CN106551423B - Negative ion melt-blown superfine fiber cigarette filter tip material and preparation method thereof - Google Patents
Negative ion melt-blown superfine fiber cigarette filter tip material and preparation method thereof Download PDFInfo
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- CN106551423B CN106551423B CN201611097430.5A CN201611097430A CN106551423B CN 106551423 B CN106551423 B CN 106551423B CN 201611097430 A CN201611097430 A CN 201611097430A CN 106551423 B CN106551423 B CN 106551423B
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- A—HUMAN NECESSITIES
- A24—TOBACCO; CIGARS; CIGARETTES; SIMULATED SMOKING DEVICES; SMOKERS' REQUISITES
- A24D—CIGARS; CIGARETTES; TOBACCO SMOKE FILTERS; MOUTHPIECES FOR CIGARS OR CIGARETTES; MANUFACTURE OF TOBACCO SMOKE FILTERS OR MOUTHPIECES
- A24D3/00—Tobacco smoke filters, e.g. filter-tips, filtering inserts; Filters specially adapted for simulated smoking devices; Mouthpieces for cigars or cigarettes
- A24D3/02—Manufacture of tobacco smoke filters
- A24D3/0229—Filter rod forming processes
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- D—TEXTILES; PAPER
- D01—NATURAL OR MAN-MADE THREADS OR FIBRES; SPINNING
- D01F—CHEMICAL FEATURES IN THE MANUFACTURE OF ARTIFICIAL FILAMENTS, THREADS, FIBRES, BRISTLES OR RIBBONS; APPARATUS SPECIALLY ADAPTED FOR THE MANUFACTURE OF CARBON FILAMENTS
- D01F1/00—General methods for the manufacture of artificial filaments or the like
- D01F1/02—Addition of substances to the spinning solution or to the melt
- D01F1/10—Other agents for modifying properties
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- D—TEXTILES; PAPER
- D01—NATURAL OR MAN-MADE THREADS OR FIBRES; SPINNING
- D01F—CHEMICAL FEATURES IN THE MANUFACTURE OF ARTIFICIAL FILAMENTS, THREADS, FIBRES, BRISTLES OR RIBBONS; APPARATUS SPECIALLY ADAPTED FOR THE MANUFACTURE OF CARBON FILAMENTS
- D01F6/00—Monocomponent artificial filaments or the like of synthetic polymers; Manufacture thereof
- D01F6/44—Monocomponent artificial filaments or the like of synthetic polymers; Manufacture thereof from mixtures of polymers obtained by reactions only involving carbon-to-carbon unsaturated bonds as major constituent with other polymers or low-molecular-weight compounds
- D01F6/46—Monocomponent artificial filaments or the like of synthetic polymers; Manufacture thereof from mixtures of polymers obtained by reactions only involving carbon-to-carbon unsaturated bonds as major constituent with other polymers or low-molecular-weight compounds of polyolefins
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- Chemical & Material Sciences (AREA)
- Chemical Kinetics & Catalysis (AREA)
- General Chemical & Material Sciences (AREA)
- Textile Engineering (AREA)
- Manufacturing & Machinery (AREA)
- Filtering Materials (AREA)
- Cigarettes, Filters, And Manufacturing Of Filters (AREA)
Abstract
The invention relates to a negative ion melt-blown superfine fiber cigarette filter material and a preparation method thereof, wherein the negative ion melt-blown superfine fiber cigarette filter material is melt-blown superfine fiber with the diameter of 1-5 mu m; the melt-blown superfine fiber is prepared from 94-99 parts by weight of polypropylene slices and 1-6 parts by weight of nano tourmaline master batches; the nanometer tourmaline master batch is prepared by mixing nanometer tourmaline powder and polypropylene slices, and the content of tourmaline is 20-40% of the mass of the nanometer tourmaline master batch; the melt-blown superfine fiber is subjected to electret treatment. The invention improves the conventional melt-blown method, changes the traditional one-time cloth forming into the direct preparation of superfine fiber bundles, has uniform fiber fineness, has the advantages of small pressure drop, good air permeability and negative ion generation for refreshing air, obviously improves the filtering effect of harmful substances in smoke and can avoid the environmental pollution problem in the production of acetate fibers.
