CN106492257A - A kind of double-deck volatile-type liquid air freshener and preparation method thereof - Google Patents
A kind of double-deck volatile-type liquid air freshener and preparation method thereof Download PDFInfo
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- CN106492257A CN106492257A CN201611256349.7A CN201611256349A CN106492257A CN 106492257 A CN106492257 A CN 106492257A CN 201611256349 A CN201611256349 A CN 201611256349A CN 106492257 A CN106492257 A CN 106492257A
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- double
- air freshener
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61L—METHODS OR APPARATUS FOR STERILISING MATERIALS OR OBJECTS IN GENERAL; DISINFECTION, STERILISATION OR DEODORISATION OF AIR; CHEMICAL ASPECTS OF BANDAGES, DRESSINGS, ABSORBENT PADS OR SURGICAL ARTICLES; MATERIALS FOR BANDAGES, DRESSINGS, ABSORBENT PADS OR SURGICAL ARTICLES
- A61L9/00—Disinfection, sterilisation or deodorisation of air
- A61L9/015—Disinfection, sterilisation or deodorisation of air using gaseous or vaporous substances, e.g. ozone
- A61L9/04—Disinfection, sterilisation or deodorisation of air using gaseous or vaporous substances, e.g. ozone using substances evaporated in the air without heating
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61L—METHODS OR APPARATUS FOR STERILISING MATERIALS OR OBJECTS IN GENERAL; DISINFECTION, STERILISATION OR DEODORISATION OF AIR; CHEMICAL ASPECTS OF BANDAGES, DRESSINGS, ABSORBENT PADS OR SURGICAL ARTICLES; MATERIALS FOR BANDAGES, DRESSINGS, ABSORBENT PADS OR SURGICAL ARTICLES
- A61L9/00—Disinfection, sterilisation or deodorisation of air
- A61L9/01—Deodorant compositions
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61L—METHODS OR APPARATUS FOR STERILISING MATERIALS OR OBJECTS IN GENERAL; DISINFECTION, STERILISATION OR DEODORISATION OF AIR; CHEMICAL ASPECTS OF BANDAGES, DRESSINGS, ABSORBENT PADS OR SURGICAL ARTICLES; MATERIALS FOR BANDAGES, DRESSINGS, ABSORBENT PADS OR SURGICAL ARTICLES
- A61L2209/00—Aspects relating to disinfection, sterilisation or deodorisation of air
- A61L2209/20—Method-related aspects
- A61L2209/21—Use of chemical compounds for treating air or the like
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- Health & Medical Sciences (AREA)
- Epidemiology (AREA)
- Life Sciences & Earth Sciences (AREA)
- Animal Behavior & Ethology (AREA)
- General Health & Medical Sciences (AREA)
- Public Health (AREA)
- Veterinary Medicine (AREA)
- Disinfection, Sterilisation Or Deodorisation Of Air (AREA)
- Fats And Perfumes (AREA)
Abstract
The invention discloses a kind of double-deck volatile-type liquid air freshener, including following weight percent composition：Isoparaffin 30%～50%, diethylene glycol ether 1%～10%, ethanol 30%～50%, essence 1%～10%.The invention also discloses the preparation method of the double-deck volatile-type liquid air freshener.The double-deck volatilization liquid volume ratio of two-layer up and down in use obtained by the present invention can be maintained in the range of (0.9～1.1) ± 0.2, biphase remain incompatible, and the state of continuous uniform volatilization.The invention belongs to air freshener field.
Description
Technical field
The invention belongs to air freshener field, more particularly to a kind of double-deck volatile-type liquid air freshener and its preparation
Method.
Background technology
Current most of on the market volatile liquid air freshener, abbreviation aromatherapy volatile liquid or rattan volatilization liquid, with rattan
Bar is used as the medium for assisting fragrance emissions.All it is single-phase homogeneous transparency liquid.As consumer is for volatilization liquid outward appearance and individual
Property continuous pursuit, minimal air freshener company developed biphase double-deck outward appearance volatilization liquid, but its biphase volatilization
Speed is extremely inconsistent, i.e., when product does not break a seal, the outward appearance of liquid is double-decker respectively, and works as product Kaifeng using simultaneously
During gradually volatilizing, double-decker is progressively destroyed, and becomes single-phase volatilization liquid.Therefore, it is necessary to develop one make
Double-decker and the volatilization formula of liquid at the uniform velocity volatilizing can be also kept with during.
Content of the invention
The invention discloses a kind of double-deck volatile-type liquid air freshener and preparation method thereof, double obtained by the present invention
The layer volatilization liquid volume ratio of two-layer up and down in use can be maintained in the range of (0.9～1.1) ± 0.2, the biphase beginning
Keep incompatible eventually, and the state of continuous uniform volatilization.
