CN106492051A - A kind of spot mold of scorpion control agent and preparation method thereof - Google Patents

A kind of spot mold of scorpion control agent and preparation method thereof Download PDF

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CN106492051A
CN106492051A CN201610953433.8A CN201610953433A CN106492051A CN 106492051 A CN106492051 A CN 106492051A CN 201610953433 A CN201610953433 A CN 201610953433A CN 106492051 A CN106492051 A CN 106492051A
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parts
powder
folium
control agent
acrylic acid
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邢桂生
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TONGLING GUISHENG ECOLOGICAL BREEDING Co Ltd
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TONGLING GUISHENG ECOLOGICAL BREEDING Co Ltd
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    • A—HUMAN NECESSITIES
    • A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K36/00—Medicinal preparations of undetermined constitution containing material from algae, lichens, fungi or plants, or derivatives thereof, e.g. traditional herbal medicines
    • A61K36/18—Magnoliophyta (angiosperms)
    • A61K36/185—Magnoliopsida (dicotyledons)
    • A61K36/46—Eucommiaceae (Eucommia family), e.g. hardy rubber tree
    • A—HUMAN NECESSITIES
    • A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K36/00—Medicinal preparations of undetermined constitution containing material from algae, lichens, fungi or plants, or derivatives thereof, e.g. traditional herbal medicines
    • A61K36/13—Coniferophyta (gymnosperms)
    • A61K36/15—Pinaceae (Pine family), e.g. pine or cedar
    • A—HUMAN NECESSITIES
    • A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K36/00—Medicinal preparations of undetermined constitution containing material from algae, lichens, fungi or plants, or derivatives thereof, e.g. traditional herbal medicines
    • A61K36/18—Magnoliophyta (angiosperms)
    • A61K36/185—Magnoliopsida (dicotyledons)
    • A61K36/53—Lamiaceae or Labiatae (Mint family), e.g. thyme, rosemary or lavender
    • A61K36/535—Perilla (beefsteak plant)
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    • A61K36/00—Medicinal preparations of undetermined constitution containing material from algae, lichens, fungi or plants, or derivatives thereof, e.g. traditional herbal medicines
    • A61K36/18—Magnoliophyta (angiosperms)
    • A61K36/185—Magnoliopsida (dicotyledons)
    • A61K36/73—Rosaceae (Rose family), e.g. strawberry, chokeberry, blackberry, pear or firethorn
    • A61K36/734—Crataegus (hawthorn)
    • A—HUMAN NECESSITIES
    • A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K36/00—Medicinal preparations of undetermined constitution containing material from algae, lichens, fungi or plants, or derivatives thereof, e.g. traditional herbal medicines
    • A61K36/18—Magnoliophyta (angiosperms)
    • A61K36/185—Magnoliopsida (dicotyledons)
    • A61K36/81—Solanaceae (Potato family), e.g. tobacco, nightshade, tomato, belladonna, capsicum or jimsonweed
    • A—HUMAN NECESSITIES
    • A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K36/00—Medicinal preparations of undetermined constitution containing material from algae, lichens, fungi or plants, or derivatives thereof, e.g. traditional herbal medicines
    • A61K36/18—Magnoliophyta (angiosperms)
    • A61K36/185—Magnoliopsida (dicotyledons)
    • A61K36/87—Vitaceae or Ampelidaceae (Vine or Grape family), e.g. wine grapes, muscadine or peppervine
    • A—HUMAN NECESSITIES
