CN106511174A - Preparation method of psophocarpus tetragonolobus polysaccharides and application of psophocarpus tetragonolobus polysaccharides in preparation of anti-aging cosmetics - Google Patents
Preparation method of psophocarpus tetragonolobus polysaccharides and application of psophocarpus tetragonolobus polysaccharides in preparation of anti-aging cosmetics Download PDFInfo
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- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/96—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution
- A61K8/97—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution from algae, fungi, lichens or plants; from derivatives thereof
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- A61K8/30—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
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Abstract
The invention discloses a preparation method of psophocarpus tetragonolobus polysaccharides and an application of the psophocarpus tetragonolobus polysaccharides in preparation of anti-aging cosmetics. A psophocarpus tetragonolobus polysaccharide extracting solution can be prepared through process steps including cleaning, drying, grinding, ultrasonic extraction, separation, enzymolysis, deproteinization, concentration and the like and can be applied to preparation of the anti-aging cosmetics. The invention further discloses skin tightening and wrinkle removing body wash. The skin tightening and wrinkle removing body wash comprises raw materials in percentage by weight as follows: 0.3%-0.6% of the psophocarpus tetragonolobus polysaccharides, 8%-10% of ammonium laureth sulfate, 4%-5% of sodium cocoamphoacetate, 3%-4% of ammonium lauryl sulfate, 2.5%-3.5% of cocamidopropyl betaine, 0.8%-1.2% of PEG-7 glyceryl cocoate, 0.08%-0.1% of PEG-160 sorbitan triisostearate, 0.08%-0.1% of PEG-120 methyl glucose dioleate, 0.08%-0.1% of EDTA-2Na, 0.2%-0.3% of DMDM hydantoin, 0.1%-0.15% of fructooligosaccharides, 0.25%-0.35% of citric acid and the balance of deionized water. The body wash can moisturize skin, scavenge free radicals of cells and prevent skin aging and can further promote forming of a hydrolipidic film, prevent bacterial infection and form double protection for the skin.
Description
Technical field
The invention belongs to cosmetic technical field, and in particular to the preparation method of a kind of Semen Psophocarpi tetragonolobi polysaccharide and its anti-preparing
Application in aging cosmetics.
Background technology
Aging be cell must Jing a process for persistently changing, all annoying the mankind always up to now.Affect thin
The factor of born of the same parents' senescence process has a lot, such as work and rest, diet, heavy metal, Exposure to Sunlight, weather etc..The mankind use most extensive now
Defying age means be that but price is uneven using the cosmetics with anti-aging effects, better expensive of effect, just
Suitable effect is bad, thus people always for seek a kind of high anti-aging cosmetics of cost performance and effort.
The Chinese invention patent application of Application No. 201510843396.0 provides a kind of bath gel and preparation method thereof,
It is composed of the following raw materials by weight：Aloe extraction solution 10-20 parts, dendrobium candidum solution 10-20 part, emulsified silicone oil 30-40 parts, bigcatkin willow
Sour 1-2 parts, almond oil 20-40 parts, deionized water 1000-2000 parts, MES 50-60 parts, coconut oil fat
Sour diglycollic amide 30-40 parts, essence 2-8 parts, preservative 2-6 parts, glycine betaine 90-100 parts.
The Chinese invention patent application of Application No. 201610215449.9 provides a kind of awake skin bath gel of Fructus Pruni pseudocerasi, by under
State component to constitute by weight percentage：Water 62%-72%, sodium laureth sulfate 12%-17%, cocos nucifera oil acyl both sexes base second
Sour sodium 2%-6%, cocamido propyl betaine 1%-5%, lauryl heteroside 1%-5%, olive oil PEG-7 esters
0.2%-0.7%, Fructus Pruni pseudocerasi berry extract 1%-3%, Radix Ophiopogoniss flower extract 0.5%-1.5%, Flos Inulae extract 0.5%-
1.5%th, golden yellow camomile extract 0.5%-1.5%, glycerol 0.5%-1.5%, Sodium Chloride 0.5%-1.5%, citric acid
0.1%-0.4%, essence 0.2%-0.7%, EDETATE SODIUM 0.02%-0.07%, Methylisothiazolinone 0.0012%-
0.0017%th, coloring agent 0.0005%-0.OOO9%.
