CN106531443A - 650V high-voltage aluminium electrolytic capacitor working electrolyte and preparation method thereof - Google Patents
650V high-voltage aluminium electrolytic capacitor working electrolyte and preparation method thereof Download PDFInfo
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- CN106531443A CN106531443A CN201611078824.6A CN201611078824A CN106531443A CN 106531443 A CN106531443 A CN 106531443A CN 201611078824 A CN201611078824 A CN 201611078824A CN 106531443 A CN106531443 A CN 106531443A
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- acid
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- over voltage
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Classifications
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- H—ELECTRICITY
- H01—ELECTRIC ELEMENTS
- H01G—CAPACITORS; CAPACITORS, RECTIFIERS, DETECTORS, SWITCHING DEVICES OR LIGHT-SENSITIVE DEVICES, OF THE ELECTROLYTIC TYPE
- H01G9/00—Electrolytic capacitors, rectifiers, detectors, switching devices, light-sensitive or temperature-sensitive devices; Processes of their manufacture
- H01G9/004—Details
- H01G9/022—Electrolytes; Absorbents
- H01G9/035—Liquid electrolytes, e.g. impregnating materials
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- H—ELECTRICITY
- H01—ELECTRIC ELEMENTS
- H01G—CAPACITORS; CAPACITORS, RECTIFIERS, DETECTORS, SWITCHING DEVICES OR LIGHT-SENSITIVE DEVICES, OF THE ELECTROLYTIC TYPE
- H01G9/00—Electrolytic capacitors, rectifiers, detectors, switching devices, light-sensitive or temperature-sensitive devices; Processes of their manufacture
- H01G9/145—Liquid electrolytic capacitors
Abstract
A 650V high-voltage aluminium electrolytic capacitor working electrolyte includes, in percentage by mass, 50% to 80% of a main solvent, 20% to 40% of auxiliary solvents, 5% to 15% of solutes, 1% to 8% of a sparking voltage enhancing agent; and the auxiliary solvents are two or more of a gamma-butyrolactone, DMF, polyethylene glycol 200, polyethylene glycol 400, a nano silica solution, glycerol, propylene carbonate, ethylene carbonate, tributyl phosphate, diethylene glycol monobutyl ether, trienthylene glycol dimethacrylate and diethylene glycol. The 650V high-voltage aluminium electrolytic capacitor working electrolyte has the advantages of low viscosity and high conductivity.
Description
Technical field
The present invention relates to a kind of electrolyte of aluminium electrolutic capacitor, more particularly to a kind of 650V high-pressure aluminum electrolytic capacitors work
Make electrolyte and preparation method thereof.
Background technology
Aluminium electrolutic capacitor is one of base components of electronic product, with the continuous improvement of Quality of electronic products, to aluminium
The performances such as the operating voltage of electrolytic capacitor, service life, upper limit working temperature it is also proposed higher and higher requirement.At present,
Many famous brand name capacitor producers such as the Japan taken its place in the front ranks of the world have released one after another rated operational voltage higher than 650V's
Product, also, the new product family released by they is all in terms of super-pressure mostly, it is seen then that ultra-high voltage aluminum electrochemical capacitor
Device is a kind of trend of future development.Although the market share that the aluminium electrolutic capacitor of China accounts for the world is increasing, super
Still air switch area is there is on high-pressure aluminum electrolytic capacitor, and world's advanced technology also has a certain distance.
