CN106517141A - Novel hair charring method - Google Patents
Novel hair charring method Download PDFInfo
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- CN106517141A CN106517141A CN201611228322.7A CN201611228322A CN106517141A CN 106517141 A CN106517141 A CN 106517141A CN 201611228322 A CN201611228322 A CN 201611228322A CN 106517141 A CN106517141 A CN 106517141A
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- hair
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- C—CHEMISTRY; METALLURGY
- C01—INORGANIC CHEMISTRY
- C01P—INDEXING SCHEME RELATING TO STRUCTURAL AND PHYSICAL ASPECTS OF SOLID INORGANIC COMPOUNDS
- C01P2002/00—Crystal-structural characteristics
- C01P2002/80—Crystal-structural characteristics defined by measured data other than those specified in group C01P2002/70
- C01P2002/85—Crystal-structural characteristics defined by measured data other than those specified in group C01P2002/70 by XPS, EDX or EDAX data
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Abstract
The invention belongs to the field of diamond manufacturing, and particularly relates to a novel hair charring method. The method comprises the following steps: removing impurities from hair, deoiling, and cleaning; drying, and pulverizing; putting the pulverized hair into a vacuum charring machine, and vacuumizing to 10<-3> pa; heating the hair to 600 DEG C, keeping the temperature for 30 minutes, heating to 1000 DEG C, keeping the temperature for 10 minutes, heating to 1250 DEG C, and keeping the temperature for 10 minutes; and cooling to room temperature to finish charring. According to the method, the charring process is simple, causes less environmental pollution and achieves high charring rate; carbon-containing substances in hair can be completely charred basically, thereby being beneficial to graphitizing treatment in an artificial diamond manufacturing process; the charring method is wide in application range, can be used for charring human or animal hair as well as human or animal bones, and provides a novel raw material for artificial diamond manufacturing; and the charred hair can be also made into souvenirs and artware, thereby having high artistic value and commercial value.
Description
Technical field
The invention belongs to diamond fabrication field, and in particular to a kind of new hair charing method.
Background technology
Diamond, also known as diamond, are that, by C atoms and 4 adjacent C atomic building positive tetrahedron structures, this structure makes
Obtain diamond and there is high rigidity, stable chemical nature, be to be currently known most hard material, belong to isometric system, Chang Han
The impurity element of 0.05%-0.2%, is in octahedron, granatohedron, tetrahedron and their combinate form crystal habit more, pure
Diamond water white transparency, being mixed into and different colours be presented due to trace element, index of refraction 2.417, hardness is 10, absolute hardness
It is 1000 times of quartz, 150 times of corundum, is afraid of bang, can crushes along its cleavage after bang, density 3.52g/cm3。
As diamond is very rare, hard, honorable exquisitely carved, dazzling, given with the emblem of love as eternal by people
Lover Yu, relatives, but in order to preferably express the love to lover and relatives, people are wanted the hair system of relatives and lover
Diamond is made, but hair is complex as the technique that raw material makes diamond, it is therefore desirable to the technology is further ground
Study carefully.
The content of the invention
It is an object of the invention to provide hair first can be carbonized by one kind is subsequently converted into graphite, produce as diamond
The method of raw material.
Based on above-mentioned purpose, the present invention is adopted the following technical scheme that：
Hair is first put into vacuum carbonized machine, is evacuated to 10 by a kind of new hair charing method-3Pa, then hair is heated to
600 DEG C, be incubated 30min, then be warming up to 1000 DEG C, be incubated 10min, then be warmed up to 1250 DEG C, be incubated 10min, after be cooled to room
Temperature, charing are completed.
Further, hair is carried out into following pretreatment first before carbonizing, concrete pretreatment is：First by hair removal of impurities, deoil,
After cleaning, drying, crushing.
Further, the concrete operations of removal of impurities are：The impurity of hair in pallet is removed with tweezers；The concrete operations deoiled
For：Hair after removal of impurities is put in the vessel for filling hair cleansing composition, then vessel are put into into the ultrasonic wave equipped with deionized water
Clean in cleaning machine, 10-20min is cleaned under the conditions of supersonic frequency 40-60KHz, 55-60 DEG C of cleaning temperature；It is first hot during cleaning
Cold rinse again is cleaned, thermal cleaning is that the hair after deoiling is put in the vessel equipped with deionized water, vessel are put into be equipped with and are gone
Clean in the supersonic wave cleaning machine of ionized water, cleaning temperature is 55-60 DEG C, and supersonic frequency is 40-60KHz, clean 5-10min；
Cold rinse is to be put into fill the hair after thermal cleaning in the vessel of water, and vessel are put into the ultrasonic wave equipped with deionized water
Normal temperature cleaning in cleaning machine, supersonic frequency is 40-60KHz, cleans 1-10min；The concrete operations of drying are：By the hair after cleaning
Send out and dry in vacuum drying oven, baking temperature is 55-60 DEG C, toasts 4-12h；The concrete operations of crushing are：By the hair after drying
Broken section of 0.5-1.5mm is ground in providing hair grinder.
