOMS-UHFFFAOYSA-M 0.000 description 2
- 239000001103 potassium chloride Substances 0.000 description 2
- 235000011164 potassium chloride Nutrition 0.000 description 2
- 235000014347 soups Nutrition 0.000 description 2
- 230000001629 suppression Effects 0.000 description 2
- 235000013616 tea Nutrition 0.000 description 2
- ODIGIKRIUKFKHP-UHFFFAOYSA-N (n-propan-2-yloxycarbonylanilino) acetate Chemical compound CC(C)OC(=O)N(OC(C)=O)C1=CC=CC=C1 ODIGIKRIUKFKHP-UHFFFAOYSA-N 0.000 description 1
- IXPNQXFRVYWDDI-UHFFFAOYSA-N 1-methyl-2,4-dioxo-1,3-diazinane-5-carboximidamide Chemical compound CN1CC(C(N)=N)C(=O)NC1=O IXPNQXFRVYWDDI-UHFFFAOYSA-N 0.000 description 1
- GJCOSYZMQJWQCA-UHFFFAOYSA-N 9H-xanthene Chemical compound C1=CC=C2CC3=CC=CC=C3OC2=C1 GJCOSYZMQJWQCA-UHFFFAOYSA-N 0.000 description 1
- UXVMQQNJUSDDNG-UHFFFAOYSA-L Calcium chloride Chemical compound [Cl-].[Cl-].[Ca+2] UXVMQQNJUSDDNG-UHFFFAOYSA-L 0.000 description 1
- 240000007154 Coffea arabica Species 0.000 description 1
- 244000241257 Cucumis melo Species 0.000 description 1
- 235000015510 Cucumis melo subsp melo Nutrition 0.000 description 1
- 229920002558 Curdlan Polymers 0.000 description 1
- 239000001879 Curdlan Substances 0.000 description 1
- RGHNJXZEOKUKBD-SQOUGZDYSA-M D-gluconate Chemical compound OC[C@@H](O)[C@@H](O)[C@H](O)[C@@H](O)C([O-])=O RGHNJXZEOKUKBD-SQOUGZDYSA-M 0.000 description 1
- RGHNJXZEOKUKBD-UHFFFAOYSA-N D-gluconic acid Natural products OCC(O)C(O)C(O)C(O)C(O)=O RGHNJXZEOKUKBD-UHFFFAOYSA-N 0.000 description 1
- 108010010803 Gelatin Proteins 0.000 description 1
- 229920002148 Gellan gum Polymers 0.000 description 1
- DGAQECJNVWCQMB-PUAWFVPOSA-M Ilexoside XXIX Chemical compound C[C@@H]1CC[C@@]2(CC[C@@]3(C(=CC[C@H]4[C@]3(CC[C@@H]5[C@@]4(CC[C@@H](C5(C)C)OS(=O)(=O)[O-])C)C)[C@@H]2[C@]1(C)O)C)C(=O)O[C@H]6[C@@H]([C@H]([C@@H]([C@H](O6)CO)O)O)O.[Na+] DGAQECJNVWCQMB-PUAWFVPOSA-M 0.000 description 1
- 229920000057 Mannan Polymers 0.000 description 1
- 244000294411 Mirabilis expansa Species 0.000 description 1
- 235000015429 Mirabilis expansa Nutrition 0.000 description 1
- 229920000881 Modified starch Polymers 0.000 description 1
- 235000010451 Plantago psyllium Nutrition 0.000 description 1
- 244000090599 Plantago psyllium Species 0.000 description 1
- 239000004698 Polyethylene Substances 0.000 description 1
- HLCFGWHYROZGBI-JJKGCWMISA-M Potassium gluconate Chemical compound [K+].OC[C@@H](O)[C@@H](O)[C@H](O)[C@@H](O)C([O-])=O HLCFGWHYROZGBI-JJKGCWMISA-M 0.000 description 1
- 240000004584 Tamarindus indica Species 0.000 description 1
- 235000004298 Tamarindus indica Nutrition 0.000 description 1
- 235000006468 Thea sinensis Nutrition 0.000 description 1
- FJJCIZWZNKZHII-UHFFFAOYSA-N [4,6-bis(cyanoamino)-1,3,5-triazin-2-yl]cyanamide Chemical compound N#CNC1=NC(NC#N)=NC(NC#N)=N1 FJJCIZWZNKZHII-UHFFFAOYSA-N 0.000 description 1
- 235000010489 acacia gum Nutrition 0.000 description 1
- 239000001785 acacia senegal l. willd gum Substances 0.000 description 1
- 230000032683 aging Effects 0.000 description 1
- 235000010443 alginic acid Nutrition 0.000 description 1
- 239000000783 alginic acid Substances 0.000 description 1
- 229920000615 alginic acid Polymers 0.000 description 1
- 229960001126 alginic acid Drugs 0.000 description 1
- 150000004781 alginic acids Chemical class 0.000 description 1
- WQZGKKKJIJFFOK-VFUOTHLCSA-N beta-D-glucose Chemical compound OC[C@H]1O[C@@H](O)[C@H](O)[C@@H](O)[C@@H]1O WQZGKKKJIJFFOK-VFUOTHLCSA-N 0.000 description 1
- 235000020279 black tea Nutrition 0.000 description 1
- 239000001110 calcium chloride Substances 0.000 description 1
- 229910001628 calcium chloride Inorganic materials 0.000 description 1
- MKJXYGKVIBWPFZ-UHFFFAOYSA-L calcium lactate Chemical compound [Ca+2].CC(O)C([O-])=O.CC(O)C([O-])=O MKJXYGKVIBWPFZ-UHFFFAOYSA-L 0.000 description 1
- 239000001527 calcium lactate Substances 0.000 description 1
- 235000011086 calcium lactate Nutrition 0.000 description 1
- 229960002401 calcium lactate Drugs 0.000 description 1
- 235000010418 carrageenan Nutrition 0.000 description 1
- 239000000679 carrageenan Substances 0.000 description 1
- 229920001525 carrageenan Polymers 0.000 description 1
- 229940113118 carrageenan Drugs 0.000 description 1
- 235000016213 coffee Nutrition 0.000 description 1
- 235000013353 coffee beverage Nutrition 0.000 description 1
- 238000012790 confirmation Methods 0.000 description 1
- 235000019316 curdlan Nutrition 0.000 description 1
- 229940078035 curdlan Drugs 0.000 description 1
- 230000000694 effects Effects 0.000 description 1
- 238000005485 electric heating Methods 0.000 description 1
- 229920000159 gelatin Polymers 0.000 description 1