The bath gel with senile-resistant efficacy of above-mentioned offer, its senile-resistant efficacy composition addition are more, and price is high
Expensive, dendrobium candidum solution extracts from Herba Dendrobii, and the price of Herba Dendrobii is sufficiently expensive, and other raw materials such as Fructus Pruni pseudocerasi is extracted
The price of thing, Radix Ophiopogoniss flower extract, golden yellow camomile extract etc. is also of a relatively high, these can increase cosmetics it is overall into
This, its selling price also can be of a relatively high.Therefore, one kind is searched out with good senile-resistant efficacy but low-cost raw material is
Urgent problem.
The content of the invention
The invention provides it is a kind of with good senile-resistant efficacy, the low-cost natural of cosmetics can be prepared into
Plant material, solves good but expensive existing anti-aging cosmetics effect or low price but effect is undesirable asks
Topic, specific technical scheme are as follows：
The invention provides application of the Semen Psophocarpi tetragonolobi polysaccharide in anti-aging cosmetics are prepared, wherein, the system of Semen Psophocarpi tetragonolobi polysaccharide
Preparation Method comprises the steps：
(1) Semen Psophocarpi tetragonolobi is cleaned up, and microwave drying is to constant weight；
(2) dried Semen Psophocarpi tetragonolobi is crushed to into 20-30 mesh；
(3) deionized water is added in the Semen Psophocarpi tetragonolobi powder toward after crushing, solid-liquid ratio is 1：10-15, ultrasonic extraction
40min, extracts once；
(4) centrifugation goes out supernatant, and be evaporated to original volume 1/10 is stand-by；
(5) amylase is weighed, deionized water is added, dissolving is complete, is configured to amylase solution；
(6) amylase solution is added to into the extracting solution in step (4) after concentration, is stirred, adjust solution PH；
(7) heating in water bath, keeps solution temperature, digests 4-6h；
(8) after digesting, temperature is increased to 75 DEG C, enzyme denaturing 10min；
(9) centrifugation goes out supernatant；
(10) deproteination matter, is concentrated into the 1/10 of original volume, obtains Semen Psophocarpi tetragonolobi polysaccharide extraction liquid.
Semen Psophocarpi tetragonolobi (scientific name：Psophocarpus tetragonolobus (L.) DC.) in containing abundant polysaccharide thing
Matter, containing various saccharides material, such as sucrose, maltose, cotton in above-mentioned steps extract the Semen Psophocarpi tetragonolobi polysaccharide extraction liquid for obtaining
Seed sugar, verbascose etc. and some other oligosaccharide, with good senile-resistant efficacy, can be used for the system of anti-aging cosmetics
In standby.Semen Psophocarpi tetragonolobi polysaccharide extraction liquid is added in cosmetics, can form one layer of hydration shell in skin surface, prevent moisture of skin
It is lost in, and also there is water sorption, cuticular moisture can be kept, xerosis cutiss are prevented；Freedom that can be unnecessary in scavenger cell
Base, prevents the hydrolysis of tissue elasticity albumen and collagen protein, maintains the elasticity of skin；Amino in intercellular substance substrate can be prevented
The decomposition of polysaccharide component, delay skin aging.In addition, Semen Psophocarpi tetragonolobi polysaccharide extraction liquid has certain viscosity, can increase
The skin adhesion of skin-moisturizing, skin composition in cosmetic, further prevents the loss of moisture of skin, skin care.
Further, the amylase in the preparation method step (5) is beta amylase.
Further, the beta amylase is bacillus cereuss beta amylase.
Further, in the preparation method step (5), the addition of beta amylase is 10U/g, i.e., add per 1g Semen Psophocarpi tetragonolobis
Enter the enzyme of 10 units.
Further, in the preparation method step (5), the concentration of amylase solution is 5U/mL.
Further, in the preparation method step (6), the PH of solution is 5.0-6.0.
Further, the solution temperature in the preparation method step (7) is 40 DEG C -50 DEG C.
Further, the anti-aging cosmetics are Firm wrinkle removing bath gel.
