CN106564869A - A preparing method of a thin tough hypersensitive material - Google Patents
A preparing method of a thin tough hypersensitive material Download PDFInfo
- Publication number
- CN106564869A CN106564869A CN201610887285.4A CN201610887285A CN106564869A CN 106564869 A CN106564869 A CN 106564869A CN 201610887285 A CN201610887285 A CN 201610887285A CN 106564869 A CN106564869 A CN 106564869A
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- China
- Prior art keywords
- hypersensitive
- thin
- thin tough
- tough
- carbon materials
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- C—CHEMISTRY; METALLURGY
- C01—INORGANIC CHEMISTRY
- C01P—INDEXING SCHEME RELATING TO STRUCTURAL AND PHYSICAL ASPECTS OF SOLID INORGANIC COMPOUNDS
- C01P2004/00—Particle morphology
- C01P2004/20—Particle morphology extending in two dimensions, e.g. plate-like
Abstract
A preparing method of a thin tough hypersensitive material is provided. Firstly, a two-dimensional carbon material and a boride are homogenized, and are polymerized and layered at specific temperature conditions; and then a thin tough hypersensitive material is formed by adopting a crystal nucleus manner, and is subjected to temperature control treatment, decomposition and polymerization to finally prepare a thin tough hypersensitive composite material. The method is simple, feasible, natural in material selection and free of pollution. The two-dimensional carbon material and a boride-containing fine-grain composite material can be adopted as substrates. The composite material is thin, tough and hypersensitive and facilitates social production and livelihood application in a plurality of fields such as flavor sensitivity and microearthquake.
Description
Technical field
The present invention relates to field of nano material preparation, more particularly to a kind of preparation side of two-dimentional carbon materials nano material
Method.
Background technology
Even two-dimentional carbon materials nano composite material, with its superior physical and chemical performance, causes the concern of Chan Yan all circles,
Usual general field highlights efficiency from needless to say in the polynary special dimensions such as the quick, microseism of taste.
At present, although the preparation method multiterminal of two-dimentional carbon materials, but from terms of ecological, environmental protective angle, mechanical stripping method is most safe,
It is using the friction and relative motion between object and two-dimentional carbon materials, the method for obtaining two-dimentional carbon materials layer material.This side
Method is simple to operate, and the two-dimentional carbon materials for obtaining generally remain complete crystal structure.This method is mainly for the preparation of high-quality
Two-dimentional carbon materials material.
The extensive method for preparing two-dimentional carbon materials is presently used for, is mainly realized by chemical stripping method.This method institute
The material preparation process being related to is more complicated, and has used the materials such as strong acid, strong oxidizer, pollutes environment.
We have separately warded off a kind of preparation method of thin tough super quick material using two-dimentional carbon materials.It is brief easy based on the method,
Draw materials natural, it is pollution-free.The optional two-dimentional carbon materials of base material, the fine granularity composite containing boride.Gained composite is thin tough super
It is quick, be conducive to social production and people's livelihood application in polynary fields such as the quick, microseisms of taste.
The content of the invention
Based on above-mentioned present situation, it is an object of the invention to intend providing a kind of preparation method of thin tough super quick material.This side
Method is to prepare the new method of thin tough super quick material along with the effect of boride based on two-dimentional carbon materials.Because they are all hardness
The very high crystal with fusing point, stable chemical nature, the red fuming nitric acid (RFNA) of heat can not dissolve it, by the direct chemical combination of element, or can use
Active metal reduced oxide is produced, as fire resisting, grinding and super quick material.Positive 60, since the seventies, increasing scholar
It was found that the coating or pigment used by we are daily, in addition to generally having color, often having some compounds to be also equipped with can be with outer
Boundary's condition changes and produces the characteristic of the phenomenons such as luminous or color change, thus has widened their application significantly.These
Compound has a common ground, that is, have certain pi-conjugated system.With the change of external condition, pi-conjugated system also there occurs
Change, causes color of compound etc. to there occurs change.It is this kind of can the change of condition to external world produce the compound of " response ", it is logical
Often it is assigned " functional material ".
For achieving the above object, the technical solution adopted in the present invention is：Specifically, above-mentioned a kind of thin tough super quick material
The preparation method of material is, first, by two-dimentional carbon materials polymer and is homogenized, and at a temperature of setting gathers two-dimentional carbon materials
Compound presoma aggregates into two-dimentional carbon materials compound；Then, thin tough super quick material is synthesized by nucleation mode；It is then based on high temperature
Process, decompose, it is final to obtain the required super quick composite of two-dimentional carbon materials.The air-sensitive of thin tough super quick material prepared by the present invention
Property and mechanical property it is good, technique is brief, low cost, tool are repeatable, environment friendly and pollution-free, is conducive to social production and the people should
With.
Improvement, development, research for the demand present situation, the invention has benefit that, the one of present invention offer
The preparation method of kind thin tough super quick material, solves that technique in the presence of existing air-sensitive membrane preparation method is miscellaneous, repeatability
Problem poor, with high costs, by the preparation of two-dimentional carbon materials the sensitive property of material is increased, and is improve by adding boride
Comprehensive mechanical property.Can effectively lift the feature of above-mentioned thin tough super quick material and reach satisfied effect with time saving and energy saving
The problem of fruit.