Description
Technical Field
The invention relates to the field of cigarette filter materials and non-woven fields, in particular to a negative ion melt-blown superfine fiber cigarette filter material and a preparation method thereof.
Background
Cigarette smoke contains particulates, commonly referred to as tar. Tar contains a large number of chemical components, 4000 to 5000 being products of incomplete combustion of tobacco. The cigarette filter is used for filtering substances harmful to human bodies, such as tar in tobacco. The present common cigarette filter tip material is acetate fiber cigarette filter tip, and the acetate fiber is produced through wet spinning, and has long production process, harmful solvent and three-waste pollution. In addition, the effect of the cellulose acetate fiber in filtering harmful carcinogenic substances (such as polycyclic aromatic hydrocarbon and aldehyde substances) in the cigarette mainstream smoke is not very ideal, and only about 40% of polycyclic aromatic hydrocarbon substances are removed.
The cigarette filter can filter smoke components to reduce the inhalation amount of tar and nicotine. However, after the cigarette is provided with the cigarette filter, the suction resistance is greatly increased, and the more toxic substances are. Such as carbon monoxide and benzopyrene, are generated by incomplete combustion of organic substances contained in tobacco during smoking, and the larger the resistance is, the less sufficient the oxygen supply is, the more incomplete the combustion is, and the more toxic substances are generated. The finer the fiber, the better the filtration performance. The three main functions of cigarette filters include direct interception, inertial compaction and diffusion precipitation, the most common being direct interception of cigarette filters. Filtration is a complex process, i.e. droplets of tar separate from the smoke and adhere to the surface of the cigarette filter material when they reach it. The thinner the fiber is, the higher the filtering efficiency of the cigarette filter, and the diameter of the acetate fiber used by the conventional filter is 7-20 μm.
Disclosure of Invention
The invention provides a negative ion melt-blown superfine fiber cigarette filter tip material and a preparation method thereof, aiming at solving the problem of low filter efficiency of cigarette filter materials in the prior art.
The technical scheme for solving the technical problems is as follows:
a negative ion melt-blown superfine fiber cigarette filter tip material, the diameter of the melt-blown superfine fiber is 1-5 μm.
Furthermore, the melt-blown superfine fiber is prepared from 94-99 parts by weight of polypropylene material and 1-6 parts by weight of nano tourmaline master batch.
Furthermore, the melt-blown superfine fiber is subjected to electret treatment.
A preparation method of a negative ion melt-blown superfine fiber cigarette filter tip material is characterized by comprising the following steps:
step S1, mixing 94-99 parts by weight of polypropylene material and 1-6 parts by weight of nano tourmaline master batch uniformly to obtain a mixture;
s2, preparing the melt-blown superfine fiber by the melt-blown device by using the mixture;
s3, cooling and bundling the melt-blown superfine fibers sprayed by the melt-blowing device by the cooling and bundling device;
and step S4, the collecting device performs electret treatment and collection on the melt-blown superfine fibers to obtain the electret superfine fiber cigarette filter tip material.
Further, the nano tourmaline master batch of the step S1 is prepared by mixing nano tourmaline materials and polypropylene materials, and the content of tourmaline is 20-40% of the mass of the nano tourmaline master batch.
Further, the cooling bundling device of the step S3 includes a cold air box and a curtain net receiving device; the step S3 specifically includes: the cold air box cools the melt-blown superfine fibers, the cooled melt-blown superfine fibers sequentially fall on a curtain receiving device which is driven along the width direction of a melt-blown die head in a melt-blown device, and the curtain receiving device bundles the melt-blown superfine fibers to obtain superfine fiber bundles.
Further, the cooling bundling device of the step S3 includes a cold air box and a first bundling device; the step S3 specifically includes: the cold air box cools the melt-blown superfine fibers sprayed by the melt-blowing device, and the first bundling device bundles the cooled melt-blown superfine fibers; and the width of the first bundling device along the width direction is not less than the width of a melt-blown die head in the melt-blown device along the width direction.
