CN106479140A - A kind of PET color master batch - Google Patents
A kind of PET color master batch Download PDFInfo
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- CN106479140A CN106479140A CN201610945025.8A CN201610945025A CN106479140A CN 106479140 A CN106479140 A CN 106479140A CN 201610945025 A CN201610945025 A CN 201610945025A CN 106479140 A CN106479140 A CN 106479140A
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- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08L—COMPOSITIONS OF MACROMOLECULAR COMPOUNDS
- C08L67/00—Compositions of polyesters obtained by reactions forming a carboxylic ester link in the main chain; Compositions of derivatives of such polymers
- C08L67/02—Polyesters derived from dicarboxylic acids and dihydroxy compounds
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- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08K—Use of inorganic or non-macromolecular organic substances as compounding ingredients
- C08K2201/00—Specific properties of additives
- C08K2201/002—Physical properties
- C08K2201/003—Additives being defined by their diameter
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- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08L—COMPOSITIONS OF MACROMOLECULAR COMPOUNDS
- C08L2201/00—Properties
- C08L2201/08—Stabilised against heat, light or radiation or oxydation
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- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08L—COMPOSITIONS OF MACROMOLECULAR COMPOUNDS
- C08L2205/00—Polymer mixtures characterised by other features
- C08L2205/03—Polymer mixtures characterised by other features containing three or more polymers in a blend
- C08L2205/035—Polymer mixtures characterised by other features containing three or more polymers in a blend containing four or more polymers in a blend
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- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08L—COMPOSITIONS OF MACROMOLECULAR COMPOUNDS
- C08L2310/00—Masterbatches
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Abstract
The invention belongs to technical field of polymer materials, specifically provide a kind of PET color master batch, be grouped into by the group of following weight portion：30～60 parts of pet vector, 3～12 parts of Oleum Terebinthinae, 5～15 parts of antiblocking agent, 10～20 parts of slipping agent, 10～20 parts of antistatic additive, 10～25 parts of pigment, 2～5 parts of nucleator, 5 10 parts of soap lye, 6～12 parts of antioxidant, 15～25 parts of fire retardant, moistureproof 10～15 parts of additive, 5～15 parts of polydimethylsiloxane, 2～10 parts of antibacterial, 58 parts of polyethylene low-molecular-weight wax, 5～10 parts of delustering agent；Processing technology is simple, and cost is relatively low, and prepared Masterbatch coloring effect is good, and environmental pollution is less.
Description
Technical field
The invention belongs to technical field of polymer materials is and in particular to a kind of PET color master batch.
Background technology
Polyethylene terephthalate (PET) is a kind of crystalline polymer, due to it have excellent mechanical strength,
Electrical insulating property, thermostability and chemical-resistant, thus it is mainly used in the neck such as synthetic fibers, electrical apparatus insulation material and film.
At present, about 20,000,000 tons of China PET yield, wherein 1/3rd need coloring to use, and will be brought every year using colouring method
60000000 tons of coloured sewage discharge color method has toner coloring, dyeing to draw grain coloring and Masterbatch to colour three kinds.Directly adopt
When being coloured with toner, coloring is very simple, but exists and easily produce that color dot, aberration be wayward, larger the lacking of environmental pollution
Point.It is carrying out melt blending using mixing facilities such as double screw extruder after raw material and toner mixing that grain coloring is drawn in dyeing
Color, compared with using toner coloring, draws a coloring effect to be greatly improved, but need to experience and heat twice, not only increase
Production cost, and compromise the mechanical performance of product to a certain extent.When being coloured using Masterbatch, pigment is through pretreatment
And be dispersed in vector resin, substantially increase dispersive property and the coloration efficiency of pigment, there is simple to operate, low cost
The advantages of honest and clean, environmentally safe.
Content of the invention
The purpose of the present invention is the defect overcoming prior art, provides a kind of PET color master batch, and coloring effect preferably, produces
Low cost, production process environmental pollution is less.
