CN106497229A - A kind of quick-dry type heat sublimation ink - Google Patents
A kind of quick-dry type heat sublimation ink Download PDFInfo
- Publication number
- CN106497229A CN106497229A CN201610991032.1A CN201610991032A CN106497229A CN 106497229 A CN106497229 A CN 106497229A CN 201610991032 A CN201610991032 A CN 201610991032A CN 106497229 A CN106497229 A CN 106497229A
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- parts
- heat sublimation
- sublimation ink
- quick
- preservative
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Classifications
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- C—CHEMISTRY; METALLURGY
- C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
- C09D—COATING COMPOSITIONS, e.g. PAINTS, VARNISHES OR LACQUERS; FILLING PASTES; CHEMICAL PAINT OR INK REMOVERS; INKS; CORRECTING FLUIDS; WOODSTAINS; PASTES OR SOLIDS FOR COLOURING OR PRINTING; USE OF MATERIALS THEREFOR
- C09D11/00—Inks
- C09D11/30—Inkjet printing inks
-
- C—CHEMISTRY; METALLURGY
- C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
- C09D—COATING COMPOSITIONS, e.g. PAINTS, VARNISHES OR LACQUERS; FILLING PASTES; CHEMICAL PAINT OR INK REMOVERS; INKS; CORRECTING FLUIDS; WOODSTAINS; PASTES OR SOLIDS FOR COLOURING OR PRINTING; USE OF MATERIALS THEREFOR
- C09D11/00—Inks
- C09D11/30—Inkjet printing inks
- C09D11/32—Inkjet printing inks characterised by colouring agents
- C09D11/328—Inkjet printing inks characterised by colouring agents characterised by dyes
-
- C—CHEMISTRY; METALLURGY
- C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
- C09D—COATING COMPOSITIONS, e.g. PAINTS, VARNISHES OR LACQUERS; FILLING PASTES; CHEMICAL PAINT OR INK REMOVERS; INKS; CORRECTING FLUIDS; WOODSTAINS; PASTES OR SOLIDS FOR COLOURING OR PRINTING; USE OF MATERIALS THEREFOR
- C09D11/00—Inks
- C09D11/30—Inkjet printing inks
- C09D11/38—Inkjet printing inks characterised by non-macromolecular additives other than solvents, pigments or dyes
Abstract
The invention discloses a kind of quick-dry type heat sublimation ink, including 20 50 parts of disperse dyes, 3 10 parts of PH regulators, 4 10 parts of surfactant, 10 20 parts of sodium lignin sulfonate, 28 parts of antibacterial, 27 parts of preservative, 10 22 parts of carboxymethyl cellulose, 4 12 parts of styrene acrylic resin, 10 15 parts of barium sulfate, 10 20 parts of aluminium oxide, 38 parts of 8 17 parts of Titanium Dioxide and polyvinyl alcohol, preparation process is simple of the present invention, preparation process is environment friendly and pollution-free, prepared heat sublimation ink has good fluency and stability, and drying efficiency is fast, there is sterilization simultaneously, antisepsises, the storage time of ink-jet products can be extended.
Description
Technical field
The present invention relates to heat sublimation ink preparing technical field, specially a kind of quick-dry type heat sublimation ink.
Background technology
Heat sublimation ink (also known as thermal transfer ink) is exactly that the disperse dyes of easily distillation are fabricated to digital printing low energy
Ink, is printed upon on transfer paper, by heating, can be within the most short time by image making to exquisite porcelain, metal, very
In the materials such as silk, chemical fiber fabric, the market demand of individualized development and the requirement of environmental protection is especially suitable for.Heat sublimation ink is mostly
Prepared by the disperse dyes of weaving.Disperse dyes are due to color and the good weatherability of its saturation, so printing in weaving
Catch and have a wide range of applications, remain one of primary raw material of printing and dyeing industry so far.Traditional fabrics printing and dyeing industry
There is serious problem of environmental pollution during using dispersion pigment dyeing, and be not suitable for the production of small lot.Existing
Heat sublimation ink complicated process of preparation, and stability is poor, the rate of transform is low, drying efficiency is low, strong influence production efficiency.