    • A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K36/00—Medicinal preparations of undetermined constitution containing material from algae, lichens, fungi or plants, or derivatives thereof, e.g. traditional herbal medicines
    • A61K36/18—Magnoliophyta (angiosperms)
    • A61K36/88—Liliopsida (monocotyledons)
    • A61K36/899—Poaceae or Gramineae (Grass family), e.g. bamboo, corn or sugar cane
    • A—HUMAN NECESSITIES
    • A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K36/00—Medicinal preparations of undetermined constitution containing material from algae, lichens, fungi or plants, or derivatives thereof, e.g. traditional herbal medicines
    • A61K36/18—Magnoliophyta (angiosperms)
    • A61K36/88—Liliopsida (monocotyledons)
    • A61K36/899—Poaceae or Gramineae (Grass family), e.g. bamboo, corn or sugar cane
    • A61K36/8994—Coix (Job's tears)
    • A—HUMAN NECESSITIES
    • A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K47/00—Medicinal preparations characterised by the non-active ingredients used, e.g. carriers or inert additives; Targeting or modifying agents chemically bound to the active ingredient
    • A61K47/02—Inorganic compounds
    • A—HUMAN NECESSITIES
    • A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K47/00—Medicinal preparations characterised by the non-active ingredients used, e.g. carriers or inert additives; Targeting or modifying agents chemically bound to the active ingredient
    • A61K47/06—Organic compounds, e.g. natural or synthetic hydrocarbons, polyolefins, mineral oil, petrolatum or ozokerite
    • A61K47/08—Organic compounds, e.g. natural or synthetic hydrocarbons, polyolefins, mineral oil, petrolatum or ozokerite containing oxygen, e.g. ethers, acetals, ketones, quinones, aldehydes, peroxides
    • A61K47/10—Alcohols; Phenols; Salts thereof, e.g. glycerol; Polyethylene glycols [PEG]; Poloxamers; PEG/POE alkyl ethers
    • A—HUMAN NECESSITIES
    • A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K47/00—Medicinal preparations characterised by the non-active ingredients used, e.g. carriers or inert additives; Targeting or modifying agents chemically bound to the active ingredient
    • A61K47/30—Macromolecular organic or inorganic compounds, e.g. inorganic polyphosphates
    • A61K47/32—Macromolecular compounds obtained by reactions only involving carbon-to-carbon unsaturated bonds, e.g. carbomers, poly(meth)acrylates, or polyvinyl pyrrolidone
    • A—HUMAN NECESSITIES
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    • A61K47/00—Medicinal preparations characterised by the non-active ingredients used, e.g. carriers or inert additives; Targeting or modifying agents chemically bound to the active ingredient
    • A61K47/44—Oils, fats or waxes according to two or more groups of A61K47/02-A61K47/42; Natural or modified natural oils, fats or waxes, e.g. castor oil, polyethoxylated castor oil, montan wax, lignite, shellac, rosin, beeswax or lanolin
    • A—HUMAN NECESSITIES
    • A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K9/00—Medicinal preparations characterised by special physical form
    • A61K9/0002—Galenical forms characterised by the drug release technique; Application systems commanded by energy
    • A—HUMAN NECESSITIES
    • A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K9/00—Medicinal preparations characterised by special physical form
    • A61K9/14—Particulate form, e.g. powders, Processes for size reducing of pure drugs or the resulting products, Pure drug nanoparticles