Furthermore, the melt-blown superfine fibers are cooled and converged by a cooling and bundling device, and are subjected to electret treatment by an electret treatment device.
Furthermore, the electret voltage of the electret processing device is 5-20kV, the electret interval is 20-60mm, and the electret time is 5-10 s.
The invention has the beneficial effects that: the thinner the fiber is, the higher the filtering efficiency of the cigarette filter, the diameter of acetate fiber used by the conventional filter is 7-20 μm, the conventional melt-blowing method cannot prepare fiber bundles, and only fiber non-woven fabric can be prepared. Meanwhile, the curtain net is changed from the movement perpendicular to the width direction of the fiber net of the traditional non-woven fabric preparation into the movement along the width direction of the fiber net, so that the superfine fiber bundle with the diameter of 1-5 mu m can be directly prepared. By adopting the technical scheme of the invention, the fiber with smaller diameter can be prepared, so that the filtering effect of the fiber is improved. The invention also adopts tourmaline as a manufacturing raw material, and the tourmaline can continuously release negative ions. The negative ions are called vitamins in the air, and after being inhaled into a human body, the negative ions can regulate the excitation state of nerve centers, improve the ventilation function of lungs, improve blood circulation, promote metabolism and enhance the immunity of the human body.
The anion melt-blown superfine fiber filter tip material has the advantages of small pressure drop, good air permeability, anion generation, fresh air, obvious improvement on the filtering effect of harmful substances in smoke, and capability of avoiding the environmental pollution problem in the production of acetate fibers. The cigarette filter material adopted by the invention is a thermoplastic material, has rich sources and low price, and the superfine fiber cigarette filter tip material produced by adopting the melt-blowing method has the advantages of simple production process, no pollution and high production efficiency, and the diameter of the obtained superfine fiber is between 1 and 5 mu m, and the diameter is uniformly changed little, so the filter effect is high. Meanwhile, the tourmaline mineral uniformly embedded in the superfine fibers can continuously release high-concentration negative ions, and the cigarette with the negative ion melt-blown superfine fiber cigarette filter tip is manufactured from cigarettes, is packaged into a box, is discarded until being used up, and is always under the action of the negative ions. The long-term effect results in that the content of harmful substances of tar and nicotine is reduced, and a certain fresh-keeping and mildew-proof effect is achieved, so that the irritation of the cigarette is reduced, and the taste is soft. In the smoking process of the cigarette, the smoke after combustion violently collides with high-concentration negative ions when passing through the filter tip by virtue of suction, and harmful components such as tar, nicotine and carbon monoxide in the smoke are further decomposed. Because the length of the filter tip is limited, most negative ions can not work in time and can be sucked into the mouth together with the smoke, but the decomposition effect of the negative ions on harmful ingredients in the smoke is continuously carried out in the oral cavity, the trachea and the lung lobes even in residual smoke discharged by smokers until the smoke is completely exhausted, the electret charge storage performance is good after electret treatment, and the charge retention rate can reach more than 2 years.
Drawings
FIG. 1 is a schematic view of a manufacturing apparatus in a first embodiment of a cooling cluster tool;
FIG. 2 is a schematic view of a manufacturing apparatus in a second embodiment of a cooling cluster tool.
In the drawings, the reference numerals designate the following parts:
1. a melt-blowing device; 2. a cold air box; 3. a screen receiving device; 4. a first bundling device; 5. a collection device; 6. melt-blowing ultrafine fibers; 7. an electret processing device; 8. a fiber channel; 9. an oil tanker; 10. second bundling device
Detailed Description
The principles and features of this invention are described below in conjunction with the following drawings, which are set forth by way of illustration only and are not intended to limit the scope of the invention.
A negative ion melt-blown superfine fiber cigarette filter tip material is melt-blown superfine fiber with the diameter of 1-5 mu m.
The melt-blown superfine fiber is prepared from 94-99 parts by weight of polypropylene material and 1-6 parts by weight of nano tourmaline master batch.
The melt-blown superfine fiber is subjected to electret treatment.
