CN106518949A - Tea saponin membrane extracting process - Google Patents
Tea saponin membrane extracting process Download PDFInfo
- Publication number
- CN106518949A CN106518949A CN201610845328.2A CN201610845328A CN106518949A CN 106518949 A CN106518949 A CN 106518949A CN 201610845328 A CN201610845328 A CN 201610845328A CN 106518949 A CN106518949 A CN 106518949A
- Authority
- CN
- China
- Prior art keywords
- film
- membrane
- tea saponin
- tea
- ceramic
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Pending
Links
Classifications
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07J—STEROIDS
- C07J63/00—Steroids in which the cyclopenta(a)hydrophenanthrene skeleton has been modified by expansion of only one ring by one or two atoms
- C07J63/008—Expansion of ring D by one atom, e.g. D homo steroids
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07H—SUGARS; DERIVATIVES THEREOF; NUCLEOSIDES; NUCLEOTIDES; NUCLEIC ACIDS
- C07H1/00—Processes for the preparation of sugar derivatives
- C07H1/06—Separation; Purification
- C07H1/08—Separation; Purification from natural products
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07H—SUGARS; DERIVATIVES THEREOF; NUCLEOSIDES; NUCLEOTIDES; NUCLEIC ACIDS
- C07H15/00—Compounds containing hydrocarbon or substituted hydrocarbon radicals directly attached to hetero atoms of saccharide radicals
- C07H15/20—Carbocyclic rings
- C07H15/24—Condensed ring systems having three or more rings
- C07H15/256—Polyterpene radicals
Landscapes
- Chemical & Material Sciences (AREA)
- Organic Chemistry (AREA)
- Health & Medical Sciences (AREA)
- General Health & Medical Sciences (AREA)
- Life Sciences & Earth Sciences (AREA)
- Engineering & Computer Science (AREA)
- Biochemistry (AREA)
- Biotechnology (AREA)
- Genetics & Genomics (AREA)
- Molecular Biology (AREA)
- Saccharide Compounds (AREA)
Abstract
The invention discloses a tea saponin membrane extracting process. The tea saponin membrane extracting process comprises a series of steps of: drying and crushing tea seed meal, performing extracting and filtering, performing membrane filtering, performing separating, performing membrane concentrating, and performing drying; specific operating steps are as follows: first, drying the tea seed meal in a drying oven at the temperature of 50 to 70 DEG C, and then stirring and crushing the tea seal meal by using a machine; second, adding water, performing heating to 60 DEG C, performing keeping at a constant temperature, performing extracting for two hours for two to three times, and performing filtering by using ultrafine fibre cloth; thirdly, performing treating by using a ceramic membrane, and collecting ceramic membrane permeating liquid; fourthly, performing concentrating treatment on the ceramic membrane permeating liquid through a concentrating membrane, and collecting concentrating membrane permeating liquid; fifthly, performing low-temperature vacuum drying on the concentrating membrane concentrated liquid until powder is obtained, and taking out the powder to obtain the finished product tea saponin. The tea saponin membrane extracting process disclosed by the invention is simple in process, reasonable in design, high in tea saponin extracting purity, stable in performance, low in energy consumption and free of pollution.
Description
Technical field
The invention belongs to technical field of membrane separation, and in particular to a kind of Tea Saponin film extraction process.
Background technology
Tea Saponin also known as TS, it, by the class candy glucoside compound extracted in tea tree seed, is that a kind of performance is good to be
Good natural surfactant, it can be widely applied to light industry, chemical industry, agricultural chemicals, feed, cultivation, weaving, oil recovery, mining, building materials
With the field such as expressway construction.Tea seed cake is remaining slag after the oil expression of tea tree seed, has many tea seed cakes to be taken as waste material every year
Burn, waste substantial amounts of resource.The Tea Saponin containing 12-18% in tea seed cake, extracts Tea Saponin with tea seed cake, with very wide
Wealthy application prospect and considerable economic benefit.At present, the extracting method of Tea Saponin is mainly organic solvent method and water extract-alcohol precipitation
Method, and the new method promoted on this basis, but most of method uses part chemical extraction agent, there is DNA purity
Low, unstable properties, waste a series of problems, such as reagent and production pollution.
The content of the invention
It is an object of the invention to provide a kind of behaviour reasonable in design, DNA purity is high, stable performance, high income, without dirt
The Tea Saponin film extraction process of dye.
