CN106566599A - Multifunctional lubricating oil annexing agent - Google Patents

Multifunctional lubricating oil annexing agent Download PDF

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Publication number
CN106566599A
CN106566599A CN201610882405.1A CN201610882405A CN106566599A CN 106566599 A CN106566599 A CN 106566599A CN 201610882405 A CN201610882405 A CN 201610882405A CN 106566599 A CN106566599 A CN 106566599A
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China
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parts
powder
sodium
acid
calcium carbonate
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廖苑蓓
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Anlu City Innovation Technology Co Ltd
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Anlu City Innovation Technology Co Ltd
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Priority to CN201610882405.1A priority Critical patent/CN106566599A/en
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    • C—CHEMISTRY; METALLURGY
    • C10—PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
    • C10M—LUBRICATING COMPOSITIONS; USE OF CHEMICAL SUBSTANCES EITHER ALONE OR AS LUBRICATING INGREDIENTS IN A LUBRICATING COMPOSITION
    • C10M167/00—Lubricating compositions characterised by the additive being a mixture of a macromolecular compound, a non-macromolecular compound and a compound of unknown or incompletely defined constitution, each of these compounds being essential
    • C—CHEMISTRY; METALLURGY
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    • C10M—LUBRICATING COMPOSITIONS; USE OF CHEMICAL SUBSTANCES EITHER ALONE OR AS LUBRICATING INGREDIENTS IN A LUBRICATING COMPOSITION
    • C10M2201/00—Inorganic compounds or elements as ingredients in lubricant compositions
    • C10M2201/04—Elements
    • C10M2201/05—Metals; Alloys
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    • C10M2201/00—Inorganic compounds or elements as ingredients in lubricant compositions
    • C10M2201/06—Metal compounds
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    • C10M2201/00—Inorganic compounds or elements as ingredients in lubricant compositions
    • C10M2201/06—Metal compounds
    • C10M2201/062—Oxides; Hydroxides; Carbonates or bicarbonates
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    • C10M2201/08—Inorganic acids or salts thereof
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    • C10M2201/00—Inorganic compounds or elements as ingredients in lubricant compositions
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    • C10M2201/102—Silicates
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    • C10M2205/04—Organic macromolecular hydrocarbon compounds or fractions, whether or not modified by oxidation as ingredients in lubricant compositions containing aromatic monomers, e.g. styrene
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    • C10M2205/06—Organic macromolecular hydrocarbon compounds or fractions, whether or not modified by oxidation as ingredients in lubricant compositions containing conjugated dienes
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    • C10M2205/00—Organic macromolecular hydrocarbon compounds or fractions, whether or not modified by oxidation as ingredients in lubricant compositions
    • C10M2205/16—Paraffin waxes; Petrolatum, e.g. slack wax
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    • C10M2207/10—Carboxylix acids; Neutral salts thereof
    • C10M2207/12—Carboxylix acids; Neutral salts thereof having carboxyl groups bound to acyclic or cycloaliphatic carbon atoms
    • C10M2207/121—Carboxylix acids; Neutral salts thereof having carboxyl groups bound to acyclic or cycloaliphatic carbon atoms having hydrocarbon chains of seven or less carbon atoms
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    • C10M2207/10—Carboxylix acids; Neutral salts thereof
    • C10M2207/12—Carboxylix acids; Neutral salts thereof having carboxyl groups bound to acyclic or cycloaliphatic carbon atoms
    • C10M2207/125—Carboxylix acids; Neutral salts thereof having carboxyl groups bound to acyclic or cycloaliphatic carbon atoms having hydrocarbon chains of eight up to twenty-nine carbon atoms, i.e. fatty acids
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    • C10M2207/00—Organic non-macromolecular hydrocarbon compounds containing hydrogen, carbon and oxygen as ingredients in lubricant compositions
    • C10M2207/10—Carboxylix acids; Neutral salts thereof
    • C10M2207/16—Naphthenic acids
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    • C10M2207/00—Organic non-macromolecular hydrocarbon compounds containing hydrogen, carbon and oxygen as ingredients in lubricant compositions
    • C10M2207/10—Carboxylix acids; Neutral salts thereof
    • C10M2207/24—Epoxidised acids; Ester derivatives thereof
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    • C10M2207/00—Organic non-macromolecular hydrocarbon compounds containing hydrogen, carbon and oxygen as ingredients in lubricant compositions
    • C10M2207/28—Esters
    • C10M2207/287—Partial esters