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  • Health & Medical Sciences (AREA)
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  • Life Sciences & Earth Sciences (AREA)
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Abstract

The invention discloses a kind of spot mold of scorpion control agent and preparation method thereof, is related to scorpion breeding technical field, it is made up of the raw material of following parts by weight：10 15 parts of Folium Eucommiae, 10 15 parts of Folium Perillae, 5 10 parts of Folium Crataegi, 5 10 parts of macropore acidulous acrylic acid's cation exchanger resin, 48 parts of Folium Capsici, 36 parts of grape skin, 36 parts of active hargil, 24 parts of furfural dregs, 24 parts of Semen Coicis rice flour, 24 parts of pine needle powder, 12 parts of vermiculite power, 12 parts of polyethylene glycol oxide, 12 parts of Pollen Maydiss, 12 parts of Bis(pentaerythritol), 0.5 1 parts of haze tallow, 0.5 1 parts of aluminium polychlorid, 0.5 1 parts of sulfated castor oil.The prevention effect of speckle mildew control agent of the present invention is good, and the effect by macropore acidulous acrylic acid's cation exchanger resin, active hargil and vermiculite power reaches drug effect slow release effect.

Description

A kind of spot mold of scorpion control agent and preparation method thereof
Technical field：
The present invention relates to scorpion breeding technical field, and in particular to a kind of spot mold of scorpion control agent and preparation method thereof.
Background technology：
Scorpio is arachnid, typical feature include tall and thin body, sting, bending section and the tail with telson. From the point of view of the developing history of China artificial scorpion breeding, from after 20th century the mid-80s, except a small amount of Scorpio continues to meet Chinese medicine Outside the needs of development, a large amount of Scorpio products are consumed as food and health-care tonic product.For many years, the Scorpio market supply is more Wild seizure is relied on, but with chemical fertilizer, a large amount of uses of pesticide, wild Scorpio ecological environment is destroyed, in order to meet for not The market that should be asked, people start artificial cultivation Scorpio.
Speckle mildew, because habitat is hot and humid, causes funguses parasitic in Scorpio body surface and falls ill.Originally sick scorpion performance is slow-witted Stagnant do not eat, until dead, scorpion corpse often lumpd with corruption feedstuff together mouldy, in vivo full of yellowish-brown or green mustiness mycelium The truffle that assembles.In order to reduce impact of the speckle mildew to Scorpio survival rate, need to prevent and treat speckle mildew in advance, and It is required that used control agent can not affect the normal growth of Scorpio.
Content of the invention：
The technical problem to be solved is to provide a kind of by spraying to be prevented and treated and prevention effect is notable Spot mold of scorpion control agent and preparation method thereof.
The technical problem to be solved is realized using following technical scheme：
A kind of spot mold of scorpion control agent, is made up of the raw material of following parts by weight：
Folium Eucommiae 10-15 parts, Folium Perillae 10-15 parts, Folium Crataegi 5-10 parts, macropore acidulous acrylic acid cation are exchanged Resin 5-10 parts, Folium Capsici 4-8 parts, grape skin 3-6 parts, active hargil 3-6 parts, furfural dregs 2-4 parts, Semen Coicis rice flour 2-4 parts, Pine needle powder 2-4 parts, vermiculite power 1-2 parts, polyethylene glycol oxide 1-2 parts, Pollen Maydiss 1-2 parts, Bis(pentaerythritol) 1-2 parts, haze tallow 0.5-1 parts, aluminium polychlorid 0.5-1 parts, sulfated castor oil 0.5-1 parts.
The macropore acidulous acrylic acid cation exchanger resin is selected from D113 macropore acidulous acrylic acid's cations A kind of or both mixing in exchanger resin, D111 macropore acidulous acrylic acid's cation exchanger resins.
Using front through pretreatment, its processing method is the grape skin：1-2 is added in 15-20 part grape skins Part polyethylene glycol 6000 and 0.5-1 part spermols, are sufficiently mixed rear sealing and standing 15min, are again heated to 50-60 DEG C of insulation mixing 10min, filter pressing, 10-15 DEG C of cold water of gained filtering residue are washed twice, then add in filtering residue 1-2 parts water-soluble chitosan and 0.5-1 part Rhizoma Solani tuber osi Pregelatinized Starch, is sufficiently mixed, and most under microwave frequency 2450MHz, power 700W, microwave treatment 5min is Can.