Electrolyte is the actual negative electrode of aluminium electrolutic capacitor, plays a part of to provide oxonium ion, repairs anode oxide film, because
This, high performance electrolyte plays vital effect for the quality for ensureing aluminium electrolutic capacitor.At present, for super-pressure
(More than 650V)The exploitation of electrolyte, main preferential ammonium carboxylate salt or carboxylic acid from Long carbon chain, but research and development length used at present
, essentially from foreign countries, domestic production technology is simultaneously immature, therefore can cause the production of electrolyte for carbon chain carboxylic acids' ammonium salt or carboxylic acid
High cost, and the inapplicable production with reality.Additionally, the ammonium carboxylate salt or carboxylic acid of Long carbon chain are due to its carbon chain length, its solubility
It is relatively low, the electrical conductivity of electrolyte can be caused relatively low.Patent CN103811183A provides a kind of aluminium electrolutic capacitor of 630V;Patent
CN103794369A provides a kind of aluminium electrolutic capacitor of 700V;Patent CN104465100A provides a kind of 800V alminium electrolytic condensers
Device, but, they adopt solute based on Long carbon chain ammonium carboxylate salt or carboxylic acid, and its electrolytic conductivity is than relatively low, product damage
Consumption is larger.
The content of the invention
The technical problem to be solved in the present invention is to overcome the deficiencies in the prior art, there is provided a kind of 650V high-voltage aluminium electrolysis capacitances
Device Working electrolyte and preparation method thereof.
To solve above-mentioned technical problem, technical scheme proposed by the present invention is:A kind of 650V high-pressure aluminum electrolytic capacitors work
Make electrolyte, including main solvent 50%-80%, secondary solvent 20%-40%, solute 5%-15%, flash over voltage elevator 1%-8%, with
Upper is mass percent;The main solvent is ethylene glycol, and the secondary solvent is gamma-butyrolacton, DMF, polyethylene glycol 200, poly-
Ethylene glycol 400, nanosilica solution, glycerine, propene carbonate, ethylene carbonate, tributyl phosphate, diglycol
Two or more in monobutyl ether, TEGDMA, diglycol;The solute is decanedioic acid
Ammonium, decanedioic acid, adipic acid, azelaic acid hydrogen ammonium, dodecandioic acid ammonium, 1,7- dodecandioic acid ammoniums, ammonium benzoate, mannitol, sorbierite,
Two or more in citric acid, salicylic acid, phytic acid, phosphotungstic acid, ethylenediamine, disodium ethylene diamine tetraacetate;The scintillation
Voltage riser is boric acid, ammonium pentaborate, sodium tetraborate, polyvinyl alcohol, boric acid polyglycol ester, boric acid propanediol polyester, boron
One or more in sour glycerine polyester, boric acid polyethylene glycol polyester, Macrogol 6000.
In the present invention, main solvent is good to the dissolubility of solute, and viscosity is low, and dielectric constant is big, it is easy to improve the electricity of electrolyte
Conductance.In the present invention, secondary solvent primarily serves the oxidation efficiency of the viscosity and electrolyte that improve electrolyte so that electrolyte
Viscosity the oxidation efficiency of electrolyte is accelerated, be capable of a certain degree of flash over voltage for improving electrolyte.This
In invention, the secondary solvent for being added can reduce main solvent intermolecular force, improve electrolysis fluid viscosity so as to play
Effect;Secondary solvent has preferable electrocatalysis characteristic simultaneously, can produce Electro Sorb in the breakdown point of anode oxide film, improve sun
The reaction efficiency of pole paper tinsel surface aluminum oxidation, so that oxidation efficiency is accelerated.
In the present invention, solute is short chain solute, due to its solubility property than long-chain solute more preferably, the short carbon of such homogenous quantities
Chain solute its NH4+Ion concentration can be higher than Long carbon chain, so can keep higher in the case where higher flash over voltage is ensured
Electrical conductivity, simultaneously as its carbochain is short, molecular weight is little, electrolysis fluid viscosity also can accordingly diminish.
Flash over voltage elevator can be preferentially adsorbed on anode due to borate or negatively charged former its of boric acid polyester ion
The surface of paper tinsel;As the reaction of formation of polyester can produce water, aggregated good polyester is added in the electrolytic solution, because reaction is flat
The presence of weighing apparatus, therefore the generation of water can be suppressed, can further improve flash over voltage.
