CN106544083A - A kind of lubricating oil flame-proof antibiotic additive - Google Patents

A kind of lubricating oil flame-proof antibiotic additive Download PDF

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Publication number
CN106544083A
CN106544083A CN201610876384.2A CN201610876384A CN106544083A CN 106544083 A CN106544083 A CN 106544083A CN 201610876384 A CN201610876384 A CN 201610876384A CN 106544083 A CN106544083 A CN 106544083A
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parts
powder
rubber
lubricating oil
sulfenamide
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田斗金
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Foshan Man Technology Co Ltd
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Foshan Man Technology Co Ltd
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    • C—CHEMISTRY; METALLURGY
    • C10—PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
    • C10M—LUBRICATING COMPOSITIONS; USE OF CHEMICAL SUBSTANCES EITHER ALONE OR AS LUBRICATING INGREDIENTS IN A LUBRICATING COMPOSITION
    • C10M167/00—Lubricating compositions characterised by the additive being a mixture of a macromolecular compound, a non-macromolecular compound and a compound of unknown or incompletely defined constitution, each of these compounds being essential
    • C—CHEMISTRY; METALLURGY
    • C10—PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
    • C10M—LUBRICATING COMPOSITIONS; USE OF CHEMICAL SUBSTANCES EITHER ALONE OR AS LUBRICATING INGREDIENTS IN A LUBRICATING COMPOSITION
    • C10M2201/00—Inorganic compounds or elements as ingredients in lubricant compositions
    • C10M2201/06—Metal compounds
    • C10M2201/065—Sulfides; Selenides; Tellurides
    • C—CHEMISTRY; METALLURGY
    • C10—PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
    • C10M—LUBRICATING COMPOSITIONS; USE OF CHEMICAL SUBSTANCES EITHER ALONE OR AS LUBRICATING INGREDIENTS IN A LUBRICATING COMPOSITION
    • C10M2201/00—Inorganic compounds or elements as ingredients in lubricant compositions
    • C10M2201/08—Inorganic acids or salts thereof
    • C—CHEMISTRY; METALLURGY
    • C10—PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
    • C10M—LUBRICATING COMPOSITIONS; USE OF CHEMICAL SUBSTANCES EITHER ALONE OR AS LUBRICATING INGREDIENTS IN A LUBRICATING COMPOSITION
    • C10M2201/00—Inorganic compounds or elements as ingredients in lubricant compositions
    • C10M2201/08—Inorganic acids or salts thereof
    • C10M2201/081—Inorganic acids or salts thereof containing halogen
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    • C10—PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
    • C10M—LUBRICATING COMPOSITIONS; USE OF CHEMICAL SUBSTANCES EITHER ALONE OR AS LUBRICATING INGREDIENTS IN A LUBRICATING COMPOSITION
    • C10M2201/00—Inorganic compounds or elements as ingredients in lubricant compositions
    • C10M2201/08—Inorganic acids or salts thereof
    • C10M2201/084—Inorganic acids or salts thereof containing sulfur, selenium or tellurium
    • C—CHEMISTRY; METALLURGY
    • C10—PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
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    • C10M2201/00—Inorganic compounds or elements as ingredients in lubricant compositions
    • C10M2201/10—Compounds containing silicon
    • C10M2201/102—Silicates
    • C10M2201/103—Clays; Mica; Zeolites
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    • C10M2207/00—Organic non-macromolecular hydrocarbon compounds containing hydrogen, carbon and oxygen as ingredients in lubricant compositions
    • C10M2207/10—Carboxylix acids; Neutral salts thereof
    • C10M2207/16—Naphthenic acids
    • C—CHEMISTRY; METALLURGY
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    • C10M2207/00—Organic non-macromolecular hydrocarbon compounds containing hydrogen, carbon and oxygen as ingredients in lubricant compositions
    • C10M2207/10—Carboxylix acids; Neutral salts thereof
    • C10M2207/24—Epoxidised acids; Ester derivatives thereof
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    • C10M2207/00—Organic non-macromolecular hydrocarbon compounds containing hydrogen, carbon and oxygen as ingredients in lubricant compositions
    • C10M2207/28—Esters
    • C10M2207/283—Esters of polyhydroxy compounds
    • C—CHEMISTRY; METALLURGY
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    • C10M—LUBRICATING COMPOSITIONS; USE OF CHEMICAL SUBSTANCES EITHER ALONE OR AS LUBRICATING INGREDIENTS IN A LUBRICATING COMPOSITION
    • C10M2207/00—Organic non-macromolecular hydrocarbon compounds containing hydrogen, carbon and oxygen as ingredients in lubricant compositions
    • C10M2207/28—Esters
    • C10M2207/284—Esters of aromatic monocarboxylic acids
    • C—CHEMISTRY; METALLURGY
    • C10—PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
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    • C10M2207/00—Organic non-macromolecular hydrocarbon compounds containing hydrogen, carbon and oxygen as ingredients in lubricant compositions