- 239000008273 gelatin Substances 0.000 description 1
- 235000019322 gelatine Nutrition 0.000 description 1
- 235000011852 gelatine desserts Nutrition 0.000 description 1
- 235000010492 gellan gum Nutrition 0.000 description 1
- 239000000216 gellan gum Substances 0.000 description 1
- 229940050410 gluconate Drugs 0.000 description 1
- 235000012208 gluconic acid Nutrition 0.000 description 1
- 239000000174 gluconic acid Substances 0.000 description 1
- 238000009413 insulation Methods 0.000 description 1
- 159000000003 magnesium salts Chemical class 0.000 description 1
- 229910052751 metal Inorganic materials 0.000 description 1
- 239000002184 metal Substances 0.000 description 1
- 235000013336 milk Nutrition 0.000 description 1
- 239000008267 milk Substances 0.000 description 1
- 210000004080 milk Anatomy 0.000 description 1
- 235000013536 miso Nutrition 0.000 description 1
- 239000003595 mist Substances 0.000 description 1
- 235000019426 modified starch Nutrition 0.000 description 1
- 239000004570 mortar (masonry) Substances 0.000 description 1
- 150000007524 organic acids Chemical class 0.000 description 1
- 235000010987 pectin Nutrition 0.000 description 1
- 229920001277 pectin Polymers 0.000 description 1
- 239000001814 pectin Substances 0.000 description 1
- 230000000704 physical effect Effects 0.000 description 1
- -1 polyethylene Polymers 0.000 description 1
- 229920000573 polyethylene Polymers 0.000 description 1
- 235000013926 potassium gluconate Nutrition 0.000 description 1
- 239000004224 potassium gluconate Substances 0.000 description 1
- 229960003189 potassium gluconate Drugs 0.000 description 1
- 238000002360 preparation method Methods 0.000 description 1
- 238000005204 segregation Methods 0.000 description 1
- 239000011734 sodium Substances 0.000 description 1
- 229910052708 sodium Inorganic materials 0.000 description 1
- 235000010413 sodium alginate Nutrition 0.000 description 1
- 239000000661 sodium alginate Substances 0.000 description 1
- 229940005550 sodium alginate Drugs 0.000 description 1
- 239000011780 sodium chloride Substances 0.000 description 1
- 159000000000 sodium salts Chemical class 0.000 description 1
- 241000894007 species Species 0.000 description 1
- 230000008961 swelling Effects 0.000 description 1
- 239000008399 tap water Substances 0.000 description 1
- 235000020679 tap water Nutrition 0.000 description 1
- 210000003437 trachea Anatomy 0.000 description 1
- 229920003169 water-soluble polymer Polymers 0.000 description 1
- UHVMMEOXYDMDKI-JKYCWFKZSA-L zinc;1-(5-cyanopyridin-2-yl)-3-[(1s,2s)-2-(6-fluoro-2-hydroxy-3-propanoylphenyl)cyclopropyl]urea;diacetate Chemical compound [Zn+2].CC([O-])=O.CC([O-])=O.CCC(=O)C1=CC=C(F)C([C@H]2[C@H](C2)NC(=O)NC=2N=CC(=CC=2)C#N)=C1O UHVMMEOXYDMDKI-JKYCWFKZSA-L 0.000 description 1
Classifications
-
- A—HUMAN NECESSITIES
- A23—FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
- A23L—FOODS, FOODSTUFFS, OR NON-ALCOHOLIC BEVERAGES, NOT COVERED BY SUBCLASSES A21D OR A23B-A23J; THEIR PREPARATION OR TREATMENT, e.g. COOKING, MODIFICATION OF NUTRITIVE QUALITIES, PHYSICAL TREATMENT; PRESERVATION OF FOODS OR FOODSTUFFS, IN GENERAL
- A23L29/00—Foods or foodstuffs containing additives; Preparation or treatment thereof
- A23L29/20—Foods or foodstuffs containing additives; Preparation or treatment thereof containing gelling or thickening agents
-
- A—HUMAN NECESSITIES
- A23—FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
- A23L—FOODS, FOODSTUFFS, OR NON-ALCOHOLIC BEVERAGES, NOT COVERED BY SUBCLASSES A21D OR A23B-A23J; THEIR PREPARATION OR TREATMENT, e.g. COOKING, MODIFICATION OF NUTRITIVE QUALITIES, PHYSICAL TREATMENT; PRESERVATION OF FOODS OR FOODSTUFFS, IN GENERAL
- A23L29/00—Foods or foodstuffs containing additives; Preparation or treatment thereof
- A23L29/20—Foods or foodstuffs containing additives; Preparation or treatment thereof containing gelling or thickening agents
- A23L29/206—Foods or foodstuffs containing additives; Preparation or treatment thereof containing gelling or thickening agents of vegetable origin
- A23L29/238—Foods or foodstuffs containing additives; Preparation or treatment thereof containing gelling or thickening agents of vegetable origin from seeds, e.g. locust bean gum or guar gum
-
- A—HUMAN NECESSITIES
- A23—FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
- A23L—FOODS, FOODSTUFFS, OR NON-ALCOHOLIC BEVERAGES, NOT COVERED BY SUBCLASSES A21D OR A23B-A23J; THEIR PREPARATION OR TREATMENT, e.g. COOKING, MODIFICATION OF NUTRITIVE QUALITIES, PHYSICAL TREATMENT; PRESERVATION OF FOODS OR FOODSTUFFS, IN GENERAL
- A23L29/00—Foods or foodstuffs containing additives; Preparation or treatment thereof