In order to increase the function of the generation of prior art, there is provided a kind of workable, offer design is brief, and multiple-effect is common
Enjoy, the preparation method of the convenient and safe a kind of thin tough super quick material for using, properties of product are high, integrated cost is low, prepares and uses
Method is simple, and applied widely, can meet the growing production and construction of diversification and living needs, is section
, ecological, environmental protection, the multi-effect scheme of sustainable development.
Described above is only the general introduction of technical solution of the present invention, in order to be able to better understand the technological means of the present invention, and
Can be practiced according to the content of specification, and be allow the present invention above and other objects, features and advantages can be brighter
It is aobvious understandable, below especially exemplified by preferred embodiment, describe in detail as follows.
Specific embodiment
Further to illustrate the present invention to reach technological means and effect that predetermined goal of the invention is taken, below in conjunction with
Preferred embodiment, to according to a kind of preparation method of thin tough super quick material proposed by the present invention, its specific embodiment, feature
Deng after describing in detail such as.
Embodiment
The present invention intends the preparation method of a kind of thin tough super quick material for providing, and first, is adopted its two-dimentional carbon materials and two
Titanium boride carries out homogenize process, and two-dimentional carbon materials polymer polymerizing is made at a temperature of 450-600 degree into compound；Then,
Thin tough super quick material is synthesized by nucleation mode；It is then based on the high-temperature process of 800-1150 degree, decomposes, needed for final acquisition
The super quick composite of two-dimentional carbon materials.The gas sensing property and mechanical property of thin tough super quick material prepared by the present invention is good, using two dimension
Carbon materials have separately warded off a kind of preparation method of thin tough super quick material.It is brief easy based on the method, draw materials natural, it is pollution-free.Base material
Optional two-dimentional carbon materials, the fine granularity composite containing boride.Gained composite is thin tough super quick, polynary in the quick, microseism of taste etc.
Field is conducive to social production and people's livelihood application.Technique is brief, low cost, tool repeatability, environment friendly and pollution-free, is conducive to society
Production and people's application.
The above, is only presently preferred embodiments of the present invention, and any pro forma restriction is not made to the present invention, though
So the present invention is disclosed above with preferred embodiment, but is not limited to the present invention, any to be familiar with this professional technology people
Member, in the range of without departing from technical solution of the present invention, when making a little change or modification using the technology contents of the disclosure above
For the Equivalent embodiments of equivalent variations, as long as being the content without departing from technical solution of the present invention, the technical spirit of the foundation present invention
Any simple modification, equivalent variations and the modification made to above example, still falls within the range of technical solution of the present invention.
Claims (1)
1. a kind of preparation method of thin tough super quick material, it is characterised in that：Homogenized based on two-dimentional carbon materials and boride and
Its polymerization layering is made under set temperature conditionss；Then, nucleus mode is taken to form thin tough super quick material；And at temperature control
Reason, decomposes polymerization, eventually into thin tough super quick composite.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201610887285.4A CN106564869A (en) | 2016-10-12 | 2016-10-12 | A preparing method of a thin tough hypersensitive material |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201610887285.4A CN106564869A (en) | 2016-10-12 | 2016-10-12 | A preparing method of a thin tough hypersensitive material |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| CN106564869A true CN106564869A (en) | 2017-04-19 |
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Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN201610887285.4A Pending CN106564869A (en) | 2016-10-12 | 2016-10-12 | A preparing method of a thin tough hypersensitive material |
Country Status (1)
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| CN (1) | CN106564869A (en) |
Citations (4)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US6193915B1 (en) * | 1999-09-03 | 2001-02-27 | Her Majesty The Queen In Right Of Canada, As Represented By The Minister Of Natural Resources | Process for fabricating low volume fraction metal matrix preforms |
| CN1428311A (en) * | 2001-12-28 | 2003-07-09 | 武汉科技大学 | Preparation method of titanium biboride composite material |
| CN102126710A (en) * | 2011-05-04 | 2011-07-20 | 中国人民解放军国防科学技术大学 | Method for preparing boron nitride nanowire by cracking of polymer |
| CN103570014A (en) * | 2013-11-15 | 2014-02-12 | 中国人民解放军国防科学技术大学 | Graphene/boron nitride layered composite material and preparation method thereof |
-
2016
- 2016-10-12 CN CN201610887285.4A patent/CN106564869A/en active Pending
Patent Citations (4)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US6193915B1 (en) * | 1999-09-03 | 2001-02-27 | Her Majesty The Queen In Right Of Canada, As Represented By The Minister Of Natural Resources | Process for fabricating low volume fraction metal matrix preforms |
| CN1428311A (en) * | 2001-12-28 | 2003-07-09 | 武汉科技大学 | Preparation method of titanium biboride composite material |
| CN102126710A (en) * | 2011-05-04 | 2011-07-20 | 中国人民解放军国防科学技术大学 | Method for preparing boron nitride nanowire by cracking of polymer |
| CN103570014A (en) * | 2013-11-15 | 2014-02-12 | 中国人民解放军国防科学技术大学 | Graphene/boron nitride layered composite material and preparation method thereof |
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| SE01 | Entry into force of request for substantive examination | ||
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| WD01 | Invention patent application deemed withdrawn after publication |
Application publication date: 20170419 |
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| WD01 | Invention patent application deemed withdrawn after publication |