CN106562492A - Tangerine powder microcapsule anti-oxidation face mask liner, preparation method and application - Google Patents
Tangerine powder microcapsule anti-oxidation face mask liner, preparation method and application Download PDFInfo
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- CN106562492A CN106562492A CN201510654120.8A CN201510654120A CN106562492A CN 106562492 A CN106562492 A CN 106562492A CN 201510654120 A CN201510654120 A CN 201510654120A CN 106562492 A CN106562492 A CN 106562492A
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- fructus citri
- citri tangerinae
- powder capsule
- tangerinae powder
- mask liner
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Abstract
The invention relates to a tangerine powder microcapsule anti-oxidation face mask liner, a preparation method and application of the same. The face mask liner is prepared through post-arrangement and post-processing of a tangerine powder microcapsule finishing agent on a non-woven fabric; and the non-woven fabric face mask liner is placed between the inner layer and the outer layer of the face mask as an interlayer material. The involved tangerine powder anti-oxidation microcapsule finishing agent is prepared by a microcapsule technology. Flavonoid compounds in tangerine powder have obvious effects of oxidation resistance and free radical scavenging, and have assistant effects in aspects such as inflammation diminishment, cancer prevention, anticoagulation, thrombus prevention and prevention and treatment of heart and cerebral vessel diseases. Hence, the face mask liner provided by the invention is characterized in that the liner is efficient in oxidation resistance, can scavenge free radicals in air, is safe and pollution-free, has a good scent, etc. The liner is a green, environment-friendly, anti-oxidation and multi-functional textile product.
Description
Technical field
The invention belongs to protection technology field, particularly relate to a kind of Fructus Citri tangerinae powder capsule antioxidation mask liner,
Preparation method and application.
Background technology
Antioxidation is exactly any material that there is the oxidation reaction that just can effectively suppress free radical with low concentration, its
The mechanism of action can act directly on free radical, or consume the material for easily generating free radical indirectly,
Prevent further reaction.Human body is also being produced naturally while free radical is inevitably generated
The antioxidant of opposing free radical, to offset oxidative attacks of the free radical to human body cell.So-called free radical
It is exactly the group of the free property containing oxidisability, including molecular radical, atomic radical or ionic group.
Pericarpium Citri tangerinae is one of Chinese medicine common medicine, and flavone compound is the most class feature of content in orange peel
Composition, is the general name of the phenolic compound with C6-C3-C6 structures, is the derivative of chromone or chromanane
Thing.Substantial amounts of pharmacology proves that pyrite class compound has obvious non-oxidizability effect of scavenging radical in Pericarpium Citri tangerinae,
Also there is in addition the assosting effects such as antiinflammatory, anti-cancer, anticoagulation, antithrombotic and preventing and treating cardiovascular and cerebrovascular disease.And
And with wide, low cost of originating, economic and environment-friendly, the advantage of energy-saving recycling.
But Fructus Citri tangerinae powder effective ingredient itself is unstable, easily changes, and is unfavorable for storing and transports, and makes Fructus Citri tangerinae
The range of application of powder is greatly limited.Fructus Citri tangerinae powder capsuleization is not only solved into Fructus Citri tangerinae powder above-mentioned
Shortcoming and because the particle diameter of microcapsule is little, specific surface area is big, can reach control Fructus Citri tangerinae powder effective ingredient
Releasing effect, extends the advantage of anti oxidation time, makes Fructus Citri tangerinae powder anti-oxidation characteristics be fully utilized.
Traditional microcapsules manufacture method has three major types：
1) physical method：Prepare microcapsule using the method for physics and theory of mechanics, mainly have air suspension,
Spray drying method, electrostatical binding method, inclusion complexation method etc..
2) chemical method：Mainly using monomeric small molecule occur polyreaction generate macromolecule or membrane material and by
Core is coated, and often uses interfacial polymerization and situ aggregation method.
3) physical-chemical process：Dissolved state is made by changing condition (temperature, pH value add electrolyte etc.)
