CN106554068A - A kind of neutral saturation hydrogen water and preparation method thereof and a kind of system for preparing neutral saturation hydrogen water - Google Patents
A kind of neutral saturation hydrogen water and preparation method thereof and a kind of system for preparing neutral saturation hydrogen water Download PDFInfo
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Abstract
The invention provides a kind of system for preparing neutral saturation hydrogen water, including：Water tank (1)；The supersonic generator (2) that entrance is connected with the outlet of the water tank (1)；The hydrogen ejector (3) that entrance is connected with the outlet of the supersonic generator (2)；Hydrogen water mixer (4) that entrance is connected with the outlet of the hydrogen ejector (3)；The isobar filling machine (5) that outlet with the hydrogen water mixer (4) is connected；Hydrogen generator (6), the first gas outlet of the hydrogen generator (6) is connected with the first gas entrance of the hydrogen ejector (3), the second gas outlet of the hydrogen generator is connected with the second gas entrance of the hydrogen water mixer (4), and the third gas outlet of the hydrogen generator is connected with the third gas entrance of the isobar filling machine (5).
Description
Technical field
The invention belongs to hydrogen water technical field, and in particular to a kind of neutral saturation hydrogen water and preparation method thereof with
And a kind of system for preparing neutral saturation hydrogen water.
Background technology
Hydrogen molecule has selective antioxidation, due to small volume, can be very good through cell wall,
Eliminate intracellular oxygen-derived free radicals.The hydrogen of animal breath 2% can effectively remove free radical, significantly improve
Brain, liver and myocardial ischemia reperfusion injury, can effectively mitigate inflammation damnification and improvement that small intestine transplantation causes
Newborn baby hypoxic-ischemic state etc..Directly drink saturation hydrogen water to stress cause nerve injury, people
Injury of kidney that class type ii diabetes, murine genes defect eremacausis stress damage, chemotherapeutic drugs Cisplatin cause and
Parkinson disease etc. also have obvious curative effects.Current research discovery, can using the culture medium culturing containing saturation hydrogen
Effectively damage of the antagonism ototoxic drug to internal ear sensory epithelium and vestibular hair cells.Drink saturation hydrogen water
The hearing impairment that white noise causes can be mitigated.Saturation hydrogen water penetration is fast, have no toxic side effect, low price,
The a large amount of free radicals for producing can be caused by blood-lost barrier removes noise effectively, reduce the apoptosis of hair cell.
But, hydrogen is generally insoluble in water, to produce more efficiently at saturation hydrogen water, at present frequently with side
Method has：Pressurization production hydrogen water, hydrogen lavage produce hydrogen water, prepare hydrogen water or supercritical ultrasonics technology using hydrogen rod
Prepare hydrogen water.
Wherein, in the hydrogen water of pressurization production, hydrogen solubility is low, the time length, yield needed for pressurization production
It is low；During hydrogen lavage production hydrogen water, hydrogen water has blast possible in atmosphere more than 4%, this side
Method is dangerous big, needs special ventilation unit；When hydrogen rod prepares hydrogen water, in hydrogen rod, main reactant is
Magnesium metal, usual magnesium metal are extremely violent with the reaction of water, to delay being reacted to give for magnesium metal and water
Continual hydrogen water need to add other heavy metals in magnesium rod, so can bring about serious heavy metal-polluted
Dye, harm of the life-time service to environment and health are self-evident.
Hydrogen water method is prepared simply using supercritical ultrasonics technology, the used time is short, but ultrasound wave is in hydrogen water production process
In and in being not apparent from increasing water and hydrogen contact area and probability, compared with by production of pressurizeing, in hydrogen water
Hydrogen content is had no without substantially increase, and in the hydrogen water after the method process, hydrogen content is unstable, easily overflows
Go out, hydrogen content can reduce 2/1 to three/2nds within the shelf-life, therefore when being extremely difficult to fill
The content and correlation function of hydrogeneous water.
The content of the invention
In view of this, the technical problem to be solved in the present invention is to provide a kind of neutral saturation hydrogen water and its system
Preparation Method and a kind of system for preparing neutral saturation hydrogen water, the preparation neutrality saturation provided using the present invention
The hydrogen water hydrogen content for obtaining prepared by the system of hydrogen water is high, and not reducing in shelf-life hydrogen content or
Shade few.
