CN106477889A - Your porcelain agate viridescent glaze a kind of and its processing method, your porcelain and its method for cooking - Google Patents
Your porcelain agate viridescent glaze a kind of and its processing method, your porcelain and its method for cooking Download PDFInfo
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- CN106477889A CN106477889A CN201610955345.1A CN201610955345A CN106477889A CN 106477889 A CN106477889 A CN 106477889A CN 201610955345 A CN201610955345 A CN 201610955345A CN 106477889 A CN106477889 A CN 106477889A
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- porcelain
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- C—CHEMISTRY; METALLURGY
- C03—GLASS; MINERAL OR SLAG WOOL
- C03C—CHEMICAL COMPOSITION OF GLASSES, GLAZES OR VITREOUS ENAMELS; SURFACE TREATMENT OF GLASS; SURFACE TREATMENT OF FIBRES OR FILAMENTS MADE FROM GLASS, MINERALS OR SLAGS; JOINING GLASS TO GLASS OR OTHER MATERIALS
- C03C8/00—Enamels; Glazes; Fusion seal compositions being frit compositions having non-frit additions
- C03C8/14—Glass frit mixtures having non-frit additions, e.g. opacifiers, colorants, mill-additions
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- C—CHEMISTRY; METALLURGY
- C03—GLASS; MINERAL OR SLAG WOOL
- C03C—CHEMICAL COMPOSITION OF GLASSES, GLAZES OR VITREOUS ENAMELS; SURFACE TREATMENT OF GLASS; SURFACE TREATMENT OF FIBRES OR FILAMENTS MADE FROM GLASS, MINERALS OR SLAGS; JOINING GLASS TO GLASS OR OTHER MATERIALS
- C03C1/00—Ingredients generally applicable to manufacture of glasses, glazes, or vitreous enamels
- C03C1/04—Opacifiers, e.g. fluorides or phosphates; Pigments
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- C—CHEMISTRY; METALLURGY
- C04—CEMENTS; CONCRETE; ARTIFICIAL STONE; CERAMICS; REFRACTORIES
- C04B—LIME, MAGNESIA; SLAG; CEMENTS; COMPOSITIONS THEREOF, e.g. MORTARS, CONCRETE OR LIKE BUILDING MATERIALS; ARTIFICIAL STONE; CERAMICS; REFRACTORIES; TREATMENT OF NATURAL STONE
- C04B35/00—Shaped ceramic products characterised by their composition; Ceramics compositions; Processing powders of inorganic compounds preparatory to the manufacturing of ceramic products
- C04B35/622—Forming processes; Processing powders of inorganic compounds preparatory to the manufacturing of ceramic products
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- C—CHEMISTRY; METALLURGY
- C04—CEMENTS; CONCRETE; ARTIFICIAL STONE; CERAMICS; REFRACTORIES
- C04B—LIME, MAGNESIA; SLAG; CEMENTS; COMPOSITIONS THEREOF, e.g. MORTARS, CONCRETE OR LIKE BUILDING MATERIALS; ARTIFICIAL STONE; CERAMICS; REFRACTORIES; TREATMENT OF NATURAL STONE
- C04B41/00—After-treatment of mortars, concrete, artificial stone or ceramics; Treatment of natural stone
- C04B41/45—Coating or impregnating, e.g. injection in masonry, partial coating of green or fired ceramics, organic coating compositions for adhering together two concrete elements
- C04B41/50—Coating or impregnating, e.g. injection in masonry, partial coating of green or fired ceramics, organic coating compositions for adhering together two concrete elements with inorganic materials
- C04B41/5022—Coating or impregnating, e.g. injection in masonry, partial coating of green or fired ceramics, organic coating compositions for adhering together two concrete elements with inorganic materials with vitreous materials
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- C—CHEMISTRY; METALLURGY
- C04—CEMENTS; CONCRETE; ARTIFICIAL STONE; CERAMICS; REFRACTORIES
- C04B—LIME, MAGNESIA; SLAG; CEMENTS; COMPOSITIONS THEREOF, e.g. MORTARS, CONCRETE OR LIKE BUILDING MATERIALS; ARTIFICIAL STONE; CERAMICS; REFRACTORIES; TREATMENT OF NATURAL STONE
- C04B41/00—After-treatment of mortars, concrete, artificial stone or ceramics; Treatment of natural stone
- C04B41/80—After-treatment of mortars, concrete, artificial stone or ceramics; Treatment of natural stone of only ceramics
- C04B41/81—Coating or impregnation