Filmogen from solution coagulation out and by core coat to form microcapsule, specifically have coacervation, oil phase
Partition method, it is dried bath method, pore membrane squeezing and pressing method, fusing dispersion condensation method etc..
Prior art proposes that the method that microcapsule is attached on fabric has：1) it is dispersed in after microcapsule is dried molten
Coating is directly used in agent or is sprayed on fabric；2) microcapsule adds other auxiliary agent groups in fabric post-treatment
Into dressing liquid, microcapsule is attached on fabric by way of padding；3) microcapsule is placed in into spinning
Fiber of the spinning containing microcapsule and yarn in liquid.
Its conventional process has：Dip method, infusion process and Decal.The characteristics of generally speaking dipping method needs to apply
Plus external force, microcapsule is easily broken；The process characteristic of stamp is that technique is more complicated；The characteristics of infusion process, exists
Microcapsule content on fabric is few.
The content of the invention
It is an object of the invention to provide a kind of Fructus Citri tangerinae powder capsule antioxidation mask liner, the liner can be effective
The free radical in air is removed, while microcapsule-type mask liner has washing fastness.
It is a further object to provide a kind of preparation method of mask liner, this preparation method is simply easy
OK, environmental protection, low cost, it is easy to industrialized production.
The present invention is achieved by the following technical solutions：
A kind of Fructus Citri tangerinae powder capsule antioxidation mask liner, by Fructus Citri tangerinae powder capsule finishing agent by non-woven fabrics
Carry out Final finishing processing on fabric to be prepared from.
The non-woven fabrics fabric is fusion spray cloth non-woven fabrics.
The Fructus Citri tangerinae powder capsule finishing agent, consisting of by mass fraction：Fructus Citri tangerinae powder capsule is 40-50
Part, deionized water are 40-60 parts and dispersant is 5-10 parts.
The Fructus Citri tangerinae powder capsule coagulates again method and prepares using methylcellulose, concretely comprises the following steps：
1) methylcellulose is added and prepare in deionized water methylcellulose of the mass concentration for 2-3%
Solution；
2) Fructus Citri tangerinae powder emulsifying under agitation is added；
3) add glacial acetic acid to adjust pH value in the solution of emulsifying and coagulated reaction again for acidity；
4) by step 3) in suspension lower the temperature in ice-water bath after with aqueous slkali adjust pH value be after alkalescence
Add and continue ice bath after glutaraldehyde solution；
5) after heating up after crosslinking curing setting time, Fructus Citri tangerinae powder capsule is obtained.
The dispersant is sodium methylene bis-naphthalene sulfonate.
The amount containing the Fructus Citri tangerinae powder capsule is 0.6-2 gram in 100 grams of non-woven fabrics fabrics.
A kind of preparation method of any of the above-described Fructus Citri tangerinae powder capsule antioxidation mask liner, by non-woven fabrics fabric
One-bath finishing in the solution being made up of Fructus Citri tangerinae powder capsule finishing agent and cross-linking agent is immersed, leaching is then passed sequentially through
Roll operation, preliminary drying operation and bake the preparation that operation completes Fructus Citri tangerinae powder capsule antioxidation mask liner.
The cross-linking agent is shitosan and 1,2,3,4- BTCAs are 1 in mass ratio:1 ratio mixing,
It is dissolved in 1% acetic acid and makes the cross-linking agent of 3% shitosan and 1,2,3,4- BTCA mixed liquors.
It is described pad operation and include two leachings two roll, pick-up rate is 80-100%.
Fructus Citri tangerinae powder capsule antioxidation mask liner described in any of the above-described is positioned over mask as sandwich material
Ectonexine between.
The invention has the beneficial effects as follows：
The Fructus Citri tangerinae powder capsule antioxidation mask liner of the present invention, is to be prepared into Fructus Citri tangerinae powder by raw material of Fructus Citri tangerinae powder
Microcapsule, Fructus Citri tangerinae powder capsule through being re-dubbed Fructus Citri tangerinae powder capsule dressing liquid after to fabric treating so that Fructus Citri tangerinae
Reaction is crosslinked by cross-linking agent between sub- powder capsule and fabric fibre and forms chemical bonded, Fructus Citri tangerinae powder
Microcapsule antioxidant is firmly attached on fabric fibre, after arranging to fabric, by fabric application
In preparing mask material so that Fructus Citri tangerinae powder capsule can reach good adhesion effect and washability on fabric
Can, the antioxygenic property with the long period.
