CN107441314A - A kind of pyrus nivalis honeybee broken wall bulbus fritillariae cirrhosae flour producing process - Google Patents
A kind of pyrus nivalis honeybee broken wall bulbus fritillariae cirrhosae flour producing process Download PDFInfo
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- CN107441314A CN107441314A CN201710656544.7A CN201710656544A CN107441314A CN 107441314 A CN107441314 A CN 107441314A CN 201710656544 A CN201710656544 A CN 201710656544A CN 107441314 A CN107441314 A CN 107441314A
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- bulbus fritillariae
- fritillariae cirrhosae
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- 241000287420 Pyrus x nivalis Species 0.000 title claims abstract description 65
- 241000256844 Apis mellifera Species 0.000 title claims abstract description 33
- 238000000034 method Methods 0.000 title claims abstract description 27
- 235000013312 flour Nutrition 0.000 title claims abstract description 12
- 235000012907 honey Nutrition 0.000 claims abstract description 101
- 235000009508 confectionery Nutrition 0.000 claims abstract description 44
- 238000009777 vacuum freeze-drying Methods 0.000 claims abstract description 26
- 235000015206 pear juice Nutrition 0.000 claims abstract description 22
- 239000002994 raw material Substances 0.000 claims abstract description 12
- 239000000843 powder Substances 0.000 claims description 59
- 241000935235 Fritillaria meleagris Species 0.000 claims description 46
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 claims description 35
- 238000001035 drying Methods 0.000 claims description 27
- 238000004140 cleaning Methods 0.000 claims description 12
- 239000000463 material Substances 0.000 claims description 12
- 238000009835 boiling Methods 0.000 claims description 11
- 239000002689 soil Substances 0.000 claims description 11
- 238000004821 distillation Methods 0.000 claims description 10
- 238000003756 stirring Methods 0.000 claims description 10
- 239000007788 liquid Substances 0.000 claims description 8
- 241000251468 Actinopterygii Species 0.000 claims description 7
- 241000256846 Apis cerana Species 0.000 claims description 7
- 239000006260 foam Substances 0.000 claims description 7
- 238000004108 freeze drying Methods 0.000 claims description 7
- 235000021022 fresh fruits Nutrition 0.000 claims description 7
- 230000007721 medicinal effect Effects 0.000 claims description 7
- 238000009991 scouring Methods 0.000 claims description 7
- 238000000227 grinding Methods 0.000 claims description 6
- 239000012535 impurity Substances 0.000 claims description 6
- 238000006243 chemical reaction Methods 0.000 claims description 5
- 238000001816 cooling Methods 0.000 claims description 5
- 238000007710 freezing Methods 0.000 claims description 5
- 230000008014 freezing Effects 0.000 claims description 5
- 238000007667 floating Methods 0.000 claims description 4
- 230000002000 scavenging effect Effects 0.000 claims description 4
- 238000010792 warming Methods 0.000 claims description 4
- 238000010438 heat treatment Methods 0.000 claims description 2
- 239000007921 spray Substances 0.000 claims description 2
- 238000010025 steaming Methods 0.000 claims description 2
- 238000004519 manufacturing process Methods 0.000 claims 1
- 238000007670 refining Methods 0.000 claims 1
- OVHUAFPHYGFWPY-UHFFFAOYSA-N Imperialin Natural products CC1CN2CC3C(CCC4C3CC5C4CC(=O)C6CC(O)CCC56C)CC2C(C)(O)C1 OVHUAFPHYGFWPY-UHFFFAOYSA-N 0.000 abstract description 15
- IQDIERHFZVCNRZ-LZOOXBQUSA-N Imperialine Natural products O=C1[C@@H]2[C@@](C)([C@@H]3[C@H]([C@@H]4[C@H]([C@H]5[C@H]([C@@](O)(C)[C@H]6N(C[C@@H](C)CC6)C5)CC4)C3)C1)CC[C@@H](O)C2 IQDIERHFZVCNRZ-LZOOXBQUSA-N 0.000 abstract description 15
- IQDIERHFZVCNRZ-LRCDAWNTSA-N Sipeimine Chemical compound C([C@@H]1C(=O)C[C@H]2[C@@H]3CC[C@H]4[C@]5(C)O)[C@@H](O)CC[C@]1(C)[C@H]2C[C@H]3[C@@H]4CN1[C@H]5CC[C@H](C)C1 IQDIERHFZVCNRZ-LRCDAWNTSA-N 0.000 abstract description 15
- HIDAYMRWVVNXAO-UHFFFAOYSA-N imperialone Natural products CC1(O)C2CCC3C4CC(=O)C5CC(=O)CCC5(C)C4CC3C2CN2C1CCC(C)C2 HIDAYMRWVVNXAO-UHFFFAOYSA-N 0.000 abstract description 15
- 238000005516 engineering process Methods 0.000 abstract description 12
- 239000004480 active ingredient Substances 0.000 abstract description 7
- 230000006378 damage Effects 0.000 abstract description 2
- 239000003814 drug Substances 0.000 description 12
- 241000605372 Fritillaria Species 0.000 description 11
- 230000000052 comparative effect Effects 0.000 description 9
- 238000004806 packaging method and process Methods 0.000 description 8
- 239000003651 drinking water Substances 0.000 description 7
- 235000020188 drinking water Nutrition 0.000 description 7
- 206010011224 Cough Diseases 0.000 description 4
- 238000010790 dilution Methods 0.000 description 4
- 239000012895 dilution Substances 0.000 description 4
- 230000000694 effects Effects 0.000 description 4
- 210000004072 lung Anatomy 0.000 description 4
- 235000015170 shellfish Nutrition 0.000 description 4
- 241000256837 Apidae Species 0.000 description 3
- 239000003513 alkali Substances 0.000 description 3
- 238000007598 dipping method Methods 0.000 description 3
- 238000011049 filling Methods 0.000 description 3
- 238000004321 preservation Methods 0.000 description 3
- 230000001954 sterilising effect Effects 0.000 description 3
- 238000004659 sterilization and disinfection Methods 0.000 description 3
- 241001644290 Fritillaria unibracteata Species 0.000 description 2
- 108700039708 galantide Proteins 0.000 description 2
- 238000002156 mixing Methods 0.000 description 2
- 239000000203 mixture Substances 0.000 description 2
- 238000002791 soaking Methods 0.000 description 2
- 239000000243 solution Substances 0.000 description 2
- 206010010904 Convulsion Diseases 0.000 description 1