The invention provides a kind of system for preparing neutral saturation hydrogen water, including：
Water tank (1)；
The supersonic generator (2) that entrance is connected with the outlet of the water tank (1)；
The hydrogen ejector (3) that entrance is connected with the outlet of the supersonic generator (2)；
Hydrogen water mixer (4) that entrance is connected with the outlet of the hydrogen ejector (3)；
The isobar filling machine (5) that outlet with the hydrogen water mixer (4) is connected；
Hydrogen generator (6), first gas outlet and the hydrogen ejector of the hydrogen generator (6)
(3) first gas entrance is connected, and the second gas outlet of the hydrogen generator is mixed with the hydrogen water
The second gas entrance of machine (4) is connected, and the third gas outlet of the hydrogen generator and the equipressure are filled
The third gas entrance of installation (5) is connected.
Preferably, the sealer (7) being also connected with the outlet of the isobar filling machine (5) including entrance.
Preferably, pump is additionally provided between the water tank (1) and the supersonic generator (2)
(8)。
Present invention also offers a kind of preparation method of neutral saturation hydrogen water, comprises the following steps：
Hydrogen generator is to the hydrogen ejector, hydrogen water mixer and waits stream pressure filling machine to provide hydrogen
Meanwhile, the water after supersonic generator ultrasound is sequentially passed through into hydrogen ejector pre-hydrogenation, the mixing of hydrogen water
After machine mixing and isobar filling machine fill, neutral saturation hydrogen water is obtained.
Preferably, also include the neutral saturation hydrogen water is sealed in sealer.
Preferably, the wet concentration is from natural spring water, natural mineral water or pure water.
Preferably, the ultrasound is carried out in accordance with the following methods：
Water acts under the Ultrasonic Conditions of 20-40Hz the 50-70 seconds to be de-gassed again.
Preferably, the pressure of the hydrogen ejector pre-hydrogenation is 0.2-0.4MPa.
Preferably, the hydrogen water mixer mixing is carried out as follows：
Spray in the hydrogen room through the water of hydrogen ejector and pre-hydrogenation in hydrogen water mixer, obtain little
The water of micel；
The water of the subset is mixed with hydrogen, obtains the hydrogeneous water of saturation.
Preferably, the pressure in the hydrogen room is 0.2～0.4MPa.
Preferably, the time of the mixing is 15～20min.
Preferably, the pressure in the isobar filling machine and the pressure ratio in the hydrogen water mixer are 1:
0.95-1.05。
Present invention also offers a kind of neutral saturation hydrogen prepared by the preparation method of the claims
Water, the hydrogen content in the neutral saturation hydrogen water are 1.0～1.2ppm.
Compared with prior art, the invention provides a kind of system for preparing neutral saturation hydrogen water, including：
Water tank (1)；The supersonic generator (2) that entrance is connected with the outlet of the water tank (1)；Entrance
The hydrogen ejector (3) being connected with the outlet of the supersonic generator (2)；Entrance and the hydrogen ejector
(3) hydrogen water mixer (4) that outlet is connected；What the outlet with the hydrogen water mixer (4) was connected
Isobar filling machine (5)；Hydrogen generator (6), the hydrogen generator (6) first gas outlet with
The first gas entrance of the hydrogen ejector (3) is connected, the second gas outlet of the hydrogen generator with
The second gas entrance of the hydrogen water mixer (4) is connected, the third gas outlet of the hydrogen generator
It is connected with the third gas entrance of the isobar filling machine (5).The preparation neutrality saturation hydrogen that the present invention is provided
Water through the multi task process of pre-hydrogenation, spraying mixing and isobar filling, is included by the system of water in the shelf-life
Hydrogen amount is not reduced or is shaded less, reaches function hydrogen content >=0.8PPM.
Description of the drawings
The schematic diagram of the system of the preparation neutrality saturation hydrogen water that Fig. 1 is provided for the present invention.
Specific embodiment
The invention provides a kind of system for preparing neutral saturation hydrogen water, it is characterised in that include：
Water tank (1)；
The supersonic generator (2) that entrance is connected with the outlet of the water tank (1)；
The hydrogen ejector (3) that entrance is connected with the outlet of the supersonic generator (2)；
Hydrogen water mixer (4) that entrance is connected with the outlet of the hydrogen ejector (3)；
The isobar filling machine (5) that outlet with the hydrogen water mixer (4) is connected；
Hydrogen generator (6), first gas outlet and the hydrogen ejector of the hydrogen generator (6)
(3) first gas entrance is connected, and the second gas outlet of the hydrogen generator is mixed with the hydrogen water
The second gas entrance of machine (4) is connected, and the third gas outlet of the hydrogen generator and the equipressure are filled
The third gas entrance of installation (5) is connected.
The system that the system of the neutral saturation hydrogen water of preparation that the present invention is provided is provided for the present invention referring to Fig. 1, Fig. 1
The schematic diagram of the system of standby neutrality saturation hydrogen water, in Fig. 1,1 is water tank, and 2 is supersonic generator,
3 is hydrogen ejector, and 4 is hydrogen water mixer, and 5 is isobar filling machine, and 6 is hydrogen generator, and 7 are sealing
Machine, 8 is pump.