    • C10M2207/289—Partial esters containing free hydroxy groups
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    • C10M2207/00—Organic non-macromolecular hydrocarbon compounds containing hydrogen, carbon and oxygen as ingredients in lubricant compositions
    • C10M2207/40—Fatty vegetable or animal oils
    • C—CHEMISTRY; METALLURGY
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    • C10M2209/00—Organic macromolecular compounds containing oxygen as ingredients in lubricant compositions
    • C10M2209/02—Macromolecular compounds obtained by reactions only involving carbon-to-carbon unsaturated bonds
    • C10M2209/08—Macromolecular compounds obtained by reactions only involving carbon-to-carbon unsaturated bonds containing monomers having an unsaturated radical bound to a carboxyl radical, e.g. acrylate type
    • C10M2209/082—Macromolecular compounds obtained by reactions only involving carbon-to-carbon unsaturated bonds containing monomers having an unsaturated radical bound to a carboxyl radical, e.g. acrylate type monocarboxylic
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    • C10M2209/00—Organic macromolecular compounds containing oxygen as ingredients in lubricant compositions
    • C10M2209/10—Macromolecular compoundss obtained otherwise than by reactions only involving carbon-to-carbon unsaturated bonds
    • C10M2209/101—Condensation polymers of aldehydes or ketones and phenols, e.g. Also polyoxyalkylene ether derivatives thereof
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    • C10M2211/00—Organic non-macromolecular compounds containing halogen as ingredients in lubricant compositions
    • C10M2211/02—Organic non-macromolecular compounds containing halogen as ingredients in lubricant compositions containing carbon, hydrogen and halogen only
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    • C10M2215/00—Organic non-macromolecular compounds containing nitrogen as ingredients in lubricant compositions
    • C10M2215/20—Containing nitrogen-to-oxygen bonds
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    • C10M2215/00—Organic non-macromolecular compounds containing nitrogen as ingredients in lubricant compositions
    • C10M2215/22—Heterocyclic nitrogen compounds
    • C10M2215/221—Six-membered rings containing nitrogen and carbon only
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    • C10M2215/00—Organic non-macromolecular compounds containing nitrogen as ingredients in lubricant compositions
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    • C10M2215/221—Six-membered rings containing nitrogen and carbon only
    • C10M2215/222—Triazines
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    • C10M2215/22—Heterocyclic nitrogen compounds
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    • C10M2223/00—Organic non-macromolecular compounds containing phosphorus as ingredients in lubricant compositions
    • C10M2223/02—Organic non-macromolecular compounds containing phosphorus as ingredients in lubricant compositions having no phosphorus-to-carbon bonds
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    • C10M2227/08—Organic non-macromolecular compounds containing atoms of elements not provided for in groups C10M2203/00, C10M2207/00, C10M2211/00, C10M2215/00, C10M2219/00 or C10M2223/00 as ingredients in lubricant compositions having metal-to-carbon bonds
    • C10M2227/083—Sn compounds
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    • C10N2030/00—Specified physical or chemical properties which is improved by the additive characterising the lubricating composition, e.g. multifunctional additives
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  • Chemical & Material Sciences (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • General Chemical & Material Sciences (AREA)
  • Oil, Petroleum & Natural Gas (AREA)
  • Organic Chemistry (AREA)
  • Lubricants (AREA)

Abstract

The invention relates to a multifunctional lubricating oil annexing agent. The multifunctional lubricating oil annexing agent is composed of the following components including a styrene-butadiene-styrene segmented copolymer, polyacrylate rubber, o-cresol formaldehyde epoxy resin, fatty acid sodium, single lauryl alcohol phosphate acid ester, balm essential oil, chenopodium ambrosioides oil, 2-ethylhexyl epoxystearate, benzalkonium chloride, dichloro isocyanuric acid sodium, piperine, prochloraz, ammonium bicarbonate, nanometer aluminum powder, activated calcium carbonate, zinc isoocatanoate, nanometer activated calcium carbonate, paraffin, spodumene powder, molybdenum disilicide powder, polychlorinated biphenyl, decabrominated dipheny ethane, hexahydro-phthalic anhydride, sodium antimonite powder, fluoboric acid, fumaric acid, pentaerythritol triarylate, methyl ethyl ketoxime, dibutyltin dilaurate and sodium hexametaphosphate. The multifunctional lubricating oil annexing agent has the excellent inflaming retarding performance, acid-base resistance, anti-mildew performance and anti-microbial performance, and the product performance is improved.

