CN106544170A - A kind of preparation method of the quick-acting adhesive removers of green broad spectrum - Google Patents
A kind of preparation method of the quick-acting adhesive removers of green broad spectrum Download PDFInfo
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- CN106544170A CN106544170A CN201610879939.9A CN201610879939A CN106544170A CN 106544170 A CN106544170 A CN 106544170A CN 201610879939 A CN201610879939 A CN 201610879939A CN 106544170 A CN106544170 A CN 106544170A
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- China
- Prior art keywords
- arachidis hypogaeae
- semen arachidis
- quick
- broad spectrum
- fructus gleditsia
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Classifications
-
- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
- C11D1/00—Detergent compositions based essentially on surface-active compounds; Use of these compounds as a detergent
- C11D1/66—Non-ionic compounds
- C11D1/83—Mixtures of non-ionic with anionic compounds
-
- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
- C11D3/00—Other compounding ingredients of detergent compositions covered in group C11D1/00
- C11D3/16—Organic compounds
- C11D3/38—Products with no well-defined composition, e.g. natural products
- C11D3/382—Vegetable products, e.g. soya meal, wood flour, sawdust
-
- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
- C11D3/00—Other compounding ingredients of detergent compositions covered in group C11D1/00
- C11D3/16—Organic compounds
- C11D3/38—Products with no well-defined composition, e.g. natural products
- C11D3/384—Animal products
-
- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
- C11D1/00—Detergent compositions based essentially on surface-active compounds; Use of these compounds as a detergent
- C11D1/02—Anionic compounds
- C11D1/12—Sulfonic acids or sulfuric acid esters; Salts thereof
- C11D1/22—Sulfonic acids or sulfuric acid esters; Salts thereof derived from aromatic compounds
-
- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
- C11D1/00—Detergent compositions based essentially on surface-active compounds; Use of these compounds as a detergent
- C11D1/66—Non-ionic compounds
- C11D1/662—Carbohydrates or derivatives
Abstract
The invention discloses a kind of preparation method of the quick-acting adhesive removers of green broad spectrum, belongs to adhesive remover preparing technical field.Fructus Gleditsia fruit is made concentrated by rotary evaporation after serosity by the present invention first, the heated evaporative crystallization of concentrated solution for obtaining, obtain Fructus Gleditsia berry extract, subsequently baking after peanut husking is broken into pieces, remove Testa arachidis hypogaeae and ball milling is into slurry, obtain Semen arachidis hypogaeae slurry, its surface mucus is obtained by artificial cultivation Misgurni anguillicaudati again, rotate after being sterilized, the stick-slip concentrated solution for obtaining and Fructus Gleditsia berry extract, Semen arachidis hypogaeae slurry and dodecylbenzene sodium sulfonate high-speed stirred make emulsion, fill, obtain final product the quick-acting adhesive removers of green broad spectrum, the quick-acting adhesive remover strong applicabilities of green broad spectrum obtained in of the invention, use without the need for heating, fouled surfaces need to be sprayed on only, removing glue speed is fast, and do not contain toxic solvent, will not be to human body and environmental concerns during use, with wide application space.
Description
Technical field
The invention discloses a kind of preparation method of the quick-acting adhesive removers of green broad spectrum, belongs to adhesive remover preparing technical field.
Background technology
According to statistics, after annual golden week, 400,000 square metres of the Tian'anmen Square will remain 40～600,000 pieces of discarded mouths
Fragrant sugar, it is extremely difficult because removing chewing gum residue, and appearance of the city civilization is had a strong impact on, country is by public place discarded chewing gum
Removing is classified as problem demanding prompt solution.Additionally, the illegal ad in each city covers the sky and the earth, these label pasters, oil pen are formed
Fouling Cleaning gets up abnormal difficult, is referred to as " city psoriasis " by vivid.
The main method for removing discarded chewing gum both at home and abroad has solvent method, emulsion method, the cleaning of high pressure wetting system, dry ice equipment
Cleaning and mechanical cleaning.Raw material used in solvent and emulsion method cleaning mostly is not environmentally solvent such as tetrachloroethylene, ethyl acetate
Toxic solvents are belonged to Deng, these solvents, the suction of Jing human bodies there can be hepatic injury, dermatitis and eczema etc., severe patient can be caused even to cause
Extremely, while causing serious harm to environment.Though water under high pressure and dry ice cleaning method safety and environmental protection, thoroughly can quickly remove mouth fragrant
Sugared dirt, but equipment initial stage input is big, should not promote the use of.Portable cleaning device tool has that removing is halfway.