Above-mentioned 650V range high voltage aluminum electrolysis capacitor working electrolytes and preparation method thereof, it is preferred that the high jewelling electricity of 650V
Other additives of electrolysis condenser Working electrolyte also including 0.1%-2%, described other additives are phosphoric acid, ortho phosphorous acid
Two or more in ammonium, ammonium hypophosphite, paranitrobenzoic acid, p nitrobenzyl alcohol, paranitrobenzoic acid ammonium.
A kind of preparation method for such as weighing above-mentioned 650V range high voltage aluminum electrolysis capacitor working electrolytes, comprises the following steps:
1) main solvent and secondary solvent are well mixed;
2)It is the solute that 30%-40% is added under conditions of 40-70 degree Celsius in temperature, stirs and to be warming up to 120-13- Celsius
Degree;
3)130-150 degree Celsius of addition flash over voltage elevator is warmed up to, and continues to heat up until flash over voltage elevator
Dissolving;
4)After flash over voltage dissolving completely, 125-135 degree Celsius is cooled to, adds remaining solute, and be incubated 60-90 point
Clock;
5)It is cooled to 100-105 degree Celsius and adds other additives.
In the present invention, flash over voltage elevator needs higher solution temperature, solute promote flash over voltage elevator
Dissolving, but too high temperature can make solute decompose and moisture evaporation, therefore, in order to ensure electrolyte have it is higher
Electrical conductivity, takes the method that solute is added at twice, that is, be initially charged part solute, then adds flash over voltage elevator, then
Remaining solute is added.
Compared with prior art, it is an advantage of the current invention that:1st, viscosity is low, the 650V high-pressure aluminum electrolytic capacitors of the present invention
Selected by Working electrolyte, solvent viscosity is low, and solute carbochain is short, molecular weight is little and solutes content account for electrolysis liquid hold-up proportion it is little,
The viscosity of electrolyte can be made to diminish.2nd, electrical conductivity is high, short carbon chain solute its NH of homogenous quantities in the present invention4+Ion concentration can be than long
The want height, the addition of secondary solvent of carbochain has substantially no effect on the electrical conductivity of electrolyte, can so allow electrolyte to ensure high scintillation electricity
Higher electrical conductivity is kept in the case of pressure.
Specific embodiment
For the ease of understanding the present invention, present invention work more comprehensively, is meticulously described below in conjunction with preferred embodiment,
But protection scope of the present invention is not limited to embodiment in detail below.
It should be strongly noted that when a certain element, to be described as " be fixed on, be fixed in, be connected to or be communicated in " another
When on element, it can be directly fixed, affixed, connection or connect on another element, or by connecting in the middle of other
Fitting is indirectly fixed, affixed, connection or connection are on another element.
Unless otherwise defined, the implication that all technical terms used hereinafter are generally understood that with those skilled in the art
It is identical.Technical term used herein is intended merely to the purpose for describing specific embodiment, is not intended to limit the present invention
Protection domain.
A kind of 650V range high voltage aluminum electrolysis capacitor working electrolytes, it is characterised in that:Including main solvent 50%-80%, auxiliary
Solvent 20%-40%, solute 5%-15%, flash over voltage elevator 1%-8%, are more than mass percent;The main solvent is second two
Alcohol, the secondary solvent be gamma-butyrolacton, DMF, polyethylene glycol 200, PEG400, nanosilica solution, glycerine,
Propene carbonate, ethylene carbonate, tributyl phosphate, diethylene glycol monobutyl ether, TEGDMA, one
Two or more in diglycol ethylene;The solute be ammonium sebacate, decanedioic acid, adipic acid, azelaic acid hydrogen ammonium, 12
Bisgallic acid ammonium, 1,7- dodecandioic acid ammoniums, ammonium benzoate, mannitol, sorbierite, citric acid, salicylic acid, phytic acid, phosphotungstic acid, second two
Two or more in amine, disodium ethylene diamine tetraacetate;The flash over voltage elevator is boric acid, ammonium pentaborate, four boron
Sour sodium, polyvinyl alcohol, boric acid polyglycol ester, boric acid propanediol polyester, boric acid glycerine polyester, boric acid polyethylene glycol polyester,
One or more in Macrogol 6000.