Content of the invention
It is an object of the invention to provide a kind of quick-dry type heat sublimation ink, with asking for solving to propose in above-mentioned background technology
Topic.
For achieving the above object, the present invention provides following technical scheme：A kind of quick-dry type heat sublimation ink, including dispersion dye
Material 20-50 parts, PH regulator 3-10 parts, surfactant 4-10 parts, sodium lignin sulfonate 10-20 parts, antibacterial 2-8 parts, anti-
Rotten agent 2-7 parts, carboxymethyl cellulose 10-22 parts, styrene acrylic resin 4-12 parts, barium sulfate 10-15 parts, aluminium oxide 10-
20 parts, Titanium Dioxide 8-17 part and polyvinyl alcohol 3-8 parts.
Preferably, the preservative is made up of 60% sodium benzoate, 40% Potassium Benzoate.
Preferably, the corrosion inhibiter is made up of 30% water solublity mercapto benzothiazole and the mixing of 70% TTA.
Preferably, preferred composition proportion is：35 parts of disperse dyes, 6 parts of PH regulators, 7 parts of surfactant, lignin
15 parts of sodium sulfonate, 5 parts of antibacterial, 5 parts of preservative, 16 parts of carboxymethyl cellulose, 8 parts of styrene acrylic resin, barium sulfate 12
Part, 15 parts of aluminium oxide, 13 parts of Titanium Dioxide and 5 parts of polyvinyl alcohol.
Preferably, its preparation method is comprised the following steps：
A, will disperse dyes, barium sulfate, aluminium oxide, Titanium Dioxide mixing after be ground, milling time is 4h, obtains mixture
A；
B, in mixture A add face activating agent, sodium lignin sulfonate, antibacterial, preservative, carboxymethyl cellulose, styrene
Acrylic resin and polyvinyl alcohol, add in blender after mixing and stir, and blender rotating speed is 4000 revs/min, mixing time
For 15min, mixture B is obtained；
C, will in mixture B add PH regulators, stand 2h after, use 0.3u membrane filtrations, that is, obtain heat sublimation ink.
Compared with prior art, the invention has the beneficial effects as follows：
（1）Preparation process is simple of the present invention, preparation process are environment friendly and pollution-free, prepared heat sublimation ink have good fluency and
Stability, while having sterilization, antisepsises, can extend the storage time of ink-jet products.
（2）Styrene acrylic resin and polyvinyl alcohol is added with the present invention, it is possible to increase the levelability of ink, prevent
Only shower nozzle is blocked in transfer process ink inside, improve transfer quality.
（3）Barium sulfate, aluminium oxide is also added with the present invention, it is possible to increase the drying efficiency of ink, further increase
Transfer quality.
Specific embodiment
Below to the embodiment of the present invention in technical scheme be clearly and completely described, it is clear that described embodiment
Only a part of embodiment of the invention, rather than whole embodiments.Embodiment in based on the present invention, the common skill in this area
The every other embodiment obtained under the premise of creative work is not made by art personnel, belongs to the model of present invention protection
Enclose.
The present invention provides a kind of technical scheme：A kind of quick-dry type heat sublimation ink, adjusts including disperse dyes 20-50 parts, PH
Section agent 3-10 parts, surfactant 4-10 parts, sodium lignin sulfonate 10-20 parts, antibacterial 2-8 parts, preservative 2-7 parts, carboxylic first
Base cellulose 10-22 parts, styrene acrylic resin 4-12 parts, barium sulfate 10-15 parts, aluminium oxide 10-20 parts, Titanium Dioxide 8-
17 parts and polyvinyl alcohol 3-8 parts.
Embodiment one：
The composition proportion for adopting for：Including 20 parts of disperse dyes, 3 parts of PH regulators, 4 parts of surfactant, sodium lignin sulfonate
10 parts, 2 parts of antibacterial, 2 parts of preservative, 10 parts of carboxymethyl cellulose, 4 parts of styrene acrylic resin, 10 parts of barium sulfate, oxidation
3 parts of 10 parts of aluminum, 8 parts of Titanium Dioxide and polyvinyl alcohol.
In the present embodiment, preservative is made up of 60% sodium benzoate, 40% Potassium Benzoate.