For this reason, the invention provides a kind of PET color master batch, being grouped into by the group of following weight portion：
30～60 parts of pet vector, 3～12 parts of Oleum Terebinthinae, 5～15 parts of antiblocking agent, 10～20 parts of slipping agent, antistatic additive
10～20 parts, 10～25 parts of pigment, 2～5 parts of nucleator, soap lye 5-10 part, 6～12 parts of antioxidant, 15～25 parts of fire retardant, anti-
10～15 parts of damp additive, 5～15 parts of polydimethylsiloxane, 2～10 parts of antibacterial, polyethylene low-molecular-weight wax 5-8 part, delustring
5～10 parts of agent；
Polyethylene low-molecular-weight wax can promote that pigment is dispersed not to be re-united, and has preferable affinity with pigment.
Oleum Terebinthinae makes dyestuff compatible well with carrier.
Polydimethylsiloxane is heat-resisting, resistance to oxidation, shear resistant are strong, it is possible to increase material waterproofing and non-oxidizability.
The preparation method of described PET color master batch, comprises the steps：
(1) first each component is carried out dispensing according to weight portion, pigment is ground by grinder, after grinding, pigment particle size is
0.8～1.5um, soap lye is added in the pigment after grinding, makes each pigment particle surface layer equably by the moistening of soap lye institute, shape
Become one layer of saponification liquor；
(2) pet vector, Oleum Terebinthinae, polydimethylsiloxane, polyethylene low-molecular-weight wax are sent in mixer, stir 3-
5min, mixing speed is 80-100r/min；Add antiblocking agent, slipping agent, antistatic additive, nucleator, antioxidant, fire-retardant
The pigment that agent, moistureproof additive, antibacterial, delustering agent and step (1) obtain, mixing time is 30-60min, and mixing speed is
350-500r/min, standby after being sufficiently stirred for；
(3) compound obtaining in step (2) feeding double screw extruder is carried out melt extruded, in double screw extruder
At 100-150 DEG C, screw speed is 100-400r/min to temperature control, extrudes many colored lines, many colored lines are put
Enter tank cooling；
(4) colored line after cooling in step (3) is delivered in exsiccator and is dried process, baking temperature controls
At 60-80 DEG C, 30-40min is dried；
(5) dried colored line in step (4) is delivered to pelleter and carries out pelletizing process, colored line is cut off
For Masterbatch；The Masterbatch of acquisition is put in clear water and rinses；
(6) Masterbatch obtaining step (5) is put into dried in exsiccator, obtains color masterbatch granule product after cooling.
Preferably, described antibacterial is silver-ion antibiotic zeolite.Anti-microbial property lasting stability.
Preferably, described protection against the tide additive is by each component preparation of following mass percent：Stannum oxide 30～60%, resistance to
Shine bright red 20～30% and Tissuemat E 15～30%.
Preferably, described pigment be inorganic pigment or organic pigment, described inorganic pigment be titanium dioxide (titanium dioxide),
One of white carbon black, cadmium yellow, cadmium red, barba hispanica, chrome oxide green or combination in any, described organic pigment is AZOpigments, phthalocyanine face
One of material and Heterocyclics Pigments.
Preferably, described antiblocking agent is lightweight synthetic silica between 2～6 μm for the particle diameter.
Preferably, described slipping agent be oleamide, erucyl amide, calcium stearate, in pentaerythritol tetrastearate
One or more.Smooth effect is good.
Preferably, described delustering agent is cross-linked styrene-acrylonitrile copolymer
Preferably, described antioxidant is hindered phenol antioxygen 1010 or 1076 and phosphite ester kind antioxidant 168
Compound.
Beneficial effects of the present invention：This PET color master batch that the present invention provides, coloring effect is good, improves PET color masterbatch
Non-oxidizability, water proofing property, thermostability, antibiotic property and retention of color, processing technology simple it is easy to operation, production cost
Low, environmental pollution is less, has wide application prospect.
Specific embodiment
With reference to specific embodiment, it is further elucidated with the present invention.