In the present invention, other additives of 650V range high voltage aluminum electrolysis capacitor working electrolytes also including 0.1%-2% are described
Described other additives are phosphoric acid, ammonium hypophosphite, ammonium hypophosphite, paranitrobenzoic acid, p nitrobenzyl alcohol, p-nitrophenyl first
Two or more in sour ammonium.
A kind of preparation method of 650V range high voltage aluminum electrolysis capacitor working electrolytes, comprises the following steps:1) by main solvent
It is well mixed with secondary solvent;
2)It is the solute that 30%-40% is added under conditions of 40-70 degree Celsius in temperature, stirs and to be warming up to 120-13- Celsius
Degree;
3)130-150 degree Celsius of addition flash over voltage elevator is warmed up to, and continues to heat up until flash over voltage elevator
Dissolving;
4)After flash over voltage dissolving completely, 125-135 degree Celsius is cooled to, adds remaining solute, and be incubated 60-90 point
Clock;
5)It is cooled to 100-105 degree Celsius and adds other additives.
Embodiment 1
The 650V range high voltage aluminum electrolysis capacitor working electrolytes of the present embodiment include that 75% ethylene glycol, 5% are received as shown in Table 1
Rice silicon dioxde solution, 5% glycerine, 6.5% ammonium sebacate, 2% mannitol, 0.5% 1,7- dodecandioic acid ammoniums, 3% boron
Acid polyethylene glycol polyester, 2% polyvinyl alcohol, 0.5% ammonium hypophosphite and 0.5% p nitrobenzyl alcohol, the above be quality hundred
Divide ratio.When preparing, 75% ethylene glycol of mass percent, 5% nanosilica solution, 5% glycerine Hybrid Heating are arrived
40-50 DEG C, add 3% ammonium sebacate, 2% mannitol and 0.5%1,7- dodecandioic acid ammonium.Continue to be heated to 130-135 DEG C, add
Boric acid polyethylene glycol polyester 3%, polyvinyl alcohol 2%, add to its dissolving, are then cooled to 125-135 DEG C, add ammonium sebacate
3.5%, and it is incubated 60min.100-105 DEG C is cooled to, ammonium hypophosphite and p nitrobenzyl alcohol each 0.5% is added, configuration is finished.
As shown in table 2, product electrical characteristic is as shown in table 3 for working electrolyte for aluminium electrolytic capacitor performance parameters
Embodiment 2
As shown in Table 1 the 650V range high voltage aluminum electrolysis capacitor working electrolytes of the present embodiment include 55% ethylene glycol, 10% it is poly-
Ethylene glycol, 5% diethylene glycol monobutyl ether, 6% nanosilica solution, 7% ammonium sebacate, 3% decanedioic acid, 1%
Mannitol, 3% citric acid, 1% 1,7- dodecandioic acid ammoniums, 2% boric acid, 3% polyvinyl alcohol, 2% sodium tetraborate, 1%
Ammonium hypophosphite and 1% p nitrobenzyl alcohol;It is mass percent above.By 55% second of mass percent when preparing
Glycol, 10% PEG400,5% diethylene glycol monobutyl ether, 6% nanosilica solution Hybrid Heating to 40-50 DEG C,
Add 3% ammonium sebacate, 3% decanedioic acid, 1% mannitol and 1%1,7- dodecandioic acid ammoniums.Continue to be heated to 130-135 DEG C, add boron
Acid 2%, polyvinyl alcohol 3%, sodium tetraborate 2%, add to its dissolving, are then cooled to 125-135 DEG C, add ammonium sebacate 4%, lemon
Lemon acid 3%, and it is incubated 70min.100-105 DEG C is cooled to, ammonium hypophosphite and p nitrobenzyl alcohol each 1% is added, configuration is finished.