Specific embodiment
By the following examples describing technical scheme in detail, below example is only exemplary
, it is only capable of for explaining and illustrating technical scheme, and be not to be construed as to the technology of the present invention side
The restriction of case.
The present invention provides a kind of Fructus Citri tangerinae powder capsule antioxidation mask liner, is led to by Fructus Citri tangerinae powder capsule finishing agent
Cross carry out on non-woven fabrics fabric Final finishing processing be prepared from.The non-woven fabrics fabric is fusion spray cloth non-woven fabrics.
Non-woven fabrics in present embodiments are existing commercially available prod.
In present embodiments, the Fructus Citri tangerinae powder capsule antioxidation mask liner after arrangement, institute
It is 0.6-2 gram to state the amount containing the Fructus Citri tangerinae powder capsule in 100 grams of non-woven fabrics fabrics.
It is with methylcellulose as wall material, with Fructus Citri tangerinae powder as core, using the method for complex coacervation in the application
Processing procedure Fructus Citri tangerinae powder capsule, then adds dispersant NNO and is re-dubbed a kind of Fructus Citri tangerinae powder capsule dressing liquid, leads to
Cross with the dressing liquid to the application in textile finishing, give fabric and there is lasting anti-oxidation function.
The Fructus Citri tangerinae powder capsule coagulates again method and prepares using methylcellulose, concretely comprises the following steps：
1) methylcellulose is added and prepare in deionized water methylcellulose of the mass concentration for 2-3%
Solution；Reaction temperature is controlled at 50-60 DEG C；
2) Fructus Citri tangerinae powder emulsifying under agitation is added；
3) add glacial acetic acid to adjust pH value in the solution of emulsifying and coagulated reaction again for 4.0；
4) by step 3) in suspension 0 DEG C is cooled in ice-water bath after with sodium hydroxide solution adjust pH
It is worth to 8.0-9.0 adds and continue ice bath 30 minutes after glutaraldehyde solution；
5) to proceed to and continue crosslinking curing 2 hours in 50 DEG C of water-baths, obtain Fructus Citri tangerinae powder capsule.
By the way that in Fructus Citri tangerinae powder capsule prepared by said method, the weight/mass percentage composition of Fructus Citri tangerinae powder core material is
5-10%.
Fructus Citri tangerinae powder capsule finishing agent, consisting of by mass fraction：Fructus Citri tangerinae powder capsule be 40-50 parts,
Deionized water is 40-60 parts and dispersant is 5-10 parts；The dispersant is sodium methylene bis-naphthalene sulfonate
(NNO).Above-mentioned each composition is obtained into Fructus Citri tangerinae powder capsule dressing liquid for 1 hour by uniform stirring.
The preparation method of Fructus Citri tangerinae powder capsule antioxidation mask liner, immerses micro- by Fructus Citri tangerinae powder by non-woven fabrics fabric
Capsule finishing agent and one-bath finishing in the solution of cross-linking agent composition, then pass sequentially through and pad operation, preliminary drying work
Sequence and bake the preparation that operation completes Fructus Citri tangerinae powder capsule antioxidation mask liner.
The cross-linking agent is that shitosan (CTA) and 1,2,3,4- BTCAs (BTCA) are in mass ratio
1:1 ratio mixing, is dissolved in 1% acetic acid and makes 3% shitosan and 1, the mixing of 2,3,4- BTCAs
The cross-linking agent of liquid.
During arrangement, after being rolled by two leachings two, pick-up rate 80-100%, the preliminary drying 5 at 100-120 DEG C
Minute, then at 160-180 DEG C bakee 3 minutes afterwards cool drying be obtained Fructus Citri tangerinae powder capsule resist
Oxidation mask liner.