Present invention also offers a kind of Firm wrinkle removing bath gel, including the raw material of following weight percentage ratio：Semen Psophocarpi tetragonolobi polysaccharide
0.3%-0.6%, laureth sulfuric ester ammonium 8%-10%, sodium cocoamphoacetate 4%-5%, Laurel alcohol sulfuric ester
Ammonium 3%-4%, cocamido propyl betaine 2.5%-3.5%, PEG-7 glyceryl cocoate 0.8%-1.2%, PEG-160
Three isostearate 0.08%-0.1%, PEG-120 methyl dioleate 0.08%-0.1%, EDTA bis- of anhydrous sorbitol
Sodium 0.08%-0.1%, DMDM Hydantoin 0.2%-0.3%, oligofructose 0.1%-0.15%, citric acid 0.25%-
0.35%th, deionized water surplus.
Further, the Firm wrinkle removing bath gel includes the raw material of following weight percentage ratio：Semen Psophocarpi tetragonolobi polysaccharide 0.5%,
Laureth sulfuric ester ammonium 10%, sodium cocoamphoacetate 5%, Laurel alcohol sulfuric ester ammonium 4%, cocamidopropyl propyl amide are sweet
Dish alkali 3%, PEG-7 glyceryl cocoates 1%, three isostearate 0.1% of PEG-160 anhydrous sorbitols, PEG-120 methyl Portugal
Sugared dioleate 0.1%, EDETATE SODIUM 0.1%, DMDM Hydantoin 0.3%, oligofructose 0.1%, citric acid 0.3%, go
Ion water surplus.
Beneficial effects of the present invention are：The Semen Psophocarpi tetragonolobi Polyose extraction of the present invention is from natural plant material Semen Psophocarpi tetragonolobi, source
Extensively, it is cheap, with good senile-resistant efficacy, can be used for the preparation of cosmetics.Firm wrinkle removing obtained in of the invention is washed one's hair
Bath lotion, can effectively maintain the moisture of skin, prevent xerosis cutiss and accelerate the aging of skin；Free radical can be removed, skin is maintained
Elasticity, delay skin aging；With the addition of tax fat agent PEG-7 glyceryl cocoates so that bath gel is washing away skin surface
Help skin to quickly form new sebum film after the booties such as oils and fatss, dust, hinder the injury of outer bound pair skin；With the addition of oligomeric fruit
Sugar, can suppress growing for antibacterial, it is to avoid skin is encroached on by antibacterial；In formula of bath cream, the addition of active component is few, but anti-
Aging effects are good, and overall cost is not high, meet the level of consumption of general population.
Specific embodiment
In order that those skilled in the art more fully understand technical scheme, with reference to embodiment to this
Bright technical scheme is described in further detail.
Embodiment 1
Take 1000g Semen Psophocarpi tetragonolobis to clean up, microwave drying is to constant weight；Dried Semen Psophocarpi tetragonolobi is crushed to into 20 mesh；Toward powder
Deionized water is added in Semen Psophocarpi tetragonolobi powder after broken, solid-liquid ratio is 1：10, ultrasonic extraction 40min is extracted once；Centrifugation
Go out supernatant, be evaporated to original volume 1/10 is stand-by；Bacillus cereuss beta amylase 10U/g is weighed, deionized water is added, it is molten
Solution is complete, is configured to the amylase solution that concentration is 5U/mL；Amylase solution is added to into the extraction in step (4) after concentration
Liquid, stirs, and adjusts solution PH to 5.0；Heating in water bath, keeps solution temperature in 40 DEG C, digests 4-6h；Temperature liter after enzymolysis
Up to 75 DEG C, enzyme denaturing 10min；Centrifugation goes out supernatant；Sevage methods are combined deproteination matter with enzyme process, are concentrated into original volume
1/10, obtain Semen Psophocarpi tetragonolobi polysaccharide extraction liquid.
Embodiment 2
Take 1000g Semen Psophocarpi tetragonolobis to clean up, microwave drying is to constant weight；Dried Semen Psophocarpi tetragonolobi is crushed to into 28 mesh；Toward powder
Deionized water is added in Semen Psophocarpi tetragonolobi powder after broken, solid-liquid ratio is 1：14, ultrasonic extraction 40min is extracted once；Centrifugation
Go out supernatant, be evaporated to original volume 1/10 is stand-by；Bacillus cereuss beta amylase 10U/g is weighed, deionized water is added, it is molten
Solution is complete, is configured to the amylase solution that concentration is 5U/mL；Amylase solution is added to into the extraction in step (4) after concentration
Liquid, stirs, and adjusts solution PH to 6.0；Heating in water bath, keeps solution temperature in 48 DEG C, digests 4-6h；Temperature liter after enzymolysis
Up to 75 DEG C, enzyme denaturing 10min；Centrifugation goes out supernatant；Sevage methods are combined deproteination matter with enzyme process, are concentrated into original volume
1/10, obtain Semen Psophocarpi tetragonolobi polysaccharide extraction liquid.