The technical scheme is that a kind of Tea Saponin film extraction process, including tea seed cake dries pulverizing, extraction filtration, film mistake
Filter, film are concentrated and are dried series of steps, and concrete operation step is as follows：Step one, tea seed cake is put into baking oven in 50-70 DEG C of temperature
Lower drying, then rolls powdering with machine stirring is broken；Step 2, addition water, are heated to 60 DEG C, keep constant temperature, extraction time 2
Hour, extracting times 2-3 time are filtered with superfine fibre cloth；Step 3, under the high temperature conditions with ceramic film process, obtain ceramics
Film permeate and separation of ceramic film dope collect ceramic membrane permeate；Step 4, by ceramic membrane permeate by concentrate film carry out
Concentration, obtains concentrating film concentrate and concentration film permeate, collects concentration film concentrate；
Step 5, concentration film dope is carried out into low-temperature vacuum drying, be dried to powder and take out, obtain finished product Tea Saponin.
Preferably, the water and the mass ratio of tea seed cake powder that step 2 is added is 10:1.
Preferably, the ceramic membrane in step 3 is tubular ceramic microfiltration membranes.
Preferably, it is hollow fiber ultrafiltration membrane to concentrate film described in step 4.
The present invention is a kind of Tea Saponin film extraction process, is crushed by raw material stoving, extracts filtration, membrane filtration, film concentration
Highly purified Tea Saponin finished product is finally given with dried process, sealing stored under refrigeration is carried out.
Beneficial effects of the present invention：
The present invention is a kind of Tea Saponin film extraction process, process is simple, reasonable in design, and Tea Saponin DNA purity is high, the impact of performance
Stable, energy consumption is low, pollution-free and the Tea Saponin paler colour that extracts, can be extensive with field.
Specific embodiment
For ease of skilled artisan understands that the present invention program, in conjunction with specific embodiment to the technology of the present invention side
Case is further described in detail.
The present invention is a kind of Tea Saponin film extraction process, including tea seed cake dries pulverizing, extraction filtration, membrane filtration, film concentration
Be dried series of steps, concrete operation step is as follows：
Step one, tea seed cake is put into baking oven dries at a temperature of 50-70 DEG C, then powdering is rolled with machine stirring is broken；
Step 2, addition water, are heated to 60 DEG C, holding constant temperature, extraction time 2 hours, and extracting times 2-3 time use superfine fibre
Cloth is filtered；
Step 3, under the high temperature conditions with ceramic film process, obtain ceramic membrane permeate and separation of ceramic film dope collect ceramics
Film permeate；
Step 4, by ceramic membrane permeate by concentrate film carry out concentration, obtain concentrate film concentrate and concentration film pass through
Liquid, collects concentration film concentrate；
Step 5, concentration film dope is carried out into low-temperature vacuum drying, be dried to powder and take out, obtain finished product Tea Saponin.
The water and the mass ratio of tea seed cake powder that step 2 is added is 10:1, the ceramic membrane in step 3 is tubular ceramic micro-filtration
Film, it is hollow fiber ultrafiltration membrane to concentrate film described in step 4.
The present invention is a kind of Tea Saponin film extraction process, is crushed by raw material stoving, extracts filtration, membrane filtration, film concentration
Highly purified Tea Saponin finished product is finally given with dried process, sealing stored under refrigeration is carried out, the Tea Saponin of extraction is a kind of
The natural nonionic surface active agent of function admirable, it has foaming, emulsification, dispersion, a performance such as gentle, and have it is impervious, disappear
The pharmacological action of the aspects such as scorching, analgesia.Therefore, may be utilized in fabricating various types of emulsifying agents, detergent, foaming agent, preservative,
Insecticide and other medicaments.
The present invention program is invented above and is exemplarily described, it is clear that the present invention is implemented
The restriction of formula, if the various unsubstantialities for employing method of the present invention design and technical scheme and carrying out are improved, or without changing
Enter and the design of invention and technical scheme are directly applied to into other occasions, within protection scope of the present invention.
Claims (4)
1. a kind of Tea Saponin film extraction process, concentrates including tea seed cake dries pulverizing, extraction filtration, membrane filtration, film and drying one is
Row step, concrete operation step are as follows：
Step one, tea seed cake is put into baking oven dries at a temperature of 50-70 DEG C, then powdering is rolled with machine stirring is broken；
Step 2, addition water, are heated to 60 DEG C, holding constant temperature, extraction time 2 hours, extracting times 2-3 time,
Filtered with superfine fibre cloth；
Step 3, under the high temperature conditions with ceramic film process, obtain ceramic membrane permeate and separation of ceramic film dope collect ceramics
Film permeate；
Step 4, by ceramic membrane permeate by concentrate film carry out concentration, obtain concentrate film concentrate and concentration film pass through
Liquid, collects concentration film concentrate；
Step 5, concentration film dope is carried out into low-temperature vacuum drying, be dried to powder and take out, obtain finished product Tea Saponin.