    • C10M2207/40—Fatty vegetable or animal oils
    • C—CHEMISTRY; METALLURGY
    • C10—PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
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    • C10M2211/00—Organic non-macromolecular compounds containing halogen as ingredients in lubricant compositions
    • C10M2211/04—Organic non-macromolecular compounds containing halogen as ingredients in lubricant compositions containing carbon, hydrogen, halogen, and oxygen
    • C10M2211/042—Alcohols; Ethers; Aldehydes; Ketones
    • C—CHEMISTRY; METALLURGY
    • C10—PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
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    • C10M2215/00—Organic non-macromolecular compounds containing nitrogen as ingredients in lubricant compositions
    • C10M2215/02—Amines, e.g. polyalkylene polyamines; Quaternary amines
    • C10M2215/04—Amines, e.g. polyalkylene polyamines; Quaternary amines having amino groups bound to acyclic or cycloaliphatic carbon atoms
    • C—CHEMISTRY; METALLURGY
    • C10—PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
    • C10M—LUBRICATING COMPOSITIONS; USE OF CHEMICAL SUBSTANCES EITHER ALONE OR AS LUBRICATING INGREDIENTS IN A LUBRICATING COMPOSITION
    • C10M2215/00—Organic non-macromolecular compounds containing nitrogen as ingredients in lubricant compositions
    • C10M2215/08—Amides
    • C—CHEMISTRY; METALLURGY
    • C10—PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
    • C10M—LUBRICATING COMPOSITIONS; USE OF CHEMICAL SUBSTANCES EITHER ALONE OR AS LUBRICATING INGREDIENTS IN A LUBRICATING COMPOSITION
    • C10M2215/00—Organic non-macromolecular compounds containing nitrogen as ingredients in lubricant compositions
    • C10M2215/10—Amides of carbonic or haloformic acids
    • C10M2215/102—Ureas; Semicarbazides; Allophanates
    • C—CHEMISTRY; METALLURGY
    • C10—PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
    • C10M—LUBRICATING COMPOSITIONS; USE OF CHEMICAL SUBSTANCES EITHER ALONE OR AS LUBRICATING INGREDIENTS IN A LUBRICATING COMPOSITION
    • C10M2217/00—Organic macromolecular compounds containing nitrogen as ingredients in lubricant compositions
    • C10M2217/02—Macromolecular compounds obtained from nitrogen containing monomers by reactions only involving carbon-to-carbon unsaturated bonds
    • C10M2217/026—Macromolecular compounds obtained from nitrogen containing monomers by reactions only involving carbon-to-carbon unsaturated bonds containing monomers having an unsaturated radical bound to a nitrile group
    • C—CHEMISTRY; METALLURGY
    • C10—PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
    • C10M—LUBRICATING COMPOSITIONS; USE OF CHEMICAL SUBSTANCES EITHER ALONE OR AS LUBRICATING INGREDIENTS IN A LUBRICATING COMPOSITION
    • C10M2217/00—Organic macromolecular compounds containing nitrogen as ingredients in lubricant compositions
    • C10M2217/04—Macromolecular compounds from nitrogen-containing monomers obtained otherwise than by reactions only involving carbon-to-carbon unsaturated bonds
    • C10M2217/045—Polyureas; Polyurethanes
    • C—CHEMISTRY; METALLURGY
    • C10—PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
    • C10M—LUBRICATING COMPOSITIONS; USE OF CHEMICAL SUBSTANCES EITHER ALONE OR AS LUBRICATING INGREDIENTS IN A LUBRICATING COMPOSITION
    • C10M2219/00—Organic non-macromolecular compounds containing sulfur, selenium or tellurium as ingredients in lubricant compositions
    • C10M2219/10—Heterocyclic compounds containing sulfur, selenium or tellurium compounds in the ring
    • C10M2219/104—Heterocyclic compounds containing sulfur, selenium or tellurium compounds in the ring containing sulfur and carbon with nitrogen or oxygen in the ring
    • C—CHEMISTRY; METALLURGY
    • C10—PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
    • C10M—LUBRICATING COMPOSITIONS; USE OF CHEMICAL SUBSTANCES EITHER ALONE OR AS LUBRICATING INGREDIENTS IN A LUBRICATING COMPOSITION
    • C10M2223/00—Organic non-macromolecular compounds containing phosphorus as ingredients in lubricant compositions
    • C10M2223/02—Organic non-macromolecular compounds containing phosphorus as ingredients in lubricant compositions having no phosphorus-to-carbon bonds
    • C10M2223/04—Phosphate esters
    • C—CHEMISTRY; METALLURGY
    • C10—PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
    • C10M—LUBRICATING COMPOSITIONS; USE OF CHEMICAL SUBSTANCES EITHER ALONE OR AS LUBRICATING INGREDIENTS IN A LUBRICATING COMPOSITION
    • C10M2229/00—Organic macromolecular compounds containing atoms of elements not provided for in groups C10M2205/00, C10M2209/00, C10M2213/00, C10M2217/00, C10M2221/00 or C10M2225/00 as ingredients in lubricant compositions
    • C10M2229/04—Siloxanes with specific structure