- 206010013954 Dysphoria Diseases 0.000 description 1
- 241000196324 Embryophyta Species 0.000 description 1
- 241001092070 Eriobotrya Species 0.000 description 1
- 235000009008 Eriobotrya japonica Nutrition 0.000 description 1
- 241001547127 Fritillaria cirrhosa Species 0.000 description 1
- 241001644297 Fritillaria delavayi Species 0.000 description 1
- 241001644295 Fritillaria przewalskii Species 0.000 description 1
- 241001644292 Fritillaria taipaiensis Species 0.000 description 1
- 206010019909 Hernia Diseases 0.000 description 1
- 206010062717 Increased upper airway secretion Diseases 0.000 description 1
- 206010036790 Productive cough Diseases 0.000 description 1
- 206010044302 Tracheitis Diseases 0.000 description 1
- 208000037386 Typhoid Diseases 0.000 description 1
- 208000006673 asthma Diseases 0.000 description 1
- 239000008280 blood Substances 0.000 description 1
- 210000004369 blood Anatomy 0.000 description 1
- 210000000481 breast Anatomy 0.000 description 1
- 206010006451 bronchitis Diseases 0.000 description 1
- 235000013339 cereals Nutrition 0.000 description 1
- 239000003795 chemical substances by application Substances 0.000 description 1
- 208000013116 chronic cough Diseases 0.000 description 1
- 238000004891 communication Methods 0.000 description 1
- 230000036461 convulsion Effects 0.000 description 1
- 229940079593 drug Drugs 0.000 description 1
- 230000000857 drug effect Effects 0.000 description 1
- 239000004744 fabric Substances 0.000 description 1
- 238000001914 filtration Methods 0.000 description 1
- 239000002421 finishing Substances 0.000 description 1
- 239000000796 flavoring agent Substances 0.000 description 1
- 235000019634 flavors Nutrition 0.000 description 1
- 238000009472 formulation Methods 0.000 description 1
- 235000011389 fruit/vegetable juice Nutrition 0.000 description 1
- 210000000867 larynx Anatomy 0.000 description 1
- 238000002386 leaching Methods 0.000 description 1
- 231100000862 numbness Toxicity 0.000 description 1
- 208000026435 phlegm Diseases 0.000 description 1
- 238000002360 preparation method Methods 0.000 description 1
- 230000002035 prolonged effect Effects 0.000 description 1
- 208000008128 pulmonary tuberculosis Diseases 0.000 description 1
- 230000000630 rising effect Effects 0.000 description 1
- 230000035807 sensation Effects 0.000 description 1
- 235000019615 sensations Nutrition 0.000 description 1
- 208000024794 sputum Diseases 0.000 description 1
- 210000003802 sputum Anatomy 0.000 description 1
- 238000006467 substitution reaction Methods 0.000 description 1
- 201000008297 typhoid fever Diseases 0.000 description 1
- 239000001993 wax Substances 0.000 description 1
Classifications
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K36/00—Medicinal preparations of undetermined constitution containing material from algae, lichens, fungi or plants, or derivatives thereof, e.g. traditional herbal medicines
- A61K36/18—Magnoliophyta (angiosperms)
- A61K36/88—Liliopsida (monocotyledons)
- A61K36/896—Liliaceae (Lily family), e.g. daylily, plantain lily, Hyacinth or narcissus
- A61K36/8966—Fritillaria, e.g. checker lily or mission bells
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K9/00—Medicinal preparations characterised by special physical form
- A61K9/14—Particulate form, e.g. powders, Processes for size reducing of pure drugs or the resulting products, Pure drug nanoparticles
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K2236/00—Isolation or extraction methods of medicinal preparations of undetermined constitution containing material from algae, lichens, fungi or plants, or derivatives thereof, e.g. traditional herbal medicine
- A61K2236/10—Preparation or pretreatment of starting material
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K2236/00—Isolation or extraction methods of medicinal preparations of undetermined constitution containing material from algae, lichens, fungi or plants, or derivatives thereof, e.g. traditional herbal medicine
- A61K2236/10—Preparation or pretreatment of starting material
- A61K2236/15—Preparation or pretreatment of starting material involving mechanical treatment, e.g. chopping up, cutting or grinding
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K2236/00—Isolation or extraction methods of medicinal preparations of undetermined constitution containing material from algae, lichens, fungi or plants, or derivatives thereof, e.g. traditional herbal medicine
- A61K2236/10—Preparation or pretreatment of starting material
- A61K2236/17—Preparation or pretreatment of starting material involving drying, e.g. sun-drying or wilting
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Abstract
A kind of pyrus nivalis honeybee broken wall bulbus fritillariae cirrhosae flour producing process, comprises the following steps：A) net system processing early stage is carried out to bulbus fritillariae cirrhosae raw material；B) bulbus fritillariae cirrhosae after processing is subjected to vacuum freeze drying：C) bulbus fritillariae cirrhosae is crushed：D) the tender sweet mixed liquor of pyrus nivalis is made：E) honey bulbus fritillariae cirrhosae：F) bulbus fritillariae cirrhosae of vacuum freeze drying honey system：G) bulbus fritillariae cirrhosae is crushed again：H) finished product is made.For bulbus fritillariae cirrhosae present in prior art and honey snow pear juice be soaked not exclusively, be soaked the destruction of overlong time and whole processing technology high temperature to bulbus fritillariae cirrhosae active ingredient (imperialine); the invention provides a kind of simple to operate, the pyrus nivalis honeybee broken wall bulbus fritillariae cirrhosae flour producing process of wherein active ingredient (imperialine) can be effectively protected.