The system of the neutral saturation hydrogen water of preparation that the present invention is provided includes water tank (1), the water tank (1)
For storing raw water.
The system of the neutral saturation hydrogen water of preparation that the present invention is provided also includes entrance and the water tank (1)
The supersonic generator (2) that outlet is connected, the supersonic generator (2) is for making the macromolecular mass of water
Some subsets are split into, thus by a macromolecular mass surface fracture of water into N number of little moisture
Son group surface contacts mixing with hydrogen, so as to increase the contact area of hydrone and hydrogen.
The system of the neutral saturation hydrogen water of preparation that the present invention is provided also includes entrance and the supersonic generator
(2) the hydrogen ejector (3) that outlet is connected, used in hydrogen water treatment procedure, hydrogen ejector (3) is by original
Water pre-hydrogenation, makes water bound fraction hydrogen molecule first in the middle of the flowing.
The system of the neutral saturation hydrogen water of preparation that the present invention is provided is in the water tank (1) and the ultrasound wave
Pump (8) is additionally provided between generator (2).The pump (8) is for by the water pump excess of imports in water tank
In sonic generator (2).
The system of the neutral saturation hydrogen water of preparation that the present invention is provided also includes entrance and the hydrogen ejector (3)
Hydrogen water mixer (4) that is connected of outlet, the hydrogen room of the hydrogen water mixer (4) is for by pre-hydrogenation
Water is sprayed, and obtains the water of subset, and the water of the subset can be made with fully being mixed with hydrogen
In water, the content of hydrogen reaches full conjunction state.
The system of the neutral saturation hydrogen water of preparation that the present invention is provided also includes and the hydrogen water mixer (4)
The isobar filling machine (5) that outlet is connected, the isobar filling machine (5) is that the saturation hydrogen water that will be obtained is carried out
The place of fill.In the present invention, the pressure in pouring process is substantially same with the pressure of hydrogen water mixer presses,
The full hydrogen water for closing is not decayed detached condition, makes the hydrogeneous water of full conjunction ensure to irrigate in the state of full conjunction
To in the strong container of sealing.
The system of the neutral saturation hydrogen water of preparation that the present invention is provided also includes hydrogen generator (6), the hydrogen
The first gas outlet of gas generator (6) is connected with the first gas entrance of the hydrogen ejector (3),
The second gas outlet of the hydrogen generator is connected with the second gas entrance of the hydrogen water mixer (4),
The third gas outlet of the hydrogen generator is connected with the third gas entrance of the isobar filling machine (5).
The hydrogen of generation is transported in hydrogen ejector (3), hydrogen water mixer (4) and is waited by the hydrogen generator
In pressure filling machine (5), so as to mix with water.
The system of the neutral saturation hydrogen water of preparation that the present invention is provided also includes entrance and the isobar filling machine
(5) sealer (7) that outlet is connected.The sealer (7) for by the fill in container
Neutral saturation hydrogen water-stop.
Present invention also offers a kind of preparation method of neutral saturation hydrogen water, comprises the following steps：
Hydrogen generator provides the same of hydrogen to the hydrogen ejector, hydrogen water mixer and isobar filling machine
When, the water after supersonic generator ultrasound is sequentially passed through into hydrogen ejector pre-hydrogenation, hydrogen water mixer
After mixing and isobar filling machine fill, neutral saturation hydrogen water is obtained.
Water is carried out ultrasound in supersonic generator by the present invention first, wherein, it is in the present invention, described
Water is preferably natural spring water, natural mineral water or pure water, more preferably natural spring water or natural ore
Spring water.The present invention does not have particular restriction to the method for the ultrasound, well known to a person skilled in the art super
Method for acoustic, in the present invention, the ultrasound is preferably carried out in accordance with the following methods：
Water acts under the Ultrasonic Conditions of 20-40Hz the 50-70 seconds to be de-gassed again.
The present invention carries out water after ultrasound, the oxygen contained in water and CO2It is ultrasonic etc. gas Jing soluble in water
The effect of ripple is discharged, and can dissolve in hydrogen Jing after vacuum outgass to a greater extent.
Also, water is after the ultrasound of the supersonic generator (2), split into the macromolecular mass of water
Some subsets, thus by a macromolecular mass surface fracture of water into N number of little water clusters table
Face contacts mixing with hydrogen, so as to increase the contact area of hydrone and hydrogen.