    • C10M2229/05—Siloxanes with specific structure containing atoms other than silicon, hydrogen, oxygen or carbon
    • C10M2229/051—Siloxanes with specific structure containing atoms other than silicon, hydrogen, oxygen or carbon containing halogen
    • C—CHEMISTRY; METALLURGY
    • C10—PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
    • C10N—INDEXING SCHEME ASSOCIATED WITH SUBCLASS C10M RELATING TO LUBRICATING COMPOSITIONS
    • C10N2030/00—Specified physical or chemical properties which is improved by the additive characterising the lubricating composition, e.g. multifunctional additives
    • C10N2030/12—Inhibition of corrosion, e.g. anti-rust agents or anti-corrosives
    • C—CHEMISTRY; METALLURGY
    • C10—PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
    • C10N—INDEXING SCHEME ASSOCIATED WITH SUBCLASS C10M RELATING TO LUBRICATING COMPOSITIONS
    • C10N2030/00—Specified physical or chemical properties which is improved by the additive characterising the lubricating composition, e.g. multifunctional additives
    • C10N2030/16—Antiseptic; (micro) biocidal or bactericidal

Abstract

The present invention relates to a kind of lubricating oil flame-proof antibiotic additive, composed of the following components：Fluorosioloxane rubber, hydrogenated nitrile-butadiene rubber, Lauxite, phosphotriester, hexahydro phthalic anhydride, deca-BDE, sodium antimonate, dibromodimethyl hydantoin, dioctadecyl dimethyl ammonium chloride, ethylparaben, aphthenic acids, copper sulfate, potassium fluotitanate, modified attapulgite powder end, Fructus Canarii albi stone powder, magnesite powder, zinc sulfide powder, pearl essence, CuPc, sodium dichromate, mica powder, conch meal, dimethylformamide, tricaprylin, Herba Lysimachiae foenum-graeci quintessence oil, N n-methylolacrylamide, 2 benzothiazole sulfenamide of the N tert-butyl groups, 2 benzothiazole sulfenamide of N oxydiethylenes, α-cyanogen is for acrylate, rubber oil.Product of the present invention has more superior fire-retardant, acid and alkali-resistance, anti-mildew anti-microbial property, improves properties of product.

Description

A kind of lubricating oil flame-proof antibiotic additive
Technical field
The present invention relates to a kind of lubricating oil flame-proof antibiotic additive, belongs to technical field of lubricating oil.
Background technology
Lubricating oil is used in all kinds automobile, plant equipment reducing the liquid of friction, protection machinery and workpiece Or semisolid lubricants, act primarily as the effects such as lubrication, supplement heat rejecter, antirust, cleaning, sealing and buffering.As long as it is applied to two Between the object of individual relative motion, and friction and the function of abrasion that two articles are produced because of contact can be reduced, as be lubricated Oil.Lubricating oil is typically made up of base oil and additive two parts.Base oil is the main component of lubricating oil, decides lubricating oil Fundamental property, additive can then make up and improve the deficiency of base oil aspect of performance, give some new performances, be lubricating oil Important component part.General lube oil additive, its performance are single, it is necessary to improved using suitable mode.
The content of the invention
It is an object of the invention to provide a kind of lubricating oil flame-proof antibiotic additive, fire-retardant so that lubricating oil is better achieved The use function of antibacterial additives, makes product have fire-retardant, acid and alkali-resistance, anti-mildew anti-microbial property, improves product performance.
To achieve these goals, technical scheme is as follows.
A kind of lubricating oil flame-proof antibiotic additive, is made up of the component of following mass fraction：18～22 parts of fluorosioloxane rubber, hydrogen Change 16～20 parts of nitrile rubber, 16～20 parts of Lauxite, 14～18 parts of phosphotriester, hexahydro phthalic anhydride 16～20 Part, 16～20 parts of deca-BDE, 14～18 parts of sodium antimonate, 16～20 parts of dibromodimethyl hydantoin, double octadecyls two 16～20 parts of ammonio methacrylate, 14～18 parts of ethylparaben, 14～18 parts of aphthenic acids, 14～18 parts of copper sulfate, fluorine 16～20 parts of potassium titanate, 14～18 parts of modified attapulgite powder end, 12～16 parts of Fructus Canarii albi stone powder, 16～20 parts of magnesite powder, 14～18 parts of zinc sulfide powder, 12～16 parts of pearl essence, 14～18 parts of CuPc, 12～16 parts of sodium dichromate, mica powder 12～ 16 parts, 14～18 parts of conch meal, 14～18 parts of dimethylformamide, 14～18 parts of tricaprylin, Herba Lysimachiae foenum-graeci quintessence oil 14～ 18 parts, 14～18 parts of N hydroxymethyl acrylamide, 14～18 parts of N tert butyl benzothiazole 2 sulfenamide, N- oxygen di- it is sub- Ethyl -14～18 parts of 2-[4-morpholinodithio sulfenamide, α-cyanogen are for 14～18 parts of acrylate, 12～16 parts of rubber oil.