Description
Technical field
The present invention relates to herbal pharmaceutical processing technology, and in particular to the process technology of bulbus fritillariae cirrhosae.
Background technology
The name of fritillaria, first recorded in《Sheng Nong's herbal classic》, middle product are classified as, are said：" fritillaria.Acrid flavour is put down, main typhoid fever dysphoria with smothery sensation, leaching drip,
Perverse trend hernia, larynx numbness breast is difficult, metal-inflicted wound wind convulsion." Tao Hongjing meaning：" being similar to poly- shellfish, therefore named fritillaria ".《Chinese Pharmacopoeia》The tendril-leaved fritillary bulb recorded
Mother stock is bulbus fritillariae cirrhosae Fritillaria cirrhosa D.Don, Fritillaria unibracteata Fritillaria unibracteata Hsiao
Et K.C.Hsia, Gansu fritillaria Fritillaria przewalskii Maxim., Bulbus Fritillariae cirrhosae Fritillaria
Delavayi Franch., taipei fritillary bulb Fritillaria taipaiensis P.Y.Li or watt cloth fritillaria Fritillaria
Unibracteata Hsiao et K.C.Hsiavar wabuensis (S.Y.Tang et S.C.Yue) Z.D.Liu,
S.Wang et S.C.Chen。
Bulbus fritillariae cirrhosae is the rare traditional Chinese medicine to moisten the lung and relieve the cough, and applicating history is long, and curative effect is distinguished, is had won fame both at home and abroad.Due to tendril-leaved fritillary bulb
It is female that not only there is good relieving cough and reducing sputum effect, and can support lung yin, facilitaing lung, moistening lung and clearing lung-heat is hot, be to treat chronic cough phlegm simply
The good medicine of asthma, therefore, in the Chinese medicinal formulae or Chinese patent drug system of the illnesss such as many treatment acute tracheitis, bronchitis, pulmonary tuberculosis
There are tendril-leaved fritillary bulb, such as Succus Fel Serpentis et Bulbus Fritillariae Cirrhosae, fritillary and loquat cough mixture in agent.Chinese medicine will be processed when being processed into medicine, in
In the concocting process of medicine, the degree of grinding of temperature and medicine has tremendous influence to the effect of medicine.Traditional honey tendril-leaved fritillary bulb
Female method is steamed again after whole bulbus fritillariae cirrhosae is soaked, and high temperature can be used to carry out bulbus fritillariae cirrhosae in whole process
Bake, be by whole river in this patent as CN201410103497.X discloses a kind of preparation method of honey bulbus fritillariae cirrhosae
Fritillaria is soaked with honey snow pear juice, and the equipment for drying fritillaria is baking oven, is had the following disadvantages：1st, to original resource just
Rare bulbus fritillariae cirrhosae raw material selectivity is strong, it is necessary to use the relatively uniform raw material of size；2nd, bulbus fritillariae cirrhosae is not by grinding or powder
Just it is soaked after broken with honey snow pear juice, honey snow pear juice completely can not enter in medicinal material, when using this medicine, want to reach same
The drug effect of sample, it must just use bigger dosage；3rd, it is prolonged be soaked to exist make honey and snow pear juice is rotten, spoiled wind
Danger；4th, the bulbus fritillariae cirrhosae sugar increase after honey system, also brings difficulty to crushing；5th, high temperature drying is carried out to fritillaria using baking oven,
The risk being lost in the presence of the active ingredient (imperialine etc.) made in fritillaria.So creating a kind of new concocting method turns into one kind
Urgent demand.
The content of the invention
For bulbus fritillariae cirrhosae present in prior art and honey snow pear juice be soaked not exclusively, be soaked overlong time and whole
Destruction of the processing technology high temperature to bulbus fritillariae cirrhosae active ingredient, the invention provides a kind of pyrus nivalis honeybee broken wall tendril-leaved fritillary bulb female powder to add
Work technique.
To achieve the above object, present invention employs following technical scheme：
A kind of pyrus nivalis honeybee broken wall bulbus fritillariae cirrhosae flour producing process, comprises the following steps：
A) net system processing early stage is carried out to bulbus fritillariae cirrhosae raw material；
B) bulbus fritillariae cirrhosae after processing is subjected to vacuum freeze drying：Bulbus fritillariae cirrhosae is laid in vacuum freeze drier, river
The thickness that fritillaria heap comes is no more than 2cm, and pre-freezing temperature is -40 DEG C and is incubated 1-2h, and the maximum temperature of distillation is 35 DEG C, very
Reciprocal of duty cycle 0-100Pa, drying time 10-25h；Drying finishes, and takes out standby；
C) bulbus fritillariae cirrhosae is crushed：Low-temperature grinding (0-25 is carried out to the bulbus fritillariae cirrhosae Jing Guo vacuum freeze drying with micronizer
DEG C), it is crushed to 1 μm -15 μm and obtains tendril-leaved fritillary bulb female powder, it is standby；
D) the tender sweet mixed liquor of pyrus nivalis is made：In the step a), while b) or c) carry out, in mass ratio 10:3 by pear juice
It is well mixed with tender honey, that is, obtains the tender sweet mixed liquor of pyrus nivalis, it is standby；
E) honey bulbus fritillariae cirrhosae：By weight 1:1 weighs tendril-leaved fritillary bulb female powder and the tender sweet mixed liquor of pyrus nivalis, in the tender sweet mixed liquor of pyrus nivalis
Middle addition purifying is diluted with water, and purifying is stirred with 6-7 times that the quality of water is the tender sweet mixed liquor quality of pyrus nivalis, then
The tender sweet mixed liquor of pyrus nivalis after dilution is poured into tendril-leaved fritillary bulb female powder, stirred, fully reaction, obtains the mixing of honey bulbus fritillariae cirrhosae
Liquid, it is standby；
F) bulbus fritillariae cirrhosae of vacuum freeze drying honey system：Honey bulbus fritillariae cirrhosae mixed liquor is laid in vacuum freeze drier material
In disk, liquid level thickness 0.5-1.2cm, using Freeze drying repeatedly, pre-freeze first after extremely -50 DEG C of degree of cooling, heat up by the first stage
Extremely -25 DEG C, constant temperature 1-2h；Second stage is cooled to -50 DEG C again, constant temperature 1-2h；Distillation heating maximum temperature is 35 DEG C, when drying
Between 25-40h to dry complete, vacuum 0-30Pa, obtain drying honey system tendril-leaved fritillary bulb female powder or powder agglomates, it is standby；
G) crush again：The tendril-leaved fritillary bulb female powder or powder agglomates made with pulverizer to the honey by vacuum freeze drying carry out low again
Temperature crushes, and is crushed to middle powder (180 μm -250 μm), standby；
H) finished product is made：With device of full automatic packaging will be packed as small by the tendril-leaved fritillary bulb female powder of the honey system crushed again
Packaging obtains finished product.