- A23L29/20—Foods or foodstuffs containing additives; Preparation or treatment thereof containing gelling or thickening agents
- A23L29/269—Foods or foodstuffs containing additives; Preparation or treatment thereof containing gelling or thickening agents of microbial origin, e.g. xanthan or dextran
-
- A—HUMAN NECESSITIES
- A23—FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
- A23V—INDEXING SCHEME RELATING TO FOODS, FOODSTUFFS OR NON-ALCOHOLIC BEVERAGES AND LACTIC OR PROPIONIC ACID BACTERIA USED IN FOODSTUFFS OR FOOD PREPARATION
- A23V2002/00—Food compositions, function of food ingredients or processes for food or foodstuffs
-
- A—HUMAN NECESSITIES
- A23—FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
- A23V—INDEXING SCHEME RELATING TO FOODS, FOODSTUFFS OR NON-ALCOHOLIC BEVERAGES AND LACTIC OR PROPIONIC ACID BACTERIA USED IN FOODSTUFFS OR FOOD PREPARATION
- A23V2300/00—Processes
- A23V2300/34—Membrane process
Landscapes
- Chemical & Material Sciences (AREA)
- Dispersion Chemistry (AREA)
- Health & Medical Sciences (AREA)
- Nutrition Science (AREA)
- Life Sciences & Earth Sciences (AREA)
- Engineering & Computer Science (AREA)
- Food Science & Technology (AREA)
- Polymers & Plastics (AREA)
- Jellies, Jams, And Syrups (AREA)
Abstract
Provided is a method for manufacturing a thickener composition in which lumping is minimized even when used on a high-temperature liquid, and high dispersion performance is maintained. A method for manufacturing a thickener composition is performed, said method including: (a) a step for spraying an aqueous solution containing guar gum or tara gum as a binder solution onto a raw material powder containing a thickening polysaccharide as the main component, and obtaining granules; and (b) a step for obtaining a mixture of the granules obtained in step (a) and a dissolution aid.
Description
Technical field
Even if the present invention relates to can also suppress the bonding agent composition of the formation of block when used in high-temp liquid
Manufacture method, in more detail, is related to the manufacture method of the bonding agent composition with following step (a) He step (b), described
Step (a) is on the powder stock containing thickening polysaccharide as main constituent, by the aqueous solution containing guar gum or tara gum
Sprayed as binding agent liquid, the step of obtain granules;The step (b) is the granules for obtaining gained in step (a)
The step of with the mixture of dissolution aids.
Background technology
The people for causing the chewing/dysphagia of ingesta due to aging etc. are in the low diet of particularly intake viscosity
During thing, there is the danger for producing the mistake pharynx for mistakenly making ingesta flow into trachea.In order to prevent the mistake pharynx, the drink low for viscosity
Food, can use the consistency modifiers for giving the viscosity for being suitable to swallow.For consistency modifiers, the thickening headed by xanthan gum is more
Saccharide can be used as adhesion-promoting components.But, viscosify polysaccharide itself powder by contacting with water, contact surface start it is drastically swelling,
Condense between adjacent granule, the inside for being formed in agglomerate has so-called " block " without the part contacted with water.Shape
Dissolubility into the thickening polysaccharide of block is reduced, it is impossible to give ingesta sufficient viscosity.
In order to suppress the formation of the block, by the pelletize together with the powder beyond thickening polysaccharide of thickening polysaccharide, resistance
Hinder the attachment with adjacent thickening polysaccharide granule caused by thickening polysaccharide granules swell, the suppression for seeking block to be formed
System.In the pelletize, in order that the material for boning between granule and using is referred to as binding agent, in the increasing as consistency modifiers etc.
In the preparation of adhesive composition, for the purpose of the improvement for condensing suppression, various binding agents have been used.
Patent Document 1 discloses and sprayed dextrin in aqueous solution as binding agent liquid, by thickening polysaccharide pelletize
Technology.Patent Document 2 discloses using producing starch aqueous solution as binding agent liquid, by the technology of thickening polysaccharide pelletize.
Patent Document 3 discloses using containing organic acid, acylate aqueous solution as binding agent, by water soluble polymer pelletize
Technology.Patent Document 4 discloses in addition using containing gluconic acid, gluconate aqueous solution as binding agent, by xanthan gum etc.