Further, above-mentioned lubricating oil flame-proof antibiotic additive, is made up of the component of following mass fraction：Fluorosioloxane rubber 18 Part, 16 parts of hydrogenated nitrile-butadiene rubber, 16 parts of Lauxite, 14 parts of phosphotriester, 16 parts of hexahydro phthalic anhydride, decabrominated dipheny 16 parts of ether, 14 parts of sodium antimonate, 16 parts of dibromodimethyl hydantoin, 16 parts of dioctadecyl dimethyl ammonium chloride, para hydroxybenzene 14 parts of Ethyl formate, 14 parts of aphthenic acids, 14 parts of copper sulfate, 16 parts of potassium fluotitanate, modified attapulgite powder end 14 parts, Fructus Canarii albi stone powder 12 parts of end, 16 parts of magnesite powder, 14 parts of zinc sulfide powder, 12 parts of pearl essence, 14 parts of CuPc, 12 parts of sodium dichromate, mica powder 12 parts, 14 parts of conch meal, 14 parts of dimethylformamide, 14 parts of tricaprylin, 14 parts of Herba Lysimachiae foenum-graeci quintessence oil, N- methylol propylene 14 parts of amide, 14 parts of N tert butyl benzothiazole 2 sulfenamide, N-oxy-diethlene-2-henzothiazole-sulfenamide 14 Part, α-cyanogen are for 14 parts of acrylate, 12 parts of rubber oil.
Further, above-mentioned lubricating oil flame-proof antibiotic additive, is made up of the component of following mass fraction：Fluorosioloxane rubber 20 Part, 18 parts of hydrogenated nitrile-butadiene rubber, 18 parts of Lauxite, 16 parts of phosphotriester, 18 parts of hexahydro phthalic anhydride, decabrominated dipheny 18 parts of ether, 16 parts of sodium antimonate, 18 parts of dibromodimethyl hydantoin, 18 parts of dioctadecyl dimethyl ammonium chloride, para hydroxybenzene 16 parts of Ethyl formate, 16 parts of aphthenic acids, 16 parts of copper sulfate, 18 parts of potassium fluotitanate, modified attapulgite powder end 16 parts, Fructus Canarii albi stone powder 14 parts of end, 18 parts of magnesite powder, 16 parts of zinc sulfide powder, 14 parts of pearl essence, 16 parts of CuPc, 14 parts of sodium dichromate, mica powder 14 parts, 16 parts of conch meal, 16 parts of dimethylformamide, 16 parts of tricaprylin, 16 parts of Herba Lysimachiae foenum-graeci quintessence oil, N- methylol propylene 16 parts of amide, 16 parts of N tert butyl benzothiazole 2 sulfenamide, N-oxy-diethlene-2-henzothiazole-sulfenamide 16 Part, α-cyanogen are for 16 parts of acrylate, 14 parts of rubber oil.
Further, above-mentioned lubricating oil flame-proof antibiotic additive, is made up of the component of following mass fraction：Fluorosioloxane rubber 22 Part, 20 parts of hydrogenated nitrile-butadiene rubber, 20 parts of Lauxite, 18 parts of phosphotriester, 20 parts of hexahydro phthalic anhydride, decabrominated dipheny 20 parts of ether, 18 parts of sodium antimonate, 20 parts of dibromodimethyl hydantoin, 20 parts of dioctadecyl dimethyl ammonium chloride, para hydroxybenzene 18 parts of Ethyl formate, 18 parts of aphthenic acids, 18 parts of copper sulfate, 20 parts of potassium fluotitanate, modified attapulgite powder end 18 parts, Fructus Canarii albi stone powder 16 parts of end, 20 parts of magnesite powder, 18 parts of zinc sulfide powder, 16 parts of pearl essence, 18 parts of CuPc, 16 parts of sodium dichromate, mica powder 16 parts, 18 parts of conch meal, 18 parts of dimethylformamide, 18 parts of tricaprylin, 18 parts of Herba Lysimachiae foenum-graeci quintessence oil, N- methylol propylene 18 parts of amide, 18 parts of N tert butyl benzothiazole 2 sulfenamide, N-oxy-diethlene-2-henzothiazole-sulfenamide 18 Part, α-cyanogen are for 18 parts of acrylate, 16 parts of rubber oil.
Further, above-mentioned lubricating oil flame-proof antibiotic addictive preparation method step is as follows：
（1）By the fluorosioloxane rubber of the mass fraction, hydrogenated nitrile-butadiene rubber, Lauxite, phosphotriester, hexahydro O-phthalic Anhydride, deca-BDE, sodium antimonate, dibromodimethyl hydantoin, dioctadecyl dimethyl ammonium chloride, P-hydroxybenzoic acid Ethyl ester, aphthenic acids, copper sulfate, potassium fluotitanate, modified attapulgite powder end, Fructus Canarii albi stone powder, magnesite powder, zinc sulfide powder, Pearl essence, CuPc, sodium dichromate are mixed, and ultrasound is disperseed at a high speed, and ultrasonic frequency is 20～40KHz, rate of dispersion 5000～5400r/min or so, jitter time are 30～60min；
（2）The mica powder of the mass fraction, conch meal, dimethylformamide, tricaprylin, Herba Lysimachiae foenum-graeci quintessence oil are added, Ultrasonic to disperse at a high speed, ultrasonic frequency is 20～35KHz, 4800～5200r/min of rate of dispersion or so, jitter time is 30～ 50min；
（3）Add the N hydroxymethyl acrylamide of the mass fraction, N tert butyl benzothiazole 2 sulfenamide, N- oxygen connection Diethylidene -2-[4-morpholinodithio sulfenamide, α-cyanogen disperse for acrylate, rubber oil, ultrasound at a high speed, and ultrasonic frequency is 20～30KHz, 4600～4800r/min of rate of dispersion or so, jitter time are 20～40min；This product is obtained after mix homogeneously.