Compared to prior art, the present invention has the advantages that：
1st, before honey is made, vacuum freeze drying is carried out to bulbus fritillariae cirrhosae, the active ingredient be advantageous in medicinal material has obtained maximum
The protection of limit, it ensure that the sweet quality for making the product come below；And after carrying out vacuum freeze drying, bulbus fritillariae cirrhosae is in loose
Shape, be advantageous to carry out ultramicro grinding to it；
2nd, after vacuum freeze drying, bulbus fritillariae cirrhosae is crushed using breaking-wall cell superfine communication technique, finally obtained
For tendril-leaved fritillary bulb female powder to be micron-sized, its specific surface area is big, is advantageous to fully being soaked for bulbus fritillariae cirrhosae and honey snow pear juice below；It ensure that
The active ingredient of medicine in last obtained product is fully dissolved out in human body, and the blood medicine that can rapidly improve in human body is dense
Degree, increase the absorptivity and utilization rate of medicine；
3, in honey, in the absence of in order to ensure honey system uniformity, and select bulbus fritillariae cirrhosae of uniform size, be advantageous to thing
Material makes full use of；
4th, after honey system, vacuum freeze drying is carried out to product, the fresh-keeping effect guaranteed the quality has been reached to the active ingredient of product；
The 5th, obtained bulbus fritillariae cirrhosae powder agglomates is crushed to the reality for being advantageous to follow-up technology of the package for middle powder (180 μm of -250 μm of mesh)
It is existing, it is packed as that small dimension is bottled, packed, and more convenient client's is edible.Daily health caring, mouthfeel are can also be used for clinical formulation
Well, avoid pharmacy from carrying out secondary pollution after dozen powder, there is the characteristics of taking and be easy to carry.
Brief description of the drawings
Fig. 1 is the flow chart of the present invention；
Fig. 2 is the grain size distribution of tendril-leaved fritillary bulb female powder obtained by step c).
Embodiment
Embodiment 1
A kind of pyrus nivalis honeybee broken wall bulbus fritillariae cirrhosae flour producing process, step are as follows：
A) bulbus fritillariae cirrhosae raw material are taken, after removing hair fibrous root, soil, non-medicinal effects, are first sprayed with a small amount of vaporific drinking water
Bulbus fritillariae cirrhosae is drenched, by bulbus fritillariae cirrhosae moistened surface, excessive moisture is filtered off on filter screen, stands, after surface soil is soft, then will drink
Water loads high-pressure water cleaning device by bulbus fritillariae cirrhosae Rapid Cleaning (scavenging period control in 3 minutes), clean to medicinal material surface without
Silt, drain away the water in time；
B) bulbus fritillariae cirrhosae after processing is subjected to vacuum freeze drying：Bulbus fritillariae cirrhosae is laid in vacuum freeze drier, river
In 2cm, pre-freezing temperature is -40 DEG C and is incubated 2h the thickness that fritillaria heap comes, and the temperature of distillation is 35 DEG C, vacuum 0-
100Pa, drying time 23h, drying finish, and take out standby；
C) bulbus fritillariae cirrhosae is crushed：Low-temperature grinding is carried out to the bulbus fritillariae cirrhosae Jing Guo vacuum freeze drying with micronizer, crushed
Tendril-leaved fritillary bulb female powder is obtained to 1 μm -15 μm (as shown in Figure 2), it is standby；
D) the tender sweet mixed liquor of pyrus nivalis is made：In the step a), while b) or c) carry out, from apidae insect China
The honey that honeybee Apis cerana Fabricius or apis mellifera Linnaeus Apis mellifera Linnaeus are made, takes honey to be placed in
In refined honey pot, quality is added to be stirred for 20% water of honey, heat uses slow fire instead and keep micro-boiling, removing is floated to after seething with excitement
Foam and wax impurity, finishing scouring to seethe with excitement, rise as a fish bubble eye, sth.s made by twisting compared with raw honey slightly stick；By rosaceous plant
The fresh fruit of pyrus nivalis ripe Pyrusnivalis Jacq, after peeling and stoning, Fresh sap is made in squeezing, and filtering is
；Quality is that 1kg pear juices with quality are that the tender honey of 0.3kg is well mixed, that is, obtains the tender sweet mixed liquor of pear juice, standby；
E) honey bulbus fritillariae cirrhosae：1kg tendril-leaved fritillary bulb female powder and the tender sweet mixed liquor of pyrus nivalis are weighed respectively, then to weigh quality 6.5kg pure
Change water, purifying is added in the tender sweet mixed liquor of pyrus nivalis with water, stirred, then the tender sweet mixed liquor of the pyrus nivalis after dilution is poured into
In tendril-leaved fritillary bulb female powder, stir, fully reaction, the honey bulbus fritillariae cirrhosae mixed are standby；
F) bulbus fritillariae cirrhosae of vacuum freeze drying honey system：Honey bulbus fritillariae cirrhosae mixed liquor is laid in vacuum freeze drier material
In disk, liquid level thickness 1.2cm, using Freeze drying repeatedly, for pre-freeze first after extremely -50 DEG C of degree of cooling, the first stage is warming up to -25
DEG C, constant temperature 1.5h；Second stage is cooled to -50 DEG C, constant temperature 2h again, and the temperature of distillation is 35 DEG C, drying time 35h, vacuum
5Pa, the tendril-leaved fritillary bulb female powder or powder agglomates of the honey system of drying are obtained, it is standby；
G) crush again：The tendril-leaved fritillary bulb female powder made with micronizer to the honey by vacuum freeze drying carries out low temperature again
Crush (0-25 DEG C), be crushed to middle powder (180 μm -250 μm), it is standby；
H) finished product is made：With device of full automatic packaging will be packed as small by the tendril-leaved fritillary bulb female powder of the honey system crushed again
Packaging bag.