As shown in table 2, product electrical characteristic is as shown in table 3 for working electrolyte for aluminium electrolytic capacitor performance parameters
The proportioning of each composition in 1 Working electrolyte of table
Composition | Embodiment 1 | Embodiment 2 |
Main solvent | 75% | 55% |
Secondary solvent | 10% | 21% |
Solute | 9% | 15% |
Flash over voltage elevator | 5% | 7% |
Other additives | 1% | 2% |
The test parameter of 2 Working electrolyte of table
Performance parameter | Embodiment 1 | Embodiment 2 |
Water content | 1.7% | 1.5% |
Electrical conductivity(30℃ms/cm) | 654 | 723 |
pH | 5.56 | 5.62 |
Flash over voltage | 691 | 687 |
3 capacitor electrical characteristic of table(With 650V, as a example by 330uF specifications, parameter is averaged for 10 samples of test)
Claims (3)
1. a kind of 650V range high voltage aluminum electrolysis capacitor working electrolytes, it is characterised in that:It is molten including main solvent 50%-80%, auxiliary
Agent 20%-40%, solute 5%-15%, flash over voltage elevator 1%-8%, are more than mass percent;The main solvent is ethylene glycol,
The secondary solvent is gamma-butyrolacton, DMF, polyethylene glycol 200, PEG400, nanosilica solution, glycerine, carbon
Acid propylene ester, ethylene carbonate, tributyl phosphate, diethylene glycol monobutyl ether, TEGDMA, a contracting
Two or more in diethylene glycol;The solute be ammonium sebacate, decanedioic acid, adipic acid, azelaic acid hydrogen ammonium, 12 pairs
Sour ammonium, 1,7- dodecandioic acid ammoniums, ammonium benzoate, mannitol, sorbierite, citric acid, salicylic acid, phytic acid, phosphotungstic acid, ethylenediamine,
Two or more in disodium ethylene diamine tetraacetate;The flash over voltage elevator is boric acid, ammonium pentaborate, tetraboric acid
It is sodium, polyvinyl alcohol, boric acid polyglycol ester, boric acid propanediol polyester, boric acid glycerine polyester, boric acid polyethylene glycol polyester, poly-
One or more in ethylene glycol 6000.
2. 650V range high voltage aluminum electrolysis capacitor working electrolytes according to claim 1 and preparation method thereof, its feature exists
In:Other additives of 650V range high voltage aluminum electrolysis capacitor working electrolytes also including 0.1%-2%, described other additives
For two kinds in phosphoric acid, ammonium hypophosphite, ammonium hypophosphite, paranitrobenzoic acid, p nitrobenzyl alcohol, paranitrobenzoic acid ammonium or
It is two or more.
3. a kind of preparation method of 650V range high voltage aluminum electrolysis capacitor working electrolytes as claimed in claim 1 or 2, its feature
It is:Comprise the following steps:1) main solvent and secondary solvent are well mixed;
2)It is the solute that 30%-40% is added under conditions of 40-70 degree Celsius in temperature, stirs and to be warming up to 120-13- Celsius
Degree;
3)130-150 degree Celsius of addition flash over voltage elevator is warmed up to, and continues to heat up until flash over voltage elevator
Dissolving;
4)After flash over voltage dissolving completely, 125-135 degree Celsius is cooled to, adds remaining solute, and be incubated 60-90 point
Clock;
5)It is cooled to 100-105 degree Celsius and adds other additives.