- C04B41/85—Coating or impregnation with inorganic materials
- C04B41/86—Glazes; Cold glazes
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- C—CHEMISTRY; METALLURGY
- C04—CEMENTS; CONCRETE; ARTIFICIAL STONE; CERAMICS; REFRACTORIES
- C04B—LIME, MAGNESIA; SLAG; CEMENTS; COMPOSITIONS THEREOF, e.g. MORTARS, CONCRETE OR LIKE BUILDING MATERIALS; ARTIFICIAL STONE; CERAMICS; REFRACTORIES; TREATMENT OF NATURAL STONE
- C04B2235/00—Aspects relating to ceramic starting mixtures or sintered ceramic products
- C04B2235/65—Aspects relating to heat treatments of ceramic bodies such as green ceramics or pre-sintered ceramics, e.g. burning, sintering or melting processes
- C04B2235/658—Atmosphere during thermal treatment
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- C—CHEMISTRY; METALLURGY
- C04—CEMENTS; CONCRETE; ARTIFICIAL STONE; CERAMICS; REFRACTORIES
- C04B—LIME, MAGNESIA; SLAG; CEMENTS; COMPOSITIONS THEREOF, e.g. MORTARS, CONCRETE OR LIKE BUILDING MATERIALS; ARTIFICIAL STONE; CERAMICS; REFRACTORIES; TREATMENT OF NATURAL STONE
- C04B2235/00—Aspects relating to ceramic starting mixtures or sintered ceramic products
- C04B2235/65—Aspects relating to heat treatments of ceramic bodies such as green ceramics or pre-sintered ceramics, e.g. burning, sintering or melting processes
- C04B2235/66—Specific sintering techniques, e.g. centrifugal sintering
- C04B2235/661—Multi-step sintering
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- C—CHEMISTRY; METALLURGY
- C04—CEMENTS; CONCRETE; ARTIFICIAL STONE; CERAMICS; REFRACTORIES
- C04B—LIME, MAGNESIA; SLAG; CEMENTS; COMPOSITIONS THEREOF, e.g. MORTARS, CONCRETE OR LIKE BUILDING MATERIALS; ARTIFICIAL STONE; CERAMICS; REFRACTORIES; TREATMENT OF NATURAL STONE
- C04B2235/00—Aspects relating to ceramic starting mixtures or sintered ceramic products
- C04B2235/70—Aspects relating to sintered or melt-casted ceramic products
- C04B2235/96—Properties of ceramic products, e.g. mechanical properties such as strength, toughness, wear resistance
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- C—CHEMISTRY; METALLURGY
- C04—CEMENTS; CONCRETE; ARTIFICIAL STONE; CERAMICS; REFRACTORIES
- C04B—LIME, MAGNESIA; SLAG; CEMENTS; COMPOSITIONS THEREOF, e.g. MORTARS, CONCRETE OR LIKE BUILDING MATERIALS; ARTIFICIAL STONE; CERAMICS; REFRACTORIES; TREATMENT OF NATURAL STONE
- C04B2235/00—Aspects relating to ceramic starting mixtures or sintered ceramic products
- C04B2235/70—Aspects relating to sintered or melt-casted ceramic products
- C04B2235/96—Properties of ceramic products, e.g. mechanical properties such as strength, toughness, wear resistance
- C04B2235/963—Surface properties, e.g. surface roughness
Abstract
The present invention relates to your porcelain agate viridescent glaze a kind of and its processing method, your porcelain and its method for cooking, it is related to silicate ceramics technical field.Your the porcelain agate viridescent glaze contains the component of following weight portion：Your 6～20 parts of stone, 1～15 part of Agate, 10～70 parts of feldspar, 2～8 parts of calcite, 1～20 part of wollastonite, 0～2 part of talcum, 0～15 part of chestnut ash, 1～8 part of spot fossil, 1～20 part of black green stone.Your the enamel matter for adopting that your porcelain agate viridescent glaze of the present invention burns out is with viridescent as keynote, simple and honest sky blue, the reddish black, pale blue for being full of profit of enamel, blue or green, the emerald green blue or green color and luster of bluish white, ovum can be presented, enamel can also be presented become clear pea green, the pale yellowish green color that reveals the exact details.Your porcelain jade sense and opal effect using your porcelain agate viridescent glaze of the present invention is good, and glaze is more smooth, mechanical strength is higher, water absorption rate is lower, and sintering qualified rate is high.