Grape skin can not only effectively remove the residual pesticide on grape skin, moreover it is possible to strengthen through above-mentioned pretreatment The extraction ratio of its effective ingredient.
A kind of preparation method of spot mold of scorpion control agent, comprises the steps：
(1) Folium Eucommiae, Folium Perillae, Folium Crataegi, Folium Capsici and grape skin are added in 2-3 times of weight portion water, immersion Using defibrination three times repeatedly of power 1.5kW fiberizers after 30min, reflux state insulation mixing 30min, gained slurry is again heated to Send in freezer dryer, gained solid abrasive is obtained final product powder I into powder after fully drying；
(2) furfural dregs are added in 2-3 times of weight portion water, immersion 2h post-heating is filtered to reflux state insulation mixing 1h, Semen Coicis rice flour and pine needle powder are added in gained filtrate, is sent into after being sufficiently mixed in freezer dryer, by institute after fully drying Solid abrasive is obtained into powder, powder II is obtained final product；
(3) vermiculite power and polyethylene glycol oxide is added in active hargil, and be heated to 110-120 DEG C of insulation mixing 15min, Haze tallow and sulfated castor oil is added, continues insulation mixing 10min at 110-120 DEG C, gained mixture is naturally cooled to Room temperature, then makes powder through super micron mill, obtains final product powder III；
(4) powder II, powder III and Pollen Maydiss are added in powder I, is sufficiently mixed and stands in 0-5 DEG C of environment 5h, is eventually adding macropore acidulous acrylic acid's cation exchanger resin, Bis(pentaerythritol) and aluminium polychlorid, is sufficiently mixed Even.
The invention has the beneficial effects as follows：The present invention is aided with multiple auxiliary agents and Scorpio speckle is obtained with plant component as primary raw material Mildew control agent, easy to use, spray in scorpion nest after need to being only watered dissolving during use, you can play significant prevention effect Good；And reach drug effect by the effect of macropore acidulous acrylic acid's cation exchanger resin, active hargil and vermiculite power to delay Effect is released, so as to extend the preventing and treating time, strengthens prevention effect；The control agent does not interfere with the normal growth of Scorpio simultaneously, less The using value of Scorpio can be affected.
Specific embodiment：
In order that technological means, creation characteristic, reached purpose and effect that the present invention is realized are easy to understand, tie below Specific embodiment is closed, the present invention is expanded on further.
Embodiment 1
(1) 15 parts of Folium Eucommiaes, 15 parts of Folium Perillaes, 5 parts of Folium Crataegi, 4 parts of Folium Capsici and 5 parts of grape skins are added 3 times of weights In amount part water, using defibrination three times repeatedly of power 1.5kW fiberizers after immersion 30min, reflux state insulation mixing is again heated to 30min, gained slurry are sent in freezer dryer, and gained solid abrasive is obtained final product powder I into powder after fully drying；
(2) 4 parts of furfural dregs are added in 3 times of weight portion water, immersion 2h post-heating is to reflux state insulation mixing 1h, mistake Filter, adds 2 parts of Semen Coicis rice flour and 2 parts of pine needle powder in gained filtrate, is sent in freezer dryer after being sufficiently mixed, through fully dry By gained solid abrasive into powder after dry, powder II is obtained final product；
(3) 1 part of vermiculite power and 1 part of polyethylene glycol oxide is added in 4 parts of active hargil, and be heated to 110-120 DEG C of insulation Mixing 15min, adds 0.5 part of haze tallow and 0.5 part of sulfated castor oil, continues insulation mixing 10min at 110-120 DEG C, Gained mixture naturally cools to room temperature, then makes powder through super micron mill, obtains final product powder III；