A kind of chemical agent of synthesis of adhesive remover, can be quick, convenient effective removal oils and fatss, the chemical composition such as glue,
Play a part of clean surface.Adhesive remover can remove organic gel, glass cement, double faced adhesive tape, adhesive sticker, plastic uptake glue, flexible glue, acrylic acid
Resin glue, epoxide-resin glue, polyurethane glue etc., can also will residue in the paste on surface, glue stain and remove easily, product consumption compared with
It is few.
But the existing adhesive remover suitability is not strong, need to heat and could use, longer the time required to removing glue, and in adhesive remover
Containing toxic solvent, can be to human body and environmental concerns during use.
The content of the invention
Present invention mainly solves technical problem：Not strong for the current existing adhesive remover suitability, need to heat can just make
With, it is longer the time required to removing glue, and in adhesive remover contain toxic solvent, during use can to human body and the problem of environmental concerns,
A kind of preparation method of the quick-acting adhesive removers of green broad spectrum is provided, Fructus Gleditsia fruit is made concentrated by rotary evaporation after serosity, obtained by the method first
The heated evaporative crystallization of concentrated solution for arriving, obtains Fructus Gleditsia berry extract, subsequently breaks baking after peanut husking into pieces, removes Testa arachidis hypogaeae
And ball milling is into slurry, Semen arachidis hypogaeae slurry is obtained, then its surface mucus is obtained by artificial cultivation Misgurni anguillicaudati, rotated after being sterilized, obtain
Stick-slip concentrated solution makes emulsion with Fructus Gleditsia berry extract, Semen arachidis hypogaeae slurry and dodecylbenzene sodium sulfonate high-speed stirred, and fill is obtained final product
The quick-acting adhesive removers of green broad spectrum, the quick-acting adhesive remover strong applicabilities of green broad spectrum obtained in the present invention, use without the need for heating, only need spray
Fouled surfaces are coated in, removing glue speed is fast, and does not contain toxic solvent, human body and environmental concerns will not be had during use
There is wide application space.
In order to solve above-mentioned technical problem, the technical solution adopted in the present invention is：
（1）200～300g Fructus Gleditsias fruit is weighed, deionized water is cleaned 3～5 times repeatedly, removes surface contaminants, then by after cleaning
In Fructus Gleditsia fruit input stone mortar, 15～20min is beaten with mallet, be mixed into 100～200mL deionized waters, obtain soap during beaing
Pod serosity, filters, and removes filtering residue, collects filtrate, and is proceeded in Rotary Evaporators, under the conditions of temperature is 80～85 DEG C
Concentrated by rotary evaporation obtains concentrated solution, then is proceeded in evaporating dish to the 1/2 of original volume, heating evaporation crystallization, obtains Fructus Gleditsia fruit and extracts
Thing, it is standby；
（2）Weigh 300～500g Semen arachidis hypogaeaes, peel off Pericarppium arachidis hypogaeae, gained Semen arachidis hypogaeae is placed in baking oven, in temperature be 140～150 DEG C
Under the conditions of, 4～5h is toasted, is stirred once every 30～45min, discharged, treat that Semen arachidis hypogaeae naturally cools to room temperature, will with rubber hammer
Semen arachidis hypogaeae is crushed, then is proceeded in cyclone separator, is separated off Semen arachidis hypogaeae scarlet, then Semen arachidis hypogaeae is proceeded in ball mill,
It is 30 by ratio of grinding media to material：1～45：1 adds ball milling pearl, 15～20min of ball-milling treatment, discharging to stand 36～48h, obtain Semen arachidis hypogaeae slurry,
It is standby；
（3）10～20L tap waters are added in the sink, are added 2～4kg Misgurni anguillicaudatis, and are accessed oxygen increasing pump in tank, carry out mud
Loach cultivates 3～5 days, is subsequently isolated removing Misgurni anguillicaudati, tap water in tank is stood, draw 1～2L tank superficial waters with syringe,
Be placed in beaker, with ultraviolet disinfection process 15～20min, then by burn water in the cup pour Rotary Evaporators into, in temperature be 60～
Under the conditions of 65 DEG C, the 1/3 of concentrated by rotary evaporation to original volume, obtain stick-slip concentrated solution；
（4）Count by weight, 100～120 parts of above-mentioned gained stick-slip concentrated solutions, 8～10 parts of steps are sequentially added in batch mixer
Suddenly（1）Standby Fructus Gleditsia berry extract, 60～80 parts of steps（2）Standby Semen arachidis hypogaeae slurry, 2～4 parts of dodecylbenzene sodium sulfonate, with
800～1000r/min rotating speeds stirring 45～60min of mixing, discharging, fill obtain final product the quick-acting adhesive removers of green broad spectrum.