Description
Technical field
The present invention relates to silicate ceramics technical field, and in particular to the dark green glaze of your porcelain agate of one kind and its processing method,
Further relate to your porcelain a kind of and its method for cooking.
Background technology
Ruyao, gains the name because locating Ruzhou, be China's Song dynasty you, brother, official, first of fixed, five big kilns of an ancient unit of weight, your porcelain for being produced
" juice jade-like stone pool, aqueous to be dripped, glaze such as cream liposoluble and do not flow, its glaze is thick and sound such as uses up, and becomes clear and not dazzling ", have " blue or green such as day, U.S.
Bind the feet of women as jade, cicada's wings hacking, full glaze, support pin burning " typical characteristic.But due to historical reasons, Ruyao firing time only 20
Yu Nian, burns very short, limits throughput of making the time, spreads seldom, and during the Southern Song Dynasty " near outstanding rare ", current countries in the world and China are each big
The collection in museum only more than 60 parts, become rare treasure.
When your porcelain is fired, the glaze of administration is usually first-class as original with feldspar, quartz, calcite and black stone to prior art
Material will grind, and obtain after the modulation that adds water.CN101747089A discloses a kind of Ru agate glaze and its processing method, and agate glaze contains
There is the component of following weight portion：6～26 parts of Agate, 40～65 parts of feldspar, 10～23 parts of calcite, 13～28 parts of black green stone,
3～8 parts of spot fossil, 2～4 parts of talcum, 5～10 parts of chestnut ash.The enamel of your porcelain burnt out using the agate glaze is with blue or green, green
For keynote, simple and honest sky blue, the reddish black and bluish white color for being full of profit of enamel can be presented, it is also possible to present that enamel is bright to reveal the exact details
Pea green, pale yellowish green and pale blue color；Tire matter is fine and smooth fine and close, and porcelain degree is high, and water absorption rate is less than 1.2%, tunks product sound
Sound is clear and melodious；Heat endurance is good, without through crack, seepage defect.But the glaze smoothness of your porcelain using above-mentioned Ru agate glaze
And mechanical strength all has much room for improvement.
Content of the invention
It is an object of the invention to provide a kind of can make your ceramic glaze surface smoothness more preferably, higher your the porcelain agate of mechanical strength
Dark green glaze, while your the porcelain viridescent glaze has functions that diseases prevention, health care, Long-Time Service can be prolonged using your porcelain of your porcelain viridescent glaze
Year lengthens one's life.
Present invention also offers a kind of processing method of your porcelain agate viridescent glaze, your porcelain and its method for cooking.
In order to realize object above, the technical scheme adopted by your the porcelain agate viridescent glaze of the present invention is：
The dark green glaze of your porcelain agate of one kind, the component containing following weight portion：Your 6～20 parts of stone, 1～15 part of Agate, long
10～70 parts of stone, 2～8 parts of calcite, 1～20 part of wollastonite, 0～2 part of talcum, 0～15 part of chestnut ash, 1～8 part of spot fossil,
1～20 part of black green stone.
In your the porcelain agate viridescent glaze of the present invention, the effect of each component is as follows：
Agate：That is agate, its main chemical compositions are silica, and density is 2.6～2.66g/cm3, hardness is 7,
With wax-like gloss, agate being added in base substrate and glaze, can improving the mechanical strength of your porcelain, the trace element in agate is helped
In your porcelain quality, fineness and the jade sense of your ceramic glaze surface is improved, skeleton function is played in glaze.