Fructus Citri tangerinae powder capsule antioxidation mask liner is positioned between the ectonexine of mask as sandwich material.
Embodiment 1
In present embodiments, the preparation method all same of Fructus Citri tangerinae powder capsule, different is
Different and Fructus Citri tangerinae powder capsule antioxidation mask liner the preparation methoies of composition of Fructus Citri tangerinae powder capsule dressing liquid.
Therefore, in the present embodiment and following each embodiment, the preparation side for illustrating Fructus Citri tangerinae powder capsule is not repeated
Method, only lists the different compositions and Fructus Citri tangerinae powder capsule antioxidation mask liner of Fructus Citri tangerinae powder emblem capsule finishing agent
Preparation method.
Fructus Citri tangerinae powder capsule finishing agent, consisting of by mass fraction：Fructus Citri tangerinae powder capsule be 40 parts, go from
Sub- water is 40 parts and dispersant is 5 parts；The dispersant will be above-mentioned for sodium methylene bis-naphthalene sulfonate (NNO)
Each composition obtains Fructus Citri tangerinae powder capsule dressing liquid for 1 hour by uniform stirring.
The preparation of Fructus Citri tangerinae powder capsule antioxidation mask liner：To treat that dressed nonwoven fabrics fabric immerses above-mentioned Fructus Citri tangerinae
80 parts of powder capsule dressing liquid, 5 parts of cross-linking agent, pick-up 80%, preliminary drying temperature (100 DEG C × 5min),
Baking temperature (160 DEG C × 3min), cool drying is obtained Fructus Citri tangerinae powder capsule antioxidation mask liner.
The amount containing the Fructus Citri tangerinae powder capsule is 2g in per 100 grams of non-woven fabrics fabrics.
Embodiment 2
Fructus Citri tangerinae sends out microcapsule dressing agent, consisting of by mass fraction：Fructus Citri tangerinae powder capsule be 50 parts, go from
Sub- water is 60 parts and dispersant is 10 parts；The dispersant will be upper for sodium methylene bis-naphthalene sulfonate (NNO)
State each composition and Fructus Citri tangerinae powder capsule dressing liquid is obtained for 1 hour by uniform stirring.
The preparation of Fructus Citri tangerinae powder capsule antioxidation mask liner：To treat that dressed nonwoven fabrics fabric immerses above-mentioned Fructus Citri tangerinae
110 parts of powder capsule dressing liquid, 10 parts of cross-linking agent, pick-up 90%, preliminary drying temperature (100 DEG C × 5min),
Baking temperature (180 DEG C × 3min), cool drying is obtained Fructus Citri tangerinae powder capsule antioxidation mask liner.
The amount containing the Fructus Citri tangerinae powder capsule is 1.5g in per 100 grams of non-woven fabrics fabrics.
Embodiment 3
Fructus Citri tangerinae powder capsule finishing agent, consisting of by mass fraction：Fructus Citri tangerinae powder capsule be 42 parts, go from
Sub- water is 52 parts and dispersant is 6 parts；The dispersant will be above-mentioned for sodium methylene bis-naphthalene sulfonate (NNO)
Each composition obtains Fructus Citri tangerinae powder capsule dressing liquid for 1 hour by uniform stirring.
The preparation of Fructus Citri tangerinae powder capsule antioxidation mask liner：To treat that dressed nonwoven fabrics fabric immerses above-mentioned Fructus Citri tangerinae
90 parts of powder capsule dressing liquid, 10 parts of cross-linking agent, pick-up 90%, preliminary drying temperature (120 DEG C × 5min),
Baking temperature (160 DEG C × 3min), cool drying is obtained Fructus Citri tangerinae powder capsule antioxidation mask liner.
The amount containing the Fructus Citri tangerinae powder capsule is 1.5g in per 100 grams of non-woven fabrics fabrics.
Embodiment 4
Fructus Citri tangerinae powder capsule finishing agent, consisting of by mass fraction：Fructus Citri tangerinae powder capsule be 45 parts, go from
Sub- water is 47 parts and dispersant is 8 parts；The dispersant will be above-mentioned for sodium methylene bis-naphthalene sulfonate (NNO)
Each composition obtains Fructus Citri tangerinae powder capsule dressing liquid for 1 hour by uniform stirring.