(4) powder II, powder III and 1 part of Pollen Maydis are added in powder I, is sufficiently mixed quiet in 0-5 DEG C of environment 5h is put, 8 parts of D113 macropore acidulous acrylic acid's cation exchanger resins, 1 part of Bis(pentaerythritol) and 0.5 part of polymerization is eventually adding Aluminum chloride, is sufficiently mixed uniform.
The pretreatment of grape skin：1 part of polyethylene glycol 6000 and 0.5 part of spermol are added in 20 parts of grape skins, is filled Sealing and standing 15min after point mixing, is again heated to 50-60 DEG C of insulation mixing 10min, filter pressing, and gained filtering residue is with 10-15 DEG C of cold water Washing twice, then in filtering residue adds 2 parts of water-soluble chitosans and 0.5 part of Rhizoma Solani tuber osi Pregelatinized Starch, is sufficiently mixed, most after Microwave treatment 5min under microwave frequency 2450MHz, power 700W.
Embodiment 2
(1) 10 parts of Folium Eucommiaes, 10 parts of Folium Perillaes, 8 parts of Folium Crataegi, 5 parts of Folium Capsici and 3 parts of grape skins are added 3 times of weights In amount part water, using defibrination three times repeatedly of power 1.5kW fiberizers after immersion 30min, reflux state insulation mixing is again heated to 30min, gained slurry are sent in freezer dryer, and gained solid abrasive is obtained final product powder I into powder after fully drying；
(2) 4 parts of furfural dregs are added in 3 times of weight portion water, immersion 2h post-heating is to reflux state insulation mixing 1h, mistake Filter, adds 4 parts of Semen Coicis rice flour and 2 parts of pine needle powder in gained filtrate, is sent in freezer dryer after being sufficiently mixed, through fully dry By gained solid abrasive into powder after dry, powder II is obtained final product；
(3) 1 part of vermiculite power and 2 parts of polyethylene glycol oxides are added in 6 parts of active hargil, and be heated to 110-120 DEG C of insulation Mixing 15min, adds 0.5 part of haze tallow and 1 part of sulfated castor oil, continues insulation mixing 10min, institute at 110-120 DEG C Obtain mixture and naturally cool to room temperature, then powder is made through super micron mill, obtain final product powder III；
(4) powder II, powder III and 2 parts of Pollen Maydiss are added in powder I, is sufficiently mixed quiet in 0-5 DEG C of environment 5h is put, 5 parts of D113 macropore acidulous acrylic acid's cation exchanger resins, 1 part of Bis(pentaerythritol) and 1 part of polymerization chlorine is eventually adding Change aluminum, be sufficiently mixed uniform.
The pretreatment of grape skin：2 parts of polyethylene glycol 6000s and 0.5 part of spermol are added in 20 parts of grape skins, is filled Sealing and standing 15min after point mixing, is again heated to 50-60 DEG C of insulation mixing 10min, filter pressing, and gained filtering residue is with 10-15 DEG C of cold water Washing twice, then in filtering residue adds 2 parts of water-soluble chitosans and 1 part of Rhizoma Solani tuber osi Pregelatinized Starch, is sufficiently mixed, most after micro- Microwave treatment 5min under wave frequency 2450MHz, power 700W.
Embodiment 3
Embodiment 1 and 2 made control agent of embodiment are watered dissolving to be sprayed in scorpion nest before Scorpio throws in feeding, every Spray once within 1 month, and its prevention effect is monitored.
Monitoring result shows, is less than 5% using the scorpion nest speckle mildew sickness rate of 2 made control agent of embodiment 1 and embodiment, After morbidity, each sprays once the cure rate up to more than 80% of ill Scorpio after made control agent for 1 week, and relapse rate is less than 5%.
The ultimate principle and principal character and advantages of the present invention of the present invention has been shown and described above.The technology of the industry Personnel it should be appreciated that the present invention is not restricted to the described embodiments, simply explanation described in above-described embodiment and description this The principle of invention, without departing from the spirit and scope of the present invention, the present invention also has various changes and modifications, these changes Change and improvement is both fallen within scope of the claimed invention.The claimed scope of the invention by appending claims and its Equivalent thereof.