Your stone, also known as Ruzhou is beautiful, Plum Blossom Jade, is Chinese name stone, gains the name because producing Ruzhou, main chemical compositions are titanium dioxide
Silicon, calcium oxide, quality are fine and smooth, hardness is 7, and background color has black, brown red and green three kinds, partly carry plum blossom-shaped, through country's ground ore deposit
The identification of research institute of portion physical and chemical testing, the trace element containing multiple needed by human body such as iron, zinc, sodium, magnesium, potassium, calcium in your stone, your stone
Play skeleton in glaze and reduce temperature, quality is additionally aided, combine base substrate and glaze more firm, moreover it is possible to make glaze more light
Sliding.
Feldspar is cosolvent in glaze, can increase whiteness and the glossiness of glaze.
Calcite is cosolvent in glaze, can shorten firing time, increases the light transmittance of porcelain, improves between base and glaze
Adhesion.
Wollastonite, natural mineral matter, main component are calcium oxide 48.25%, silica 51.75%, white, light gray
Color, light green color, grey, yellow, light red, redness, brown or colourless.Contraction is shunk and burnt till to wollastonite drying in base substrate
All little, constriction coefficient can be reduced, and had and help solubilization, it is possible to decrease the sintering temperature of base substrate, replace lime stone and stone with it
During English configuration glaze, glaze will not produce glaze bubble pin hole because of bubbing.Acicular wollastonite crystal of the wollastonite in base substrate
Cross arrangement is reticulated, and is around reinforced with quartz by anorthite, so the mechanical strength of product is higher.
Talcum, mainly contains magnesia, is cosolvent, promotes the generation in intermediate layer between base substrate and glaze, improve you in glaze
The heat endurance of porcelain, expands firing range, increases milkiness effect.
Chestnut ash, in glaze, can make your ceramic glaze surface that burns till produce opal effect, improves the sight of your porcelain.Using
Before, first rinsed with water, then dry.
Black green stone and spot fossil, are cosolvent and colouring agent in glaze, containing micro in black green stone and spot fossil
Di-iron trioxide, makes your porcelain being fired into assume blue or green, the emerald green blue or green or light greenish blue color and luster of pea green, reddish black, pale blue, ovum.
Your the enamel matter for adopting your the porcelain agate viridescent glaze of the present invention to burn out is as keynote with viridescent, can present
Enamel is simple and honest to be full of sky blue, the reddish black, pale blue of profit, blue or green, the emerald green blue or green color and luster of bluish white, ovum, can also present enamel and become clear the beans that reveals the exact details
Green, pale yellowish green color.Your porcelain jade sense and opal effect using your porcelain agate viridescent glaze of the present invention is good, glaze is more smooth,
Mechanical strength is higher, water absorption rate lower (less than 1%), and sintering qualified rate is high.Containing multiple needed by human body in your stone
Trace element, using your porcelain of your the porcelain agate viridescent glaze using the present invention, has functions that diseases prevention, health care, and Long-Time Service can
Promote longevity.
Technical program of the present invention also lies in：The processing method of your porcelain agate viridescent glaze above-mentioned, comprises the following steps：
1) respectively your stone and Agate are calcined at 800～900 DEG C, then crushes, obtain your stone of graininess or powdery
And Agate；
2) feldspar, calcite, wollastonite, talcum, black green stone, spot fossil are crushed respectively, obtains graininess or powdery
Building stones；
3) according to weight proportion, chestnut ash, step 1 are taken) your stone of the graininess of gained or powdery and Agate, step 2)
Each graininess of gained or the building stones of powdery, mixing, then add water ball milling, obtains glaze slip；
4) by step 3) Concentration Modulation of gained glaze slip, to 52～56 Baume degrees, then removes iron, old, obtain final product.
Preferably, step 1) in, the time of the calcining is 3.5～4h.
Preferably, step 3) in, the time of the ball milling is 34～38h.The chestnut ash is rinsed with water, is made after drying again
With.In order that glaze slip reaches certain fineness, after the ball milling that adds water, filtered using 10000-hole sieve.