2. a kind of Tea Saponin film extraction process according to claim 1, it is characterised in that water and tea seed cake that step 2 is added
The mass ratio of powder is 10:1.
3. a kind of Tea Saponin film extraction process according to claim 1, it is characterised in that the ceramic membrane in step 3 is pipe
Formula ceramic micro filter film.
4. a kind of Tea Saponin film extraction process according to claim 1, it is characterised in that concentrating film described in step 4 is
Hollow fiber ultrafiltration membrane.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201610845328.2A CN106518949A (en) | 2016-09-24 | 2016-09-24 | Tea saponin membrane extracting process |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201610845328.2A CN106518949A (en) | 2016-09-24 | 2016-09-24 | Tea saponin membrane extracting process |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| CN106518949A true CN106518949A (en) | 2017-03-22 |
Family
ID=58344164
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN201610845328.2A Pending CN106518949A (en) | 2016-09-24 | 2016-09-24 | Tea saponin membrane extracting process |
Country Status (1)
| Country | Link |
|---|---|
| CN (1) | CN106518949A (en) |
Cited By (6)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN107383153A (en) * | 2017-08-20 | 2017-11-24 | 合肥信达膜科技有限公司 | A kind of extracting method of high-purity tea saponin |
| CN109897726A (en) * | 2019-03-05 | 2019-06-18 | 石城县群鑫生态发展有限公司 | A kind of tea seed extracts the squeezing process of tea oil |
| CN109897727A (en) * | 2019-03-08 | 2019-06-18 | 石城县群鑫生态发展有限公司 | A kind of tea-seed oil leaching extraction process |
| CN110483610A (en) * | 2019-08-28 | 2019-11-22 | 中国科学院青岛生物能源与过程研究所 | A kind of refining methd of high-purity tea saponin |
| CN110483590A (en) * | 2019-08-28 | 2019-11-22 | 中国科学院青岛生物能源与过程研究所 | A kind of method of Tea Saponin green purification |
| CN110483591A (en) * | 2019-08-28 | 2019-11-22 | 中国科学院青岛生物能源与过程研究所 | A method of combination embrane method refined theasapogenin |
Citations (6)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN101440117A (en) * | 2008-12-30 | 2009-05-27 | 广东新大地生物科技股份有限公司 | Method for extracting tea saponin from tea cake |
| CN101817865A (en) * | 2010-04-20 | 2010-09-01 | 浙江大学 | Method for extracting and separating tea saponin and feeding proteoglycan by using residue-removed oil-tea camellia cake |
| CN101829501A (en) * | 2010-04-21 | 2010-09-15 | 周滨江 | Combined membrane filtering method for Chinese traditional medicine extraction, separation and concentration |
| CN102018835A (en) * | 2009-09-18 | 2011-04-20 | 劲牌有限公司 | Method for separating effective components in traditional Chinese medicine curculigo orchioides by membrane separation method |
| CN102351938A (en) * | 2011-09-01 | 2012-02-15 | 安徽农业大学 | Preparation method of high-purity tea saponin |
| CN203677997U (en) * | 2014-01-27 | 2014-07-02 | 贵州周以晴生物科技有限公司 | Device for extracting tea saponin by adopting water extraction method |
-
2016
- 2016-09-24 CN CN201610845328.2A patent/CN106518949A/en active Pending
Patent Citations (6)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN101440117A (en) * | 2008-12-30 | 2009-05-27 | 广东新大地生物科技股份有限公司 | Method for extracting tea saponin from tea cake |
| CN102018835A (en) * | 2009-09-18 | 2011-04-20 | 劲牌有限公司 | Method for separating effective components in traditional Chinese medicine curculigo orchioides by membrane separation method |
| CN101817865A (en) * | 2010-04-20 | 2010-09-01 | 浙江大学 | Method for extracting and separating tea saponin and feeding proteoglycan by using residue-removed oil-tea camellia cake |
| CN101829501A (en) * | 2010-04-21 | 2010-09-15 | 周滨江 | Combined membrane filtering method for Chinese traditional medicine extraction, separation and concentration |
| CN102351938A (en) * | 2011-09-01 | 2012-02-15 | 安徽农业大学 | Preparation method of high-purity tea saponin |