Water after ultrasound sequentially passes through hydrogen ejector pre-hydrogenation, the mixing of hydrogen water mixer and isobaric filling
Installation fill, also, while above-mentioned steps are carried out, hydrogen generator is to the hydrogen ejector, hydrogen
Water mixer and isobar filling machine provide hydrogen.
Wherein, the hydrogen generator produces hydrogen by electrolysis water, and the yield of the hydrogen is
250～300 cubic meters/hour, aerogenesis pressure 0.2-0.4MPa.The hydrogen input hydrogen ejector of generation,
Hydrogen water mixer and wait stream pressure filling machine, mixed with water therethrough, in preparing
Property saturation hydrogen water.
Specifically, the water after ultrasound initially enters hydrogen ejector and carries out pre-hydrogenation, obtains pre- hydrogen
The water of change.The pressure of the pre-hydrogenation is 0.2-0.4MPa, preferably 0.25-0.3MPa.In pre-hydrogenation mistake
Cheng Zhong, water bound fraction hydrogen molecule first in ejector.
Water after pre-hydrogenation is mixed with hydrogen in hydrogen water mixer, specifically,
Spray in hydrogen room of the water of the pre-hydrogenation after hydrogen ejector in hydrogen water mixer, obtain little
The water of micel；
The water of the subset is mixed with hydrogen, obtains the hydrogeneous water of saturation.
Wherein, the pressure in the hydrogen room is 0.2～0.4MPa, preferably 0.25～0.3MPa；The mixing
Time be 15～20min, preferably 16～18min.
The hydrogeneous water of the saturation for obtaining is input in isobar filling machine, wherein, in the isobar filling machine
Pressure is 1 with the pressure ratio in the hydrogen water mixer:(0.95～1.05), preferably 1:1.Full conjunction state
Hydrogeneous water in pouring process, may part not by hydrone wrap up firm hydrogen molecule produce it is free,
Separate with hydrone.Therefore in the present invention, isobar filling, such pouring process are adopted in pouring process
In pressure and hydrogen water mixer pressure substantially with pressing, the full hydrogen water for closing is not decayed detached condition,
The hydrogeneous water of full conjunction is made to ensure to be filled in the strong container of sealing in the state of full conjunction.
The preparation method of the neutral saturation hydrogen water that the present invention is provided also is included the saturation hydrogen water after the fill
Sealed, after sealing, obtained neutral saturation hydrogen aquatic products.
Present invention also offers the neutral saturation hydrogen water that a kind of said method is prepared, wherein, it is described in
Property saturation hydrogen water in hydrogen content be 1.0～1.2ppm.
The system of the neutral saturation hydrogen water of preparation that the present invention is provided is by water is through pre-hydrogenation, spraying mixing and waits
The multi task process of pressure fill, shelf-life hydrogen content do not reduce or shade it is few, reach function hydrogen content >=
0.8PPM。
For a further understanding of the present invention, with reference to the neutral saturation hydrogen water that embodiment is provided to the present invention
And preparation method thereof and a kind of system for preparing neutral saturation hydrogen water illustrate, the present invention protection model
Enclose and be not limited by the following examples.
The system of the neutral saturation hydrogen water of preparation of 1 laboratory level of embodiment
Using the container of 50L volumes as water tank, the outlet of the water tank and the supersonic generator
Entrance be connected, be provided with a pump between the entrance of water tank outlet and the supersonic generator,
For the water in water tank is pumped in supersonic generator, the outlet of the supersonic generator with it is described
The entrance of hydrogen ejector is connected, and the outlet of the hydrogen ejector is connected with the entrance of the hydrogen water mixer
Logical, the outlet of the hydrogen water mixer is connected with the isobar filling machine, wherein, the hydrogen water mixing
Machine is identical with the pressure of the isobar filling machine.The outlet of the isobar filling machine is entered with the sealer
Mouth is connected.Also, the system for preparing neutral saturation hydrogen water also includes hydrogen generator, the hydrogen
The first gas outlet of gas generator is connected with the first gas entrance of the hydrogen ejector, and the hydrogen is sent out
The second gas outlet of raw device is connected with the second gas entrance of the hydrogen water mixer, and the hydrogen occurs
The third gas outlet of device is connected with the third gas entrance of the isobar filling machine.