Preferably, step 4) in, it is Baume degrees proportion instrument to modulate the measuring instrument adopted during concentration.Before iron is removed, first
The later glaze slip of concentration will be modulated sieve.
Technical program of the present invention also lies in：Your porcelain a kind of, including your porcelain agate viridescent glaze and base substrate；Your porcelain agate
Dark green glaze contains the component of following weight portion：Your 6～20 parts of stone, 1～15 part of Agate, 10～70 parts of feldspar, calcite 2～8
Part, 1～20 part of wollastonite, 0～2 part of talcum, 0～15 part of chestnut ash, 1～8 part of spot fossil, 1～20 part of black green stone.
Your enamel matter of the present invention with blue or green, green as keynote, can present simple and honest sky blue, the reddish black, pale blue for being full of profit of enamel,
Blue or green, the emerald green blue or green color and luster of bluish white, ovum, can also present enamel and become clear pea green, the pale yellowish green color that reveals the exact details.
Your porcelain jade sense of the present invention and opal effect good, glaze is more smooth, and mechanical strength is higher, and water absorption rate is lower (no
More than 1%), while tunking clear, heat endurance is good, without through crack, seepage defect.There are diseases prevention, guarantor in use
Strong effect, Long-Time Service can be promoted longevity.
Preferably, the base substrate contains following components in percentage by weight：Wollastonite 1～5%, your stone 2～10%.Base substrate
In other components be your common component of porcelain base substrate.Wollastonite in base substrate and your stone can make the tire matter more refinement of your porcelain
Greasy, fine and close, porcelain degree is higher.
Technical program of the present invention also lies in：The method for cooking of your porcelain above-mentioned, comprises the following steps：
1) your the porcelain agate viridescent glaze for stirring equably is applied on base substrate, obtains glazed body；
2) by step 1) gained glazed body is fired, and is first fired with oxidizing flame in sintering procedure, temperature is risen to 950～
1050 DEG C, then fired with reduction flame, temperature is continued 1230～1260 DEG C are risen to, 15～20min is incubated, stop burning, drop naturally
Warm to room temperature, obtain final product.
Your porcelain of the present invention with the raising of firing temperature, the wollastonite expanded by heating in base substrate, is supported in sintering procedure
The drying for base substrate that disappeared is shunk, and shortens drying time, and then shortens the production cycle, reduce production cost, while also carrying
The high plasticity of base substrate；When firing temperature continues to improve, your stone in glaze can improve the viscosity of liquid phase, in filling base substrate
Space, reaches base substrate densified, not only improves the mechanical strength for improving your porcelain, contributes to health again.Additionally, base substrate and
The agate not melted in glaze may be constructed the skeleton of porcelain body, it is to avoid the deformation of your porcelain and cracking, improve sintering qualified rate.
Step 1) in, before your porcelain agate viridescent glaze is applied on the base substrate, base substrate be pre-processed；The pretreatment
It is that base substrate first to forming carries out biscuiting, then the base substrate good to biscuiting is polished, then dedusting, finally carries out moisturizing.
Step 2) in, when firing using oxidizing flame, temperature is risen to 950～1050 DEG C with 5～6h.Using reduction flame
During firing, temperature is continued to rise to 1230～1260 DEG C with 6～7h.
Your porcelain of the present invention is divided into five stages during firing：First stage is the hydrofuge stage, using oxidizing fire
Flame is fired, and temperature is risen to 550～600 DEG C, keeps furnace air unobstructed, the moisture in glazed body is removed；Second stage is for rising
Temperature is risen to 950～1050 DEG C with oxidizing flame by thermophase, so that the moisture in glazed body is discharged more thoroughly, is also made in glazed body
Organic matter and carbon are fully flared off；Phase III is fired using reduction flame, continues for temperature to rise to 1230～1260 DEG C,
The ferric iron contained by spot fossil and black green stone in glaze starts to be reduced to ferrous iron to become ferrous silicon salt, and glaze starts to assume difference
The dark green of degree；Fourth stage is holding stage, temperature is kept 15～20min at 1230～1260 DEG C, so that glaze is fully melted
Melt, carry out ferric reduction reaction more thorough, it is ensured that ferrous silicon salt is assumed dark green purity；5th stage is for stopping burning
Temperature-fall period, is naturally cooling to room temperature, makes glaze have a good Crystallization Process, it is ensured that the presented cyan of ferrous silicon salt in glaze
Stability, if cooling too fast, can cause glaze colours in weight cyan.