Embodiment 1：
Present embodiments provide a kind of PET color master batch, be grouped into by the group of following weight portion：
30 parts of pet vector, 3 parts of Oleum Terebinthinae, 5 parts of antiblocking agent, 10 parts of slipping agent, 10 parts of antistatic additive, 10 parts of pigment, one-tenth
2 parts of core agent, 5 parts of soap lye, 6 parts of antioxidant, 15 parts of fire retardant, moistureproof 10 parts of additive, 5 parts of polydimethylsiloxane, antibacterial 2
Part, 5 parts of polyethylene low-molecular-weight wax, 5 parts of delustering agent；Preferably, described antibacterial is silver-ion antibiotic zeolite.Anti-microbial property is held
Stable long.
Described protection against the tide additive is by each component preparation of following mass percent：Stannum oxide 30～60%, everbright fast red 20
～30% and Tissuemat E 15～30%.Described pigment is inorganic pigment or organic pigment, and described inorganic pigment is titanium dioxide (two
Titanium oxide), white carbon black, cadmium yellow, cadmium red, barba hispanica, one of chrome oxide green or combination in any, described organic pigment is azo face
One of material, phthalocyanine color and Heterocyclics Pigments.Described antiblocking agent is particle diameter in 2 μm of lightweight synthetic silica.Described
Slipping agent is one or more of oleamide, erucyl amide, calcium stearate, pentaerythritol tetrastearate.Smooth effect
Good.Described delustering agent is the antioxidant described in cross-linked styrene-acrylonitrile copolymer is hindered phenol antioxygen 1010 or 1076
Compound with phosphite ester kind antioxidant 168.
The preparation method of described PET color master batch, comprises the steps：
(1) first each component is carried out dispensing according to weight portion, pigment is ground by grinder, after grinding, pigment particle size is
0.8um, soap lye is added in the pigment after grinding, and makes each pigment particle surface layer equably by the moistening of soap lye institute, forms one
Layer saponification liquor；
(2) pet vector, Oleum Terebinthinae, polydimethylsiloxane, polyethylene low-molecular-weight wax are sent in mixer, stirring
3min, mixing speed is 80r/min；Add antiblocking agent, slipping agent, antistatic additive, nucleator, antioxidant, fire retardant, prevent
The pigment that damp additive, antibacterial, delustering agent and step (1) obtain, mixing time is 30min, and mixing speed is 350r/min,
Standby after being sufficiently stirred for；
(3) compound obtaining in step (2) feeding double screw extruder is carried out melt extruded, in double screw extruder
At 100 DEG C, screw speed is 100r/min to temperature control, extrudes many colored lines, many colored lines is put into tank cold
But；
(4) colored line after cooling in step (3) is delivered in exsiccator and is dried process, baking temperature controls
At 60 DEG C, 30min is dried；
(5) dried colored line in step (4) is delivered to pelleter and carries out pelletizing process, colored line is cut off
For Masterbatch；The Masterbatch of acquisition is put in clear water and rinses；
(6) Masterbatch obtaining step (5) is put into dried in exsiccator, obtains color masterbatch granule product after cooling.
Embodiment 2：
Present embodiments provide a kind of PET color master batch, be grouped into by the group of following weight portion：
60 parts of pet vector, 12 parts of Oleum Terebinthinae, 15 parts of antiblocking agent, 20 parts of slipping agent, 20 parts of antistatic additive, 25 parts of pigment,
5 parts of nucleator, 10 parts of soap lye, 12 parts of antioxidant, 25 parts of fire retardant, moistureproof 15 parts of additive, 15 parts of polydimethylsiloxane, anti-
10 parts of microbial inoculum, 8 parts of polyethylene low-molecular-weight wax, 10 parts of delustering agent；
Described antibacterial is silver-ion antibiotic zeolite.Anti-microbial property lasting stability.Described protection against the tide additive is by following quality
Each component preparation of percentage ratio：Stannum oxide 30～60%, everbright fast red 20～30% and Tissuemat E 15～30%.
Described pigment is inorganic pigment or organic pigment, and described inorganic pigment is titanium dioxide (titanium dioxide), white carbon black, cadmium
One of Huang, cadmium red, barba hispanica, chrome oxide green or combination in any, described organic pigment is AZOpigments, phthalocyanine color and heterocycle
One of pigment.Described antiblocking agent is particle diameter in 6 μm of lightweight synthetic silica.