The system of the neutral saturation hydrogen water of preparation of 2 factory-level of embodiment
Using the container of 5000L volumes as water tank, the outlet of the water tank is occurred with the ultrasound wave
The entrance of device is connected, and is provided with one between the entrance of the water tank outlet and the supersonic generator
Pump, for the water in water tank is pumped in supersonic generator, the outlet of the supersonic generator with
The entrance of the hydrogen ejector is connected, the entrance of the outlet of the hydrogen ejector and the hydrogen water mixer
It is connected, the outlet of the hydrogen water mixer is connected with the isobar filling machine, wherein, the hydrogen water
Mixer is identical with the pressure of the isobar filling machine.The outlet of the isobar filling machine and the sealer
Entrance be connected.Also, the system for preparing neutral saturation hydrogen water also includes hydrogen generator, institute
The first gas outlet for stating hydrogen generator is connected with the first gas entrance of the hydrogen ejector, the hydrogen
The second gas outlet of gas generator is connected with the second gas entrance of the hydrogen water mixer, the hydrogen
The third gas outlet of generator is connected with the third gas entrance of the isobar filling machine.
Embodiment 3
The system of the neutral saturation hydrogen water of preparation provided using embodiment 1 carries out the preparation of neutral saturation hydrogen water,
Under 25 DEG C of room temperature condition, the natural spring water of 20～21 degrees Celsius of temperature is chosen as raw water, the day
So spring water is selected from the gone out natural spring water of Shandong Laoshan gentleman's spring water factory.
Above-mentioned natural spring water under the Ultrasonic Conditions of 30Hz is acted on 60 seconds entering under vacuum again
Row degassing, obtains the raw water after ultrasound.
Raw water after the ultrasound is carried out into pre-hydrogenation under conditions of 0.3MPa, the water after pre-hydrogenation is obtained.
To spray in hydrogen room of the water after the pre-hydrogenation in hydrogen water mixer, obtain the water of subset,
The water of the subset and hydrogen mixing 20min, obtain the hydrogeneous water of saturation.Wherein, the pressure of hydrogen room
For 0.3MPa, saturation hydrogen water is obtained, the saturation hydrogen water is carried out into fill, wherein, filling pressure is
0.3MPa.The neutral saturation hydrogen water is sealed after fill, obtained product.
The product is carried out into the detection of hydrogen content, wherein hydrogen content is 1.05-1.2ppm.
Product after packaged Jing after calorstat (37 degrees Celsius) is preserved for 90 days determines experiment therein and contains
Hydrogen amount is 0.85-0.9ppm；
By the product after packaged Jing after calorstat (37 degrees Celsius) is preserved for 360 days, determine therein
Experiment hydrogen content is 0.84-0.9ppm.
Embodiment 4
The system of the neutral saturation hydrogen water of preparation provided using embodiment 1 carries out the preparation of neutral saturation hydrogen water,
Under 25 DEG C of room temperature condition, the natural mineral water of 20～21 degrees Celsius of temperature is chosen as raw water, the day
So mineral water is selected from the gone out natural mineral water of Shandong Laoshan gentleman's spring water factory.
Above-mentioned natural mineral water under the Ultrasonic Conditions of 30Hz is acted on 60 seconds entering under vacuum again
Row degassing, obtains the raw water after ultrasound.
Raw water after the ultrasound is carried out into pre-hydrogenation under conditions of 0.3MPa, the water after pre-hydrogenation is obtained.
To spray in hydrogen room of the water after the pre-hydrogenation in hydrogen water mixer, obtain the water of subset,
The water of the subset and hydrogen mixing 15min, obtain the hydrogeneous water of saturation.Wherein, the pressure of hydrogen room
For 0.25MPa, saturation hydrogen water is obtained, the saturation hydrogen water is carried out into fill, wherein, filling pressure is
0.25MPa.The neutral saturation hydrogen water is sealed after fill, obtained product.
The product is carried out into the detection of hydrogen content, wherein hydrogen content is 1.0-1.2ppm.
Product after packaged Jing after calorstat (37 degrees Celsius) is preserved for 90 days determines experiment therein and contains
Hydrogen amount is 0.83-0.91ppm；
By the product after packaged Jing after calorstat (37 degrees Celsius) is preserved for 360 days, determine therein
Experiment hydrogen content is 0.82-0.9ppm.
Embodiment 5
The system of the neutral saturation hydrogen water of preparation provided using embodiment 1 carries out the preparation of neutral saturation hydrogen water,
Under 25 DEG C of room temperature condition, the natural spring water of 20～21 degrees Celsius of temperature is chosen as raw water, the day
So spring water is selected from the gone out natural spring water of Shandong Laoshan gentleman's spring water factory.
Above-mentioned natural spring water under the Ultrasonic Conditions of 20Hz is acted on 60 seconds entering under vacuum again
Row degassing, obtains the raw water after ultrasound.
Raw water after the ultrasound is carried out into pre-hydrogenation under conditions of 0.25MPa, after obtaining pre-hydrogenation
Water.