Step 2) in, the gas containing following percentage by weight in gas atmosphere when being fired using reduction flame：Oxygen
0.8～1%, carbon monoxide 2.5～9.5%.Impact of the carbon monoxide content in atmosphere to glaze colours is larger, carbon monoxide
Too high levels then make the glaze colours blue or green or sootiness of ash black, and content is too low, and ferrous silicon salt is reoxidized and makes glaze assume yellow.
Specific embodiment
Technical scheme is further described below in conjunction with specific embodiment.
In specific embodiment, chestnut ash is first rinsed with water, is dried, is then reused.Dense to glaze slip in embodiment 1～3
When degree is modulated, during measurement concentration, Baume degrees proportion instrument is used.
Embodiment 1
Your the porcelain agate viridescent glaze of the present embodiment contains the component of following weight portion：Your 13 parts of stone, 15 parts of Agate, feldspar
40 parts, 2 parts of calcite, 15 parts of wollastonite, 15 parts of chestnut ash, 8 parts of spot fossil, 1 part of black green stone.
The processing method of your the porcelain agate viridescent glaze of the present embodiment, comprises the following steps：
1) respectively your stone and Agate are put in kiln and calcine 3.5h at 800 DEG C, then crush respectively, obtain graininess or
Your stone of powdery and Agate；
2) feldspar, calcite, wollastonite, talcum, black green stone, spot fossil are crushed respectively, obtains graininess or powdery
Building stones；
3) according to weight proportion, chestnut ash, step 1 are taken) your stone of the graininess of gained or powdery and Agate, step 2)
Each graininess of gained or the building stones of powdery, mixing, then add water ball milling 36h, is filtered with 10000-hole sieve, obtains glaze slip；
4) by step 3) Concentration Modulation of gained glaze slip, to 52 Baume degrees, then sieves, except iron, old, obtain final product.
Embodiment 2
Your the porcelain agate viridescent glaze of the present embodiment contains the component of following weight portion：Your 6 parts of stone, 1 part of Agate, feldspar 70
Part, 5 parts of calcite, 1 part of wollastonite, 2 parts of talcum, 1 part of spot fossil, 20 parts of black green stone.
The processing method of your the porcelain agate viridescent glaze of the present embodiment, comprises the following steps：
1) your stone respectively and Agate are put in kiln and 4h are calcined at 850 DEG C, then crush respectively, obtain graininess or powder
Your stone of shape and Agate；
2) feldspar, calcite, wollastonite, talcum, black green stone, spot fossil are crushed respectively, obtains graininess or powdery
Building stones；
3) according to weight proportion, step 1 is taken) your stone of the graininess of gained or powdery and Agate, step 2) gained
Each graininess or the building stones of powdery, mixing, then add water ball milling 36h, is filtered with 10000-hole sieve, obtains glaze slip；
4) by step 3) Concentration Modulation of gained glaze slip, to 54 Baume degrees, then sieves, except iron, old, obtain final product.
Embodiment 3
Your the porcelain agate viridescent glaze of the present embodiment contains the component of following weight portion：Your 20 parts of stone, 13 parts of Agate, feldspar
10 parts, 8 parts of calcite, 20 parts of wollastonite, 1 part of talcum, 8 parts of chestnut ash, 5 parts of spot fossil, 15 parts of black green stone.