Claims (4)

1. a kind of spot mold of scorpion control agent, it is characterised in that be made up of the raw material of following parts by weight：
Folium Eucommiae 10-15 parts, Folium Perillae 10-15 parts, Folium Crataegi 5-10 parts, macropore acidulous acrylic acid's cation exchanger resin 5-10 parts, Folium Capsici 4-8 parts, grape skin 3-6 parts, active hargil 3-6 parts, furfural dregs 2-4 parts, Semen Coicis rice flour 2-4 parts, Folium Pini Powder 2-4 parts, vermiculite power 1-2 parts, polyethylene glycol oxide 1-2 parts, Pollen Maydiss 1-2 parts, Bis(pentaerythritol) 1-2 parts, haze tallow 0.5-1 Part, aluminium polychlorid 0.5-1 parts, sulfated castor oil 0.5-1 parts.
2. spot mold of scorpion control agent according to claim 1, it is characterised in that：Macropore acidulous acrylic acid system sun Ion exchange resin is selected from D113 macropore acidulous acrylic acid's cation exchanger resins, D111 macropores acidulous acrylic acid system sun A kind of or both mixing in ion exchange resin.
3. spot mold of scorpion control agent according to claim 1, it is characterised in that：The grape skin is using front through pre- Process, its processing method is：1-2 parts polyethylene glycol 6000 and 0.5-1 part spermols are added in 15-20 part grape skins, is filled Sealing and standing 15min after point mixing, is again heated to 50-60 DEG C of insulation mixing 10min, filter pressing, and gained filtering residue is with 10-15 DEG C of cold water Washing twice, then in filtering residue adds 1-2 parts water-soluble chitosan and 0.5-1 part Rhizoma Solani tuber osi Pregelatinized Starch, is sufficiently mixed, most Microwave treatment 5min under microwave frequency 2450MHz, power 700W.
4. a kind of preparation method of spot mold of scorpion control agent, it is characterised in that comprise the steps：
(1) Folium Eucommiae, Folium Perillae, Folium Crataegi, Folium Capsici and grape skin are added in 2-3 times of weight portion water, after immersion 30min Using defibrination three times repeatedly of power 1.5kW fiberizers, reflux state insulation mixing 30min is again heated to, gained slurry is sent into cold In lyophilizer, gained solid abrasive is obtained final product powder I into powder after fully drying；
(2) furfural dregs are added in 2-3 times of weight portion water, immersion 2h post-heating is filtered, to institute to reflux state insulation mixing 1h Obtain in filtrate and add Semen Coicis rice flour and pine needle powder, send into after being sufficiently mixed in freezer dryer, after fully drying by gained admittedly Body grind into powder, obtains final product powder II；
(3) vermiculite power and polyethylene glycol oxide is added in active hargil, and be heated to 110-120 DEG C of insulation mixing 15min, then plus Enter haze tallow and sulfated castor oil, continue insulation mixing 10min at 110-120 DEG C, gained mixture naturally cools to room temperature, Then powder is made through super micron mill, obtain final product powder III；
(4) powder II, powder III and Pollen Maydiss are added in powder I, is sufficiently mixed standing 5h in 0-5 DEG C of environment, most Add macropore acidulous acrylic acid's cation exchanger resin, Bis(pentaerythritol) and aluminium polychlorid afterwards, be sufficiently mixed uniform.
CN201610953433.8A 2016-11-03 2016-11-03 A kind of spot mold of scorpion control agent and preparation method thereof Pending CN106492051A (en)

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Citations (6)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN103223261A (en) * 2013-04-22 2013-07-31 华南理工大学 Apparatus and method for pulsed electric field-assisted countercurrent extraction of grape skin residue polyphenol
CN104208269A (en) * 2014-08-08 2014-12-17 北京龙程菁华生物科技有限公司 Application of capsicum polyphenol to pharmacy and preparation method of the same
CN104287996A (en) * 2013-07-15 2015-01-21 江西普正制药有限公司 Eucommia shampoo and preparing method thereof
CN105105282A (en) * 2015-09-14 2015-12-02 青岛农业大学 Composite coating fresh keeping agent containing hawthorn leaf flavone and preparation method and application thereof
CN105532753A (en) * 2016-01-06 2016-05-04 和县乌江镇雅轩家庭农场 Livestock farm disinfection spray and preparation method thereof
CN105833227A (en) * 2016-05-12 2016-08-10 郎溪县鑫旺畜牧养殖有限公司 Pheasant aspergillosis preventing and control agent

Patent Citations (6)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN103223261A (en) * 2013-04-22 2013-07-31 华南理工大学 Apparatus and method for pulsed electric field-assisted countercurrent extraction of grape skin residue polyphenol
CN104287996A (en) * 2013-07-15 2015-01-21 江西普正制药有限公司 Eucommia shampoo and preparing method thereof
CN104208269A (en) * 2014-08-08 2014-12-17 北京龙程菁华生物科技有限公司 Application of capsicum polyphenol to pharmacy and preparation method of the same
CN105105282A (en) * 2015-09-14 2015-12-02 青岛农业大学 Composite coating fresh keeping agent containing hawthorn leaf flavone and preparation method and application thereof
CN105532753A (en) * 2016-01-06 2016-05-04 和县乌江镇雅轩家庭农场 Livestock farm disinfection spray and preparation method thereof
CN105833227A (en) * 2016-05-12 2016-08-10 郎溪县鑫旺畜牧养殖有限公司 Pheasant aspergillosis preventing and control agent

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Application publication date: 20170315