A preparation method of a negative ion melt-blown superfine fiber cigarette filter tip material specifically comprises the following steps:
step S1, mixing 94-99 parts by weight of polypropylene material and 1-6 parts by weight of nano tourmaline master batch uniformly to obtain a mixture;
step S2, the melt-blowing device 1 utilizes the mixture to prepare melt-blown superfine fiber 6;
step S3, the cooling and bundling device cools and bundles the melt-blown superfine fiber 6 sprayed by the melt-blowing device 1;
and step S4, the collecting device 5 performs electret treatment and collection on the melt-blown superfine fibers 6 to obtain the electret superfine fiber cigarette filter tip material.
The nanometer tourmaline master batch of the step S1 is prepared by mixing nanometer tourmaline materials and polypropylene materials, and the content of tourmaline is 20-40% of the mass of the nanometer tourmaline master batch.
In the first embodiment of the cooling bundling apparatus, the cooling bundling apparatus of step S3 includes a cold air box 2 and a curtain receiving apparatus 3; the step S3 specifically includes: the cold air box 3 cools the melt-blown superfine fibers 6, and the cooled melt-blown superfine fibers 6 sequentially fall on the curtain receiving device 3 which is driven along the width direction of the melt-blown die head in the melt-blown device 1, so that superfine fiber bundles are obtained by bundling the melt-blown superfine fibers 6.
And after being collected by the curtain net receiving device 3, the melt-blown superfine fibers 6 are subjected to electret treatment by the electret treatment device 7, further collected by the second collecting device 10 and then enter the collecting device 5.
In the second embodiment of the cooling bundling apparatus, the cooling bundling apparatus in step S3 includes a cold air box 2 and a first bundling apparatus 4; the step S3 specifically includes: the cold air box cools the melt-blown superfine fibers 6 sprayed by the melt-blowing device 1, and the first bundling device 4 bundles the cooled melt-blown superfine fibers 6; and the width of the first bundling device 4 along the width direction is not less than the width of the melt-blowing die head in the melt-blowing device 1 along the width direction.
And after being collected by the first collecting device 4, the melt-blown superfine fibers 6 are subjected to electret treatment by the electret treatment device 7 and then enter the collecting device 5.
The electret voltage of the electret processing device is 5-20kV, the electret interval is 20-60mm, and the electret time is 5-10 s.
As shown in fig. 1 and fig. 2, a device for preparing a negative ion melt-blown ultrafine fiber cigarette filter material comprises a melt-blowing device 1, a cooling bundling device, an electret treatment device and a collecting device;
the melt-blowing device 1 is used for preparing melt-blown superfine fibers 6 and conveying the melt-blown superfine fibers 6 to a cooling bundling device;
the cooling and bundling device is arranged below the melt-blowing device 1 and is used for cooling and bundling the melt-blown superfine fibers 6 sprayed by the melt-blowing device 1 to obtain superfine fiber bundles;
the electret processing device is used for carrying out electret processing on the superfine fiber bundles;
the collecting device is used for processing and collecting the superfine fiber bundles to obtain the electret superfine fiber cigarette filter tip material.
The collecting device 5 is a cutting machine, after the oil tanker 9 oils the melt-blown superfine fiber 6, the guide wire device guides the melt-blown superfine fiber into the cutting machine, and the cutting machine cuts the melt-blown superfine fiber 6 into uniform small sections as the cigarette filter tip material of the anion melt-blown superfine fiber.
Fig. 1 shows a first embodiment of a cooling cluster device, which comprises a cold air box 2 and a curtain receiving device 3;
the cold air box 2 is arranged below a melt-blown die head in the melt-blown device 1 and used for cooling melt-blown superfine fibers 6 sprayed by the melt-blown device 1, and the curtain net receiving device 3 is arranged below the cold air box 2 and used for bundling the cooled melt-blown superfine fibers 6; the curtain net receiving device 3 is driven from one end far away from the electret treating device 7 to one end close to the electret treating device 7 along the width direction of the melt-blown die head in the melt-blown device 1.