Comparative example 1：
The step of making tendril-leaved fritillary bulb female powder with traditional method for honey preparing is as follows：
1st, take and the bulbus fritillariae cirrhosae raw material in embodiment 1 with batch, after removing hair fibrous root, soil, non-medicinal effects, use
Drinking water is got express developed, drying, 55 DEG C of drying temperature；
2nd, from apidae insect apis cerana Apis cerana Fabricius or apis mellifera Linnaeus Apis mellifera
The honey that Linnaeus is made, take honey to be placed in refined honey pot, 20% water for adding quality to be honey, stir, heat to boiling
Afterwards, use slow fire instead and keep micro-boiling, remove floating foam and wax impurity, finishing scouring is omited to seething with excitement, playing such as fish bubble eye, sth. made by twisting compared with raw honey
Stick；By the fresh fruit of pyrus nivalis ripe rosaceous plant Pyrusnivalis Jacq, after peeling and stoning, squeezing
Fresh sap is made, filters and produces；Quality is that 1kg pear juices with quality are that the tender honey of 0.3kg is well mixed, that is, it is mixed to obtain the tender honey of pear juice
Liquid is closed, it is standby；
3rd, the 1kg tender sweet mixed liquor of pyrus nivalis and bulbus fritillariae cirrhosae is weighed respectively, the tender sweet mixed liquor of pyrus nivalis is poured into bulbus fritillariae cirrhosae, together
Shi Jiare, temperature reach 45 DEG C, abundant hot dipping 15 hours, during this period every 1h stirrings once, it is evenly distributed, absorbed
Entirely, the bulbus fritillariae cirrhosae after sweet system is obtained；
4th, the bulbus fritillariae cirrhosae after the honey system obtained in step 3 is placed in baking oven, 55 DEG C of temperature, drying time 8h；
5th, dried bulbus fritillariae cirrhosae is crushed with pulverizer；
6th, tendril-leaved fritillary bulb female powder is subjected to sterilization filling, obtains sweet manufactured goods.
Example 1 carries out content analysis with the finished product in comparative example 1, analyzes the western shellfish of main component in bulbus fritillariae cirrhosae
Female alkali, finally obtain following experimental data：
As can be seen from the table, the imperialine content in the tendril-leaved fritillary bulb female powder obtained with the technology in comparative example 1 is not
It is qualified, and the content of the imperialine in the bulbus fritillariae cirrhosae obtained with the technology in embodiment 1 is qualified, and significantly larger than country's mark
Accurate or provincial standard line.Because we spray when bulbus fritillariae cirrhosae is cleaned using vaporific drinking water in embodiment 1
Bulbus fritillariae cirrhosae is drenched, then carries out Rapid Cleaning with circulating water again, the loss for the imperialine being effectively prevented in bulbus fritillariae cirrhosae, and
Low-temperature operation is used in whole technical process, is advantageous to the preservation of the imperialine of non-refractory.
Embodiment 2
A kind of pyrus nivalis honeybee broken wall bulbus fritillariae cirrhosae flour producing process, step are following (as shown in Figure 1)：
A) bulbus fritillariae cirrhosae raw material are taken, after removing hair fibrous root, soil, non-medicinal effects, are first sprayed with a small amount of vaporific drinking water
Bulbus fritillariae cirrhosae is drenched, by bulbus fritillariae cirrhosae moistened surface, excessive moisture is filtered off on filter screen, stands, after surface soil is soft, then will drink
Water loads high-pressure water cleaning device by bulbus fritillariae cirrhosae Rapid Cleaning (scavenging period was controlled in 3 minutes).Cleaning to medicinal material surface without
Silt, drain away the water in time；
B) bulbus fritillariae cirrhosae after processing is subjected to vacuum freeze drying：Bulbus fritillariae cirrhosae is laid in vacuum freeze drier, river
For the thickness that fritillaria heap comes in 1.5cm, pre-freezing temperature is -40 DEG C, soaking time 1.5h, and the temperature of distillation is 30 DEG C, very
Reciprocal of duty cycle 0-60Pa, drying time：20h.Drying finishes, and takes out standby；
C) bulbus fritillariae cirrhosae is crushed：Low temperature is carried out to the bulbus fritillariae cirrhosae Jing Guo vacuum freeze drying with micronizer, is crushed to 1 μ
M-15 μm (as shown in Figure 2) obtains tendril-leaved fritillary bulb female powder, standby；
D) the tender sweet mixed liquor of pyrus nivalis is made：In the step a), while b) or c) carry out, from apidae insect China
The honey that honeybee Apis cerana Fabricius or apis mellifera Linnaeus Apis mellifera Linnaeus are made, takes honey to be placed in
In refined honey pot, quality is added to be stirred for 25% water of honey, heat uses slow fire instead and keep micro-boiling, removing is floated to after seething with excitement
Foam and wax, impurity, finishing scouring is to seething with excitement, rising such as fish bubble eye, and sth.s made by twisting slightly sticks compared with raw honey, or steaming is to beading of dripping；Will
The fresh fruit of pyrus nivalis ripe rosaceous plant Pyrusnivalis Jacq, after peeling and stoning, fresh juice is made in squeezing
Liquid, filter and produce；It is that 1kg pear juices with quality are that the tender honey of 0.3kg is well mixed by quality, that is, obtains the tender sweet mixed liquor of pear juice, it is standby
With；
E) honey bulbus fritillariae cirrhosae：The 1.2kg tender sweet mixed liquor of pyrus nivalis and tendril-leaved fritillary bulb female powder are weighed respectively, then to weigh quality 8kg pure
Change water, purifying is added in the tender sweet mixed liquor of pyrus nivalis with water, stirred, then the tender sweet mixed liquor of the pyrus nivalis after dilution is poured into
In tendril-leaved fritillary bulb female powder, stir, fully reaction, the honey bulbus fritillariae cirrhosae mixed are standby；
F) bulbus fritillariae cirrhosae of vacuum freeze drying honey system：Honey bulbus fritillariae cirrhosae mixed liquor is laid in vacuum freeze drier material
In disk, liquid level 0.8cm, using Freeze drying repeatedly, for pre-freeze first after extremely -50 DEG C of degree of cooling, the first stage is warming up to -25 DEG C,
Constant temperature 1h；Second stage is cooled to -50 DEG C, constant temperature 2h again, and the temperature of distillation is 35 DEG C, freeze-drying time 32h, vacuum：0-30Pa,
Obtain the tendril-leaved fritillary bulb female powder or powder agglomates of the honey system of drying；
G) crush again：Low temperature powder again is carried out to the honey bulbus fritillariae cirrhosae Jing Guo vacuum freeze drying with micronizer
Broken, it is middle powder (180 μm -250 μm) to be crushed to crushing again, standby；
H) finished product is made：With device of full automatic packaging will be packed as small by the tendril-leaved fritillary bulb female powder of the honey system crushed again
Packaging Bottle.