Thickening polysaccharide pelletize technology.
Although however, with the bonding agent composition of these prior art manufactures in the cryogenic liquid for water, juice etc.
Certain dispersibility is shown, but in the high-temp liquid for tea, soup etc., can not still suppress the generation of block, it is impossible to fast
Speed gives the suitable viscosity of ingesta as chewing, dysphagia person.
Prior art literature
Patent documentation
Patent documentation 1:Japanese Unexamined Patent Publication 2011-229440 publications
Patent documentation 2:Japanese Unexamined Patent Publication 2004-147567 publications
Patent documentation 3:Japanese Unexamined Patent Publication 2009-001532 publications
Patent documentation 4:Japanese Unexamined Patent Publication 2008-161092 publications
The content of the invention
The invention problem to be solved
Even if the problem of the present invention is to provide and can also suppress the generation of block when used in the liquid of high temperature, remain high
The manufacture method of the bonding agent composition of dispersibility.
Solve the scheme of problem
The present inventor etc. have carried out making great efforts research to solve above-mentioned problem, as a result find to draw containing guar gum or tower
The aqueous solution of glue is sprayed, pelletize as binding agent liquid to viscosifying polysaccharide, and in the granules dissolution aids are added
Afterwards, even if the bonding agent composition of the dispersibility for displaying that high in the liquid of high temperature as a result can be manufactured, so as to complete this
Invention.
That is, the present invention is invention disclosed as follows.
(1) manufacture method of bonding agent composition, it is characterised in that have steps of (a) and (b), (a) containing increasing
Mucopolysaccharide is sprayed as on the powder stock of main constituent using the aqueous solution containing guar gum or tara gum as binding agent liquid
Mist and the step of obtain granules;The step of b () obtains the mixture of the granules of gained and dissolution aids in step (a).
(2) manufacture method of the bonding agent composition according to above-mentioned (1), it is characterised in that in step (a), phase
For the mass parts of powder stock 100, the guar gum or tara gum in the aqueous solution containing guar gum or tara gum is 0.01~0.5
Mass parts.
(3) manufacture method of the bonding agent composition according to above-mentioned (1) or (2), it is characterised in that in step (a)
In, using the powder stock or binding agent liquid that are compounded with slaine.
(4) manufacture method of the bonding agent composition according to any one of above-mentioned (1)~(3), it is characterised in that make
The granules in step (a) are sieved with the sieve that mesh is more than 1000 μm and sieve that mesh is less than 300 μm.
(5) manufacture method of the bonding agent composition according to any one of above-mentioned (1)~(4), it is characterised in that also
With following step (c),
On secondary powder stock of the c mixture that () obtains in containing step (b) as main constituent, guar gum will be contained
Or the aqueous solution or water of tara gum as binding agent liquid the step of sprayed and obtained secondary granulation thing.
(6) manufacture method of the bonding agent composition according to above-mentioned (5), it is characterised in that in step (c), phase
For the mass parts of secondary powder stock 100, the guar gum or tara gum in the aqueous solution containing guar gum or tara gum is 0.01
~0.5 mass parts.
(7) manufacture method of the bonding agent composition according to above-mentioned (5) or (6), it is characterised in that be using mesh
More than 1000 μm of sieve and mesh are that less than 300 μm of sieve is sieved the granules of gained in step (c).
(8) manufacture method of the bonding agent composition according to any one of above-mentioned (1)~(7), it is characterised in that increase
Mucopolysaccharide is xanthan gum.
(9) manufacture method of the bonding agent composition according to any one of above-mentioned (1)~(8), it is characterised in that molten
Enzymolysis auxiliary agent is dextrin.
(10) manufacture method of the bonding agent composition according to any one of above-mentioned (1)~(9), it is characterised in that
Bonding agent composition is applicable to the liquid of more than 60 DEG C of high temperature.
(11) diet product, it is characterised in that containing using the manufacture method manufacture any one of above-mentioned (1)~(10)
Bonding agent composition.
The effect of invention
Even if according to the present invention it is possible to manufacturing not only low temperature but also can also suppress block when used in high-temp liquid
Generation, maintain the bonding agent composition of high dispersibility.Due to the generation of block can be suppressed, with polymolecularity, therefore
Can serve as giving using the bonding agent composition of present invention manufacture and be suitable to diet product, particularly chew, swallow suffering person's
The diet usable consistency modifiers of the viscosity of diet product.
Specific embodiment
As the manufacture method of the bonding agent composition of the present invention, as long as there are the viscosifier of following step (a) and (b)
The manufacture method of compositionss is just not particularly limited, and the step (a) is in the powder for containing thickening polysaccharide as main constituent
On raw material, sprayed the aqueous solution containing guar gum or tara gum as binding agent liquid, the step of obtain granules;It is described
Step (b) is the step of obtaining the mixture of the granules of gained and dissolution aids in step (a), and then preferably has step
C (), the step (c) is on secondary powder stock of the mixture of the gained in containing step (b) as main constituent, will to contain melon
The aqueous solution or water of your glue or tara gum is sprayed as binding agent liquid, the step of obtain secondary granulation thing.By with step
Suddenly (c), the segregation of the powder body for stockpiling medium generation in the bonding agent composition for manufacturing can more be reduced.