The present invention application process be：Adhesive remover obtained in the present invention is sprayed on into viscosity glue stain surface, 5～10s is crossed, is used
Rag is cleaned to glue stain, you can thoroughly taken out stains.After testing, adhesive remover speed of the invention is fast, and the removing glue time is more former
50～60% are first shortened, removing glue effect is good, all there is stronger scavenging action, removing glue rate to various viscosity glue stains or bur
Up to more than 98%.
The invention has the beneficial effects as follows：
（1）Obtained in of the invention, various viscosity glue stains and chewing gum dirt are all had by the quick-acting adhesive remover strong applicabilities of green broad spectrum
There is quick scavenging action, and the adhesive remover is used without the need for heating, removing glue speed is fast；
（2）Obtained in of the invention, the quick-acting adhesive removers of green broad spectrum do not contain toxic solvent, human body and environment will not be caused during use
Infringement.
Specific embodiment
200～300g Fructus Gleditsias fruit is weighed first, deionized water is cleaned 3～5 times repeatedly, remove surface contaminants, then will be clear
In Fructus Gleditsia fruit input stone mortar after washing, 15～20min is beaten with mallet, 100～200mL deionizations are mixed into during beaing
Water, obtains Fructus Gleditsia pulp liquid, filters, and removes filtering residue, collects filtrate, and is proceeded in Rotary Evaporators, in temperature be 80～85
Under the conditions of DEG C, concentrated by rotary evaporation obtains concentrated solution, then is proceeded in evaporating dish to the 1/2 of original volume, heating evaporation crystallization, obtains Fructus Gleditsia
Berry extract, it is standby；300～500g Semen arachidis hypogaeaes are subsequently weighed, Pericarppium arachidis hypogaeae is peelled off, gained Semen arachidis hypogaeae is placed in baking oven, in temperature
Under the conditions of 140～150 DEG C, 4～5h is toasted, is stirred once every 30～45min, discharged, treat that Semen arachidis hypogaeae naturally cools to room
Semen arachidis hypogaeae is crushed by temperature with rubber hammer, then is proceeded in cyclone separator, is separated off Semen arachidis hypogaeae scarlet, then by Semen arachidis hypogaeae
Proceed in ball mill, be 30 by ratio of grinding media to material：1～45：1 add ball milling pearl, 15～20min of ball-milling treatment, discharging, stand 36～
48h, obtains Semen arachidis hypogaeae slurry, standby；10～20L tap waters are subsequently added in the sink, add 2～4kg Misgurni anguillicaudatis, and in tank
Oxygen increasing pump is accessed, loach breeding is carried out 3～5 days, removing Misgurni anguillicaudati is subsequently isolated, tap water in tank is stood, is inhaled with syringe
1～2L tank superficial waters are taken, is placed in beaker, 15～20min is processed with ultraviolet disinfection, then will burn water in the cup and pour rotation steaming into
Instrument is sent out, under the conditions of temperature is 60～65 DEG C, the 1/3 of concentrated by rotary evaporation to original volume, obtain stick-slip concentrated solution；By weight finally
Meter, sequentially adds 100～120 parts of above-mentioned gained stick-slip concentrated solutions in batch mixer, and standby Fructus Gleditsia fruit carries for 8～10 parts of above-mentioned steps
Take thing, the standby Semen arachidis hypogaeae slurry of 60～80 parts of above-mentioned steps, 2～4 parts of dodecylbenzene sodium sulfonate, with 800～1000r/min rotating speeds
Stirring 45～60min of mixing, discharging, fill obtain final product the quick-acting adhesive removers of green broad spectrum.