The beneficial effect of the invention is：Lubricating oil flame-proof antibiotic additive in the present invention, it is composed of the following components：Fluorine Silicone rubber, hydrogenated nitrile-butadiene rubber, Lauxite, phosphotriester, hexahydro phthalic anhydride, deca-BDE, sodium antimonate, two Bromine dimethyl hydantoin, dioctadecyl dimethyl ammonium chloride, ethylparaben, aphthenic acids, copper sulfate, fluotitanic acid Potassium, modified attapulgite powder end, Fructus Canarii albi stone powder, magnesite powder, zinc sulfide powder, pearl essence, CuPc, sodium dichromate, cloud Female powder, conch meal, dimethylformamide, tricaprylin, Herba Lysimachiae foenum-graeci quintessence oil, N hydroxymethyl acrylamide, the N- tert-butyl group -2- Benzothiazole sulfenamide, N-oxy-diethlene-2-henzothiazole-sulfenamide, α-cyanogen are for acrylate, rubber oil.This Invention product has more superior fire-retardant, acid and alkali-resistance, anti-mildew anti-microbial property, improves properties of product.
Specific embodiment
The specific embodiment of the present invention is described with reference to embodiment, to be better understood from the present invention.
Embodiment 1
Lubricating oil flame-proof antibiotic additive in the present embodiment, is made up of the component of following mass fraction：18 parts of fluorosioloxane rubber, hydrogen Change 16 parts of nitrile rubber, 16 parts of Lauxite, 14 parts of phosphotriester, 16 parts of hexahydro phthalic anhydride, deca-BDE 16 Part, 14 parts of sodium antimonate, 16 parts of dibromodimethyl hydantoin, 16 parts of dioctadecyl dimethyl ammonium chloride, P-hydroxybenzoic acid 14 parts of ethyl ester, 14 parts of aphthenic acids, 14 parts of copper sulfate, 16 parts of potassium fluotitanate, modified attapulgite powder end 14 parts, Fructus Canarii albi stone powder 12 Part, 16 parts of magnesite powder, 14 parts of zinc sulfide powder, 12 parts of pearl essence, 14 parts of CuPc, 12 parts of sodium dichromate, 12 parts of mica powder, 14 parts of conch meal, 14 parts of dimethylformamide, 14 parts of tricaprylin, 14 parts of Herba Lysimachiae foenum-graeci quintessence oil, N hydroxymethyl acrylamide 14 parts, 14 parts of N tert butyl benzothiazole 2 sulfenamide, 14 parts of N-oxy-diethlene-2-henzothiazole-sulfenamide, α-cyanogen is for 14 parts of acrylate, 12 parts of rubber oil.
Above-mentioned lubricating oil flame-proof antibiotic addictive preparation method step is as follows：
（1）By the fluorosioloxane rubber of the mass fraction, hydrogenated nitrile-butadiene rubber, Lauxite, phosphotriester, hexahydro O-phthalic Anhydride, deca-BDE, sodium antimonate, dibromodimethyl hydantoin, dioctadecyl dimethyl ammonium chloride, P-hydroxybenzoic acid Ethyl ester, aphthenic acids, copper sulfate, potassium fluotitanate, modified attapulgite powder end, Fructus Canarii albi stone powder, magnesite powder, zinc sulfide powder, Pearl essence, CuPc, sodium dichromate are mixed, and ultrasound is disperseed at a high speed, and ultrasonic frequency is 20kHz, rate of dispersion 5400r/ Min or so, jitter time are 60min；
（2）The mica powder of the mass fraction, conch meal, dimethylformamide, tricaprylin, Herba Lysimachiae foenum-graeci quintessence oil are added, Ultrasonic to disperse at a high speed, ultrasonic frequency is 20kHz, rate of dispersion 5200r/min or so, and jitter time is 50min；
（3）Add the N hydroxymethyl acrylamide of the mass fraction, N tert butyl benzothiazole 2 sulfenamide, N- oxygen connection Diethylidene -2-[4-morpholinodithio sulfenamide, α-cyanogen disperse for acrylate, rubber oil, ultrasound at a high speed, and ultrasonic frequency is 20kHz, rate of dispersion 4800r/min or so, jitter time is 40min；This product is obtained after mix homogeneously.