Comparative example 2：
The step of making tendril-leaved fritillary bulb female powder with traditional method for honey preparing is as follows：
1st, take and the bulbus fritillariae cirrhosae raw material in embodiment 2 with batch, after removing hair fibrous root, soil, non-medicinal effects, use
Water is rinsed well, dries (drying temperature：50℃)；
2nd, from apidae insect apis cerana Apis cerana Fabricius or apis mellifera Linnaeus Apis mellifera
The honey that Linnaeus is made, take honey to be placed in refined honey pot, 25% water for adding quality to be honey, stir, heat to boiling
Afterwards, use slow fire instead and keep micro-boiling, remove floating foam and wax, filter off dead honeybee, impurity, finishing scouring is extremely seethed with excitement, risen such as fish bubble eye, sth. made by twisting
It is slightly glutinous compared with raw honey；By the fresh fruit of pyrus nivalis ripe rosaceous plant Pyrusnivalis Jacq, through removing the peel and going
After core, Fresh sap is made in squeezing, filters and produces；It is that 1kg pear juices with quality are that the tender honey of 0.3kg is well mixed by quality, produces
It is standby to the tender sweet mixed liquor of pear juice；
3rd, the 1.2kg tender sweet mixed liquor of pyrus nivalis and bulbus fritillariae cirrhosae is weighed respectively, the tender sweet mixed liquor of pyrus nivalis is poured into bulbus fritillariae cirrhosae, together
Shi Jiare, temperature reach 47 DEG C, abundant hot dipping 13 hours, during this period every 1h stirrings once, it is evenly distributed, absorbed
Entirely, the bulbus fritillariae cirrhosae after sweet system is obtained；
4th, the bulbus fritillariae cirrhosae after the honey system obtained in step 3 is placed in baking oven, temperature 60 C, drying time 6h；
5th, dried bulbus fritillariae cirrhosae is crushed with pulverizer；
6th, tendril-leaved fritillary bulb female powder is subjected to sterilization filling, obtains sweet manufactured goods.
Example 2 carries out content analysis with the finished product in comparative example 2, analyzes the western shellfish of main component in bulbus fritillariae cirrhosae
Female alkali, finally obtain following experimental data：
As can be seen from the table, the imperialine content in the tendril-leaved fritillary bulb female powder obtained with the technology in comparative example 2 is not
It is qualified, and the content of the imperialine in the bulbus fritillariae cirrhosae obtained with the technology in embodiment 2 is qualified, and significantly larger than country's mark
Accurate or provincial standard line.Because sprayed in example 2 first when bulbus fritillariae cirrhosae is cleaned using vaporific drinking water
Bulbus fritillariae cirrhosae is drenched, is then carrying out Rapid Cleaning with circulating water, the loss for the imperialine being effectively prevented in bulbus fritillariae cirrhosae, then
Low-temperature operation is all used in whole technical process, is advantageous to the preservation of the imperialine of non-refractory.