In the present embodiment, corrosion inhibiter is made up of 30% water solublity mercapto benzothiazole and the mixing of 70% TTA.
The preparation method of the present embodiment is comprised the following steps：
A, will disperse dyes, barium sulfate, aluminium oxide, Titanium Dioxide mixing after be ground, milling time is 4h, obtains mixture
A；
B, in mixture A add face activating agent, sodium lignin sulfonate, antibacterial, preservative, carboxymethyl cellulose, styrene
Acrylic resin and polyvinyl alcohol, add in blender after mixing and stir, and blender rotating speed is 4000 revs/min, mixing time
For 15min, mixture B is obtained；
C, will in mixture B add PH regulators, stand 2h after, use 0.3u membrane filtrations, that is, obtain heat sublimation ink.
Embodiment two：
The composition proportion for adopting for：50 parts of disperse dyes, 10 parts of PH regulators, 10 parts of surfactant, sodium lignin sulfonate 20
Part, 8 parts of antibacterial, 7 parts of preservative, 22 parts of carboxymethyl cellulose, 12 parts of styrene acrylic resin, 15 parts of barium sulfate, oxidation
8 parts of 20 parts of aluminum, 17 parts of Titanium Dioxide and polyvinyl alcohol.
In the present embodiment, preservative is made up of 60% sodium benzoate, 40% Potassium Benzoate.
In the present embodiment, corrosion inhibiter is made up of 30% water solublity mercapto benzothiazole and the mixing of 70% TTA.
The preparation method of the present embodiment is comprised the following steps：
A, will disperse dyes, barium sulfate, aluminium oxide, Titanium Dioxide mixing after be ground, milling time is 4h, obtains mixture
A；
B, in mixture A add face activating agent, sodium lignin sulfonate, antibacterial, preservative, carboxymethyl cellulose, styrene
Acrylic resin and polyvinyl alcohol, add in blender after mixing and stir, and blender rotating speed is 4000 revs/min, mixing time
For 15min, mixture B is obtained；
C, will in mixture B add PH regulators, stand 2h after, use 0.3u membrane filtrations, that is, obtain heat sublimation ink.
Embodiment three：
The composition proportion for adopting for：25 parts of disperse dyes, 4 parts of PH regulators, 5 parts of surfactant, 12 parts of sodium lignin sulfonate,
3 parts of antibacterial, 3 parts of preservative, 12 parts of carboxymethyl cellulose, 5 parts of styrene acrylic resin, 11 parts of barium sulfate, aluminium oxide 12
4 parts of part, 9 parts of Titanium Dioxide and polyvinyl alcohol.
In the present embodiment, preservative is made up of 60% sodium benzoate, 40% Potassium Benzoate.
In the present embodiment, corrosion inhibiter is made up of 30% water solublity mercapto benzothiazole and the mixing of 70% TTA.
The preparation method of the present embodiment is comprised the following steps：
A, will disperse dyes, barium sulfate, aluminium oxide, Titanium Dioxide mixing after be ground, milling time is 4h, obtains mixture
A；
B, in mixture A add face activating agent, sodium lignin sulfonate, antibacterial, preservative, carboxymethyl cellulose, styrene
Acrylic resin and polyvinyl alcohol, add in blender after mixing and stir, and blender rotating speed is 4000 revs/min, mixing time
For 15min, mixture B is obtained；
C, will in mixture B add PH regulators, stand 2h after, use 0.3u membrane filtrations, that is, obtain heat sublimation ink.
Example IV：
The composition proportion for adopting for：45 parts of disperse dyes, 8 parts of PH regulators, 8 parts of surfactant, 18 parts of sodium lignin sulfonate,
7 parts of antibacterial, 6 parts of preservative, 20 parts of carboxymethyl cellulose, 10 parts of styrene acrylic resin, 14 parts of barium sulfate, aluminium oxide 18
7 parts of part, 15 parts of Titanium Dioxide and polyvinyl alcohol.
In the present embodiment, preservative is made up of 60% sodium benzoate, 40% Potassium Benzoate.
In the present embodiment, corrosion inhibiter is made up of 30% water solublity mercapto benzothiazole and the mixing of 70% TTA.