Embodiment 2
Lubricating oil flame-proof antibiotic additive in the present embodiment, is made up of the component of following mass fraction：20 parts of fluorosioloxane rubber, hydrogen Change 18 parts of nitrile rubber, 18 parts of Lauxite, 16 parts of phosphotriester, 18 parts of hexahydro phthalic anhydride, deca-BDE 18 Part, 16 parts of sodium antimonate, 18 parts of dibromodimethyl hydantoin, 18 parts of dioctadecyl dimethyl ammonium chloride, P-hydroxybenzoic acid 16 parts of ethyl ester, 16 parts of aphthenic acids, 16 parts of copper sulfate, 18 parts of potassium fluotitanate, modified attapulgite powder end 16 parts, Fructus Canarii albi stone powder 14 Part, 18 parts of magnesite powder, 16 parts of zinc sulfide powder, 14 parts of pearl essence, 16 parts of CuPc, 14 parts of sodium dichromate, 14 parts of mica powder, 16 parts of conch meal, 16 parts of dimethylformamide, 16 parts of tricaprylin, 16 parts of Herba Lysimachiae foenum-graeci quintessence oil, N hydroxymethyl acrylamide 16 parts, 16 parts of N tert butyl benzothiazole 2 sulfenamide, 16 parts of N-oxy-diethlene-2-henzothiazole-sulfenamide, α-cyanogen is for 16 parts of acrylate, 14 parts of rubber oil.
Above-mentioned lubricating oil flame-proof antibiotic addictive preparation method step is as follows：
（1）By the fluorosioloxane rubber of the mass fraction, hydrogenated nitrile-butadiene rubber, Lauxite, phosphotriester, hexahydro O-phthalic Anhydride, deca-BDE, sodium antimonate, dibromodimethyl hydantoin, dioctadecyl dimethyl ammonium chloride, P-hydroxybenzoic acid Ethyl ester, aphthenic acids, copper sulfate, potassium fluotitanate, modified attapulgite powder end, Fructus Canarii albi stone powder, magnesite powder, zinc sulfide powder, Pearl essence, CuPc, sodium dichromate are mixed, and ultrasound is disperseed at a high speed, and ultrasonic frequency is 30kHz, rate of dispersion 5200r/ Min or so, jitter time are 45min；
（2）The mica powder of the mass fraction, conch meal, dimethylformamide, tricaprylin, Herba Lysimachiae foenum-graeci quintessence oil are added, Ultrasonic to disperse at a high speed, ultrasonic frequency is 27kHz, rate of dispersion 5000r/min or so, and jitter time is 40min；
（3）Add the N hydroxymethyl acrylamide of the mass fraction, N tert butyl benzothiazole 2 sulfenamide, N- oxygen connection Diethylidene -2-[4-morpholinodithio sulfenamide, α-cyanogen disperse for acrylate, rubber oil, ultrasound at a high speed, and ultrasonic frequency is 25kHz, rate of dispersion 4700r/min or so, jitter time is 30min；This product is obtained after mix homogeneously.
Embodiment 3
Lubricating oil flame-proof antibiotic additive in the present embodiment, is made up of the component of following mass fraction：22 parts of fluorosioloxane rubber, hydrogen Change 20 parts of nitrile rubber, 20 parts of Lauxite, 18 parts of phosphotriester, 20 parts of hexahydro phthalic anhydride, deca-BDE 20 Part, 18 parts of sodium antimonate, 20 parts of dibromodimethyl hydantoin, 20 parts of dioctadecyl dimethyl ammonium chloride, P-hydroxybenzoic acid 18 parts of ethyl ester, 18 parts of aphthenic acids, 18 parts of copper sulfate, 20 parts of potassium fluotitanate, modified attapulgite powder end 18 parts, Fructus Canarii albi stone powder 16 Part, 20 parts of magnesite powder, 18 parts of zinc sulfide powder, 16 parts of pearl essence, 18 parts of CuPc, 16 parts of sodium dichromate, 16 parts of mica powder, 18 parts of conch meal, 18 parts of dimethylformamide, 18 parts of tricaprylin, 18 parts of Herba Lysimachiae foenum-graeci quintessence oil, N hydroxymethyl acrylamide 18 parts, 18 parts of N tert butyl benzothiazole 2 sulfenamide, 18 parts of N-oxy-diethlene-2-henzothiazole-sulfenamide, α-cyanogen is for 18 parts of acrylate, 16 parts of rubber oil.
Above-mentioned lubricating oil flame-proof antibiotic addictive preparation method step is as follows：
（1）By the fluorosioloxane rubber of the mass fraction, hydrogenated nitrile-butadiene rubber, Lauxite, phosphotriester, hexahydro O-phthalic Anhydride, deca-BDE, sodium antimonate, dibromodimethyl hydantoin, dioctadecyl dimethyl ammonium chloride, P-hydroxybenzoic acid Ethyl ester, aphthenic acids, copper sulfate, potassium fluotitanate, modified attapulgite powder end, Fructus Canarii albi stone powder, magnesite powder, zinc sulfide powder, Pearl essence, CuPc, sodium dichromate are mixed, and ultrasound is disperseed at a high speed, and ultrasonic frequency is 40kHz, rate of dispersion 5000r/ Min, jitter time are 30min；
（2）The mica powder of the mass fraction, conch meal, dimethylformamide, tricaprylin, Herba Lysimachiae foenum-graeci quintessence oil are added, Ultrasonic to disperse at a high speed, ultrasonic frequency is 35kHz, and rate of dispersion 4800r/min, jitter time are 30min；
（3）Add the N hydroxymethyl acrylamide of the mass fraction, N tert butyl benzothiazole 2 sulfenamide, N- oxygen connection Diethylidene -2-[4-morpholinodithio sulfenamide, α-cyanogen disperse for acrylate, rubber oil, ultrasound at a high speed, and ultrasonic frequency is 30kHz, rate of dispersion 4600r/min or so, jitter time is 20min；This product is obtained after mix homogeneously.