In order to realize above-mentioned technique effect, the technical scheme that the present invention is provided is such：A kind of double-deck volatile-type liquid
Air freshener, including following weight percent composition：Isoparaffin 30%～50%, diethylene glycol ether 1%～10%, second
Alcohol 30%～50%, essence 1%～10%.
It should be noted that the upper liquid of described double-deck volatile-type liquid air freshener is isoparaffin, described
The subnatant of double-deck volatile-type liquid air freshener is diethylene glycol ether, and essence is distributed in upper liquid and subnatant.
It should be noted that described isoparaffin is C12-C16 isoparaffins, Exxon Mobil Corporation, model is purchased from
Commodity for Isopar.
A kind of preparation method of double-deck volatile-type liquid air freshener as above, comprises the following steps：
Step 1：Isoparaffin, diethylene glycol ether, ethanol, essence are mixed dispersion；
Step 2：Stand, treat which is gradually layered.
In particular, the preparation method of bilayer volatile-type liquid air freshener as above, comprises the following steps：
Step 1：Isoparaffin, diethylene glycol ether, ethanol, essence are mixed dispersion, mixing speed is 800rpm
～1500rpm, mixing time are 10min～20min；
Step 2：30min～60min is stood, treats which is gradually layered.
The present invention is had the advantage that compared with traditional method：
1. the double-deck volatilization liquid volume ratio of two-layer up and down in use of the present invention can be maintained at (0.9～
1.1) in the range of ± 0.2；
2. biphase remain incompatible, and continuous uniform volatilization state.
Description of the drawings
Fig. 1 is the weight-loss curve figure of the double-deck volatilization liquid obtained by embodiment 1；
Fig. 2 is the weight-loss curve figure of the double-deck volatilization liquid obtained by embodiment 2；
Fig. 3 is the weight-loss curve figure of the double-deck volatilization liquid obtained by embodiment 3；
Fig. 4 is the weight-loss curve figure of the double-deck volatilization liquid obtained by embodiment 4；
Fig. 5 is the weight-loss curve figure of the double-deck volatilization liquid obtained by embodiment 5；
Double-deck volatilization liquid weightlessness ratio ranges figures of the Fig. 6 for embodiment 1-5.
Specific embodiment
Claims of the present invention is described further with reference to specific embodiment, but is not constituted to the present invention's
Any restriction, any the present invention is made limited number of time modification technical scheme still fall within invention which is intended to be protected.
Embodiment 1
Step 1：Following percentage by weights are pressed by C12～C16 isoparaffins 47%, ethanol 33%, diethylene glycol ether
10%, essence 10% mixes；
Step 2：The mixture of step 1 gained is stirred, mixing speed is 800rpm, and mixing time is 20min；
Step 3：30min is stood, treats which is gradually layered.
Obtained in the formula, double-deck volatilization liquid levels are incompatible.
Levels volume ratio when unused be 1.08, in its volatilization process volume ratio 1.08 ± 0.2 scope float
Dynamic, the average external volume ratio in volatilization process is 1.13.
As shown in figure 1, wherein, in figure, Maximum End LIFE are represented the weight-loss curve of the double-deck volatilization liquid of the present embodiment
For maximum service life (MSL), Minimum End Life are expressed as minimum service life, the hatched triangle in figure represent one pre-
If scope, and curve represents the line of the weightless ratio of the actual volatilization measurement of formula, the actual mistake of the double-deck liquid that volatilizees to be measured
As long as the curve of anharmonic ratio rate composition is i.e. qualified in this range.
Embodiment 2
Step 1：Following percentage by weights are pressed by C12～C16 isoparaffins 46%, ethanol 44%, diethylene glycol ether
5%, essence 5% mixes；
Step 2：The mixture of step 1 gained is stirred, mixing speed is 1500rpm, and mixing time is 10min；
Step 3：60min is stood, treats which is gradually layered.
Obtained in the formula, double-deck volatilization liquid levels are incompatible.
Levels volume ratio when unused be 0.94, in its volatilization process volume ratio 0.94 ± 0.2 scope float
Dynamic, the average external volume ratio in volatilization process is 0.96.
As shown in Figure 2 wherein, in figure, Maximum End LIFE are represented the weight-loss curve of the double-deck volatilization liquid of the present embodiment
For maximum service life (MSL), Minimum End Life are expressed as minimum service life, the hatched triangle in figure represent one pre-
If scope, and curve represents the line of the weightless ratio of the actual volatilization measurement of formula, the actual mistake of the double-deck liquid that volatilizees to be measured
As long as the curve of anharmonic ratio rate composition is i.e. qualified in this range.