Embodiment 3
Take 1000g Semen Psophocarpi tetragonolobis to clean up, microwave drying is to constant weight；Dried Semen Psophocarpi tetragonolobi is crushed to into 24 mesh；Toward powder
Deionized water is added in Semen Psophocarpi tetragonolobi powder after broken, solid-liquid ratio is 1：12, ultrasonic extraction 40min is extracted once；Centrifugation
Go out supernatant, be evaporated to original volume 1/10 is stand-by；Bacillus cereuss beta amylase 10U/g is weighed, deionized water is added, it is molten
Solution is complete, is configured to the amylase solution that concentration is 5U/mL；Amylase solution is added to into the extraction in step (4) after concentration
Liquid, stirs, and adjusts solution PH to 5.3；Heating in water bath, keeps solution temperature in 46 DEG C, digests 4-6h；Temperature liter after enzymolysis
Up to 75 DEG C, enzyme denaturing 10min；Centrifugation goes out supernatant；Sevage methods are combined deproteination matter with enzyme process, are concentrated into original volume
1/10, obtain Semen Psophocarpi tetragonolobi polysaccharide extraction liquid.
Embodiment 4
Take 1000g Semen Psophocarpi tetragonolobis to clean up, microwave drying is to constant weight；Dried Semen Psophocarpi tetragonolobi is crushed to into 30 mesh；Toward powder
Deionized water is added in Semen Psophocarpi tetragonolobi powder after broken, solid-liquid ratio is 1：13, ultrasonic extraction 40min is extracted once；Centrifugation
Go out supernatant, be evaporated to original volume 1/10 is stand-by；Bacillus cereuss beta amylase 10U/g is weighed, deionized water is added, it is molten
Solution is complete, is configured to the amylase solution that concentration is 5U/mL；Amylase solution is added to into the extraction in step (4) after concentration
Liquid, stirs, and adjusts solution PH to 5.6；Heating in water bath, keeps solution temperature in 50 DEG C, digests 4-6h；Temperature liter after enzymolysis
Up to 75 DEG C, enzyme denaturing 10min；Centrifugation goes out supernatant；Sevage methods are combined deproteination matter with enzyme process, are concentrated into original volume
1/10, obtain Semen Psophocarpi tetragonolobi polysaccharide extraction liquid.
Embodiment 5
Take 1000g Semen Psophocarpi tetragonolobis to clean up, microwave drying is to constant weight；Dried Semen Psophocarpi tetragonolobi is crushed to into 24 mesh；Toward powder
Deionized water is added in Semen Psophocarpi tetragonolobi powder after broken, solid-liquid ratio is 1：15, ultrasonic extraction 40min is extracted once；Centrifugation
Go out supernatant, be evaporated to original volume 1/10 is stand-by；Bacillus cereuss beta amylase 10U/g is weighed, deionized water is added, it is molten
Solution is complete, is configured to the amylase solution that concentration is 5U/mL；Amylase solution is added to into the extraction in step (4) after concentration
Liquid, stirs, and adjusts solution PH to 5.8；Heating in water bath, keeps solution temperature in 43 DEG C, digests 4-6h；Temperature liter after enzymolysis
Up to 75 DEG C, enzyme denaturing 10min；Centrifugation goes out supernatant；Sevage methods are combined deproteination matter with enzyme process, are concentrated into original volume
1/10, obtain Semen Psophocarpi tetragonolobi polysaccharide extraction liquid.
Embodiment 6-10
Embodiment 1-5 is extracted the Semen Psophocarpi tetragonolobi polysaccharide extraction liquid for obtaining and is prepared into Firm wrinkle removing bath gel, embodiment 6-10
Extract the Semen Psophocarpi tetragonolobi polysaccharide extraction liquid for obtaining, Firm wrinkle removing formula of bath cream each component and its weight respectively containing embodiment 1-5
Percentage ratio is shown in Table 1.