Further, the carbonated material prepared by described a kind of new hair charing method.
Compared with prior art, technique effect of the invention is：The invention carbonization process is simple, and environmental pollution is little, charcoal
Rate is high, can carbonize the material of carbon containing in hair completely substantially, is conducive at the graphitization in rhinestone manufacturing process
Reason, charing method use range are wide, can be applied not only to human or animal's hair, it is also possible to for the charing of human or animal's bone,
Making for rhinestone provides new raw material, and the hair after charing can be utilized to make souvenir and handicraft, tool
There are higher artistic value and commercial value.
Description of the drawings
Fig. 1 is the electron-microscope scanning figure using the hair after new hair charing method；
Fig. 2 is in step in method using the present embodiment 3（6）Hair for charing is electric in the scanning of EDSTESCAN VEGA3 types
Mirror EDS phenograms；
Fig. 3 be carbonize in method using the present embodiment 3 after in EDSTESCAN VEGA3 type ESEM EDS phenograms.
Specific embodiment
Embodiment 1
A kind of novel hair charing method, comprises the following steps that：
(1) removal of impurities：The impurity in pallet in 100g hairs is removed with tweezers；
(2) deoil：Hair after removal of impurities is put in the vessel for filling shampoo, then vessel is put into super equipped with deionized water
Clean in sound wave cleaning machine, 10min is cleaned under the conditions of supersonic frequency 40KHz, 55 DEG C of cleaning temperature；
(3) thermal cleaning：Hair after deoiling is put in the vessel equipped with deionized water, vessel are put into equipped with deionized water
Clean in supersonic wave cleaning machine, cleaning temperature is 55 DEG C, and supersonic frequency is 40KHz, clean 5min；
(4) cold rinse：Hair after thermal cleaning is put into and is filled in the vessel of water, vessel are put into equipped with deionized water
Normal temperature cleaning in supersonic wave cleaning machine, supersonic frequency is 40KHz, cleans 1min；
(5) dry：Hair after cleaning is dried in vacuum drying oven, baking temperature is 55 DEG C, toasts 4h；
(6) crush：Hair after drying is put in hair grinder be ground into 0.5mm broken section；
(7) charing process：The hair after crushing is put into into vacuum carbonized machine first, 10 are evacuated to-3Pa, then hair is heated to
600 DEG C, be incubated 30min, then be warming up to 1000 DEG C, be incubated 10min, then be warmed up to 1250 DEG C, be incubated 10min, after be cooled to room
Temperature, charing are completed.
Embodiment 2
A kind of Novel wool charing method, comprises the following steps that：
(1) removal of impurities：100g impuritiess of wool in pallet are removed with tweezers；
(2) deoil：Wool after removal of impurities is put in the vessel for filling shampoo, then vessel is put into super equipped with deionized water
Clean in sound wave cleaning machine, 15min is cleaned under the conditions of supersonic frequency 50KHz, 57 DEG C of cleaning temperature；
(3) thermal cleaning：Wool after deoiling is put in the vessel equipped with deionized water, vessel are put into equipped with deionized water
Clean in supersonic wave cleaning machine, cleaning temperature is 57 DEG C, and supersonic frequency is 50KHz, clean 7min；
(4) cold rinse：Wool after thermal cleaning is put into and is filled in the vessel of water, vessel are put into equipped with deionized water
Normal temperature cleaning in supersonic wave cleaning machine, supersonic frequency is 50KHz, cleans 5.5min；
(5) dry：Wool after cleaning is dried in vacuum drying oven, baking temperature is 57 DEG C, toasts 8h；
(6) crush：Wool after drying is put in hair grinder be ground into 1mm broken section；
(7) charing process：The wool after crushing is put into into vacuum carbonized machine first, 10 are evacuated to-3Pa, then wool is heated to
600 DEG C, be incubated 30min, then be warming up to 1000 DEG C, be incubated 10min, then be warmed up to 1250 DEG C, be incubated 10min, after be cooled to room
Temperature, charing are completed.