Embodiment 3
A kind of pyrus nivalis honeybee broken wall bulbus fritillariae cirrhosae flour producing process, step are following (as shown in Figure 1)：
A) bulbus fritillariae cirrhosae raw material are taken, after removing hair fibrous root, soil, non-medicinal effects, are first sprayed with a small amount of vaporific drinking water
Bulbus fritillariae cirrhosae is drenched, by bulbus fritillariae cirrhosae moistened surface, excessive moisture is filtered off on filter screen, stands, after surface soil is soft, then will drink
Water loads high-pressure water cleaning device by bulbus fritillariae cirrhosae Rapid Cleaning (scavenging period control in 3 minutes), clean to medicinal material surface without
Silt, drain away the water in time；
B) bulbus fritillariae cirrhosae is crushed：Low temperature is carried out to the bulbus fritillariae cirrhosae Jing Guo vacuum freeze drying with micronizer, is crushed to 1 μ
M-15 μm (as shown in Figure 2) obtains tendril-leaved fritillary bulb female powder, standby；
C) bulbus fritillariae cirrhosae after processing is subjected to vacuum freeze drying：Bulbus fritillariae cirrhosae is laid in vacuum freeze drier, river
For the thickness that fritillaria heap comes in 1cm, pre-freezing temperature is -40 DEG C, soaking time 1h, and the temperature of distillation is 30 DEG C, vacuum
0-50Pa, drying time 18h, drying finish, and take out standby；
D) the tender sweet mixed liquor of pyrus nivalis is made：In the step a), while b) or c) carry out, from apidae insect China
The honey that honeybee Apis cerana Fabricius or apis mellifera Linnaeus Apis mellifera Linnaeus are made, takes honey to be placed in
In refined honey pot, quality is added to be stirred for 30% water of honey, heat uses slow fire instead and keep micro-boiling, removing is floated to after seething with excitement
Foam and wax, finishing scouring to seethe with excitement, rise as a fish bubble eye, sth.s made by twisting compared with raw honey slightly stick；By rosaceous plant Pyrusnivalis
The fresh fruit of pyrus nivalis ripe Jacq, after peeling and stoning, Fresh sap is made in squeezing, filters and produces；It is 1kg by quality
Pear juice is that the tender honey of 0.3kg is well mixed with quality, that is, obtains the tender sweet mixed liquor of pear juice, standby；
E) honey bulbus fritillariae cirrhosae：The 0.9kg tender sweet mixed liquor of pyrus nivalis and tendril-leaved fritillary bulb female powder are weighed respectively, then to weigh quality 6kg pure
Change water, purifying is added in the tender sweet mixed liquor of pyrus nivalis with water, stirred, then the tender sweet mixed liquor of the pyrus nivalis after dilution is poured into
In tendril-leaved fritillary bulb female powder, stir, fully reaction, the honey bulbus fritillariae cirrhosae mixed are standby；
F) bulbus fritillariae cirrhosae of vacuum freeze drying honey system：The honey bulbus fritillariae cirrhosae mixed liquor of mixing, vacuum is laid in by mixed liquor
In freeze drier material disc, liquid level 0.5cm, using Freeze drying repeatedly, first degree of cooling is to after -50 DEG C for pre-freeze, the first rank
Section is warming up to -25 DEG C, constant temperature 1h；Second stage is cooled to -50 DEG C, constant temperature 2h again, and the temperature of distillation is 32 DEG C, freeze-drying time
30h, vacuum 5-25Pa, obtain the tendril-leaved fritillary bulb female powder or powder agglomates of the honey system of drying；
G) crush again：Low temperature powder again is carried out to the honey bulbus fritillariae cirrhosae Jing Guo vacuum freeze drying with micronizer
Broken, it is middle powder (180 μm -250 μm) to be crushed to crushing again, standby；
H) finished product is made：With device of full automatic packaging will be packed as small by the tendril-leaved fritillary bulb female powder of the honey system crushed again
Packaging bag.
Comparative example 3：
The step of making tendril-leaved fritillary bulb female powder with traditional method for honey preparing is as follows：
1st, take and the bulbus fritillariae cirrhosae raw material in embodiment 3 with batch, after removing hair fibrous root, soil, non-medicinal effects, use
Water is rinsed well, dries (drying temperature：60℃)；
2nd, from apidae insect apis cerana Apis cerana Fabricius or apis mellifera Linnaeus Apis mellifera
The honey that Linnaeus is made, take honey to be placed in refined honey pot, 30% water for adding quality to be honey, stir, heat to boiling
Afterwards, use slow fire instead and keep micro-boiling, remove floating foam and wax, filter off dead honeybee, impurity, finishing scouring is extremely seethed with excitement, risen such as fish bubble eye, sth. made by twisting
It is slightly glutinous compared with raw honey；By the fresh fruit of pyrus nivalis ripe rosaceous plant Pyrusnivalis Jacq, through removing the peel and going
After core, Fresh sap is made in squeezing, filters and produces；It is that 1kg pear juices with quality are that the tender honey of 0.3kg is well mixed by quality, produces
It is standby to the tender sweet mixed liquor of pear juice；
3rd, the 0.9kg tender sweet mixed liquor of pyrus nivalis and bulbus fritillariae cirrhosae is weighed respectively, and the tender sweet mixed liquor of pyrus nivalis is poured into bulbus fritillariae cirrhosae,
Heat simultaneously, under the conditions of temperature reaches 50 DEG C, abundant hot dipping 10 hours, during this period every 1h stirrings once, make its distribution equal
It is even, absorb completely, obtain the bulbus fritillariae cirrhosae after sweet system；
4th, the bulbus fritillariae cirrhosae after the honey system obtained in step 3 is placed in baking oven, temperature 70 C, drying time 4h；
5th, dried bulbus fritillariae cirrhosae is crushed with pulverizer；
6th, tendril-leaved fritillary bulb female powder is subjected to sterilization filling, obtains sweet manufactured goods.
Example 3 carries out content analysis with the finished product in comparative example 3, analyzes the western shellfish of main component in bulbus fritillariae cirrhosae
Female alkali, finally obtain following experimental data：
As can be seen from the table, the imperialine content in the tendril-leaved fritillary bulb female powder obtained with the technology in comparative example 3 is not
It is qualified, and the content of the imperialine in the bulbus fritillariae cirrhosae obtained with the technology in embodiment 3 is qualified, and significantly larger than country's mark
Accurate or provincial standard line.Because sprayed in embodiment 3 first when bulbus fritillariae cirrhosae is cleaned using vaporific drinking water
Bulbus fritillariae cirrhosae is drenched, is then carrying out Rapid Cleaning with circulating water, the loss for the imperialine being effectively prevented in bulbus fritillariae cirrhosae, then
Low-temperature operation is all used in whole technical process, is advantageous to the preservation of the imperialine of non-refractory.
Finally illustrate, the above embodiments are merely illustrative of the technical solutions of the present invention and it is unrestricted, although with reference to compared with
The present invention is described in detail good embodiment, it will be understood by those within the art that, can be to the skill of the present invention
Art scheme is modified or equivalent substitution, and without departing from the objective and scope of technical solution of the present invention, it all should cover at this
Among the right of invention.