| CN203677997U (en) * | 2014-01-27 | 2014-07-02 | 贵州周以晴生物科技有限公司 | Device for extracting tea saponin by adopting water extraction method |
Cited By (8)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN107383153A (en) * | 2017-08-20 | 2017-11-24 | 合肥信达膜科技有限公司 | A kind of extracting method of high-purity tea saponin |
| CN109897726A (en) * | 2019-03-05 | 2019-06-18 | 石城县群鑫生态发展有限公司 | A kind of tea seed extracts the squeezing process of tea oil |
| CN109897727A (en) * | 2019-03-08 | 2019-06-18 | 石城县群鑫生态发展有限公司 | A kind of tea-seed oil leaching extraction process |
| CN110483610A (en) * | 2019-08-28 | 2019-11-22 | 中国科学院青岛生物能源与过程研究所 | A kind of refining methd of high-purity tea saponin |
| CN110483590A (en) * | 2019-08-28 | 2019-11-22 | 中国科学院青岛生物能源与过程研究所 | A kind of method of Tea Saponin green purification |
| CN110483591A (en) * | 2019-08-28 | 2019-11-22 | 中国科学院青岛生物能源与过程研究所 | A method of combination embrane method refined theasapogenin |
| CN110483590B (en) * | 2019-08-28 | 2021-10-01 | 中国科学院青岛生物能源与过程研究所 | Green refining method of tea saponin |
| CN110483591B (en) * | 2019-08-28 | 2022-02-15 | 中国科学院青岛生物能源与过程研究所 | Method for refining tea saponin by combined membrane method |
Similar Documents
| Publication | Publication Date | Title |
|---|---|---|
| CN106518949A (en) | Tea saponin membrane extracting process | |
| CN108003215A (en) | The cleaning extracting method of Tea Saponin | |
| CN102161689B (en) | Method for extracting tea saponin from oil-tea-cake | |
| CN101863950A (en) | Method for extracting tea saponin from oil tea cakes | |
| CN104530173A (en) | Process for extracting tea saponin from oil tea cake | |
| CN100447206C (en) | Method of extracting and preparing yellow pigment of pagodatree flower | |
| CN108997471A (en) | A kind of environment-friendly preparation method thereof of high-purity tea saponin | |
| CN102229637B (en) | A kind of technique of extracting Tea Saponin employing membrane separation concentration | |
| CN105461778A (en) | Method for extracting tea saponin from sasangua cake | |
| CN106823552A (en) | A kind of efficiently quick Tea Polyphenols tea grounds separator | |
| CN102617693B (en) | Method utilizing subcritical water extraction technology to extract and prepare ursolic acid from loquat leaves | |
| CN112225774A (en) | Novel method for extracting tea saponin with high purity and high extraction rate | |
| CN104945463A (en) | Extracting method for tea saponin | |
| CN104045681A (en) | Method for extracting tea saponin by utilizing biotechnology | |
| CN103012544A (en) | Method for extracting saponin and polysaccharide from tea-seed pancake | |
| CN101007905A (en) | Method of extracting and preparing Ma chestnut shell brown pigment | |
| CN101747662A (en) | Method for preparing hematoxylin powder dyes | |
| CN108948124A (en) | A kind of preparation method of Tea Saponin | |
| CN1978458A (en) | New cleanproduction process for extracting saponin from dioscorea zingiberensis | |
| CN107383153A (en) | A kind of extracting method of high-purity tea saponin | |
| CN106188213B (en) | A kind of Simple Purification method of Tea Saponin | |
| CN102464898B (en) | Method for recovering yellow ginger pigment from yellow ginger hydrolysate saponin extraction waste liquid | |
| CN106518863A (en) | Berberine film extraction technique | |
| CN203677997U (en) | Device for extracting tea saponin by adopting water extraction method | |
| CN106543199A (en) | A kind of arteannuin film extraction process |
Legal Events
| Date | Code | Title | Description |
|---|---|---|---|
| C06 | Publication | ||
| PB01 | Publication | ||
| SE01 | Entry into force of request for substantive examination | ||
| SE01 | Entry into force of request for substantive examination | ||
| WD01 | Invention patent application deemed withdrawn after publication | ||
| WD01 | Invention patent application deemed withdrawn after publication |
Application publication date: 20170322 |