To spray in hydrogen room of the water after the pre-hydrogenation in hydrogen water mixer, obtain the water of subset,
The water of the subset and hydrogen mixing 16min, obtain the hydrogeneous water of saturation.Wherein, the pressure of hydrogen room
For 0.25MPa, saturation hydrogen water is obtained, the saturation hydrogen water is carried out into fill, wherein, filling pressure is
0.25MPa.The neutral saturation hydrogen water is sealed after fill, obtained product.
The product is carried out into the detection of hydrogen content, wherein hydrogen content is 1.0-1.1ppm.
Product after packaged Jing after calorstat (37 degrees Celsius) is preserved for 90 days determines experiment therein and contains
Hydrogen amount is 0.80-0.83ppm；
By the product after packaged Jing after calorstat (37 degrees Celsius) is preserved for 360 days, determine therein
Experiment hydrogen content is 0.80-0.82ppm.
Embodiment 6
The system of the neutral saturation hydrogen water of preparation provided using embodiment 1 carries out the preparation of neutral saturation hydrogen water,
Under 25 DEG C of room temperature condition, the natural mineral water of 20～21 degrees Celsius of temperature is chosen as raw water, the day
So mineral water is selected from the gone out natural mineral water of Shandong Laoshan gentleman's spring water factory.
Above-mentioned natural mineral water under the Ultrasonic Conditions of 40Hz is acted on 60 seconds entering under vacuum again
Row degassing, obtains the raw water after ultrasound.
Raw water after the ultrasound is carried out into pre-hydrogenation under conditions of 0.3MPa, the water after pre-hydrogenation is obtained.
To spray in hydrogen room of the water after the pre-hydrogenation in hydrogen water mixer, obtain the water of subset,
The water of the subset and hydrogen mixing 18min, obtain the hydrogeneous water of saturation.Wherein, the pressure of hydrogen room
For 0.3MPa, saturation hydrogen water is obtained, the saturation hydrogen water is carried out into fill, wherein, filling pressure is
0.3MPa.The neutral saturation hydrogen water is sealed after fill, obtained product.
The product is carried out into the detection of hydrogen content, wherein hydrogen content is 1.1-1.4ppm.
Product after packaged Jing after calorstat (37 degrees Celsius) is preserved for 90 days determines experiment therein and contains
Hydrogen amount is 0.82-0.92ppm；
By the product after packaged Jing after calorstat (37 degrees Celsius) is preserved for 360 days, determine therein
Experiment hydrogen content is 0.81-0.87ppm.
Embodiment 7
The system of the neutral saturation hydrogen water of preparation provided using embodiment 2 carries out the preparation of neutral saturation hydrogen water,
Under 25 DEG C of room temperature condition, the pure water of 20～21 degrees Celsius of temperature is chosen as raw water, the natural mountain
Spring water is selected from the gone out pure water of Shandong Laoshan gentleman's spring water factory.
Above-mentioned natural spring water under the Ultrasonic Conditions of 30Hz is acted on 60 seconds entering under vacuum again
Row degassing, obtains the raw water after ultrasound.
Raw water after the ultrasound is carried out into pre-hydrogenation under conditions of 0.3MPa, the water after pre-hydrogenation is obtained.
To spray in hydrogen room of the water after the pre-hydrogenation in hydrogen water mixer, obtain the water of subset,
The water of the subset and hydrogen mixing 20min, obtain the hydrogeneous water of saturation.Wherein, the pressure of hydrogen room
For 0.3MPa, saturation hydrogen water is obtained, the saturation hydrogen water is carried out into fill, wherein, filling pressure is
0.3MPa.The neutral saturation hydrogen water is sealed after fill, obtained product.
The product is carried out into the detection of hydrogen content, wherein hydrogen content is 1.03-1.2ppm.
Product after packaged Jing after calorstat (37 degrees Celsius) is preserved for 90 days determines experiment therein and contains
Hydrogen amount is 0.85-0.94ppm；
By the product after packaged Jing after calorstat (37 degrees Celsius) is preserved for 360 days, determine therein
Experiment hydrogen content is 0.83-0.90ppm.
Embodiment 8
The system of the neutral saturation hydrogen water of preparation provided using embodiment 2 carries out the preparation of neutral saturation hydrogen water,
Under 25 DEG C of room temperature condition, the natural mineral water of 20～21 degrees Celsius of temperature is chosen as raw water, the day
So spring water is selected from the gone out mineral water of Shandong Laoshan gentleman's spring water factory.
Above-mentioned natural spring water under the Ultrasonic Conditions of 25Hz is acted on 55 seconds entering under vacuum again
Row degassing, obtains the raw water after ultrasound.
Raw water after the ultrasound is carried out into pre-hydrogenation under conditions of 0.3MPa, the water after pre-hydrogenation is obtained.