Description

A kind of lubricating grease multiple function additive
Technical field
The present invention relates to a kind of lubricating grease multiple function additive, belongs to technical field of lubricating oil.
Background technology
Lubricating oil is used in all kinds automobile, plant equipment reducing the liquid of friction, protection machinery and workpiece Or semisolid lubricants, act primarily as the effects such as lubrication, supplement heat rejecter, antirust, cleaning, sealing and buffering.As long as it is applied to two Between the object of individual relative motion, and friction and the function of abrasion that two articles are produced because of contact can be reduced, as be lubricated Oil.Lubricating oil is typically made up of base oil and additive two parts.Base oil is the main component of lubricating oil, decides lubricating oil Fundamental property, additive can then make up and improve the deficiency of base oil aspect of performance, give some new performances, be lubricating oil Important component part.General lube oil additive, its performance are single, it is necessary to improved using suitable mode.
The content of the invention
It is an object of the invention to provide a kind of lubricating grease multiple function additive, so that lubricating grease multiple function is better achieved The use function of additive, makes product have fire-retardant, acid and alkali-resistance, anti-mildew anti-microbial property, improves product performance.
To achieve these goals, technical scheme is as follows.
A kind of lubricating grease multiple function additive, is made up of the component of following mass fraction：S-B-S 26～30 parts of block copolymer, 24～28 parts of lactoprene, 24～28 parts of o-cresol formaldehyde epoxy resin, sodium soap 22 ～26 parts, single 24～28 parts of Tryfac 5573,24～28 parts of Herba Melissae officinalis essential oil, 22～26 parts of Chenopodium Oil, epoxystearic acid 24～28 parts of monooctyl ester, 24～28 parts of benzalkonium chloride, 22～26 parts of dichloroisocyanuric acid sodium, 22～26 parts of piperine, Prochloraz 22 ～26 parts, 24～28 parts of ammonium hydrogen carbonate, 22～26 parts of nanometer aluminium powder, 20～24 parts of activated Calcium carbonate, 24～28 parts of zinc Isoocatanoate, It is 22～26 parts of nm-class active calcium carbonate, 20～24 parts of paraffin, 22～26 parts of spodumene powder, 20～24 parts of molybdenum silicide powder, many 20～24 parts of chlordiphenyl, 20～24 parts of TDE, 18～22 parts of hexahydro phthalic anhydride, sodium antimonate powder 14～ 18 parts, 12～16 parts of fluoboric acid, 12～16 parts of fumaric acid, 12～16 parts of pentaerythritol triacrylate, methyl ethyl ketone 12～16 parts of oxime, 12～16 parts of dibutyl tin laurate, 12～16 parts of sodium hexameta phosphate.
Further, above-mentioned lubricating grease multiple function additive, is made up of the component of following mass fraction：Styrene-fourth two 26 parts of alkene-styrene block copolymer, 24 parts of lactoprene, 24 parts of o-cresol formaldehyde epoxy resin, 22 parts of sodium soap, 24 parts of single Tryfac 5573,24 parts of Herba Melissae officinalis essential oil, 22 parts of Chenopodium Oil, 24 parts of octyl epoxy stearate, benzalkonium chloride 24 Part, 22 parts of dichloroisocyanuric acid sodium, 22 parts of piperine, 22 parts of Prochloraz, 24 parts of ammonium hydrogen carbonate, 22 parts of nanometer aluminium powder, activated carbon 20 parts of sour calcium, 24 parts of zinc Isoocatanoate, 22 parts of nm-class active calcium carbonate, 20 parts of paraffin, 22 parts of spodumene powder, molybdenum silicide powder 20 Part, 20 parts of Polychlorinated biphenyls, 20 parts of TDE, 18 parts of hexahydro phthalic anhydride, 14 parts of sodium antimonate powder, fluoboric acid 12 parts, 12 parts of fumaric acid, 12 parts of pentaerythritol triacrylate, 12 parts of methyl ethyl ketone oxime, dibutyl tin laurate 12 parts, 12 parts of sodium hexameta phosphate.