In the present invention, viscosify polysaccharide and refer to the high-viscosity water miscible polysaccharide of display, as the thickening polysaccharide
Class, can enumerate xanthan gum, carrageenan, arabic gum, locust bean gum, curdlan, tamarind gum, guar gum, tara gum,
Pulullan polysaccharide, pectin, gellan gum, alginic acid, psyllium seed gum, it may be preferred to enumerate xanthan gum.In addition, respectively viscosifying polysaccharide not
Can use by its salt form.
As containing thickening polysaccharide as main constituent powder stock, as long as containing above-mentioned thickening polysaccharide as it is main into
Point, thickening polysaccharide can contain a kind, can also contain two or more, but during containing two or more, preferably comprise xanthan
Glue.
In containing thickening powder stock of the polysaccharide as main constituent, it is also possible to containing less than 50 mass %, preferably little
Composition beyond 25 mass %, the thickening polysaccharide of more preferably less than 10 mass %, beyond the thickening polysaccharide
Composition, can enumerate starch derivatives, calcium salt, the sodium of gelating agent, dextrin, the starch of mannan, agar, gelatin etc. etc.
The salt of salt, potassium salt, magnesium salt etc..
In the present invention, as the aqueous solution containing guar gum or tara gum, as long as containing guar gum or tara gum
The aqueous solution of at least one is just not particularly limited, or the aqueous solution containing guar gum and tara gum, can will be described
Aqueous solution is used as binding agent liquid.Should illustrate, binding agent liquid is referred to make the table of particles of powdered ingredient when granules are obtained
Face is dissolved a little or in order to be made to be bondd between particles of powdered ingredient using the composition contained by binding agent liquid, and in raw material powder
The liquid of water, the aqueous solution added in end etc..
In the step (a) of the present invention, the binding agent liquid used when granules are obtained is containing guar gum or tara gum
Aqueous solution, in step (c), the binding agent liquid for obtaining being used during secondary granulation thing is water-soluble containing guar gum or tara gum
Liquid or water, it may be preferred to enumerate the aqueous solution containing guar gum or tara gum.
Can also be in the powder stock of the step (a) of the present invention or binding agent liquid, the secondary powder stock of step (c) or viscous
Slaine is compounded in Mixture Liquid.In thickening polysaccharide, having cause dissolubility, the change of viscosity expression power due to the metal for coexisting
Material, by the addition of slaine, scalable will be added to using the bonding agent composition that obtains of manufacture method of the present invention
Physical property when in diet product etc..As described slaine, can enumerate gluconic acid sodium salt, sodium alginate, Sodium Chloride etc. sodium salt,
Calcium salt of potassium salt, calcium lactate, the calcium chloride of potassium gluconate, potassium chloride etc. etc. etc..
In the present invention, as dissolution aids, as long as auxiliary thickening polysaccharide dissolving, i.e. hinder thickening polysaccharide it
Between cohesion material, dextrin, starch, reduction starch sugar compound etc. can be enumerated, it may be preferred to enumerate dextrin.By
Mixed dissolution auxiliary agent in granules obtained by step (a), can be produced in the liquid of high temperature and show the thickening of high dispersibility
Agent compositionss.
In the step (a) of the present invention, relative to the mass parts of powder stock 100, the water containing guar gum or tara gum
Guar gum or tara gum amount in solution can enumerate 0.01~0.5 mass parts, preferably enumerate 0.1~0.3 mass parts.
In addition, in the step (b) of the present invention, in the mixture of the granules obtained by step (a) and dissolution aids, phase
For the dissolution aids amount of the mass parts of granules 100 obtained by step (a) can enumerate 50~300 mass parts, preferably enumerate 80
~150 mass parts.
Further, in the step (c) of the present invention, relative to containing mixture (the viscosifier combination obtained by step (b)
Thing) as the mass parts of secondary powder stock 100 of main constituent, the guar gum or tower in the aqueous solution containing guar gum or tara gum
Glue amount is drawn to enumerate 0.01~0.5 mass parts, preferably enumerate 0.05~0.2 mass parts.
In the present invention, as the method for obtaining granules, it is not particularly limited, can enumerates using fluidized bed pelletize
The method that the comminutor of machine, stirring granulating machine, extruding granulator, rotational flow layer comminutor etc. obtains granules.
For granules, secondary granulation thing (the secondary viscosifier group obtained by step (c) obtained by step (a) of the invention
Compound), preferably use sieve and sieved, more preferably using the sieve that mesh is more than 1000 μm and sieve that mesh is less than 300 μm
Sieved.Sieved by described, eliminate powder material, crisp granules and big block for being unable to pelletize etc., it is possible thereby to
Further suppress the generation of block in dissolving.
Using the bonding agent composition that obtains of manufacture method of the bonding agent composition of the present invention be applicable to more than 60 DEG C,
It is preferred that the liquid of more than 70 DEG C of high temperature.The bonding agent composition manufactured with the manufacture method of conventional bonding agent composition exists
Show certain dispersibility in the cryogenic liquid of water, juice etc., but more than 60 DEG C at a high temperature of exist and produce block so
Problem.Even if however, using the bonding agent composition that obtains of manufacture method of the present invention suitable for more than 60 DEG C of liquid,
The generation of block can be suppressed, high dispersibility is shown.