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Cited By (11)
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CN106992075A (en) * | 2017-04-10 | 2017-07-28 | 益阳市锦汇电子有限公司 | The electrolyte and its compound method of high temperature resistance and the aluminium electrolutic capacitor of high pressure |
CN107887164A (en) * | 2016-11-26 | 2018-04-06 | 广西吉光电子科技有限公司 | A kind of 130 DEG C of range high voltage aluminum electrolysis capacitor working electrolytes and preparation method |
CN109192515A (en) * | 2018-10-11 | 2019-01-11 | 南通新三能电子有限公司 | A kind of operating voltage is 550 volts of aluminium electrolutic capacitors and its manufacturing method |
CN109192514A (en) * | 2018-09-25 | 2019-01-11 | 深圳市智胜新电子技术有限公司 | Aluminum electrolytic capacitor electrolyte and preparation method thereof and aluminium electrolutic capacitor |
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CN110718391A (en) * | 2019-11-18 | 2020-01-21 | 益阳市华琳电子有限公司 | Electrolyte for aluminum electrolytic capacitor and preparation method thereof |
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CN111681877A (en) * | 2020-06-28 | 2020-09-18 | 上海交通大学 | Ionic liquid electrolyte for ultra-high stability aluminum electrolytic capacitor and preparation method thereof |
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CN105244166A (en) * | 2015-09-08 | 2016-01-13 | 南通三鑫电子科技股份有限公司 | 650V ultrahigh voltage aluminum electrolytic capacitor working electrolyte, and preparation method and applications thereof |
CN106158380A (en) * | 2016-08-31 | 2016-11-23 | 湖南艾华集团股份有限公司 | A kind of electrolyte of high-pressure aluminum electrolytic capacitor and preparation method thereof |
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CN105244166A (en) * | 2015-09-08 | 2016-01-13 | 南通三鑫电子科技股份有限公司 | 650V ultrahigh voltage aluminum electrolytic capacitor working electrolyte, and preparation method and applications thereof |
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CN106992075A (en) * | 2017-04-10 | 2017-07-28 | 益阳市锦汇电子有限公司 | The electrolyte and its compound method of high temperature resistance and the aluminium electrolutic capacitor of high pressure |
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CN111247611A (en) * | 2017-10-24 | 2020-06-05 | 三洋化成工业株式会社 | Electrolytic solution for electrolytic capacitor and electrolytic capacitor |
CN109243859A (en) * | 2018-09-18 | 2019-01-18 | 益阳市锦汇电子有限公司 | A kind of super capacitor high-voltage electrolyte and preparation method thereof |
CN109192514A (en) * | 2018-09-25 | 2019-01-11 | 深圳市智胜新电子技术有限公司 | Aluminum electrolytic capacitor electrolyte and preparation method thereof and aluminium electrolutic capacitor |
CN109192515A (en) * | 2018-10-11 | 2019-01-11 | 南通新三能电子有限公司 | A kind of operating voltage is 550 volts of aluminium electrolutic capacitors and its manufacturing method |
CN110718391A (en) * | 2019-11-18 | 2020-01-21 | 益阳市华琳电子有限公司 | Electrolyte for aluminum electrolytic capacitor and preparation method thereof |
CN111146003A (en) * | 2020-01-14 | 2020-05-12 | 东莞台容电子有限公司 | 600V high-voltage low-impedance electrolytic capacitor working electrolyte and manufacturing method thereof |
CN111681877B (en) * | 2020-06-28 | 2021-09-07 | 上海交通大学 | Ionic liquid electrolyte for ultra-high stability aluminum electrolytic capacitor and preparation method thereof |
CN111681877A (en) * | 2020-06-28 | 2020-09-18 | 上海交通大学 | Ionic liquid electrolyte for ultra-high stability aluminum electrolytic capacitor and preparation method thereof |
CN114420455A (en) * | 2022-02-28 | 2022-04-29 | 珠海格力新元电子有限公司 | Sparking voltage improver, preparation method thereof and electrolyte |
CN116130248A (en) * | 2022-11-03 | 2023-05-16 | 江苏瑞友康电子科技有限公司 | High-stability working electrolyte for aluminum electrolytic capacitor and preparation process thereof |
CN116130248B (en) * | 2022-11-03 | 2024-03-29 | 江苏瑞友康电子科技有限公司 | High-stability working electrolyte for aluminum electrolytic capacitor and preparation process thereof |
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