Embodiment 3
A kind of new hair charing method, comprises the following steps that：
(1) removal of impurities：The impurity in pallet in 100g hairs is removed with tweezers；
(2) deoil：Hair after removal of impurities is put in the vessel for filling shampoo, then vessel is put into super equipped with deionized water
Clean in sound wave cleaning machine, 20min is cleaned under the conditions of supersonic frequency 60KHz, 60 DEG C of cleaning temperature；
(3) thermal cleaning：Hair after deoiling is put in the vessel equipped with deionized water, vessel are put into equipped with deionized water
Clean in supersonic wave cleaning machine, cleaning temperature is 60 DEG C, and supersonic frequency is 60KHz, clean 10min；
(4) cold rinse：Hair after thermal cleaning is put into and is filled in the vessel of water, vessel are put into equipped with deionized water
Normal temperature cleaning in supersonic wave cleaning machine, supersonic frequency is 60KHz, cleans 10min；
(5) dry：Hair after cleaning is dried in vacuum drying oven, baking temperature is 60 DEG C, toasts 12h；
(6) crush：Hair after drying is put in hair grinder be ground into 1.5mm broken section；
(7) charing process：The hair after crushing is put into into vacuum carbonized machine first, 10 are evacuated to-3Pa, then hair is heated to
600 DEG C, be incubated 30min, then be warming up to 1000 DEG C, be incubated 10min, then be warmed up to 1250 DEG C, be incubated 10min, after be cooled to room
Temperature, charing are completed.
Test example 1：
Using the hair after the method charing of embodiment 3, by shape appearance figure of the hair on TESCAN VEGA3 type ESEMs
For Fig. 1, as seen from the figure, the hair after charing is the particle reunited.
Test example 2：
As shown in Fig. 2 using the method in the present embodiment 3, being swept using EDSTESCAN VEGA3 types before step (7) charing
Retouching Electronic Speculum carries out EDS signs, as shown in figure 3, using the method in the present embodiment 3, will use EDSTESCAN VEGA3 after charing
Type ESEM carries out EDS signs, will Fig. 2 and Fig. 3 contrast understand, charing before carbon be 63.04wt%, carbon after charing
It is transformed into carbonizable substance for carbonaceous components such as 97.5wt%, the protein after charing in hair so as to which the content of middle carbon is increased greatly
It is high.
Claims (4)
1. a kind of new hair charing method, it is characterised in that hair is put into into vacuum carbonized machine first, 10 are evacuated to-3Pa, then
Hair is heated to into 600 DEG C, 30min is incubated, then is warming up to 1000 DEG C, be incubated 10min, then be warmed up to 1250 DEG C, be incubated
10min, after be cooled to room temperature, charing is completed.
2. a kind of new hair charing method according to claim 1, it is characterised in that before charing first by hair carry out with
Lower pretreatment, concrete pretreatment is：After first hair removal of impurities, deoiling, clean, drying, crush.
3. a kind of new hair charing method according to claim 2, it is characterised in that the concrete operations of removal of impurities are：With
Tweezers remove the impurity of hair in pallet；The concrete operations deoiled are：Hair after removal of impurities is put into and fills hair cleansing composition
In vessel, then vessel are put into into cleaning in the supersonic wave cleaning machine equipped with deionized water, in supersonic frequency 40-60KHz, cleaning temperature
10-20min is cleaned under the conditions of 55-60 DEG C of degree；First thermal cleaning cold rinse again during cleaning, thermal cleaning is to be put into the hair after deoiling
In vessel equipped with deionized water, vessel are put in the supersonic wave cleaning machine equipped with deionized water and are cleaned, cleaning temperature is 55-
60 DEG C, supersonic frequency is 40-60KHz, cleans 5-10min；Cold rinse is to be put into fill the hair after thermal cleaning from water
In vessel, vessel are put into into normal temperature cleaning in the supersonic wave cleaning machine equipped with deionized water, supersonic frequency is 40-60KHz, cleaning
1-10min；The concrete operations of drying are：Hair after cleaning is dried in vacuum drying oven, baking temperature is 55-60 DEG C, is dried
Roasting 4-12h；The concrete operations of crushing are：Hair after drying is put in hair grinder be ground into 0.5-1.5mm broken section.