As the diet product of the present invention, as long as the manufacture of the manufacture method containing the bonding agent composition using the present invention
The diet product of bonding agent composition, is just not particularly limited, and as diet product, can enumerate tea, black tea, coffee, soup, miso
Juice, warm milk etc..As the compounding amount of bonding agent composition, can suitably be adjusted according to the species of diet product, relative to drink
The mass parts of food 100, can enumerate 0.2~5 mass parts, preferably enumerate 1~4 mass parts.By using the manufacture method of the present invention
When the bonding agent composition for obtaining is added in these diet products, high dispersibility can be shown, suppress the generation of block, be assigned
Give purpose viscosity.
The preferred embodiment of the present invention is below described, but these embodiments do not limit the scope of the present invention.Should
Illustrate, for the comminutor and granulation conditions in below example, raw material, the dispersivity test in high-temp liquid, such as
Described below.
(comminutor and granulation conditions)
Comminutor uses the fluidized bed nodulizer FLO-5A of Off ロ イ Application ト company systems, in 80 DEG C of suction temperature, air-breathing wind
1~2.7m of amount3, nozzle exit pressure 0.2MPa (170L/min), spraying 30~52g/min of liquid speed under conditions of carry out pelletize, obtain
Granules.
(raw material)
In the raw material for using in the form of a powder, for more than 120 μm of salt of mean diameter, from the workability of pelletize
From the point of view of, carry out crushing as target exploitation mortar or grinder to use with 100 μm of mean diameter.
(dispersivity test in high-temp liquid)
The tap water of 100g home-use electric-heating kettle thermal-insulations to 90 DEG C (± 5 DEG C) is measured in the beaker of 300ml capacity,
Measure after bonding agent composition 2.5g in measuring cup, the moment for reaching 70 DEG C (± 5 DEG C) in water temperature disposably adds whole amount.It is quiet
The stirring (about 25 turns/10 seconds) of 30 seconds is carried out with stirring rod after putting 3 seconds, the confirmation of dissolved state is then carried out rapidly, with the institute of table 1
The benchmark for showing is evaluated, and for A, B, is evaluated as meeting the requirement level of dispersibility.
[table 1]
Comment | The number of block |
A valencys | 0-10 |
B | 11-20 |
C | 21-30 |
D | 31< |
Embodiment 1
(Production Example 1 of bonding agent composition)
Using xanthan gum and gluconic acid sodium salt as powder stock, the aqueous solution that guar gum or tara gum have been dissolved in water is made
For binding agent liquid, sprayed, pelletize, obtained granules.As comparative example, made using the aqueous solution that dextrin is dissolved in the water
For binding agent liquid.The granules of gained are sieved using the sieve that mesh is 1400 μm and 150 μm, recovery particle diameter 150~
1400 μm of the product that sieve.
The product 6g and dextrin 6g that sieves of the granules of recovery is mixed in the bag of polyethylene, obtain enforcement product 1,2, ratio
Compared with product 1.Enforcement product, the compounding for comparing the raw material in the respective granules of product are shown in table 2.For product 1,2 are implemented, in granules
In manufacture, relative to the mass parts of powder stock 100, guar gum or tara gum are 0.2 mass parts.
[table 2]
(g)
(result)
Enforcement product 1,2, the result that compares dispersivity test of the product 1 in high-temp liquid are shown in table 3.As shown in table 3 that
Sample, for enforcement product 1,2 of the aqueous solution containing guar gum or tara gum as the binding agent liquid of pelletize have been used, in high-temperature liquid
High dispersibility is shown in body.
[table 3]
Solubility test is evaluated | |
Enforcement product 1 | A |
Enforcement product 2 | A |
Compare product 1 | G |
Embodiment 2
(Production Example 2 of bonding agent composition)
Using xanthan gum as powder stock, gluconic acid sodium salt, guar gum or gluconic acid sodium salt and tara gum will be dissolved in water
Aqueous solution as binding agent liquid, sprayed, pelletize, obtain a granules.As comparative example, dissolve using in water
The aqueous solution of gluconic acid sodium salt or gluconic acid sodium salt and dextrin is used as binding agent liquid.By a granules of gained, with embodiment 1
Same method is sieved, and reclaims the product that sieve.
By sieve product and the dextrin mixing of the granules for reclaiming, secondary granulation raw material is made, will be dissolved in water
The aqueous solution of gluconic acid sodium salt and guar gum or gluconic acid sodium salt and tara gum is sprayed, pelletize as binding agent liquid, obtains two
Secondary granules.As comparative example, using the aqueous solution of gluconic acid sodium salt or gluconic acid sodium salt and dextrin has been dissolved in water as bonding
Agent liquid.Secondary granulation thing is sieved under conditions of same as described above, recovery is sieved product, obtain enforcement product 3,4, compare product
2、3.Enforcement product, the compounding for comparing the respective raw material of product are shown in table 4.Should illustrate, for product 3,4 are implemented, in a granules
Manufacture in, relative to the mass parts of powder stock 100, guar gum or tara gum are 0.15 mass parts, in the system of secondary granulation thing
In making, relative to the mass parts of secondary powder stock 100, guar gum or tara gum are 0.07 mass parts.
[table 4]
(g)
(result)
Enforcement product 3,4, the result that compares dispersivity test of the product 2,3 in high-temp liquid are shown in table 5.As shown in table 5
Like that, for enforcement product 3,4 of the aqueous solution containing guar gum or tara gum as binding agent liquid have been used, in high-temp liquid
Show high dispersibility.