Further, above-mentioned lubricating grease multiple function additive, is made up of the component of following mass fraction：Styrene-fourth two 28 parts of alkene-styrene block copolymer, 26 parts of lactoprene, 26 parts of o-cresol formaldehyde epoxy resin, 24 parts of sodium soap, 26 parts of single Tryfac 5573,26 parts of Herba Melissae officinalis essential oil, 24 parts of Chenopodium Oil, 26 parts of octyl epoxy stearate, benzalkonium chloride 26 Part, 24 parts of dichloroisocyanuric acid sodium, 24 parts of piperine, 24 parts of Prochloraz, 26 parts of ammonium hydrogen carbonate, 24 parts of nanometer aluminium powder, activated carbon 22 parts of sour calcium, 26 parts of zinc Isoocatanoate, 24 parts of nm-class active calcium carbonate, 22 parts of paraffin, 24 parts of spodumene powder, molybdenum silicide powder 22 Part, 22 parts of Polychlorinated biphenyls, 22 parts of TDE, 20 parts of hexahydro phthalic anhydride, 16 parts of sodium antimonate powder, fluoboric acid 14 parts, 14 parts of fumaric acid, 14 parts of pentaerythritol triacrylate, 14 parts of methyl ethyl ketone oxime, dibutyl tin laurate 14 parts, 14 parts of sodium hexameta phosphate.
Further, above-mentioned lubricating grease multiple function additive, is made up of the component of following mass fraction：Styrene-fourth two 30 parts of alkene-styrene block copolymer, 28 parts of lactoprene, 28 parts of o-cresol formaldehyde epoxy resin, 26 parts of sodium soap, 28 parts of single Tryfac 5573,28 parts of Herba Melissae officinalis essential oil, 26 parts of Chenopodium Oil, 28 parts of octyl epoxy stearate, benzalkonium chloride 28 Part, 26 parts of dichloroisocyanuric acid sodium, 26 parts of piperine, 26 parts of Prochloraz, 28 parts of ammonium hydrogen carbonate, 26 parts of nanometer aluminium powder, activated carbon 24 parts of sour calcium, 28 parts of zinc Isoocatanoate, 26 parts of nm-class active calcium carbonate, 24 parts of paraffin, 26 parts of spodumene powder, molybdenum silicide powder 24 Part, 24 parts of Polychlorinated biphenyls, 24 parts of TDE, 22 parts of hexahydro phthalic anhydride, 18 parts of sodium antimonate powder, fluoboric acid 16 parts, 16 parts of fumaric acid, 16 parts of pentaerythritol triacrylate, 16 parts of methyl ethyl ketone oxime, dibutyl tin laurate 16 parts, 16 parts of sodium hexameta phosphate.
Further, above-mentioned lubricating grease multiple function addictive preparation method step is as follows：
（1）By the styrene butadiene styrene block copolymer (SBS) of the mass fraction, lactoprene, o-cresol formaldehyde Epoxy resin, sodium soap, single Tryfac 5573, Herba Melissae officinalis essential oil, Chenopodium Oil, octyl epoxy stearate, benzalkonium chloride, Dichloroisocyanuric acid sodium, piperine, Prochloraz, ammonium hydrogen carbonate, nanometer aluminium powder, activated Calcium carbonate, zinc Isoocatanoate, nano active carbon Sour calcium, paraffin, spodumene powder, molybdenum silicide powder are mixed, and ultrasound is disperseed at a high speed, and ultrasonic frequency is 20～40KHz, point Scattered 5000～5400r/min of speed or so, jitter time are 30～60min；
（2）Add the Polychlorinated biphenyls of the mass fraction, TDE, hexahydro phthalic anhydride, sodium antimonate powder, Fluoboric acid, ultrasound disperse at a high speed, and ultrasonic frequency is 20～35KHz, 4800～5200r/min of rate of dispersion or so, during dispersion Between be 30～50min；
（3）Add the fumaric acid of the mass fraction, pentaerythritol triacrylate, methyl ethyl ketone oxime, tin dilaurate Dibutyl tin, sodium hexameta phosphate, ultrasound disperse at a high speed, and ultrasonic frequency is 20～30KHz, 4600～4800r/ of rate of dispersion Min or so, jitter time are 20～40min；This product is obtained after mix homogeneously.
The beneficial effect of the invention is：Lubricating grease multiple function additive in the present invention, it is composed of the following components：Benzene second Alkene-butadiene-styrene block copolymer, lactoprene, o-cresol formaldehyde epoxy resin, sodium soap, single lauryl Phosphate ester, Herba Melissae officinalis essential oil, Chenopodium Oil, octyl epoxy stearate, benzalkonium chloride, dichloroisocyanuric acid sodium, piperine, miaow are fresh Amine, ammonium hydrogen carbonate, nanometer aluminium powder, activated Calcium carbonate, zinc Isoocatanoate, nm-class active calcium carbonate, paraffin, spodumene powder, two silication Molybdenum powder, Polychlorinated biphenyls, TDE, hexahydro phthalic anhydride, sodium antimonate powder, fluoboric acid, fumaric acid, Pentaerythritol triacrylate, methyl ethyl ketone oxime, dibutyl tin laurate, sodium hexameta phosphate.Product of the present invention with compared with For superior fire-retardant, acid and alkali-resistance, anti-mildew anti-microbial property, properties of product are improved.