1 formula of bath cream of table is respectively constituted and its percentage by weight
1 efficacy assessments of test example are tested
Efficacy assessments test is carried out to Firm wrinkle removing bath gel obtained in embodiment 6-10,25-45 year body skin is chosen
Drying, peeling, experimenter wrinkly 350, are randomly divided into 7 groups, and men and women half and half, and experimental group 1-5 uses embodiment 6- respectively
Firm wrinkle removing bath gel obtained in 10, matched group 1 use the commercially available bath gel with defying age, matched group 2 to use blank
Bath gel obtained in group.Using method：Daily proof test sample is taken a shower, and continuous use observes skin after two months
And statistical result.Xerosis cutiss, peeling, the improvement situation of wrinkle are shown in Table 2.
The result of the test of 2 Firm wrinkle removing bath gel of table
Xerosis cutiss improve situation：To no effect=xerosis cutiss, tight feeling do not improve；Slightly=skin is dried a little,
Tight feeling has improvement；Substantially=skin water profit, tight feeling are completely eliminated.
Skin peeling improves situation：To no effect=skin peeling situation does not improve；Slightly=skin peeling amount is reduced, model
Enclose and diminish；Substantially=skin skin effect phenomenon improves completely substantially, and peeling amount is significantly reduced, and scope significantly diminishes.
Wrinkle of skin improves situation：To no effect=wrinkle of skin does not diminish or disappears；Slightly=wrinkle of skin is slight
Improve, wrinkle diminishes, some wrinkles disappear；Substantially=wrinkle of skin substantially diminishes, and most of wrinkle disappears.
The result of comparative example 6-10 and blank control group understands, with the addition of and extract according to preparation method of the present invention
To Semen Psophocarpi tetragonolobi polysaccharide and the Firm wrinkle removing bath gel of the present invention that is prepared into, which is at aspects such as xerosis cutiss, peeling, wrinkles
Improvement does not far superior to add the bath gel of Semen Psophocarpi tetragonolobi polysaccharide, it follows that Semen Psophocarpi tetragonolobi polysaccharide has good skin moistening
Wrinkle removing effect.The result of comparative example 6-10 and commercially available bath gel is understood, is taken a shower using Firm wrinkle removing obtained in the present invention
The problems such as dew, the xerosis cutiss of experimenter, peeling, wrinkle, obtains good improvement, and improvement be substantially better than it is commercially available
Bath gel with wrinkle removing effect, it follows that Firm wrinkle removing bath gel of the present invention has good improvement xerosis cutiss, rises
The effect of the problems such as skin, wrinkle.
There is not any untoward reaction using the experimenter of Firm wrinkle removing bath gel excessively of the invention, therefore, this
The bright obtained Firm wrinkle removing bath gel containing Semen Psophocarpi tetragonolobi polysaccharide is safe and non-stimulating.
Embodiment described above only expresses the several embodiments of the present invention, and its description is more concrete and detailed, but and
Therefore the restriction to the scope of the claims of the present invention can not be interpreted as.It should be pointed out that for one of ordinary skill in the art
For, without departing from the inventive concept of the premise, some deformations and improvement can also be made, these belong to the guarantor of the present invention
Shield scope.Therefore, the protection domain of patent of the present invention should be defined by claims.
Claims (10)
1. application of the Semen Psophocarpi tetragonolobi polysaccharide in anti-aging cosmetics are prepared, it is characterised in that the preparation side of the Semen Psophocarpi tetragonolobi polysaccharide
Method comprises the steps：
(1) Semen Psophocarpi tetragonolobi is cleaned up, and microwave drying is to constant weight；
(2) dried Semen Psophocarpi tetragonolobi is crushed to into 20-30 mesh；
(3) deionized water is added in the Semen Psophocarpi tetragonolobi powder toward after crushing, solid-liquid ratio is 1：10-15, ultrasonic extraction 40min are carried
Take once；
(4) centrifugation goes out supernatant, and be evaporated to original volume 1/10 is stand-by；
(5) amylase is weighed, deionized water is added, dissolving is complete, is configured to amylase solution；
(6) amylase solution is added to into the extracting solution in step (4) after concentration, is stirred, adjust solution PH；
(7) heating in water bath, keeps solution temperature, digests 4-6h；
(8) after digesting, temperature is increased to 75 DEG C, enzyme denaturing 10min；
(9) centrifugation goes out supernatant；
(10) deproteination matter, is concentrated into the 1/10 of original volume, obtains Semen Psophocarpi tetragonolobi polysaccharide extraction liquid.