A suction device is arranged in the curtain net receiving device 3 and is used for sucking the melt-blown superfine fibers 6 onto the upper surface of the curtain net receiving device 3.
In the first embodiment of the cooling and bundling device, a second bundling device 10 is further disposed between the electret treating device and the collecting device 5 for further bundling the microfiber bundle.
Fig. 2 shows a second embodiment of a cooling cluster device, which includes a cold air box 2 and a first cluster device 4; the cold air box 2 is arranged below a melt-blown die head in the melt-blown device 1 and used for cooling melt-blown superfine fibers 6 sprayed by the melt-blown device 1, and the first bundling device 4 is arranged below the cold air box 2 and used for bundling the cooled melt-blown superfine fibers 6 to obtain superfine fiber bundles; the superfine fiber bundle is conveyed to an electret processing device 7 through a fiber channel 8, and the superfine fiber enters a collecting device for cutting and collecting after being processed by the electret. The fiber channel 8 is used for supporting and guiding the fiber bundle and can be in the form of a supporting plate and the like. The width of the first bundling device 4 along the width direction is not less than the width of the melt-blowing die head in the melt-blowing device 1 along the width direction, so that all the superfine fibers sprayed by the melt-blowing device can enter the bundling device 4 for bundling.
The first bundling device 4 and the second bundling device 10 can both adopt horn-mouth bundling devices. The second bundling device 10, the thread guiding device and the cutting machine can be fixed by means of a bracket or the like.
Example 1
A method for melting and spraying superfine fiber cigarette filter tip material by negative ions comprises the following steps:
s1, crushing tourmaline into nano-scale, mixing with polypropylene slices to prepare nano tourmaline master batches, wherein the content of tourmaline in the nano tourmaline master batches accounts for 20% of the mass of the tourmaline master batches;
s2, uniformly mixing 96 parts by weight of polypropylene granules and 4 parts by weight of nano tourmaline master batches to obtain a mixture;
s3, setting the temperatures of four areas of a preparation device for the negative ion melt-blown superfine fiber cigarette filter material to be 260 ℃, 260 ℃, 270 ℃ and 270 ℃, respectively, feeding the mixture obtained in the step S2 into a bin of a screw extruder, and forming a melt through the screw melt extruder;
step S4, ejecting the melt through a spinneret plate after passing through a metering pump, drafting the melt at 220 ℃ and under 0.4MPa hot air to obtain melt-blown superfine fibers, and bundling the melt-blown superfine fibers by using a curtain collecting device or a bundling device after cooling;
step S5, performing electret treatment on the melt-blown superfine fibers obtained in the step S4 in a high-voltage corona discharge mode, wherein the electret voltage is 20kV, the electret interval is 20mm, and the electret time is 10S;
and step S6, collecting the melt-blown superfine fibers subjected to electret treatment into bundles in sequence, gluing, forming and cutting to obtain the negative ion melt-blown superfine fiber cigarette filter tip material.
The average diameter of the superfine fiber of the anion melt-blown superfine fiber cigarette filter material prepared by the embodiment is 4 mu m, and the anion concentration in the air can be increased by 800 pieces/cm3And the filtering efficiency reaches 95 percent.
Example 2
S1, crushing tourmaline into nano-scale, mixing with polypropylene slices to prepare nano tourmaline master batches, wherein the content of tourmaline in the nano tourmaline master batches is 30% of the mass of the tourmaline master batches;
step S2, uniformly mixing 95 parts by weight of polypropylene granules and 5 parts by weight of nano tourmaline master batches to obtain a mixture;
s3, setting the temperatures of four areas of the negative ion melt-blown superfine fiber cigarette filter material preparation device to be 260 ℃, 260 ℃, 270 ℃ and 270 ℃, respectively, feeding the mixture obtained in the step S2 into a bin of a screw extruder, and forming a melt through the screw melt extruder;
step S4, ejecting the melt through a spinneret plate after passing through a metering pump, drafting the melt at 220 ℃ and under 0.4MPa hot air to obtain melt-blown superfine fibers, and bundling the melt-blown superfine fibers by using a curtain collecting device or a bundling device after cooling;
step S5, performing electret treatment on the melt-blown superfine fibers obtained in the step S4 in a high-voltage corona discharge mode, wherein the electret voltage is 20kV, the electret interval is 20mm, and the electret time is 10S;
and step S6, collecting the melt-blown superfine fibers subjected to electret treatment into bundles in sequence, gluing, forming and cutting to obtain the negative ion melt-blown superfine fiber cigarette filter tip material.