Claims (4)
1. a kind of pyrus nivalis honeybee broken wall bulbus fritillariae cirrhosae flour producing process, it is characterised in that comprise the following steps：
A) net system processing early stage is carried out to bulbus fritillariae cirrhosae raw material；
B) bulbus fritillariae cirrhosae after processing is subjected to vacuum freeze drying：Bulbus fritillariae cirrhosae is laid in vacuum freeze drier, bulbus fritillariae cirrhosae
The thickness that heap comes is no more than 2cm, and pre-freezing temperature is -40 DEG C and is incubated 1-2h, and the maximum temperature of distillation is 35 DEG C, vacuum
0-100Pa, drying time 10-25h；Drying finishes, and takes out standby；
C) bulbus fritillariae cirrhosae is crushed：Low-temperature grinding (0-25 DEG C) is carried out to the bulbus fritillariae cirrhosae Jing Guo vacuum freeze drying with micronizer,
It is crushed to 1 μm -15 μm and obtains tendril-leaved fritillary bulb female powder, it is standby；
D) the tender sweet mixed liquor of pyrus nivalis is made：In the step a), while b) or c) carry out, in mass ratio 10:3 by pear juice with it is tender
Honey is well mixed, that is, obtains the tender sweet mixed liquor of pyrus nivalis, standby；
E) honey bulbus fritillariae cirrhosae：By weight 1:1 weighs tendril-leaved fritillary bulb female powder and the tender sweet mixed liquor of pyrus nivalis, adds in the tender sweet mixed liquor of pyrus nivalis
Enter purifying to be diluted with water, purifying is stirred with 6-7 times that the quality of water is the tender sweet mixed liquor quality of pyrus nivalis, then will be dilute
The tender sweet mixed liquor of pyrus nivalis after releasing is poured into tendril-leaved fritillary bulb female powder, is stirred, fully reaction, obtains honey bulbus fritillariae cirrhosae mixed liquor, standby
With；
F) bulbus fritillariae cirrhosae of vacuum freeze drying honey system：Honey bulbus fritillariae cirrhosae mixed liquor is laid in vacuum freeze drier material disc
In, liquid level thickness 0.5-1.2cm, using Freeze drying repeatedly, pre-freeze first degree of cooling to after -50 DEG C, the first stage is warming up to -
25 DEG C, constant temperature 1-2h；Second stage is cooled to -50 DEG C again, constant temperature 1-2h；Distillation heating maximum temperature is 35 DEG C, drying time
25-40h vacuum 0-30Pa, obtains the tendril-leaved fritillary bulb female powder or powder agglomates of the honey system of drying to completion is dried, standby；
G) crush again：The tendril-leaved fritillary bulb female powder or powder agglomates made with pulverizer to the honey by vacuum freeze drying carry out low temperature powder again
It is broken, middle powder (180 μm -250 μm) is crushed to, it is standby；
H) finished product is made：The tendril-leaved fritillary bulb female powder made by the honey crushed again is dispensed and obtains finished product.
2. a kind of pyrus nivalis honeybee broken wall bulbus fritillariae cirrhosae flour producing process as claimed in claim 1, it is characterised in that step a's
Detailed process is：Bulbus fritillariae cirrhosae raw material are taken, after removing hair fibrous root, soil, non-medicinal effects, bulbus fritillariae cirrhosae is layered on filter screen,
Water spray bulbus fritillariae cirrhosae first is drunk with vaporific on a small quantity, by bulbus fritillariae cirrhosae moistened surface, stands, after surface soil is soft, then will drink
Water loads high-pressure water cleaning device by bulbus fritillariae cirrhosae Rapid Cleaning (scavenging period control in 3 minutes), clean to medicinal material surface without
Silt, drain away the water in time.
3. a kind of pyrus nivalis honeybee broken wall bulbus fritillariae cirrhosae flour producing process as claimed in claim 1, it is characterised in that in step d
The tender sweet refining process is：From apidae insect apis cerana Apis cerana Fabricius or apis mellifera Linnaeus
The honey that Apis mellifera Linnaeus are made, takes honey to be placed in refined honey pot, adds the water for the 20-30% that quality is honey,
Stir, heat uses slow fire instead and keep micro-boiling, remove floating foam and wax, filter off dead honeybee, impurity, finishing scouring is extremely to after seething with excitement
Boiling, rise such as fish bubble eye, sth.s made by twisting slightly sticks compared with raw honey, or steaming is to beading of dripping.
4. a kind of pyrus nivalis honeybee broken wall bulbus fritillariae cirrhosae flour producing process as claimed in claim 1, it is characterised in that in step d
The manufacturing process of the pear juice is：By the fresh fruit of pyrus nivalis ripe rosaceous plant Pyrusnivalis Jacq, through peeling
After stoning, Fresh sap is made in squeezing, filters and produces.
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Cited By (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN109090457A (en) * | 2018-08-27 | 2018-12-28 | 怀宁县荣升食品厂 | A kind of bulbus fritillariae cirrhosae cake and preparation method thereof |
| CN113521181A (en) * | 2020-04-19 | 2021-10-22 | 邓学峰 | Preparation formula and preparation method of prepared fritillaria cirrhosa decoction pieces |
Citations (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN104147333A (en) * | 2014-07-28 | 2014-11-19 | 四川藏域川贝生物研究中心有限公司 | Preparation formula of bulbus fritillariae cirrhosae processed with honey and preparation method |
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2017
- 2017-08-03 CN CN201710656544.7A patent/CN107441314A/en active Pending
Patent Citations (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN104147333A (en) * | 2014-07-28 | 2014-11-19 | 四川藏域川贝生物研究中心有限公司 | Preparation formula of bulbus fritillariae cirrhosae processed with honey and preparation method |
Cited By (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN109090457A (en) * | 2018-08-27 | 2018-12-28 | 怀宁县荣升食品厂 | A kind of bulbus fritillariae cirrhosae cake and preparation method thereof |
| CN113521181A (en) * | 2020-04-19 | 2021-10-22 | 邓学峰 | Preparation formula and preparation method of prepared fritillaria cirrhosa decoction pieces |
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Application publication date: 20171208 |