Specific embodiment
The specific embodiment of the present invention is described with reference to embodiment, to be better understood from the present invention.
Embodiment 1
Lubricating grease multiple function additive in the present embodiment, is made up of the component of following mass fraction：Styrene-butadiene-benzene 26 parts of ethylene block copolymer, 24 parts of lactoprene, 24 parts of o-cresol formaldehyde epoxy resin, 22 parts of sodium soap, Dan Yue 24 parts of osmanthus base phosphate ester, 24 parts of Herba Melissae officinalis essential oil, 22 parts of Chenopodium Oil, 24 parts of octyl epoxy stearate, 24 parts of benzalkonium chloride, two 22 parts of chlorine isocyanuric acid sodium, 22 parts of piperine, 22 parts of Prochloraz, 24 parts of ammonium hydrogen carbonate, 22 parts of nanometer aluminium powder, activated Calcium carbonate 20 It is part, 24 parts of zinc Isoocatanoate, 22 parts of nm-class active calcium carbonate, 20 parts of paraffin, 22 parts of spodumene powder, 20 parts of molybdenum silicide powder, many 20 parts of chlordiphenyl, 20 parts of TDE, 18 parts of hexahydro phthalic anhydride, 14 parts of sodium antimonate powder, 12 parts of fluoboric acid, 12 parts of fumaric acid, 12 parts of pentaerythritol triacrylate, 12 parts of methyl ethyl ketone oxime, 12 parts of dibutyl tin laurate, 12 parts of sodium hexameta phosphate.
Above-mentioned lubricating grease multiple function addictive preparation method step is as follows：
（1）By the styrene butadiene styrene block copolymer (SBS) of the mass fraction, lactoprene, o-cresol formaldehyde Epoxy resin, sodium soap, single Tryfac 5573, Herba Melissae officinalis essential oil, Chenopodium Oil, octyl epoxy stearate, benzalkonium chloride, Dichloroisocyanuric acid sodium, piperine, Prochloraz, ammonium hydrogen carbonate, nanometer aluminium powder, activated Calcium carbonate, zinc Isoocatanoate, nano active carbon Sour calcium, paraffin, spodumene powder, molybdenum silicide powder are mixed, and ultrasound is disperseed at a high speed, and ultrasonic frequency is 20kHz, dispersion speed Degree 5400r/min or so, jitter time is 60min；
（2）Add the Polychlorinated biphenyls of the mass fraction, TDE, hexahydro phthalic anhydride, sodium antimonate powder, Fluoboric acid, ultrasound disperse at a high speed, and ultrasonic frequency is 20kHz, rate of dispersion 5200r/min or so, and jitter time is 50min；
（3）Add the fumaric acid of the mass fraction, pentaerythritol triacrylate, methyl ethyl ketone oxime, tin dilaurate Dibutyl tin, sodium hexameta phosphate, ultrasound disperse at a high speed, and ultrasonic frequency is 20kHz, rate of dispersion 4800r/min or so, dispersion Time is 40min；This product is obtained after mix homogeneously.
Embodiment 2
Lubricating grease multiple function additive in the present embodiment, is made up of the component of following mass fraction：Styrene-butadiene-benzene 28 parts of ethylene block copolymer, 26 parts of lactoprene, 26 parts of o-cresol formaldehyde epoxy resin, 24 parts of sodium soap, Dan Yue 26 parts of osmanthus base phosphate ester, 26 parts of Herba Melissae officinalis essential oil, 24 parts of Chenopodium Oil, 26 parts of octyl epoxy stearate, 26 parts of benzalkonium chloride, two 24 parts of chlorine isocyanuric acid sodium, 24 parts of piperine, 24 parts of Prochloraz, 26 parts of ammonium hydrogen carbonate, 24 parts of nanometer aluminium powder, activated Calcium carbonate 22 It is part, 26 parts of zinc Isoocatanoate, 24 parts of nm-class active calcium carbonate, 22 parts of paraffin, 24 parts of spodumene powder, 22 parts of molybdenum silicide powder, many 22 parts of chlordiphenyl, 22 parts of TDE, 20 parts of hexahydro phthalic anhydride, 16 parts of sodium antimonate powder, 14 parts of fluoboric acid, 14 parts of fumaric acid, 14 parts of pentaerythritol triacrylate, 14 parts of methyl ethyl ketone oxime, 14 parts of dibutyl tin laurate, 14 parts of sodium hexameta phosphate.