The processing method of your the porcelain agate viridescent glaze of the present embodiment, comprises the following steps：
1) your stone and Agate are put in kiln and 4h are calcined at 900 DEG C, then crush respectively, obtain graininess or powdery
Your stone and Agate；
2) feldspar, calcite, wollastonite, talcum, black green stone, spot fossil are crushed respectively, obtains graininess or powdery
Building stones；
3) according to weight proportion, chestnut ash, step 1 are taken) your stone of the graininess of gained or powdery and Agate, step 2)
Each graininess of gained or the building stones of powdery, mixing, then add water ball milling 36h, is filtered with 10000-hole sieve, obtains glaze slip；
4) by step 3) Concentration Modulation of gained glaze slip, to 56 Baume degrees, then sieves, except iron, old, obtain final product.
Embodiment 4
Your porcelain of the present embodiment, including your porcelain agate viridescent glaze and base substrate；Your the porcelain agate viridescent glaze is 1 institute of embodiment
Your porcelain agate viridescent glaze.
The method for cooking of your porcelain of the present embodiment, comprises the following steps：
1) base substrate is pre-processed：First the base substrate to forming carries out biscuiting, is entered with emery cloth in the base substrate good to biscuiting
Row polishing, then blows away dedusting with hair-dryer, then wipes clean base substrate with sponge and carry out moisturizing to which；
2) your the porcelain agate viridescent glaze for stirring equably is applied on base substrate, then carries out bottom trimming is wiped, obtain glazed body；
3) by step 2) gained glazed body support pin props up to insert in kiln and is fired, and first uses oxidizing flame in sintering procedure
Fire, temperature is risen to 950 DEG C with the time of 5h, then fired with reduction flame, control the gas atmosphere in kiln to include weight
The oxygen 1% of percentage, carbon monoxide 6%, temperature is continued 1230 DEG C are risen to the time of 6h, 15min is incubated, stop burning, from
So room temperature is cooled to, obtains final product.
Embodiment 5
Your porcelain of the present embodiment, including your porcelain agate viridescent glaze and base substrate；Your the porcelain agate viridescent glaze is 2 institute of embodiment
Your porcelain agate viridescent glaze.
The method for cooking of your porcelain of the present embodiment, comprises the following steps：
1) base substrate is pre-processed：First the base substrate to forming carries out biscuiting, is entered with emery cloth in the base substrate good to biscuiting
Row polishing, then blows away dedusting with hair-dryer, then wipes clean base substrate with sponge and carry out moisturizing to which；
2) your the porcelain agate viridescent glaze for stirring equably is applied on base substrate, then carries out bottom trimming is wiped, obtain glazed body；
3) by step 2) gained glazed body support pin props up to insert in kiln and is fired, and first uses oxidizing flame in sintering procedure
Fire, temperature is risen to 1050 DEG C with the time of 6h, then fired with reduction flame, control the gas atmosphere in kiln to include weight
The oxygen 0.8% of percentage, temperature is continued to rise to 1260 DEG C with the time of 7h, is incubated 20min, stops by carbon monoxide 2.5%
Burn, room temperature is naturally cooling to, is obtained final product.
Embodiment 6
Your porcelain of the present embodiment, including your porcelain agate viridescent glaze and base substrate；Your the porcelain agate viridescent glaze is 3 institute of embodiment
Your porcelain agate viridescent glaze.
The method for cooking of your porcelain of the present embodiment, comprises the following steps：
1) base substrate is pre-processed：First the base substrate to forming carries out biscuiting, is entered with emery cloth in the base substrate good to biscuiting
Row polishing, then blows away dedusting with hair-dryer, then wipes clean base substrate with sponge and carry out moisturizing to which；
2) your the porcelain agate viridescent glaze for stirring equably is applied on base substrate, then carries out bottom trimming is wiped, obtain glazed body；
3) by step 2) gained glazed body support pin props up to insert in kiln and is fired, and first uses oxidizing flame in sintering procedure
Fire, temperature is risen to 1000 DEG C with the time of 5.5h, then fired with reduction flame, control the gas atmosphere in kiln comprising weight
The oxygen 0.9% of amount percentage, carbon monoxide 9.5%, temperature is continued 1250 DEG C are risen to the time of 6.5h, 18min is incubated,
Stop burning, room temperature is naturally cooling to, is obtained final product.