Described slipping agent is one of oleamide, erucyl amide, calcium stearate, pentaerythritol tetrastearate or several
Kind.Smooth effect is good.Described delustering agent is cross-linked styrene-acrylonitrile copolymer
Described antioxidant is the compound of hindered phenol antioxygen 1010 or 1076 and phosphite ester kind antioxidant 168.
The preparation method of described PET color master batch, comprises the steps：
(1) first each component is carried out dispensing according to weight portion, pigment is ground by grinder, after grinding, pigment particle size is
1.5um, soap lye is added in the pigment after grinding, and makes each pigment particle surface layer equably by the moistening of soap lye institute, forms one
Layer saponification liquor；
(2) pet vector, Oleum Terebinthinae, polydimethylsiloxane, polyethylene low-molecular-weight wax are sent in mixer, stirring
5min, mixing speed is 100r/min；Add antiblocking agent, slipping agent, antistatic additive, nucleator, antioxidant, fire retardant,
The pigment that moistureproof additive, antibacterial, delustering agent and step (1) obtain, mixing time is 60min, and mixing speed is 500r/
Min, standby after being sufficiently stirred for；
(3) compound obtaining in step (2) feeding double screw extruder is carried out melt extruded, in double screw extruder
At 150 DEG C, screw speed is 400r/min to temperature control, extrudes many colored lines, many colored lines is put into tank cold
But；
(4) colored line after cooling in step (3) is delivered in exsiccator and is dried process, baking temperature controls
At 80 DEG C, 40min is dried；
(5) dried colored line in step (4) is delivered to pelleter and carries out pelletizing process, colored line is cut off
For Masterbatch；The Masterbatch of acquisition is put in clear water and rinses；
(6) Masterbatch obtaining step (5) is put into dried in exsiccator, obtains color masterbatch granule product after cooling.
Embodiment 3：
Present embodiments provide a kind of PET color master batch, be grouped into by the group of following weight portion：
50 parts of pet vector, 8 parts of Oleum Terebinthinae, 10 parts of antiblocking agent, 15 parts of slipping agent, 15 parts of antistatic additive, 18 parts of pigment,
3 parts of nucleator, 8 parts of soap lye, 9 parts of antioxidant, 20 parts of fire retardant, moistureproof 13 parts of additive, 8 parts of polydimethylsiloxane, antibacterial
7 parts of agent, 6 parts of polyethylene low-molecular-weight wax, 8 parts of delustering agent；
Described antibacterial is silver-ion antibiotic zeolite.Anti-microbial property lasting stability.Described protection against the tide additive is by following quality
Each component preparation of percentage ratio：Stannum oxide 30～60%, everbright fast red 20～30% and Tissuemat E 15～30%.
Described pigment is inorganic pigment or organic pigment, and described inorganic pigment is titanium dioxide (titanium dioxide), white carbon black, cadmium
One of Huang, cadmium red, barba hispanica, chrome oxide green or combination in any, described organic pigment is AZOpigments, phthalocyanine color and heterocycle
One of pigment.Described antiblocking agent is lightweight synthetic silica between 5 μm for the particle diameter.
Described slipping agent is one of oleamide, erucyl amide, calcium stearate, pentaerythritol tetrastearate or several
Kind.Smooth effect is good.Described delustering agent is cross-linked styrene-acrylonitrile copolymer
Described antioxidant is the compound of hindered phenol antioxygen 1010 or 1076 and phosphite ester kind antioxidant 168.