To spray in hydrogen room of the water after the pre-hydrogenation in hydrogen water mixer, obtain the water of subset,
The water of the subset and hydrogen mixing 20min, obtain the hydrogeneous water of saturation.Wherein, the pressure of hydrogen room
For 0.3MPa, saturation hydrogen water is obtained, the saturation hydrogen water is carried out into fill, wherein, filling pressure is
0.3MPa.The neutral saturation hydrogen water is sealed after fill, obtained product.
The product is carried out into the detection of hydrogen content, wherein hydrogen content is 1.02-1.2ppm.
Product after packaged Jing after calorstat (37 degrees Celsius) is preserved for 90 days determines experiment therein and contains
Hydrogen amount is 0.82-0.9ppm；
By the product after packaged Jing after calorstat (37 degrees Celsius) is preserved for 360 days, determine therein
Experiment hydrogen content is 0.80-0.9ppm.
Embodiment 9
The system of the neutral saturation hydrogen water of preparation provided using embodiment 2 carries out the preparation of neutral saturation hydrogen water,
Under 25 DEG C of room temperature condition, the natural mineral water of 20～21 degrees Celsius of temperature is chosen as raw water, the day
So mineral water is selected from the gone out natural mineral water of Shandong Laoshan gentleman's spring water factory.
Above-mentioned natural mineral water under the Ultrasonic Conditions of 35Hz is acted on 60 seconds entering under vacuum again
Row degassing, obtains the raw water after ultrasound.
Raw water after the ultrasound is carried out into pre-hydrogenation under conditions of 0.35MPa, after obtaining pre-hydrogenation
Water.
To spray in hydrogen room of the water after the pre-hydrogenation in hydrogen water mixer, obtain the water of subset,
The water of the subset and hydrogen mixing 18min, obtain the hydrogeneous water of saturation.Wherein, the pressure of hydrogen room
For 0.25MPa, saturation hydrogen water is obtained, the saturation hydrogen water is carried out into fill, wherein, filling pressure is
0.25MPa.The neutral saturation hydrogen water is sealed after fill, obtained product.
The product is carried out into the detection of hydrogen content, wherein hydrogen content is 1.0-1.19ppm.
Product after packaged Jing after calorstat (37 degrees Celsius) is preserved for 90 days determines experiment therein and contains
Hydrogen amount is 0.84-0.9ppm；
By the product after packaged Jing after calorstat (37 degrees Celsius) is preserved for 360 days, determine therein
Experiment hydrogen content is 0.82-0.9ppm.
It is 1.0-1.2PPM that the Jing present invention produces hydrogen content, and (37 is Celsius for packaged rear product Jing calorstats
Degree) 90 days experiment hydrogen contents are between 0.82-0.82PPM.Product detection in 360 days at normal temperatures is hydrogeneous
Amount is between 0.82-0.9PPM.
Embodiment 10
The system of the neutral saturation hydrogen water of preparation provided using embodiment 2 carries out the preparation of neutral saturation hydrogen water,
Under 25 DEG C of room temperature condition, the pure water of 20～21 degrees Celsius of temperature is chosen as raw water, the natural mountain
Spring water is selected from the gone out pure water of Shandong Laoshan gentleman's spring water factory.
Above-mentioned natural spring water under the Ultrasonic Conditions of 20Hz is acted on 60 seconds entering under vacuum again
Row degassing, obtains the raw water after ultrasound.
Raw water after the ultrasound is carried out into pre-hydrogenation under conditions of 0.25MPa, after obtaining pre-hydrogenation
Water.
To spray in hydrogen room of the water after the pre-hydrogenation in hydrogen water mixer, obtain the water of subset,
The water of the subset and hydrogen mixing 16min, obtain the hydrogeneous water of saturation.Wherein, the pressure of hydrogen room
For 0.25MPa, saturation hydrogen water is obtained, the saturation hydrogen water is carried out into fill, wherein, filling pressure is
0.25MPa.The neutral saturation hydrogen water is sealed after fill, obtained product.
The product is carried out into the detection of hydrogen content, wherein hydrogen content is 1.0-1.15ppm.
Product after packaged Jing after calorstat (37 degrees Celsius) is preserved for 90 days determines experiment therein and contains
Hydrogen amount is 0.83-0.90ppm；
By the product after packaged Jing after calorstat (37 degrees Celsius) is preserved for 360 days, determine therein
Experiment hydrogen content is 0.82-0.89ppm.
Embodiment 11
The system of the neutral saturation hydrogen water of preparation provided using embodiment 2 carries out the preparation of neutral saturation hydrogen water,
Under 25 DEG C of room temperature condition, the natural mineral water of 20～21 degrees Celsius of temperature is chosen as raw water, the day
So spring water is selected from the gone out mineral water of Shandong Laoshan gentleman's spring water factory.