Embodiment 7
Your porcelain of the present embodiment, including Ru agate glaze and base substrate；Your the porcelain agate viridescent glaze is 3 gained of embodiment
The dark green glaze of your porcelain agate；The base substrate contains following components in percentage by weight：Wollastonite 1%, your stone 2%.
Embodiment 8
Your porcelain of the present embodiment, including Ru agate glaze and base substrate；Your the porcelain agate viridescent glaze is 3 gained of embodiment
The dark green glaze of your porcelain agate；The base substrate contains following components in percentage by weight：Wollastonite 5%, your stone 10%.
Embodiment 9
Your porcelain of the present embodiment, including Ru agate glaze and base substrate；Your the porcelain agate viridescent glaze is 3 gained of embodiment
The dark green glaze of your porcelain agate；The base substrate contains following components in percentage by weight：Wollastonite 3%, your stone 6%.
Claims (7)
1. your porcelain agate viridescent glaze a kind of, it is characterised in that：Component containing following weight portion：Your 6～20 parts of stone, Agate 1
～15 parts, 10～70 parts of feldspar, 2～8 parts of calcite, 1～20 part of wollastonite, 0～2 part of talcum, 0～15 part of chestnut ash, spot
1～8 part of stone, 1～20 part of black green stone.
2. a kind of processing method of your porcelain agate viridescent glaze as claimed in claim 1, it is characterised in that：Comprise the following steps：
1) respectively your stone and Agate are calcined at 800～900 DEG C, then crushes, obtain your stone and the agate of graininess or powdery
Nao stone；
2) feldspar, calcite, wollastonite, talcum, black green stone, spot fossil are crushed respectively, obtains the building stones of graininess or powdery；
3) according to weight proportion, chestnut ash, step 1 are taken) your stone of the graininess of gained or powdery and Agate, step 2) gained
Each graininess or powdery building stones, mixing, then add water ball milling, obtains glaze slip；
4) by step 3) Concentration Modulation of gained glaze slip, to 52～56 Baume degrees, then removes iron, old, obtain final product.
3. your porcelain a kind of, it is characterised in that：Including the dark green glaze of your porcelain agate and base substrate；Your the porcelain agate viridescent glaze contains following
The component of weight portion：Your 6～20 parts of stone, 1～15 part of Agate, 10～70 parts of feldspar, 2～8 parts of calcite, wollastonite 1～20
Part, 0～2 part of talcum, 0～15 part of chestnut ash, 1～8 part of spot fossil, 1～20 part of black green stone.
4. your porcelain according to claim 3, it is characterised in that：The base substrate contains following components in percentage by weight：Silicon
Lime stone 1～5%, your stone 2～10%.
5. a kind of method for cooking of your porcelain as described in claim 3 or 4, it is characterised in that：Comprise the following steps：
1) your porcelain agate viridescent glaze is equably applied on base substrate, obtains glazed body；
2) by step 1) gained glazed body is fired, and first fired with oxidizing flame in sintering procedure, temperature is risen to 950～1050
DEG C, then fired with reduction flame, temperature is continued 1230～1260 DEG C are risen to, 15～20min is incubated, stop burning, be naturally cooling to
Room temperature, obtains final product.
6. the method for cooking of your porcelain according to claim 5, it is characterised in that：Step 1) in, by your porcelain agate viridescent glaze
Before applying on the base substrate, base substrate be pre-processed；The pretreatment is first to carry out biscuiting to the base substrate of forming, then right
The good base substrate of biscuiting is polished, then dedusting, finally carries out moisturizing.
7. the method for cooking of your porcelain according to claim 5, it is characterised in that：Step 2) in, fired using reduction flame
When gas atmosphere in the gas containing following percentage by weight：Oxygen 0.8～1%, carbon monoxide 2.5～9.5%.
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|---|---|---|---|
| CN201610955345.1A CN106477889B (en) | 2016-10-27 | 2016-10-27 | A kind of your porcelain agate viridescent glaze and its processing method, your porcelain and its method for cooking |
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| CN108640509A (en) * | 2018-06-19 | 2018-10-12 | 张玉凤 | Your a kind of porcelain glaze modelled after an antique and preparation method thereof |
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