The preparation method of described PET color master batch, comprises the steps：
(1) first each component is carried out dispensing according to weight portion, pigment is ground by grinder, after grinding, pigment particle size is
1.0um, soap lye is added in the pigment after grinding, and makes each pigment particle surface layer equably by the moistening of soap lye institute, forms one
Layer saponification liquor；
(2) pet vector, Oleum Terebinthinae, polydimethylsiloxane, polyethylene low-molecular-weight wax are sent in mixer, stirring
4min, mixing speed is 90r/min；Add antiblocking agent, slipping agent, antistatic additive, nucleator, antioxidant, fire retardant, prevent
The pigment that damp additive, antibacterial, delustering agent and step (1) obtain, mixing time is 50min, and mixing speed is 450r/min,
Standby after being sufficiently stirred for；
(3) compound obtaining in step (2) feeding double screw extruder is carried out melt extruded, in double screw extruder
At 120 DEG C, screw speed is 300r/min to temperature control, extrudes many colored lines, many colored lines is put into tank cold
But；
(4) colored line after cooling in step (3) is delivered in exsiccator and is dried process, baking temperature controls
At 70 DEG C, 35min is dried；
(5) dried colored line in step (4) is delivered to pelleter and carries out pelletizing process, colored line is cut off
For Masterbatch；The Masterbatch of acquisition is put in clear water and rinses；
(6) Masterbatch obtaining step (5) is put into dried in exsiccator, obtains color masterbatch granule product after cooling.
The only illustration to the present invention exemplified as above, does not constitute the restriction to protection scope of the present invention, all
It is that same or analogous design belongs within protection scope of the present invention with the present invention.
Claims (8)
1. a kind of PET color master batch is it is characterised in that be grouped into by the group of following weight portion：
30～60 parts of pet vector, 3～12 parts of Oleum Terebinthinae, 5～15 parts of antiblocking agent, 10～20 parts of slipping agent, antistatic additive 10～
20 parts, 10～25 parts of pigment, 2～5 parts of nucleator, soap lye 5-10 part, 6～12 parts of antioxidant, 15～25 parts of fire retardant, protection against the tide add
Plus 10～15 parts of agent, 5～15 parts of polydimethylsiloxane, 2～10 parts of antibacterial, polyethylene low-molecular-weight wax 5-8 part, delustering agent 5
～10 parts；
The preparation method of described PET color master batch, comprises the steps：
(1) first each component is carried out dispensing according to weight portion, pigment is ground by grinder, after grinding, pigment particle size is 0.8
～1.5um, soap lye is added in the pigment after grinding, and makes each pigment particle surface layer equably by the moistening of soap lye institute, is formed
One layer of saponification liquor；
(2) pet vector, Oleum Terebinthinae, polydimethylsiloxane, polyethylene low-molecular-weight wax are sent in mixer, stir 3-5min,
Mixing speed is 80-100r/min；Add antiblocking agent, slipping agent, antistatic additive, nucleator, antioxidant, fire retardant, prevent
The pigment that damp additive, antibacterial, delustering agent and step (1) obtain, mixing time is 30-60min, and mixing speed is 350-
500r/min, standby after being sufficiently stirred for；
(3) compound obtaining in step (2) feeding double screw extruder is carried out melt extruded, temperature in double screw extruder
Control at 100-150 DEG C, screw speed is 100-400r/min, extrudes many colored lines, many colored lines are put into water
Groove cools down；
(4) colored line after cooling in step (3) is delivered in exsiccator and is dried process, baking temperature controls
60-80 DEG C, 30-40min is dried；
(5) dried colored line in step (4) is delivered to pelleter and carries out pelletizing process, colored line is cut to color
Master batch；The Masterbatch of acquisition is put in clear water and rinses；
(6) Masterbatch obtaining step (5) is put into dried in exsiccator, obtains color masterbatch granule product after cooling.
2. as claimed in claim 1 a kind of PET color master batch it is characterised in that described antibacterial be silver-ion antibiotic zeolite.
3. as claimed in claim 1 a kind of PET color master batch it is characterised in that described protection against the tide additive by following percent mass
Each component preparation of ratio：Stannum oxide 30～60%, everbright fast red 20～30% and Tissuemat E 15～30%.
4. as claimed in claim 1 a kind of PET color master batch it is characterised in that described pigment be inorganic pigment or organic pigment,
Described inorganic pigment is one of titanium dioxide (titanium dioxide), white carbon black, cadmium yellow, cadmium red, barba hispanica, chrome oxide green or any group
Close, described organic pigment is one of AZOpigments, phthalocyanine color and Heterocyclics Pigments.