Above-mentioned lubricating grease multiple function addictive preparation method step is as follows：
（1）By the styrene butadiene styrene block copolymer (SBS) of the mass fraction, lactoprene, o-cresol formaldehyde Epoxy resin, sodium soap, single Tryfac 5573, Herba Melissae officinalis essential oil, Chenopodium Oil, octyl epoxy stearate, benzalkonium chloride, Dichloroisocyanuric acid sodium, piperine, Prochloraz, ammonium hydrogen carbonate, nanometer aluminium powder, activated Calcium carbonate, zinc Isoocatanoate, nano active carbon Sour calcium, paraffin, spodumene powder, molybdenum silicide powder are mixed, and ultrasound is disperseed at a high speed, and ultrasonic frequency is 30kHz, dispersion speed Degree 5200r/min or so, jitter time is 45min；
（2）Add the Polychlorinated biphenyls of the mass fraction, TDE, hexahydro phthalic anhydride, sodium antimonate powder, Fluoboric acid, ultrasound disperse at a high speed, and ultrasonic frequency is 27kHz, rate of dispersion 5000r/min or so, and jitter time is 40min；
（3）Add the fumaric acid of the mass fraction, pentaerythritol triacrylate, methyl ethyl ketone oxime, tin dilaurate Dibutyl tin, sodium hexameta phosphate, ultrasound disperse at a high speed, and ultrasonic frequency is 25kHz, rate of dispersion 4700r/min or so, dispersion Time is 30min；This product is obtained after mix homogeneously.
Embodiment 3
Lubricating grease multiple function additive in the present embodiment, is made up of the component of following mass fraction：Styrene-butadiene-benzene 30 parts of ethylene block copolymer, 28 parts of lactoprene, 28 parts of o-cresol formaldehyde epoxy resin, 26 parts of sodium soap, Dan Yue 28 parts of osmanthus base phosphate ester, 28 parts of Herba Melissae officinalis essential oil, 26 parts of Chenopodium Oil, 28 parts of octyl epoxy stearate, 28 parts of benzalkonium chloride, two 26 parts of chlorine isocyanuric acid sodium, 26 parts of piperine, 26 parts of Prochloraz, 28 parts of ammonium hydrogen carbonate, 26 parts of nanometer aluminium powder, activated Calcium carbonate 24 It is part, 28 parts of zinc Isoocatanoate, 26 parts of nm-class active calcium carbonate, 24 parts of paraffin, 26 parts of spodumene powder, 24 parts of molybdenum silicide powder, many 24 parts of chlordiphenyl, 24 parts of TDE, 22 parts of hexahydro phthalic anhydride, 18 parts of sodium antimonate powder, 16 parts of fluoboric acid, 16 parts of fumaric acid, 16 parts of pentaerythritol triacrylate, 16 parts of methyl ethyl ketone oxime, 16 parts of dibutyl tin laurate, 16 parts of sodium hexameta phosphate.
Above-mentioned lubricating grease multiple function addictive preparation method step is as follows：
（1）By the styrene butadiene styrene block copolymer (SBS) of the mass fraction, lactoprene, o-cresol formaldehyde Epoxy resin, sodium soap, single Tryfac 5573, Herba Melissae officinalis essential oil, Chenopodium Oil, octyl epoxy stearate, benzalkonium chloride, Dichloroisocyanuric acid sodium, piperine, Prochloraz, ammonium hydrogen carbonate, nanometer aluminium powder, activated Calcium carbonate, zinc Isoocatanoate, nano active carbon Sour calcium, paraffin, spodumene powder, molybdenum silicide powder are mixed, and ultrasound is disperseed at a high speed, and ultrasonic frequency is 40kHz, dispersion speed Degree 5000r/min, jitter time is 30min；
（2）Add the Polychlorinated biphenyls of the mass fraction, TDE, hexahydro phthalic anhydride, sodium antimonate powder, Fluoboric acid, ultrasound disperse at a high speed, and ultrasonic frequency is 35kHz, and rate of dispersion 4800r/min, jitter time are 30min；
（3）Add the fumaric acid of the mass fraction, pentaerythritol triacrylate, methyl ethyl ketone oxime, tin dilaurate Dibutyl tin, sodium hexameta phosphate, ultrasound disperse at a high speed, and ultrasonic frequency is 30kHz, rate of dispersion 4600r/min or so, dispersion Time is 20min；This product is obtained after mix homogeneously.