The preparation of Fructus Citri tangerinae powder capsule antioxidation mask liner：To treat that dressed nonwoven fabrics fabric immerses above-mentioned Fructus Citri tangerinae
95 parts of powder capsule dressing liquid, 5 parts of cross-linking agent, pick-up 90%, preliminary drying temperature (110 DEG C × 5min),
Baking temperature (170 DEG C × 3min), cool drying is obtained Fructus Citri tangerinae powder capsule antioxidation mask liner.
The amount containing the Fructus Citri tangerinae powder capsule is 1g in per 100 grams of non-woven fabrics fabrics.
Embodiment 5
Fructus Citri tangerinae powder capsule finishing agent, consisting of by mass fraction：Fructus Citri tangerinae powder capsule be 47 parts, go from
Sub- water is 46 parts and dispersant is 7 parts；The dispersant is sodium methylene bis-naphthalene sulfonate (NNO)；Will be upper
State each composition and Fructus Citri tangerinae powder capsule dressing liquid is obtained for 1 hour by uniform stirring.
The preparation of Fructus Citri tangerinae powder capsule antioxidation mask liner：To treat that dressed nonwoven fabrics fabric immerses above-mentioned Fructus Citri tangerinae
95 parts of powder capsule dressing liquid, 5 parts of cross-linking agent, pick-up 100%, preliminary drying temperature (120 DEG C × 5min),
Baking temperature (180 DEG C × 3min), cool drying is obtained Fructus Citri tangerinae powder capsule antioxidation mask liner.
The amount containing the Fructus Citri tangerinae powder capsule is 0.6g in per 100 grams of non-woven fabrics fabrics.
The antioxidation of Fructus Citri tangerinae powder capsule is determined：Using DPPH free radical scavengings method and ABTS free radical scavengings
Method determines antioxidant activity, and DPPH is removed before and after antioxidation certainly by the Fructus Citri tangerinae powder capsule of variable concentrations
May certify that Fructus Citri tangerinae powder capsule has anti-oxidation function by the effect of base and ABTS free radicals.
Add 3ml dehydrated alcohol to put in test tube 1ml prepare liquids, shake up, then add 1ml DPPH solution,
Shake up, lucifuge reaction 10min with dehydrated alcohol as reference, in 517am its absorbance is surveyed, each examination
Sample do 3 it is parallel, be calculated as follows clearance rate：
Clearance rate (%)=[1 one (Aj of Ai mono-)/A.] × 100%；
Ai is the absorbance of 1ml prepare liquid+3ml dehydrated alcohol+lml DPPH solution in formula；Aj
For the absorbance of 1ml prepare liquid+3ml dehydrated alcohol；Ao is that 1ml DPPH solution+3ml are anhydrous
The absorbance of ethanol.
Add 3ml ABTS to be placed in test tube 0.1ml prepare liquids, shake up, lucifuge reaction 6min gives
734min surveys its absorbance, each sample do 3 it is parallel, be calculated as follows clearance rate：
Clearance rate (%)=[1 one (Aj of Ai mono-)/A.] × 100%；
Ai is the absorbance of 0.1ml prepare liquid+3ml ABTS solution in formula；Aj is 0.1ml
The absorbance of prepare liquid+3ml distilled water；Ao is the absorbance of 3ml ABTS solution.By each concentration
Clearance rate corresponding thereto is fitted to obtain its equation, the clearance rate for calculating at 0.5 determinand it is dense
Degree is 503nhibiting concentration (IC50) value.Radical scavenging activity, AE=l/IC50.Sentenced according to AE sizes
The size of disconnected determinand Scavenging ability, AE is bigger, and the ability for removing free radical is stronger.
Although an embodiment of the present invention has been shown and described, for the ordinary skill in the art,
It is appreciated that can to carry out these embodiments without departing from the principles and spirit of the present invention various
Change, modification, replacement and modification, the scope of the present invention is limited by claims and its equivalent.