4. the carbonated material by prepared by a kind of new hair charing method described in claim 3.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201611228322.7A CN106517141A (en) | 2016-12-27 | 2016-12-27 | Novel hair charring method |
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| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201611228322.7A CN106517141A (en) | 2016-12-27 | 2016-12-27 | Novel hair charring method |
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| CN106517141A true CN106517141A (en) | 2017-03-22 |
Family
ID=58337684
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| CN201611228322.7A Pending CN106517141A (en) | 2016-12-27 | 2016-12-27 | Novel hair charring method |
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Cited By (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN115124035A (en) * | 2022-07-21 | 2022-09-30 | 生命珍宝有限公司 | Method for cultivating diamond by purifying and carbonizing quantitative hair |
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| CN102060289A (en) * | 2010-11-30 | 2011-05-18 | 王洪涛 | Method for extracting raw material carbon of organism diamond |
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| CN102352273A (en) * | 2011-06-30 | 2012-02-15 | 中南大学 | Biomass carbon for iron ore sintering, preparation thereof and application thereof |
| CN103787303A (en) * | 2014-01-24 | 2014-05-14 | 同济大学 | Natural biomass in-situ transformation preparation method of porous carbon in graded mesh structure |
| CN104030284A (en) * | 2014-06-23 | 2014-09-10 | 深圳市赛普戴蒙德科技有限公司 | Hair-based method for fabricating diamond |
| CN104071770A (en) * | 2014-07-06 | 2014-10-01 | 太原理工大学 | Method for preparing porous functional carbon fiber cluster from waste cotton textiles |
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| CN105054401A (en) * | 2014-07-06 | 2015-11-18 | 耿云花 | Modified nanometer bamboo charcoal mask |
| CN105469999A (en) * | 2015-11-20 | 2016-04-06 | 浙江农林大学 | Method of preparing electrode material for carbon-based supercapacitor by taking bamboo powder as raw material |
| CN105682442A (en) * | 2016-04-06 | 2016-06-15 | 常州市奥普泰科光电有限公司 | Preparation method for light-weight graphite fiber foam nickel electromagnetic shielding material |
| CN106083166A (en) * | 2016-06-08 | 2016-11-09 | 甘肃迅美节能科技股份有限公司 | A kind of animal hair fine-celled foam insulation pottery piece preparation method |
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Patent Citations (11)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN102060289A (en) * | 2010-11-30 | 2011-05-18 | 王洪涛 | Method for extracting raw material carbon of organism diamond |
| CN102070136A (en) * | 2010-11-30 | 2011-05-25 | 李立华 | Extraction process of organism diamond raw material carbon |
| CN102352273A (en) * | 2011-06-30 | 2012-02-15 | 中南大学 | Biomass carbon for iron ore sintering, preparation thereof and application thereof |
| CN103787303A (en) * | 2014-01-24 | 2014-05-14 | 同济大学 | Natural biomass in-situ transformation preparation method of porous carbon in graded mesh structure |
| CN104030284A (en) * | 2014-06-23 | 2014-09-10 | 深圳市赛普戴蒙德科技有限公司 | Hair-based method for fabricating diamond |
| CN104071770A (en) * | 2014-07-06 | 2014-10-01 | 太原理工大学 | Method for preparing porous functional carbon fiber cluster from waste cotton textiles |
| CN105054401A (en) * | 2014-07-06 | 2015-11-18 | 耿云花 | Modified nanometer bamboo charcoal mask |
| CN104194811A (en) * | 2014-09-22 | 2014-12-10 | 张森 | Carbon powder preparation method |
| CN105469999A (en) * | 2015-11-20 | 2016-04-06 | 浙江农林大学 | Method of preparing electrode material for carbon-based supercapacitor by taking bamboo powder as raw material |
| CN105682442A (en) * | 2016-04-06 | 2016-06-15 | 常州市奥普泰科光电有限公司 | Preparation method for light-weight graphite fiber foam nickel electromagnetic shielding material |
| CN106083166A (en) * | 2016-06-08 | 2016-11-09 | 甘肃迅美节能科技股份有限公司 | A kind of animal hair fine-celled foam insulation pottery piece preparation method |
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| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN115124035A (en) * | 2022-07-21 | 2022-09-30 | 生命珍宝有限公司 | Method for cultivating diamond by purifying and carbonizing quantitative hair |
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Application publication date: 20170322 |