Example 1
200g Fructus Gleditsias fruit is weighed first, and deionized water is cleaned 3 times repeatedly, removing surface contaminants, then by the Fructus Gleditsia after cleaning really
In input stone mortar, 15min is beaten with mallet, 100mL deionized waters are mixed into during beaing, obtain Fructus Gleditsia pulp liquid, filter, remove
Remove filtering residue, collect filtrate, and proceeded in Rotary Evaporators, in temperature be under the conditions of 80 DEG C concentrated by rotary evaporation to the 1/ of original volume
2, concentrated solution is obtained, then is proceeded in evaporating dish, heating evaporation crystallization obtains Fructus Gleditsia berry extract, standby；300g flowers are weighed subsequently
It is raw, Pericarppium arachidis hypogaeae is peelled off, gained Semen arachidis hypogaeae is placed in baking oven, under the conditions of temperature is 140 DEG C, is toasted 4h, stir every 30min
Once, discharge, treat that Semen arachidis hypogaeae naturally cools to room temperature, Semen arachidis hypogaeae is crushed with rubber hammer, then proceeded in cyclone separator,
Semen arachidis hypogaeae scarlet is separated off, then Semen arachidis hypogaeae is proceeded in ball mill, be 30 by ratio of grinding media to material：1 adds ball milling pearl, ball-milling treatment
15min, discharging stand 36h, obtain Semen arachidis hypogaeae slurry, standby；10L tap waters are subsequently added in the sink, add 2kg Misgurni anguillicaudatis, and
Oxygen increasing pump is accessed in tank, loach breeding is carried out 3 days, removing Misgurni anguillicaudati is subsequently isolated, tap water in tank is stood, with injection
Device draws 1L tank superficial waters, is placed in beaker, processes 15min with ultraviolet disinfection, then pours rotary evaporation into by water in the cup is burnt
Instrument, under the conditions of temperature is 60 DEG C, the 1/3 of concentrated by rotary evaporation to original volume, obtain stick-slip concentrated solution；Finally count by weight,
Sequentially add 100 parts of above-mentioned gained stick-slip concentrated solutions in batch mixer, the standby Fructus Gleditsia berry extract of 8 parts of above-mentioned steps, 60 parts are above-mentioned
The standby Semen arachidis hypogaeae slurry of step, 2 parts of dodecylbenzene sodium sulfonate, with 800r/min rotating speeds stirring mixing 45min, discharge, fill, i.e.,
Obtain the quick-acting adhesive removers of green broad spectrum.
This example operation is easy, during use, adhesive remover obtained in the present invention is sprayed on viscosity glue stain surface, crosses 5s, is used
Rag is cleaned to glue stain, you can thoroughly taken out stains.After testing, adhesive remover speed of the invention is fast, and the removing glue time is more former
50% is first shortened, removing glue effect is good, all there is stronger scavenging action to various viscosity glue stains or bur, removing glue rate reaches
98.5%。
Example 2
250g Fructus Gleditsias fruit is weighed first, and deionized water is cleaned 4 times repeatedly, removing surface contaminants, then by the Fructus Gleditsia after cleaning really
In input stone mortar, 18min is beaten with mallet, 150mL deionized waters are mixed into during beaing, obtain Fructus Gleditsia pulp liquid, filter, remove
Remove filtering residue, collect filtrate, and proceeded in Rotary Evaporators, in temperature be under the conditions of 83 DEG C concentrated by rotary evaporation to the 1/ of original volume
2, concentrated solution is obtained, then is proceeded in evaporating dish, heating evaporation crystallization obtains Fructus Gleditsia berry extract, standby；400g flowers are weighed subsequently
It is raw, Pericarppium arachidis hypogaeae is peelled off, gained Semen arachidis hypogaeae is placed in baking oven, under the conditions of temperature is 145 DEG C, is toasted 4.5h, turn over every 38min
Move once, discharging is treated that Semen arachidis hypogaeae naturally cools to room temperature, crushed Semen arachidis hypogaeae with rubber hammer, then proceeded to cyclone separator
In, Semen arachidis hypogaeae scarlet is separated off, then Semen arachidis hypogaeae is proceeded in ball mill, be 38 by ratio of grinding media to material：1 adds ball milling pearl, at ball milling
Reason 18min, discharging stand 42h, obtain Semen arachidis hypogaeae slurry, standby；15L tap waters are subsequently added in the sink, add 3kg Misgurni anguillicaudatis,
And oxygen increasing pump is accessed in tank, carry out loach breeding 4 days, be subsequently isolated removing Misgurni anguillicaudati, tap water in tank stood, with note
Emitter draws 1.5L tank superficial waters, is placed in beaker, processes 18min with ultraviolet disinfection, then pours rotation into by water in the cup is burnt
Evaporimeter, under the conditions of temperature is 63 DEG C, the 1/3 of concentrated by rotary evaporation to original volume, obtain stick-slip concentrated solution；By weight finally
Meter, sequentially adds 110 parts of above-mentioned gained stick-slip concentrated solutions in batch mixer, the standby Fructus Gleditsia berry extract of 9 parts of above-mentioned steps, 70 parts
The standby Semen arachidis hypogaeae slurry of above-mentioned steps, 3 parts of dodecylbenzene sodium sulfonate, with 900r/min rotating speeds stirring mixing 53min, discharging is filled
Dress, obtains final product the quick-acting adhesive removers of green broad spectrum.