Claims (10)
1. a kind of Fructus Citri tangerinae powder capsule antioxidation mask liner, it is characterised in that：Arranged by Fructus Citri tangerinae powder capsule
Agent is prepared from by carrying out Final finishing processing on non-woven fabrics fabric.
2. Fructus Citri tangerinae powder capsule antioxidation mask liner according to claim 1, it is characterised in that：Institute
Non-woven fabrics fabric is stated for fusion spray cloth non-woven fabrics.
3. Fructus Citri tangerinae powder capsule antioxidation mask liner according to claim 1, it is characterised in that：Institute
State Fructus Citri tangerinae powder capsule finishing agent, consisting of by mass fraction：Fructus Citri tangerinae powder capsule is 40-50 parts, goes
Ionized water is 40-60 parts and dispersant is 5-10 parts.
4. Fructus Citri tangerinae powder capsule antioxidation mask liner according to claim 3, it is characterised in that：Institute
State Fructus Citri tangerinae powder capsule and method preparation is coagulated again using methylcellulose, concretely comprise the following steps：
1) methylcellulose is added and prepare in deionized water methylcellulose of the mass concentration for 2-3%
Solution；
2) Fructus Citri tangerinae powder emulsifying under agitation is added；
3) add glacial acetic acid to adjust pH value in the solution of emulsifying and coagulated reaction again for acidity；
4) by step 3) in suspension lower the temperature in ice-water bath after with aqueous slkali adjust pH value be after alkalescence
Add and continue ice bath after glutaraldehyde solution；
5) after heating up after crosslinking curing setting time, Fructus Citri tangerinae powder capsule is obtained.
5. Fructus Citri tangerinae powder capsule antioxidation mask liner according to claim 3, it is characterised in that：Institute
Dispersant is stated for sodium methylene bis-naphthalene sulfonate.
6. Fructus Citri tangerinae powder capsule antioxidation mask liner according to claim 1, it is characterised in that：Institute
It is 0.6-2 gram to state the amount containing Fructus Citri tangerinae powder capsule in 100 grams of non-woven fabrics fabrics.
7. a kind of preparation method of Fructus Citri tangerinae powder capsule antioxidation mask pad, appoints in usage right requirement 1 to 6
Fructus Citri tangerinae powder capsule finishing agent described in one, it is characterised in that：Non-woven fabrics fabric is immersed by the Fructus Citri tangerinae
One-bath finishing in the solution of powder capsule finishing agent and cross-linking agent composition, then passes sequentially through and pads operation, pre-
Dry operation and bake the preparation that operation completes Fructus Citri tangerinae powder capsule antioxidation mask liner.
8. the preparation method of Fructus Citri tangerinae powder capsule antioxidation mask pad according to claim 7, its feature
It is：The cross-linking agent is shitosan and 1,2,3,4- BTCAs are 1 in mass ratio:1 ratio is mixed
Close, be dissolved in 1% acetic acid and make 3% shitosan and 1, the cross-linking agent of 2,3,4- BTCA mixed liquors.
9. the preparation method of Fructus Citri tangerinae powder capsule antioxidation mask pad according to claim 7, it is special
Levy and be：It is described pad operation and include two leachings two roll, pick-up rate is 80-100%.
10. the Fructus Citri tangerinae powder capsule antioxidation mask liner any one of the claims 1 to 9,
It is characterized in that：The Fructus Citri tangerinae powder capsule antioxidation mask liner is positioned in mask as sandwich material
Between outer layer.
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| CN201510654120.8A CN106562492A (en) | 2015-10-10 | 2015-10-10 | Tangerine powder microcapsule anti-oxidation face mask liner, preparation method and application |
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| CN201510654120.8A CN106562492A (en) | 2015-10-10 | 2015-10-10 | Tangerine powder microcapsule anti-oxidation face mask liner, preparation method and application |
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| JP2006150643A (en) * | 2004-11-26 | 2006-06-15 | Dainippon Printing Co Ltd | Printed matter with perfumed ink |
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