Above-mentioned natural spring water under the Ultrasonic Conditions of 40Hz is acted on 55 seconds entering under vacuum again
Row degassing, obtains the raw water after ultrasound.
Raw water after the ultrasound is carried out into pre-hydrogenation under conditions of 0.3MPa, the water after pre-hydrogenation is obtained.
To spray in hydrogen room of the water after the pre-hydrogenation in hydrogen water mixer, obtain the water of subset,
The water of the subset and hydrogen mixing 20min, obtain the hydrogeneous water of saturation.Wherein, the pressure of hydrogen room
For 0.3MPa, saturation hydrogen water is obtained, the saturation hydrogen water is carried out into fill, wherein, filling pressure is
0.3MPa.The neutral saturation hydrogen water is sealed after fill, obtained product.
The product is carried out into the detection of hydrogen content, wherein hydrogen content is 1.1-1.2ppm.
Product after packaged Jing after calorstat (37 degrees Celsius) is preserved for 90 days determines experiment therein and contains
Hydrogen amount is 0.81-0.92ppm；
By the product after packaged Jing after calorstat (37 degrees Celsius) is preserved for 360 days, determine therein
Experiment hydrogen content is 0.81-0.88ppm.
The above is only the preferred embodiment of the present invention, it is noted that general for the art
For logical technical staff, under the premise without departing from the principles of the invention, some improvement and profit can also be made
Decorations, these improvements and modifications also should be regarded as protection scope of the present invention.
Claims (13)
1. a kind of system for preparing neutral saturation hydrogen water, it is characterised in that include：
Water tank (1)；
The supersonic generator (2) that entrance is connected with the outlet of the water tank (1)；
The hydrogen ejector (3) that entrance is connected with the outlet of the supersonic generator (2)；
Hydrogen water mixer (4) that entrance is connected with the outlet of the hydrogen ejector (3)；
The isobar filling machine (5) that outlet with the hydrogen water mixer (4) is connected；
Hydrogen generator (6), first gas outlet and the hydrogen ejector of the hydrogen generator (6)
(3) first gas entrance is connected, and the second gas outlet of the hydrogen generator is mixed with the hydrogen water
The second gas entrance of machine (4) is connected, and the third gas outlet of the hydrogen generator and the equipressure are filled
The third gas entrance of installation (5) is connected.
2. system according to claim 1, it is characterised in that also including entrance and described isobaric fill
The sealer (7) that the outlet of installation (5) is connected.
3. system according to claim 1, it is characterised in that in the water tank (1) and institute
State and between supersonic generator (2), be additionally provided with pump (8).
4. a kind of preparation method of neutral saturation hydrogen water, it is characterised in that comprise the following steps：
Hydrogen generator is to the hydrogen ejector, hydrogen water mixer and waits stream pressure filling machine to provide hydrogen
Meanwhile, the water after supersonic generator ultrasound is sequentially passed through into hydrogen ejector pre-hydrogenation, the mixing of hydrogen water
After machine mixing and isobar filling machine fill, neutral saturation hydrogen water is obtained.
5. preparation method according to claim 4, it is characterised in that also including will be described neutral full
Sealed in sealer with hydrogen water.
6. preparation method according to claim 4, it is characterised in that the wet concentration is from natural mountain spring
Water, natural mineral water or pure water.
7. preparation method according to claim 4, it is characterised in that the ultrasound is according to lower section
Method is carried out：
Water acts under the Ultrasonic Conditions of 20-40Hz the 50-70 seconds to be de-gassed again.
8. preparation method according to claim 4, it is characterised in that the hydrogen ejector pre-hydrogenation
Pressure be 0.2～0.4MPa.
9. preparation method according to claim 4, it is characterised in that the hydrogen water mixer mixing
Carry out as follows：
Spray in the hydrogen room through the water of hydrogen ejector and pre-hydrogenation in hydrogen water mixer, obtain little
The water of micel；
The water of the subset is mixed with hydrogen, obtains the hydrogeneous water of saturation.
10. preparation method according to claim 9, it is characterised in that the pressure in the hydrogen room
For 0.2～0.4MPa.
11. preparation methoies according to claim 9, it is characterised in that the time of the mixing is
15～20min.
12. preparation methoies according to claim 4, it is characterised in that in the isobar filling machine
Pressure and the hydrogen water mixer in pressure ratio be 1：(0.95～1.05).
The neutral saturation that a kind of 13. preparation methoies by described in claim 4～12 any one are prepared
Hydrogen water, the hydrogen content in the neutral saturation hydrogen water are 1.0～1.2ppm.
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