Performance measurement is carried out for the product in embodiment 1, embodiment 2 and embodiment 3 and certain commercially available prod, it is measured Data are as shown in table 1.Fire protection flame retarding level estimate adopts UL94 standards.
1 the performance test results of table
It can be seen that, product of the present invention has preferable corrosion-resistant, fire protection flame retarding, anti-mildew, anti-microbial property.
The above is the preferred embodiment of the present invention, it is noted that for those skilled in the art For, under the premise without departing from the principles of the invention, some improvements and modifications can also be made, these improvements and modifications are also considered as Protection scope of the present invention.

Claims (5)

1. a kind of lubricating oil flame-proof antibiotic additive, it is characterised in that：It is made up of the component of following mass fraction：Fluorosioloxane rubber 18 ～22 parts, 16～20 parts of hydrogenated nitrile-butadiene rubber, 16～20 parts of Lauxite, 14～18 parts of phosphotriester, hexahydro O-phthalic It is 16～20 parts of anhydride, 16～20 parts of deca-BDE, 14～18 parts of sodium antimonate, 16～20 parts of dibromodimethyl hydantoin, double 16～20 parts of octadecyldimethyl ammonium chloride, 14～18 parts of ethylparaben, 14～18 parts of aphthenic acids, copper sulfate 14 ～18 parts, 16～20 parts of potassium fluotitanate, 14～18 parts of modified attapulgite powder end, 12～16 parts of Fructus Canarii albi stone powder, magnesite powder 16～20 parts, 14～18 parts of zinc sulfide powder, 12～16 parts of pearl essence, 14～18 parts of CuPc, 12～16 parts of sodium dichromate, cloud 12～16 parts of female powder, 14～18 parts of conch meal, 14～18 parts of dimethylformamide, 14～18 parts of tricaprylin, lavandula angustifolia 14～18 parts of quintessence oil, 14～18 parts of N hydroxymethyl acrylamide, 14～18 parts of N tert butyl benzothiazole 2 sulfenamide, N- Oxydiethylene -14～18 parts of 2-[4-morpholinodithio sulfenamide, α-cyanogen are for 14～18 parts of acrylate, rubber oil 12～16 Part.
2. lubricating oil flame-proof antibiotic additive according to claim 1, it is characterised in that：The lubricating oil flame-proof antibiotic adds Plus agent is made up of the component of following mass fraction：18 parts of fluorosioloxane rubber, 16 parts of hydrogenated nitrile-butadiene rubber, 16 parts of Lauxite, phosphoric acid Three 14 parts of esters, 16 parts of hexahydro phthalic anhydride, 16 parts of deca-BDE, 14 parts of sodium antimonate, dibromodimethyl hydantoin 16 parts, 16 parts of dioctadecyl dimethyl ammonium chloride, 14 parts of ethylparaben, 14 parts of aphthenic acids, 14 parts of copper sulfate, fluorine 16 parts of potassium titanate, 14 parts of modified attapulgite powder end, 12 parts of Fructus Canarii albi stone powder, 16 parts of magnesite powder, 14 parts of zinc sulfide powder, pearl It is 12 parts of light powder, 14 parts of CuPc, 12 parts of sodium dichromate, 12 parts of mica powder, 14 parts of conch meal, 14 parts of dimethylformamide, three pungent 14 parts of acid glyceride, 14 parts of Herba Lysimachiae foenum-graeci quintessence oil, 14 parts of N hydroxymethyl acrylamide, N tert butyl benzothiazole 2 sulfenamide 14 parts, 14 parts of N-oxy-diethlene-2-henzothiazole-sulfenamide, α-cyanogen is for 14 parts of acrylate, 12 parts of rubber oil.
3. the lubricating oil flame-proof antibiotic additive according to claim 1 to 2, it is characterised in that：The lubricating oil is fire-retardant anti- Bacteria additive is made up of the component of following mass fraction：20 parts of fluorosioloxane rubber, 18 parts of hydrogenated nitrile-butadiene rubber, 18 parts of Lauxite, In 16 parts of phosphotriester, 18 parts of hexahydro phthalic anhydride, 18 parts of deca-BDE, 16 parts of sodium antimonate, dibromo dimethyl second 18 parts of uride, 18 parts of dioctadecyl dimethyl ammonium chloride, 16 parts of ethylparaben, 16 parts of aphthenic acids, copper sulfate 16 Part, 16 parts of 18 parts of potassium fluotitanate, modified attapulgite powder end, 14 parts of Fructus Canarii albi stone powder, 18 parts of magnesite powder, zinc sulfide powder 16 Part, 14 parts of pearl essence, 16 parts of CuPc, 14 parts of sodium dichromate, 14 parts of mica powder, 16 parts of conch meal, 16 parts of dimethylformamide, 16 parts of tricaprylin, 16 parts of Herba Lysimachiae foenum-graeci quintessence oil, 16 parts of N hydroxymethyl acrylamide, the N- tert-butyl groups -2-[4-morpholinodithio time sulphur 16 parts of amide, 16 parts of N-oxy-diethlene-2-henzothiazole-sulfenamide, α-cyanogen are for 16 parts of acrylate, rubber oil 14 Part.