2. preparation method according to claim 1, it is characterised in that the amylase in the preparation method step (5) is
Beta amylase.
3. amylase according to claim 2, it is characterised in that the beta amylase is bacillus cereuss beta amylase.
4. preparation method according to claim 1, it is characterised in that beta amylase in the preparation method step (5)
Addition is 10U/g, i.e., the enzyme of 10 units is added per 1g Semen Psophocarpi tetragonolobis.
5. preparation method according to claim 1, it is characterised in that amylase solution in the preparation method step (5)
Concentration be 5U/mL.
6. preparation method according to claim 1, it is characterised in that the PH of solution is in the preparation method step (6)
5.0-6.0。
7. preparation method according to claim 1, it is characterised in that the solution temperature in the preparation method step (7)
For 40 DEG C -50 DEG C.
8. application of the Semen Psophocarpi tetragonolobi polysaccharide according to claim 1 in anti-aging cosmetics are prepared, it is characterised in that described
Anti-aging cosmetics are Firm wrinkle removing bath gel.
9. Firm wrinkle removing bath gel according to claim 8, it is characterised in that including the raw material of following weight percentage ratio：
Semen Psophocarpi tetragonolobi polysaccharide 0.3%-0.6%, laureth sulfuric ester ammonium 8%-10%, sodium cocoamphoacetate 4%-5%, the moon
Cinnamic alcohol sulfuric ester ammonium 3%-4%, cocamido propyl betaine 2.5%-3.5%, PEG-7 glyceryl cocoate 0.8%-
1.2%th, three isostearate 0.08%-0.1%, PEG-120 methyl dioleate of PEG-160 anhydrous sorbitols
0.08%-0.1%, EDETATE SODIUM 0.08%-0.1%, DMDM Hydantoin 0.2%-0.3%, oligofructose 0.1%-
0.15%th, citric acid 0.25%-0.35%, deionized water surplus.
10. Firm wrinkle removing bath gel according to claim 9, it is characterised in that including the raw material of following weight percentage ratio：
Semen Psophocarpi tetragonolobi polysaccharide 0.5%, laureth sulfuric ester ammonium 10%, sodium cocoamphoacetate 5%, Laurel alcohol sulfuric ester ammonium
4%th, cocamido propyl betaine 3%, PEG-7 glyceryl cocoates 1%, three isostearate of PEG-160 anhydrous sorbitols
0.1%th, PEG-120 methyls dioleate 0.1%, EDETATE SODIUM 0.1%, DMDM Hydantoin 0.3%, oligofructose
0.1%th, citric acid 0.3%, deionized water surplus.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201611128221.2A CN106511174A (en) | 2016-12-09 | 2016-12-09 | Preparation method of psophocarpus tetragonolobus polysaccharides and application of psophocarpus tetragonolobus polysaccharides in preparation of anti-aging cosmetics |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201611128221.2A CN106511174A (en) | 2016-12-09 | 2016-12-09 | Preparation method of psophocarpus tetragonolobus polysaccharides and application of psophocarpus tetragonolobus polysaccharides in preparation of anti-aging cosmetics |
Publications (1)
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| CN100508943C (en) * | 2001-08-21 | 2009-07-08 | 株式会社资生堂 | Substance capable of potentiating laminin 5 productivity in epidermal cells and utilization thereof |
| CN105963218A (en) * | 2016-07-11 | 2016-09-28 | 广州丹奇日用化工厂有限公司 | Shower gel containing brassica extract |
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| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN100508943C (en) * | 2001-08-21 | 2009-07-08 | 株式会社资生堂 | Substance capable of potentiating laminin 5 productivity in epidermal cells and utilization thereof |
| CN105963218A (en) * | 2016-07-11 | 2016-09-28 | 广州丹奇日用化工厂有限公司 | Shower gel containing brassica extract |
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| 邹国林等: "四棱豆与大豆的营养成份分析", 《中国油料》 * |
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