[table 5]
Solubility test is evaluated | |
Enforcement product 3 | B |
Enforcement product 4 | B |
Compare product 2 | D |
Compare product 3 | D |
Embodiment 3
(Production Example 3 of bonding agent composition)
Using xanthan gum and gluconic acid sodium salt as powder stock, the aqueous solution that guar gum or tara gum have been dissolved in water is made
For binding agent liquid, sprayed, pelletize, obtained a granules.As comparative example, dextrin is dissolved using water or in water
Aqueous solution as binding agent liquid.Granules of gained are sieved with method similarly to Example 1, recovery is sieved
Product.
The product that sieve of the granules for reclaiming are mixed with dextrin, secondary granulation raw material is made, will be dissolved in water
The aqueous solution or water of guar gum or tara gum is sprayed, pelletize as binding agent liquid, obtains secondary granulation thing.As comparing
Example, the aqueous solution of dextrin has been dissolved using water or in water as binding agent liquid.By secondary granulation thing in bar same as described above
Sieved under part, reclaimed the product that sieve, obtained enforcement product 5~8, compare product 4,5.Enforcement product, compare matching somebody with somebody for the respective raw material of product
It is mixed to be shown in table 6.For product 5~8 are implemented, in the manufacture of a granules, relative to the mass parts of powder stock 100, guar gum
Or tara gum is 0.21 mass parts, for product 5,6 are implemented, in the manufacture of secondary granulation thing, relative to secondary powder stock 100
Mass parts, guar gum or tara gum are 0.07 mass parts.
[table 6]
(g)
(result)
Enforcement product 5~8, the result for comparing dispersivity test of the product 4,5 in high-temp liquid are shown in table 7.As shown in table 7
Like that, for having used enforcement product 5~8 of the aqueous solution containing guar gum or tara gum as the binding agent liquid of a pelletize,
High dispersibility is shown in high-temp liquid.In addition, as the binding agent liquid in secondary granulation, it is clear that can also be water.
[table 7]
Solubility test is evaluated | |
Enforcement product 5 | A |
Enforcement product 6 | A |
Enforcement product 7 | B |
Enforcement product 8 | A |
Compare product 4 | D |
Compare product 5 | D |
Embodiment 4
(Production Example 4 of bonding agent composition)
Using xanthan gum, agar, locust bean gum, guar gum and KCl as powder stock, will dissolve in water guar gum or
The aqueous solution of tara gum is sprayed as binding agent liquid, pelletize, obtains a granules.As comparative example, using water as
Binding agent liquid.Granules of gained are sieved with method similarly to Example 1, the product that sieve are reclaimed.
The product that sieve of the granules for reclaiming are mixed with dextrin and as secondary granulation raw material, will be dissolved in water
The aqueous solution of guar gum or tara gum is sprayed as binding agent liquid, pelletize, obtains secondary granulation thing.As comparative example, make
With water as binding agent liquid.Secondary granulation thing is sieved under conditions of same as described above, the product that sieve are reclaimed, is implemented
Product 9,10, compare product 6.Enforcement product, the compounding for comparing the respective raw material of product are shown in table 8.For product 9,10 are implemented, in a pelletize
In the manufacture of thing, relative to the mass parts of powder stock 100, guar gum or tara gum is set to be 0.15 mass parts, in secondary granulation thing
Manufacture in, relative to the mass parts of secondary powder stock 100, make guar gum or tara gum be 0.07 mass parts.
[table 8]
(g)
(result)
Enforcement product 9,10, the result that compares dispersivity test of the product 6 in high-temp liquid are shown in table 9.As shown in table 9 that
Sample, for having used enforcement product 9,10 of the aqueous solution containing guar gum or tara gum as the binding agent liquid of a pelletize,
High dispersibility is shown in high-temp liquid.In addition, as thickening polysaccharide, it is clear that locust bean gum, guar gum can also be used.
[table 9]
Solubility test is evaluated | |
Enforcement product 9 | B |
Enforcement product 10 | B |
Compare product 6 | D |
Industrial Availability
Manufacturing method according to the invention, even if can manufacture can also suppress when used in high-temp liquid block
Produce, maintain the bonding agent composition of high dispersibility, can in diet product field, particularly chew, the drink of dysphagia person
It is advantageously employed in field of food.
Claims (11)
1. the manufacture method of bonding agent composition, it is characterised in that have steps of (a) and (b),
A () makees the aqueous solution containing guar gum or tara gum on the powder stock containing thickening polysaccharide as main constituent
Sprayed for binding agent liquid, the step of obtain granules;
The step of b () obtains the mixture of the granules of gained and dissolution aids in step (a).
2. the manufacture method of bonding agent composition according to claim 1, it is characterised in that in step (a), relative to
The mass parts of powder stock 100, the guar gum or tara gum in the aqueous solution containing guar gum or tara gum is 0.01~0.5 mass
Part.
3. the manufacture method of bonding agent composition according to claim 1 and 2, it is characterised in that in step (a), make
With the powder stock or binding agent liquid that are compounded with slaine.
4. the manufacture method of the bonding agent composition according to any one of claims 1 to 3, it is characterised in that use net
Hole is that more than 1000 μm of sieve and sieve that mesh is less than 300 μm are sieved the granules in step (a).
5. the manufacture method of the bonding agent composition according to any one of Claims 1 to 4, it is characterised in that also have
Following step (c),
On secondary powder stock of the c mixture that () obtains in containing step (b) as main constituent, will be containing guar gum or tower
The step of drawing the aqueous solution or water of glue to be sprayed as binding agent liquid and obtained secondary granulation thing.