4. the lubricating oil flame-proof antibiotic additive according to claims 1 to 3, it is characterised in that：The lubricating oil is fire-retardant anti- Bacteria additive is made up of the component of following mass fraction：22 parts of fluorosioloxane rubber, 20 parts of hydrogenated nitrile-butadiene rubber, 20 parts of Lauxite, In 18 parts of phosphotriester, 20 parts of hexahydro phthalic anhydride, 20 parts of deca-BDE, 18 parts of sodium antimonate, dibromo dimethyl second 20 parts of uride, 20 parts of dioctadecyl dimethyl ammonium chloride, 18 parts of ethylparaben, 18 parts of aphthenic acids, copper sulfate 18 Part, 18 parts of 20 parts of potassium fluotitanate, modified attapulgite powder end, 16 parts of Fructus Canarii albi stone powder, 20 parts of magnesite powder, zinc sulfide powder 18 Part, 16 parts of pearl essence, 18 parts of CuPc, 16 parts of sodium dichromate, 16 parts of mica powder, 18 parts of conch meal, 18 parts of dimethylformamide, 18 parts of tricaprylin, 18 parts of Herba Lysimachiae foenum-graeci quintessence oil, 18 parts of N hydroxymethyl acrylamide, the N- tert-butyl groups -2-[4-morpholinodithio time sulphur 18 parts of amide, 18 parts of N-oxy-diethlene-2-henzothiazole-sulfenamide, α-cyanogen are for 18 parts of acrylate, rubber oil 16 Part.
5. lubricating oil flame-proof antibiotic additive according to claim 1, it is characterised in that：The lubricating oil flame-proof antibiotic adds Plus agent preparation method step is as follows：
（1）By the fluorosioloxane rubber of the mass fraction, hydrogenated nitrile-butadiene rubber, Lauxite, phosphotriester, hexahydro O-phthalic Anhydride, deca-BDE, sodium antimonate, dibromodimethyl hydantoin, dioctadecyl dimethyl ammonium chloride, P-hydroxybenzoic acid Ethyl ester, aphthenic acids, copper sulfate, potassium fluotitanate, modified attapulgite powder end, Fructus Canarii albi stone powder, magnesite powder, zinc sulfide powder, Pearl essence, CuPc, sodium dichromate are mixed, and ultrasound is disperseed at a high speed, and ultrasonic frequency is 20～40KHz, and rate of dispersion is about 5000～5400r/min, jitter time are 30～60min or so；
（2）The mica powder of the mass fraction, conch meal, dimethylformamide, tricaprylin, Herba Lysimachiae foenum-graeci quintessence oil are added, Ultrasonic to disperse at a high speed, ultrasonic frequency is 20～35KHz, and rate of dispersion is for about 4800～5200r/min, jitter time is 30～ 50min or so；
（3）Add the N hydroxymethyl acrylamide of the mass fraction, N tert butyl benzothiazole 2 sulfenamide, N- oxygen connection Diethylidene -2-[4-morpholinodithio sulfenamide, α-cyanogen disperse for acrylate, rubber oil, ultrasound at a high speed, and ultrasonic frequency is 20～30KHz, rate of dispersion are for about 4600～4800r/min, and jitter time is 20～40min or so；It is obtained after mix homogeneously This product.
CN201610876384.2A 2016-10-08 2016-10-08 A kind of lubricating oil flame-proof antibiotic additive Pending CN106544083A (en)

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Citations (3)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US20100130392A1 (en) * 2005-02-11 2010-05-27 Johnsondiversey, Inc. Lubricant concentrate containing a phosphate triester
CN105112129A (en) * 2015-09-28 2015-12-02 龚灿锋 Flame-retardant, acid-proof, alkali-proof and anti-bacterial lubricating oil for mechanical bearing
CN105132113A (en) * 2015-09-07 2015-12-09 龚灿锋 Lubricating oil antibacterial flame retardant additive

Patent Citations (3)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US20100130392A1 (en) * 2005-02-11 2010-05-27 Johnsondiversey, Inc. Lubricant concentrate containing a phosphate triester
CN105132113A (en) * 2015-09-07 2015-12-09 龚灿锋 Lubricating oil antibacterial flame retardant additive
CN105112129A (en) * 2015-09-28 2015-12-02 龚灿锋 Flame-retardant, acid-proof, alkali-proof and anti-bacterial lubricating oil for mechanical bearing

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Application publication date: 20170329