The average diameter of the superfine fibers of the anion melt-blown superfine fiber cigarette filter material prepared by the embodiment reaches 2 mu m, and the anion concentration in the air can be increased by 1200/cm3And the filtering efficiency reaches 98 percent.
The above description is only for the purpose of illustrating the preferred embodiments of the present invention and is not to be construed as limiting the invention, and any modifications, equivalents, improvements and the like that fall within the spirit and principle of the present invention are intended to be included therein.
Claims (6)
1. A preparation method of a negative ion melt-blown superfine fiber cigarette filter tip material is characterized by comprising the following steps:
step S1, mixing 94-99 parts by weight of polypropylene material and 1-6 parts by weight of nano tourmaline master batch uniformly to obtain a mixture;
s2, preparing the melt-blown superfine fiber (6) by the melt-blowing device (1) by using the mixture;
s3, cooling and bundling the melt-blown superfine fibers (6) sprayed by the melt-blowing device (1) by the cooling and bundling device;
the cooling bundling device in the step S3 comprises a cold air box (2) and a curtain net receiving device (3); the step S3 specifically includes: the cold air box (2) cools the melt-blown superfine fibers (6), the cooled melt-blown superfine fibers (6) sequentially fall on a curtain receiving device (3) which is driven along the width direction of a melt-blown die head in the melt-blown device (1), and the curtain receiving device (3) bunches the melt-blown superfine fibers (6) to obtain superfine fiber bundles;
and S4, processing and collecting the melt-blown superfine fibers (6) by the collecting device (5) to obtain the negative ion melt-blown superfine fiber cigarette filter material.
2. The method for preparing a negative ion melt-blown ultrafine fiber cigarette filter material according to claim 1, wherein the nano tourmaline master batch of step S1 is prepared by mixing nano tourmaline material and polypropylene material, and the content of tourmaline is 20-40% of the mass of the nano tourmaline master batch.
3. The method for preparing the negative ion melt-blown ultrafine fiber cigarette filter material according to claim 1, wherein the cooling bundling device of the step S3 includes a cold air box (2) and a first bundling device (4); the step S3 specifically includes: the cold air box cools the melt-blown superfine fibers (6) sprayed by the melt-blowing device (1), and the first bundling device (4) bundles the cooled melt-blown superfine fibers (6); and the width of the first bundling device (4) along the width direction is not less than the width of the melt-blown die head in the melt-blown device (1) along the width direction.
4. The method for preparing the negative ion melt-blown superfine fiber cigarette filter material according to claim 1, wherein the melt-blown superfine fiber (6) is cooled and converged by a cooling and bundling device, and is subjected to electret treatment by an electret treatment device (4).
5. The method for preparing the anion melt-blown superfine fiber cigarette filter material according to claim 4, wherein the electret voltage of the electret treatment device (4) is 5-20kV, the electret interval is 20-60mm, and the electret time is 5-10 s.
6. An anion melt-blown ultrafine fiber cigarette filter material, characterized by being made of melt-blown ultrafine fiber bundles, wherein the melt-blown ultrafine fiber bundles are made by the method of any one of claims 1 to 5, and the diameter of the melt-blown ultrafine fibers in the melt-blown ultrafine fiber bundles is 1 to 5 μm.
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CN107981444A (en) * | 2018-01-02 | 2018-05-04 | 山东省圣泉生物质石墨烯研究院 | A kind of antibacterial oxygenation mask and preparation method thereof |
CN111548553A (en) * | 2020-03-31 | 2020-08-18 | 上海普利特复合材料股份有限公司 | Low odor, long lasting electret effect polypropylene homopolymers for melt blown fibers |
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