This example operation is easy, during use, adhesive remover obtained in the present invention is sprayed on viscosity glue stain surface, crosses 8s, is used
Rag is cleaned to glue stain, you can thoroughly taken out stains.After testing, adhesive remover speed of the invention is fast, and the removing glue time is more former
55% is first shortened, removing glue effect is good, all there is stronger scavenging action to various viscosity glue stains or bur, removing glue rate reaches
99%。
Example 3
250g Fructus Gleditsias fruit is weighed first, and deionized water is cleaned 4 times repeatedly, removing surface contaminants, then by the Fructus Gleditsia after cleaning really
In input stone mortar, 18min is beaten with mallet, 150mL deionized waters are mixed into during beaing, obtain Fructus Gleditsia pulp liquid, filter, remove
Remove filtering residue, collect filtrate, and proceeded in Rotary Evaporators, in temperature be under the conditions of 83 DEG C concentrated by rotary evaporation to the 1/ of original volume
2, concentrated solution is obtained, then is proceeded in evaporating dish, heating evaporation crystallization obtains Fructus Gleditsia berry extract, standby；400g flowers are weighed subsequently
It is raw, Pericarppium arachidis hypogaeae is peelled off, gained Semen arachidis hypogaeae is placed in baking oven, under the conditions of temperature is 145 DEG C, is toasted 4.5h, turn over every 38min
Move once, discharging is treated that Semen arachidis hypogaeae naturally cools to room temperature, crushed Semen arachidis hypogaeae with rubber hammer, then proceeded to cyclone separator
In, Semen arachidis hypogaeae scarlet is separated off, then Semen arachidis hypogaeae is proceeded in ball mill, be 45 by ratio of grinding media to material：1 adds ball milling pearl, at ball milling
Reason 20min, discharging stand 48h, obtain Semen arachidis hypogaeae slurry, standby；20L tap waters are subsequently added in the sink, add 4kg Misgurni anguillicaudatis,
And oxygen increasing pump is accessed in tank, carry out loach breeding 5 days, be subsequently isolated removing Misgurni anguillicaudati, tap water in tank stood, with note
Emitter draws 2L tank superficial waters, is placed in beaker, processes 20min with ultraviolet disinfection, then will burn water in the cup and pours rotation steaming into
Instrument is sent out, under the conditions of temperature is 65 DEG C, the 1/3 of concentrated by rotary evaporation to original volume, obtain stick-slip concentrated solution；Finally count by weight,
Sequentially add 120 parts of above-mentioned gained stick-slip concentrated solutions in batch mixer, the standby Fructus Gleditsia berry extract of 10 parts of above-mentioned steps, 80 parts
The standby Semen arachidis hypogaeae slurry of above-mentioned steps, 4 parts of dodecylbenzene sodium sulfonate, with 1000r/min rotating speeds stirring mixing 60min, discharging is filled
Dress, obtains final product the quick-acting adhesive removers of green broad spectrum.