Embodiment 3
Step 1：Following percentage by weights are pressed by C12～C16 isoparaffins 50%, ethanol 38%, diethylene glycol ether
10%, essence 2% mixes；
Step 2：The mixture of step 1 gained is stirred, mixing speed is 1300rpm, and mixing time is 15min；
Step 3：45min is stood, treats which is gradually layered.
Obtained in the formula, double-deck volatilization liquid levels are incompatible.
Levels volume ratio when unused be 1.04, in its volatilization process volume ratio 1.04 ± 0.2 scope float
Dynamic, the average external volume ratio in volatilization process is 1.14.
The weight-loss curve of the double-deck volatilization liquid of the present embodiment is as shown in figure 3, Maximum End LIFE are expressed as most in figure
Big service life, Minimum End Life are expressed as minimum service life, the hatched triangle in figure represent one default
Scope, and curve represents the line of the weightless ratio of the actual volatilization measurement of formula, the actual weightless ratio of double-deck volatilization liquid to be measured
As long as the curve of rate composition is i.e. qualified in this range.
Embodiment 4
Step 1：Following percentage by weights are pressed by C12～C16 isoparaffins 47%, ethanol 50%, diethylene glycol ether
1%, essence 2% mixes；
Step 2：The mixture of step 1 gained is stirred, mixing speed is 1000rpm, and mixing time is 12min；
Step 3：50min is stood, treats which is gradually layered.
Obtained in the formula, double-deck volatilization liquid levels are incompatible.
Levels volume ratio when unused be 0.92, in its volatilization process volume ratio 0.92 ± 0.2 scope float
Dynamic, the average external volume ratio in volatilization process is 0.92.
The weight-loss curve of the double-deck volatilization liquid of the present embodiment is as shown in figure 4, Maximum End LIFE are expressed as most in figure
Big service life, Minimum End Life are expressed as minimum service life, the hatched triangle in figure represent one default
Scope, and curve represents the line of the weightless ratio of the actual volatilization measurement of formula, the actual weightless ratio of double-deck volatilization liquid to be measured
As long as the curve of rate composition is i.e. qualified in this range.
Embodiment 5
Step 1：Following percentage by weights are pressed by C12～C16 isoparaffins 45%, ethanol 45%, diethylene glycol ether
2%, essence 8% mixes；
Step 2：The mixture of step 1 gained is stirred, mixing speed is 1100rpm, and mixing time is 18min；
Step 3：35min is stood, treats which is gradually layered.
Obtained in the formula, double-deck volatilization liquid levels are incompatible.
Levels volume ratio when unused be 0.96, in its volatilization process volume ratio 0.92 ± 0.2 scope float
Dynamic, the average external volume ratio in volatilization process is 0.93.
The weight-loss curve of the double-deck volatilization liquid of the present embodiment is as shown in figure 5, Maximum End LIFE are expressed as most in figure
Big service life, Minimum End Life are expressed as minimum service life, the hatched triangle in figure represent one default
Scope, and curve represents the line of the weightless ratio of the actual volatilization measurement of formula, the actual weightless ratio of double-deck volatilization liquid to be measured
As long as the curve of rate composition is i.e. qualified in this range.
The rate of volatilization of the double-deck volatilization liquid of embodiment 1-5 is tested：
Double-deck volatilization liquid is made by certain weight (80 grams), the rattan specification rattan of long 24cm (6 diameter 3mm)
Sample be statically placed in certain space that (25 ± 0.5 DEG C of temperature, relative humidity 40%～80%, wind speed about 0.1m/s's are relative
Constant space) in volatilize naturally, the weight of measuring samples is with the evaporation rate for determining sample, weightless ratio at set intervals.
In generally 45～60 days cycle of the experiment, on every Mondays, four example weights are weighed, until its original that evaporated is ponderable
95%, experiment terminates.
Test result is：Evaporation rate scope is 1.33 grams/day～1.78 grams/day, i.e., probably service life is 45～60
My god
Test result is as shown in fig. 6, Maximum End LIFE are expressed as maximum service life (MSL), Minimum End in figure
Life is expressed as minimum service life, and the hatched triangle in figure represents a default scope, and curve represents the reality of formula
The line of the weightless ratio of border volatilization measurement, as long as the curve of the actual weightless ratio composition of double-deck volatilization liquid to be measured is in the scope
In i.e. qualified.
Above-described be only presently preferred embodiments of the present invention, all made in the range of the spirit and principles in the present invention appoint
What modification, equivalent and improvement etc., should be included within the scope of the present invention.
Claims (5)
1. a kind of double-deck volatile-type liquid air freshener, it is characterised in that including following weight percent composition：Isoparaffin
30%～50%, diethylene glycol ether 1%～10%, ethanol 30%～50%, essence 1%～10%.