Performance measurement is carried out for the product in embodiment 1, embodiment 2 and embodiment 3 and certain commercially available prod, it is measured Data are as shown in table 1.Fire protection flame retarding level estimate adopts UL94 standards.
1 the performance test results of table
It can be seen that, product of the present invention has preferable corrosion-resistant, fire protection flame retarding, anti-mildew, anti-microbial property.
The above is the preferred embodiment of the present invention, it is noted that for those skilled in the art For, under the premise without departing from the principles of the invention, some improvements and modifications can also be made, these improvements and modifications are also considered as Protection scope of the present invention.

Claims (5)

1. a kind of lubricating grease multiple function additive, it is characterised in that：It is made up of the component of following mass fraction：Styrene-fourth two 26～30 parts of alkene-styrene block copolymer, 24～28 parts of lactoprene, 24～28 parts of o-cresol formaldehyde epoxy resin, 22～26 parts of sodium soap, single 24～28 parts of Tryfac 5573,24～28 parts of Herba Melissae officinalis essential oil, 22～26 parts of Chenopodium Oil, 24～28 parts of octyl epoxy stearate, 24～28 parts of benzalkonium chloride, 22～26 parts of dichloroisocyanuric acid sodium, piperine 22～26 Part, 22～26 parts of Prochloraz, 24～28 parts of ammonium hydrogen carbonate, 22～26 parts of nanometer aluminium powder, 20～24 parts of activated Calcium carbonate, isooctyl acid 24～28 parts of zinc, 22～26 parts of nm-class active calcium carbonate, 20～24 parts of paraffin, 22～26 parts of spodumene powder, molybdenum silicide powder 20～24 parts, 20～24 parts of Polychlorinated biphenyls, 20～24 parts of TDE, 18～22 parts of hexahydro phthalic anhydride, antimony 14～18 parts of sour sodium powder end, 12～16 parts of fluoboric acid, 12～16 parts of fumaric acid, pentaerythritol triacrylate 12～16 Part, 12～16 parts of methyl ethyl ketone oxime, 12～16 parts of dibutyl tin laurate, 12～16 parts of sodium hexameta phosphate.
2. lubricating grease multiple function additive according to claim 1, it is characterised in that：The lubricating grease multiple function additive It is made up of the component of following mass fraction：26 parts of styrene butadiene styrene block copolymer (SBS), lactoprene 24 Part, 24 parts of o-cresol formaldehyde epoxy resin, 22 parts of sodium soap, single 24 parts of Tryfac 5573,24 parts of Herba Melissae officinalis essential oil, Herba Chenopodii 22 parts of oil, 24 parts of octyl epoxy stearate, 24 parts of benzalkonium chloride, 22 parts of dichloroisocyanuric acid sodium, 22 parts of piperine, Prochloraz 22 Part, 24 parts of ammonium hydrogen carbonate, 22 parts of nanometer aluminium powder, 20 parts of activated Calcium carbonate, 24 parts of zinc Isoocatanoate, 22 parts of nm-class active calcium carbonate, 20 parts of paraffin, 22 parts of spodumene powder, 20 parts of molybdenum silicide powder, 20 parts of Polychlorinated biphenyls, 20 parts of TDE, hexahydro are adjacent 18 parts of phthalate anhydride, 14 parts of sodium antimonate powder, 12 parts of fluoboric acid, 12 parts of fumaric acid, pentaerythritol triacrylate 12 Part, 12 parts of methyl ethyl ketone oxime, 12 parts of dibutyl tin laurate, 12 parts of sodium hexameta phosphate.
3. the lubricating grease multiple function additive according to claim 1 to 2, it is characterised in that：The lubricating grease multiple function adds Plus agent is made up of the component of following mass fraction：28 parts of styrene butadiene styrene block copolymer (SBS), polyacrylate rubber 26 parts of glue, 26 parts of o-cresol formaldehyde epoxy resin, 24 parts of sodium soap, single 26 parts of Tryfac 5573,26 parts of Herba Melissae officinalis essential oil, soil 24 parts of Herba Schizonepetae oil, 26 parts of octyl epoxy stearate, 26 parts of benzalkonium chloride, 24 parts of dichloroisocyanuric acid sodium, 24 parts of piperine, miaow are fresh 24 parts of amine, 26 parts of ammonium hydrogen carbonate, 24 parts of nanometer aluminium powder, 22 parts of activated Calcium carbonate, 26 parts of zinc Isoocatanoate, nm-class active calcium carbonate 24 Part, 22 parts of paraffin, 24 parts of spodumene powder, 22 parts of molybdenum silicide powder, 22 parts of Polychlorinated biphenyls, 22 parts of TDE, hexahydro Change 20 parts of phthalic anhydride, 16 parts of sodium antimonate powder, 14 parts of fluoboric acid, 14 parts of fumaric acid, three acrylic acid of tetramethylolmethane 14 parts of ester, 14 parts of methyl ethyl ketone oxime, 14 parts of dibutyl tin laurate, 14 parts of sodium hexameta phosphate.