The preparation method of the present embodiment is comprised the following steps：
A, will disperse dyes, barium sulfate, aluminium oxide, Titanium Dioxide mixing after be ground, milling time is 4h, obtains mixture
A；
B, in mixture A add face activating agent, sodium lignin sulfonate, antibacterial, preservative, carboxymethyl cellulose, styrene
Acrylic resin and polyvinyl alcohol, add in blender after mixing and stir, and blender rotating speed is 4000 revs/min, mixing time
For 15min, mixture B is obtained；
C, will in mixture B add PH regulators, stand 2h after, use 0.3u membrane filtrations, that is, obtain heat sublimation ink.
Embodiment five：
The composition proportion for adopting for：35 parts of disperse dyes, 6 parts of PH regulators, 7 parts of surfactant, 15 parts of sodium lignin sulfonate,
5 parts of antibacterial, 5 parts of preservative, 16 parts of carboxymethyl cellulose, 8 parts of styrene acrylic resin, 12 parts of barium sulfate, aluminium oxide 15
5 parts of part, 13 parts of Titanium Dioxide and polyvinyl alcohol.
In the present embodiment, preservative is made up of 60% sodium benzoate, 40% Potassium Benzoate.
In the present embodiment, corrosion inhibiter is made up of 30% water solublity mercapto benzothiazole and the mixing of 70% TTA.
The preparation method of the present embodiment is comprised the following steps：
A, will disperse dyes, barium sulfate, aluminium oxide, Titanium Dioxide mixing after be ground, milling time is 4h, obtains mixture
A；
B, in mixture A add face activating agent, sodium lignin sulfonate, antibacterial, preservative, carboxymethyl cellulose, styrene
Acrylic resin and polyvinyl alcohol, add in blender after mixing and stir, and blender rotating speed is 4000 revs/min, mixing time
For 15min, mixture B is obtained；
C, will in mixture B add PH regulators, stand 2h after, use 0.3u membrane filtrations, that is, obtain heat sublimation ink.
Experimental example：
Common heat sublimation ink and various embodiments of the present invention are obtained heat sublimation ink carries out viscosity and Tensiometry Test, obtains
Data such as following table：
| Viscosity（mpa.s） | Surface tension (mN/m) | |
| Common heat sublimation ink | 4.8 | 55 |
| Embodiment one | 2.3 | 22 |
| Embodiment two | 2.3 | 21 |
| Embodiment three | 2.2 | 21 |
| Example IV | 2.1 | 23 |
| Embodiment five | 1.8 | 18 |
From above table data, the heat sublimation ink that embodiment five is obtained can reach optimum efficiency.
Preparation process is simple of the present invention, preparation process are environment friendly and pollution-free, and prepared heat sublimation ink has good fluency
And stability, while having sterilization, antisepsises, the storage time of ink-jet products can be extended；Benzene second is added with the present invention
Alkene acrylic resin and polyvinyl alcohol, it is possible to increase the levelability of ink, prevent from blocking shower nozzle in transfer process ink inside, carry
High transfer quality；Barium sulfate, aluminium oxide is also added with the present invention, it is possible to increase the drying efficiency of ink, further improve
Transfer quality.
Although an embodiment of the present invention has been shown and described, for the ordinary skill in the art, can be with
Understanding can carry out multiple changes, modification, replacement to these embodiments without departing from the principles and spirit of the present invention
And modification, the scope of the present invention be defined by the appended.
Claims (5)
1. a kind of quick-dry type heat sublimation ink, it is characterised in that：Including disperse dyes 20-50 parts, PH regulator 3-10 parts, surface
Activating agent 4-10 parts, sodium lignin sulfonate 10-20 parts, antibacterial 2-8 parts, preservative 2-7 parts, carboxymethyl cellulose 10-22 parts,
Styrene acrylic resin 4-12 parts, barium sulfate 10-15 parts, aluminium oxide 10-20 parts, Titanium Dioxide 8-17 part and polyvinyl alcohol
3-8 parts.
2. a kind of quick-dry type heat sublimation ink according to claim 1, it is characterised in that：The preservative is by 60% benzene first
Sour sodium, 40% Potassium Benzoate composition.