2. a kind of double-deck volatile-type liquid air freshener according to claim 1, it is characterised in that described bilayer is waved
The upper liquid of hair style liquid air freshener is isoparaffin, and the subnatant of described double-deck volatile-type liquid air freshener is
Diethylene glycol ether, essence are distributed in upper liquid and subnatant.
3. a kind of double-deck volatile-type liquid air freshener according to claim 1, it is characterised in that described isomeric alkane
Hydrocarbon is C12-C16 isoparaffins, is purchased from Exxon Mobil Corporation, the commodity of model Isopar.
4. a kind of preparation method of the double-deck volatile-type liquid air freshener as described in claim 1-3 is arbitrary, its feature exist
In comprising the following steps：
Step 1：Isoparaffin, diethylene glycol ether, ethanol, essence are mixed dispersion；
Step 2：Stand, treat which is gradually layered.
5. the preparation method of double-deck volatile-type liquid air freshener according to claim 4, it is characterised in that include with
Lower step：
Step 1：By isoparaffin, diethylene glycol ether, ethanol, essence mix dispersion, mixing speed be 800rpm～
1500rpm, mixing time are 10min～20min；
Step 2：30min～60min is stood, treats which is gradually layered.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201611256349.7A CN106492257B (en) | 2016-12-30 | 2016-12-30 | Double-layer volatile liquid air freshener and preparation method thereof |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201611256349.7A CN106492257B (en) | 2016-12-30 | 2016-12-30 | Double-layer volatile liquid air freshener and preparation method thereof |
Publications (2)
| Publication Number | Publication Date |
|---|---|
| CN106492257A true CN106492257A (en) | 2017-03-15 |
| CN106492257B CN106492257B (en) | 2020-03-17 |
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| Application Number | Title | Priority Date | Filing Date |
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| CN201611256349.7A Active CN106492257B (en) | 2016-12-30 | 2016-12-30 | Double-layer volatile liquid air freshener and preparation method thereof |
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Cited By (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN107375982A (en) * | 2017-07-17 | 2017-11-24 | 王婧宁 | A kind of air freshener for being applicable northern house |
| CN107397967A (en) * | 2017-07-17 | 2017-11-28 | 王婧宁 | Can effectively solve the air purifying preparation of parking facility air pollutants |
Citations (4)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| JP2006087512A (en) * | 2004-09-21 | 2006-04-06 | T Hasegawa Co Ltd | Composition of aromatic liquid for heating transpiration aromatic liquid composition for heating transpiration |
| CN1961968A (en) * | 2006-11-21 | 2007-05-16 | 上海和黄白猫有限公司 | Deodorant containing natural botanical deodorizing ingredient |
| CN101909662A (en) * | 2008-01-04 | 2010-12-08 | 玛奈·菲尔萨公司 | Transparent anhydrous gel comprising perfume |
| CN104524614A (en) * | 2014-12-10 | 2015-04-22 | 东莞市日友汽车用品有限公司 | Composition with luminous function and preparation method thereof |
-
2016
- 2016-12-30 CN CN201611256349.7A patent/CN106492257B/en active Active
Patent Citations (4)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| JP2006087512A (en) * | 2004-09-21 | 2006-04-06 | T Hasegawa Co Ltd | Composition of aromatic liquid for heating transpiration aromatic liquid composition for heating transpiration |
| CN1961968A (en) * | 2006-11-21 | 2007-05-16 | 上海和黄白猫有限公司 | Deodorant containing natural botanical deodorizing ingredient |
| CN101909662A (en) * | 2008-01-04 | 2010-12-08 | 玛奈·菲尔萨公司 | Transparent anhydrous gel comprising perfume |
| CN104524614A (en) * | 2014-12-10 | 2015-04-22 | 东莞市日友汽车用品有限公司 | Composition with luminous function and preparation method thereof |
Cited By (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN107375982A (en) * | 2017-07-17 | 2017-11-24 | 王婧宁 | A kind of air freshener for being applicable northern house |
| CN107397967A (en) * | 2017-07-17 | 2017-11-28 | 王婧宁 | Can effectively solve the air purifying preparation of parking facility air pollutants |
| CN107375982B (en) * | 2017-07-17 | 2020-07-03 | 王婧宁 | Air freshener suitable for northern houses |
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| Publication number | Publication date |
|---|---|
| CN106492257B (en) | 2020-03-17 |
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Address after: No. 66, Hongjing Road, East District, Guangzhou Economic and Technological Development Zone, Guangzhou, Guangdong 510000 Patentee after: Chi Hua ton flavor and fragrance (Guangzhou) Co.,Ltd. Address before: No. 66, Hongjing Road, East District, Guangzhou Economic and Technological Development Zone, Guangzhou, Guangdong 510000 Patentee before: DROM FRAGRANCES (GUANGZHOU) Co.,Ltd. |