This example operation is easy, during use, adhesive remover obtained in the present invention is sprayed on viscosity glue stain surface, crosses 10s, is used
Rag is cleaned to glue stain, you can thoroughly taken out stains.After testing, adhesive remover speed of the invention is fast, and the removing glue time is more former
60% is first shortened, removing glue effect is good, all there is stronger scavenging action to various viscosity glue stains or bur, removing glue rate reaches
99.5%。
Claims (1)
1. the preparation method of the quick-acting adhesive removers of a kind of green broad spectrum, it is characterised in that concrete preparation process is：
（1）200～300g Fructus Gleditsias fruit is weighed, deionized water is cleaned 3～5 times repeatedly, removes surface contaminants, then by after cleaning
In Fructus Gleditsia fruit input stone mortar, 15～20min is beaten with mallet, be mixed into 100～200mL deionized waters, obtain soap during beaing
Pod serosity, filters, and removes filtering residue, collects filtrate, and is proceeded in Rotary Evaporators, under the conditions of temperature is 80～85 DEG C
Concentrated by rotary evaporation obtains concentrated solution, then is proceeded in evaporating dish to the 1/2 of original volume, heating evaporation crystallization, obtains Fructus Gleditsia fruit and extracts
Thing, it is standby；
（2）Weigh 300～500g Semen arachidis hypogaeaes, peel off Pericarppium arachidis hypogaeae, gained Semen arachidis hypogaeae is placed in baking oven, in temperature be 140～150 DEG C
Under the conditions of, 4～5h is toasted, is stirred once every 30～45min, discharged, treat that Semen arachidis hypogaeae naturally cools to room temperature, will with rubber hammer
Semen arachidis hypogaeae is crushed, then is proceeded in cyclone separator, is separated off Semen arachidis hypogaeae scarlet, then Semen arachidis hypogaeae is proceeded in ball mill,
It is 30 by ratio of grinding media to material：1～45：1 adds ball milling pearl, 15～20min of ball-milling treatment, discharging to stand 36～48h, obtain Semen arachidis hypogaeae slurry,
It is standby；
（3）10～20L tap waters are added in the sink, are added 2～4kg Misgurni anguillicaudatis, and are accessed oxygen increasing pump in tank, carry out mud
Loach cultivates 3～5 days, is subsequently isolated removing Misgurni anguillicaudati, tap water in tank is stood, draw 1～2L tank superficial waters with syringe,
Be placed in beaker, with ultraviolet disinfection process 15～20min, then by burn water in the cup pour Rotary Evaporators into, in temperature be 60～
Under the conditions of 65 DEG C, the 1/3 of concentrated by rotary evaporation to original volume, obtain stick-slip concentrated solution；
（4）Count by weight, 100～120 parts of above-mentioned gained stick-slip concentrated solutions, 8～10 parts of steps are sequentially added in batch mixer
Suddenly（1）Standby Fructus Gleditsia berry extract, 60～80 parts of steps（2）Standby Semen arachidis hypogaeae slurry, 2～4 parts of dodecylbenzene sodium sulfonate, with
800～1000r/min rotating speeds stirring 45～60min of mixing, discharging, fill obtain final product the quick-acting adhesive removers of green broad spectrum.
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| CN201610879939.9A CN106544170A (en) | 2016-10-09 | 2016-10-09 | A kind of preparation method of the quick-acting adhesive removers of green broad spectrum |
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| CN201610879939.9A CN106544170A (en) | 2016-10-09 | 2016-10-09 | A kind of preparation method of the quick-acting adhesive removers of green broad spectrum |
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Cited By (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN114907918A (en) * | 2022-05-07 | 2022-08-16 | 广东粤首新科技有限公司 | Cleaning agent and preparation method thereof |
Citations (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN1796522A (en) * | 2004-12-23 | 2006-07-05 | 北京东方天甲科技发展有限公司 | Detergent of adhesive |
| CN105462708A (en) * | 2015-12-08 | 2016-04-06 | 郎桂青 | Application of gutter oil in preparation of gum residue scavenging agent |
| CN105970235A (en) * | 2016-07-02 | 2016-09-28 | 郭迎庆 | Preparation method of environment-friendly biological adhesive remover |
-
2016
- 2016-10-09 CN CN201610879939.9A patent/CN106544170A/en active Pending
Patent Citations (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN1796522A (en) * | 2004-12-23 | 2006-07-05 | 北京东方天甲科技发展有限公司 | Detergent of adhesive |
| CN105462708A (en) * | 2015-12-08 | 2016-04-06 | 郎桂青 | Application of gutter oil in preparation of gum residue scavenging agent |
| CN105970235A (en) * | 2016-07-02 | 2016-09-28 | 郭迎庆 | Preparation method of environment-friendly biological adhesive remover |
Non-Patent Citations (2)
| Title |
|---|
| 于雅婷等: "《最优健康食物排行榜速查全书》", 31 July 2014, 南京：江苏科学技术出版社 * |
| 吴成浩: "《古今洗衣有何变化？》", 30 June 2014, 北京：中国纺织出版社 * |
Cited By (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN114907918A (en) * | 2022-05-07 | 2022-08-16 | 广东粤首新科技有限公司 | Cleaning agent and preparation method thereof |
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Application publication date: 20170329 |