6. the manufacture method of bonding agent composition according to claim 5, it is characterised in that in step (c), relative to
The mass parts of secondary powder stock 100, the guar gum or tara gum in the aqueous solution containing guar gum or tara gum is 0.01~0.5
Mass parts.
7. the manufacture method of the bonding agent composition according to claim 5 or 6, it is characterised in that the use of mesh is 1000 μ
The sieve and mesh of more than m is that less than 300 μm of sieve is sieved the granules of gained in step (c).
8. the manufacture method of the bonding agent composition according to any one of claim 1~7, it is characterised in that thickening is more
Saccharide is xanthan gum.
9. the manufacture method of the bonding agent composition according to any one of claim 1~8, it is characterised in that dissolving is helped
Agent is dextrin.
10. the manufacture method of the bonding agent composition according to any one of claim 1~9, it is characterised in that viscosifier
Compositionss are applied to the liquid of more than 60 DEG C of high temperature.
11. diet products, it is characterised in that containing the increasing using the manufacture method manufacture any one of claim 1~10
Adhesive composition.
Applications Claiming Priority (3)
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JP2014164219 | 2014-08-12 | ||
JP2014-164219 | 2014-08-12 | ||
PCT/JP2015/004011 WO2016024402A1 (en) | 2014-08-12 | 2015-08-10 | Method for manufacturing thickener composition |
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JP (1) | JP6526682B2 (en) |
KR (1) | KR102490031B1 (en) |
CN (1) | CN106572689A (en) |
HK (1) | HK1231329A1 (en) |
MY (1) | MY182080A (en) |
SG (1) | SG11201700871YA (en) |
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US20200029609A1 (en) * | 2017-03-22 | 2020-01-30 | San-Ei Gen F.F.I., Inc. | Method for producing preparation containing thickening polyssaccharide |
WO2023037457A1 (en) * | 2021-09-08 | 2023-03-16 | 株式会社イルカカレッジ | Gel-forming fire extinguishing agent |
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CN102219912A (en) * | 2011-04-29 | 2011-10-19 | 淄博中轩生化有限公司 | Preparation method for granular type xanthan gum |
JP2011244809A (en) * | 2010-04-30 | 2011-12-08 | Sanei Gen Ffi Inc | Thickening agent having dispersibility and viscosity development |
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JP2619743B2 (en) * | 1990-12-10 | 1997-06-11 | 信久 川野 | Fast dissolving glucomannan composition |
JP2005525299A (en) * | 2001-09-14 | 2005-08-25 | スコラー インコーポレイテッド | Amino acid-controlled extended release dosage forms |
JP2004147567A (en) * | 2002-10-31 | 2004-05-27 | Meiji Milk Prod Co Ltd | Liquid food thickening agent and method for producing the same |
JP4781208B2 (en) * | 2006-09-13 | 2011-09-28 | 三栄源エフ・エフ・アイ株式会社 | Powder granulation method and easily dispersible and easily soluble granule composition |
JP5388414B2 (en) * | 2006-12-27 | 2014-01-15 | 三栄源エフ・エフ・アイ株式会社 | Powder granulation method |
JP5192189B2 (en) | 2007-06-22 | 2013-05-08 | 三栄源エフ・エフ・アイ株式会社 | Method for preventing ramping of water-soluble polymer and granule composition in which ramping is prevented |
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2015
- 2015-08-10 TW TW104125981A patent/TWI680153B/en active
- 2015-08-10 KR KR1020177001288A patent/KR102490031B1/en active IP Right Grant
- 2015-08-10 CN CN201580040375.3A patent/CN106572689A/en active Pending
- 2015-08-10 MY MYPI2017700388A patent/MY182080A/en unknown
- 2015-08-10 WO PCT/JP2015/004011 patent/WO2016024402A1/en active Application Filing
- 2015-08-10 SG SG11201700871YA patent/SG11201700871YA/en unknown
- 2015-08-10 JP JP2016542506A patent/JP6526682B2/en active Active
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- 2017-05-19 HK HK17105067.8A patent/HK1231329A1/en unknown
Patent Citations (6)
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JP2011010561A (en) * | 2009-06-30 | 2011-01-20 | Wakodo Co Ltd | Lumping inhibitor |
CN102883625A (en) * | 2010-04-27 | 2013-01-16 | 日清奥利友集团株式会社 | Granular thickening agent and method for producing the same |
JP2011244809A (en) * | 2010-04-30 | 2011-12-08 | Sanei Gen Ffi Inc | Thickening agent having dispersibility and viscosity development |
JP2011254709A (en) * | 2010-06-05 | 2011-12-22 | Taiyo Kagaku Co Ltd | Food quality improving agent |
CN102219912A (en) * | 2011-04-29 | 2011-10-19 | 淄博中轩生化有限公司 | Preparation method for granular type xanthan gum |
JP2013111035A (en) * | 2011-11-30 | 2013-06-10 | Nippon Starch Chemical Co Ltd | Thickened composition with improved dispersibility, and metal salt-containing decomposed starch used for the same |
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SG11201700871YA (en) | 2017-03-30 |
JP6526682B2 (en) | 2019-06-05 |
JPWO2016024402A1 (en) | 2017-06-01 |
KR20170046640A (en) | 2017-05-02 |
TW201609935A (en) | 2016-03-16 |
KR102490031B1 (en) | 2023-01-18 |
WO2016024402A1 (en) | 2016-02-18 |
TWI680153B (en) | 2019-12-21 |
HK1231329A1 (en) | 2017-12-22 |
MY182080A (en) | 2021-01-18 |
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