3. a kind of quick-dry type heat sublimation ink according to claim 1, it is characterised in that：The corrosion inhibiter is water-soluble by 30%
Property mercapto benzothiazole and 70% TTA mixing composition.
4. a kind of quick-dry type heat sublimation ink according to claim 1, it is characterised in that：Preferred composition proportion is：Point
35 parts of scattered dyestuff, 6 parts of PH regulators, 7 parts of surfactant, 15 parts of sodium lignin sulfonate, 5 parts of antibacterial, 5 parts of preservative, carboxylic
16 parts of methylcellulose, 8 parts of styrene acrylic resin, 12 parts of barium sulfate, 15 parts of aluminium oxide, 13 parts of Titanium Dioxide and poly- second
5 parts of enol.
5. a kind of preparation method of the quick-dry type heat sublimation ink described in claim 1 is realized, it is characterised in that：Its preparation method
Comprise the following steps：
A, will disperse dyes, barium sulfate, aluminium oxide, Titanium Dioxide mixing after be ground, milling time is 4h, obtains mixture
A；
B, in mixture A add face activating agent, sodium lignin sulfonate, antibacterial, preservative, carboxymethyl cellulose, styrene
Acrylic resin and polyvinyl alcohol, add in blender after mixing and stir, and blender rotating speed is 4000 revs/min, mixing time
For 15min, mixture B is obtained；
C, will in mixture B add PH regulators, stand 2h after, use 0.3u membrane filtrations, that is, obtain heat sublimation ink.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201610991032.1A CN106497229A (en) | 2016-11-11 | 2016-11-11 | A kind of quick-dry type heat sublimation ink |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201610991032.1A CN106497229A (en) | 2016-11-11 | 2016-11-11 | A kind of quick-dry type heat sublimation ink |
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| Publication Number | Publication Date |
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| CN106497229A true CN106497229A (en) | 2017-03-15 |
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| Application Number | Title | Priority Date | Filing Date |
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| CN201610991032.1A Pending CN106497229A (en) | 2016-11-11 | 2016-11-11 | A kind of quick-dry type heat sublimation ink |
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Cited By (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN107722806A (en) * | 2017-09-29 | 2018-02-23 | 江苏闽江矿业有限公司 | A kind of preparation method of water-repellent paint for mining industry disintegrating machine |
| CN109403071A (en) * | 2018-09-17 | 2019-03-01 | 苏州印丝特数码科技有限公司 | A kind of preparation method of the heterochromatic digit printing spunlace non-woven cloth of Multifunctional two-sided |
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| Publication number | Priority date | Publication date | Assignee | Title |
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| CN102585589A (en) * | 2012-03-07 | 2012-07-18 | 深圳市墨库图文技术有限公司 | Thermal sublimation ink as well as direct printing technology and equipment |
| US20130197144A1 (en) * | 2012-01-31 | 2013-08-01 | Keita Katoh | Inkjet ink and ink cartridge |
-
2016
- 2016-11-11 CN CN201610991032.1A patent/CN106497229A/en active Pending
Patent Citations (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US20130197144A1 (en) * | 2012-01-31 | 2013-08-01 | Keita Katoh | Inkjet ink and ink cartridge |
| CN102585589A (en) * | 2012-03-07 | 2012-07-18 | 深圳市墨库图文技术有限公司 | Thermal sublimation ink as well as direct printing technology and equipment |
Non-Patent Citations (2)
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| 徐清海等: "《有机化学实验与习题》", 31 March 2001, 中国农业出版社 * |
Cited By (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN107722806A (en) * | 2017-09-29 | 2018-02-23 | 江苏闽江矿业有限公司 | A kind of preparation method of water-repellent paint for mining industry disintegrating machine |
| CN109403071A (en) * | 2018-09-17 | 2019-03-01 | 苏州印丝特数码科技有限公司 | A kind of preparation method of the heterochromatic digit printing spunlace non-woven cloth of Multifunctional two-sided |
| CN109403071B (en) * | 2018-09-17 | 2021-07-16 | 苏州印丝特数码科技有限公司 | Preparation method of multifunctional double-sided heterochromatic digital printing spunlace non-woven fabric |
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Application publication date: 20170315 |