5. as claimed in claim 1 a kind of PET color master batch it is characterised in that described antiblocking agent be particle diameter 2～6 μm it
Between lightweight synthetic silica.
6. as claimed in claim 1 a kind of PET color master batch it is characterised in that described slipping agent be oleamide, erucic acid acyl
One or more of amine, calcium stearate, pentaerythritol tetrastearate.
7. as claimed in claim 1 a kind of PET color master batch it is characterised in that：Described delustering agent is cross-linked styrene-propylene
Lonitrile copolymer.
8. as claimed in claim 1 a kind of PET color master batch it is characterised in that：Described antioxidant is hindered phenol antioxygen
1010 or 1076 with the compound of phosphite ester kind antioxidant 168.
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| CN201610945025.8A CN106479140A (en) | 2016-11-02 | 2016-11-02 | A kind of PET color master batch |
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Cited By (12)
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|---|---|---|---|---|
| CN107011639A (en) * | 2017-06-13 | 2017-08-04 | 乾帛新材料科技（上海）有限公司 | A kind of Copper-cladding Aluminum Bar plastics antibacterial matrices |
| CN107629422A (en) * | 2017-10-16 | 2018-01-26 | 苏州宏泉高压电容器有限公司 | A kind of preparation method of flame-proof antibiotic PET color master batch |
| CN108314883A (en) * | 2018-01-24 | 2018-07-24 | 东莞市中嘉集成新材料科技有限公司 | PET dumb lights modified feedstock, PET dumb light modified feedstock preparation methods and PET dumb light batch mixings |
| CN108864666A (en) * | 2018-07-26 | 2018-11-23 | 苏州宝丽迪材料科技股份有限公司 | The preparation method of PET fiber master batch |
| CN108912686A (en) * | 2018-07-16 | 2018-11-30 | 江苏万纳普新材料科技有限公司 | A kind of high-efficiency antimicrobial toughening flame-proof Multi-functional plastic masterbatch and preparation method thereof |
| CN109929264A (en) * | 2019-03-25 | 2019-06-25 | 山东诺森塑胶有限公司 | A kind of modified Masterbatch and preparation method thereof |
| CN110903524A (en) * | 2019-10-22 | 2020-03-24 | 稀美师新材料科技(常州)有限公司 | White polyethylene color master batch with high-reflectivity effect and preparation method thereof |
| CN110903617A (en) * | 2019-12-23 | 2020-03-24 | 明新孟诺卡(辽宁)新材料有限公司 | PET color master batch for water-based superfine fiber and preparation method thereof |
| CN111303458A (en) * | 2020-04-16 | 2020-06-19 | 安徽缤飞塑胶科技有限公司 | Preparation method of light-resistant and antibacterial color master batch |
| CN112126224A (en) * | 2020-09-02 | 2020-12-25 | 池州九威新材料有限公司 | High-temperature-resistant flame-retardant nylon and preparation method thereof |
| CN112592564A (en) * | 2020-12-15 | 2021-04-02 | 江西省萍乡市轩品塑胶制品有限公司 | Modified master batch for lunch box sheet and preparation method thereof |
| CN113402737A (en) * | 2021-07-15 | 2021-09-17 | 邱彦州 | Color master batch and manufacturing process thereof |
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Cited By (12)
| Publication number | Priority date | Publication date | Assignee | Title |
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| CN107011639A (en) * | 2017-06-13 | 2017-08-04 | 乾帛新材料科技（上海）有限公司 | A kind of Copper-cladding Aluminum Bar plastics antibacterial matrices |
| CN107629422A (en) * | 2017-10-16 | 2018-01-26 | 苏州宏泉高压电容器有限公司 | A kind of preparation method of flame-proof antibiotic PET color master batch |
| CN108314883A (en) * | 2018-01-24 | 2018-07-24 | 东莞市中嘉集成新材料科技有限公司 | PET dumb lights modified feedstock, PET dumb light modified feedstock preparation methods and PET dumb light batch mixings |
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Application publication date: 20170308 |