4. the lubricating grease multiple function additive according to claims 1 to 3, it is characterised in that：The lubricating grease multiple function adds Plus agent is made up of the component of following mass fraction：30 parts of styrene butadiene styrene block copolymer (SBS), polyacrylate rubber 28 parts of glue, 28 parts of o-cresol formaldehyde epoxy resin, 26 parts of sodium soap, single 28 parts of Tryfac 5573,28 parts of Herba Melissae officinalis essential oil, soil 26 parts of Herba Schizonepetae oil, 28 parts of octyl epoxy stearate, 28 parts of benzalkonium chloride, 26 parts of dichloroisocyanuric acid sodium, 26 parts of piperine, miaow are fresh 26 parts of amine, 28 parts of ammonium hydrogen carbonate, 26 parts of nanometer aluminium powder, 24 parts of activated Calcium carbonate, 28 parts of zinc Isoocatanoate, nm-class active calcium carbonate 26 Part, 24 parts of paraffin, 26 parts of spodumene powder, 24 parts of molybdenum silicide powder, 24 parts of Polychlorinated biphenyls, 24 parts of TDE, hexahydro Change 22 parts of phthalic anhydride, 18 parts of sodium antimonate powder, 16 parts of fluoboric acid, 16 parts of fumaric acid, three acrylic acid of tetramethylolmethane 16 parts of ester, 16 parts of methyl ethyl ketone oxime, 16 parts of dibutyl tin laurate, 16 parts of sodium hexameta phosphate.
5. lubricating grease multiple function additive according to claim 1, it is characterised in that：The lubricating grease multiple function additive Preparation method step is as follows：
（1）By the styrene butadiene styrene block copolymer (SBS) of the mass fraction, lactoprene, o-cresol formaldehyde Epoxy resin, sodium soap, single Tryfac 5573, Herba Melissae officinalis essential oil, Chenopodium Oil, octyl epoxy stearate, benzalkonium chloride, Dichloroisocyanuric acid sodium, piperine, Prochloraz, ammonium hydrogen carbonate, nanometer aluminium powder, activated Calcium carbonate, zinc Isoocatanoate, nano active carbon Sour calcium, paraffin, spodumene powder, molybdenum silicide powder are mixed, and ultrasound is disperseed at a high speed, and ultrasonic frequency is 20～40KHz, point Scattered speed about 5000～5400r/min, jitter time are 30～60min or so；
（2）Add the Polychlorinated biphenyls of the mass fraction, TDE, hexahydro phthalic anhydride, sodium antimonate powder, Fluoboric acid, ultrasound disperse at a high speed, and ultrasonic frequency is 20～35KHz, and rate of dispersion is for about 4800～5200r/min, during dispersion Between for 30～50min or so；
（3）Add the fumaric acid of the mass fraction, pentaerythritol triacrylate, methyl ethyl ketone oxime, tin dilaurate Dibutyl tin, sodium hexameta phosphate, ultrasound disperse at a high speed, and ultrasonic frequency is 20～30KHz, and rate of dispersion is for about 4600～ 4800r/min, jitter time are 20～40min or so；This product is obtained after mix homogeneously.
CN201610882405.1A 2016-10-08 2016-10-08 Multifunctional lubricating oil annexing agent Pending CN106566599A (en)

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Cited By (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN111760550A (en) * 2020-06-24 2020-10-13 生态环境部南京环境科学研究所 Device and method for preparing porous active biochar adsorbing material

Cited By (2)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN111760550A (en) * 2020-06-24 2020-10-13 生态环境部南京环境科学研究所 Device and method for preparing porous active biochar adsorbing material
CN111760550B (en) * 2020-06-24 2022-04-08 生态环境部南京环境科学研究所 Device and method for preparing porous active biochar adsorbing material

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