CN106474766A - A kind of sucralose low energy consumption extraction equipment - Google Patents
A kind of sucralose low energy consumption extraction equipment Download PDFInfo
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- CN106474766A CN106474766A CN201611075763.8A CN201611075763A CN106474766A CN 106474766 A CN106474766 A CN 106474766A CN 201611075763 A CN201611075763 A CN 201611075763A CN 106474766 A CN106474766 A CN 106474766A
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- China
- Prior art keywords
- frame
- drain pipe
- way
- extraction
- ethyl acetate
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- 238000000605 extraction Methods 0.000 title claims abstract description 84
- 239000004376 Sucralose Substances 0.000 title claims abstract description 51
- BAQAVOSOZGMPRM-QBMZZYIRSA-N sucralose Chemical compound O[C@@H]1[C@@H](O)[C@@H](Cl)[C@@H](CO)O[C@@H]1O[C@@]1(CCl)[C@@H](O)[C@H](O)[C@@H](CCl)O1 BAQAVOSOZGMPRM-QBMZZYIRSA-N 0.000 title claims abstract description 51
- 235000019408 sucralose Nutrition 0.000 title claims abstract description 51
- 238000005265 energy consumption Methods 0.000 title claims abstract description 25
- XEKOWRVHYACXOJ-UHFFFAOYSA-N Ethyl acetate Chemical compound CCOC(C)=O XEKOWRVHYACXOJ-UHFFFAOYSA-N 0.000 claims abstract description 226
- 239000002351 wastewater Substances 0.000 claims abstract description 21
- 239000007788 liquid Substances 0.000 claims abstract description 7
- 239000000284 extract Substances 0.000 claims description 38
- 238000003466 welding Methods 0.000 claims description 17
- 229910000831 Steel Inorganic materials 0.000 claims description 13
- 239000000463 material Substances 0.000 claims description 13
- 239000010959 steel Substances 0.000 claims description 13
- 238000003756 stirring Methods 0.000 claims description 13
- 238000002604 ultrasonography Methods 0.000 claims description 11
- 238000007789 sealing Methods 0.000 claims description 10
- 238000004026 adhesive bonding Methods 0.000 claims description 3
- 239000000203 mixture Substances 0.000 claims description 2
- 238000011084 recovery Methods 0.000 abstract description 3
- 238000004064 recycling Methods 0.000 abstract description 3
- 230000000694 effects Effects 0.000 abstract description 2
- 230000007613 environmental effect Effects 0.000 abstract description 2
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 description 20
- QTBSBXVTEAMEQO-UHFFFAOYSA-N Acetic acid Chemical compound CC(O)=O QTBSBXVTEAMEQO-UHFFFAOYSA-N 0.000 description 9
- 229930006000 Sucrose Natural products 0.000 description 9
- CZMRCDWAGMRECN-UGDNZRGBSA-N Sucrose Chemical compound O[C@H]1[C@H](O)[C@@H](CO)O[C@@]1(CO)O[C@@H]1[C@H](O)[C@@H](O)[C@H](O)[C@@H](CO)O1 CZMRCDWAGMRECN-UGDNZRGBSA-N 0.000 description 9
- 239000005720 sucrose Substances 0.000 description 9
- 239000000243 solution Substances 0.000 description 7
- 238000002425 crystallisation Methods 0.000 description 4
- 230000008025 crystallization Effects 0.000 description 4
- ZAMOUSCENKQFHK-UHFFFAOYSA-N Chlorine atom Chemical compound [Cl] ZAMOUSCENKQFHK-UHFFFAOYSA-N 0.000 description 3
- 239000000460 chlorine Substances 0.000 description 3
- 229910052801 chlorine Inorganic materials 0.000 description 3
- 238000010586 diagram Methods 0.000 description 3
- XYIBRDXRRQCHLP-UHFFFAOYSA-N ethyl acetoacetate Chemical compound CCOC(=O)CC(C)=O XYIBRDXRRQCHLP-UHFFFAOYSA-N 0.000 description 3
- 239000002699 waste material Substances 0.000 description 3
- 240000000111 Saccharum officinarum Species 0.000 description 2
- 235000007201 Saccharum officinarum Nutrition 0.000 description 2
- 239000007864 aqueous solution Substances 0.000 description 2
- 239000003795 chemical substances by application Substances 0.000 description 2
- 238000003810 ethyl acetate extraction Methods 0.000 description 2
- 125000004494 ethyl ester group Chemical group 0.000 description 2
- 235000003599 food sweetener Nutrition 0.000 description 2
- 238000001556 precipitation Methods 0.000 description 2
- 238000013517 stratification Methods 0.000 description 2
- 239000003765 sweetening agent Substances 0.000 description 2
- 230000009286 beneficial effect Effects 0.000 description 1
- 238000005516 engineering process Methods 0.000 description 1
- 150000002148 esters Chemical class 0.000 description 1
- 239000002994 raw material Substances 0.000 description 1
- 235000019605 sweet taste sensations Nutrition 0.000 description 1
Classifications
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01D—SEPARATION
- B01D11/00—Solvent extraction
- B01D11/04—Solvent extraction of solutions which are liquid
- B01D11/0419—Solvent extraction of solutions which are liquid in combination with an electric or magnetic field or with vibrations
- B01D11/0423—Applying ultrasound
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01D—SEPARATION
- B01D11/00—Solvent extraction
- B01D11/04—Solvent extraction of solutions which are liquid
- B01D11/0492—Applications, solvents used
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07H—SUGARS; DERIVATIVES THEREOF; NUCLEOSIDES; NUCLEOTIDES; NUCLEIC ACIDS
- C07H1/00—Processes for the preparation of sugar derivatives
- C07H1/06—Separation; Purification
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07H—SUGARS; DERIVATIVES THEREOF; NUCLEOSIDES; NUCLEOTIDES; NUCLEIC ACIDS
- C07H5/00—Compounds containing saccharide radicals in which the hetero bonds to oxygen have been replaced by the same number of hetero bonds to halogen, nitrogen, sulfur, selenium, or tellurium
- C07H5/02—Compounds containing saccharide radicals in which the hetero bonds to oxygen have been replaced by the same number of hetero bonds to halogen, nitrogen, sulfur, selenium, or tellurium to halogen
Landscapes
- Chemical & Material Sciences (AREA)
- Organic Chemistry (AREA)
- Health & Medical Sciences (AREA)
- Life Sciences & Earth Sciences (AREA)
- Engineering & Computer Science (AREA)
- Biochemistry (AREA)
- Biotechnology (AREA)
- General Health & Medical Sciences (AREA)
- Genetics & Genomics (AREA)
- Molecular Biology (AREA)
- Chemical Kinetics & Catalysis (AREA)
- Extraction Or Liquid Replacement (AREA)
Abstract
The present invention relates to a kind of extraction equipment, more particularly, to a kind of sucralose low energy consumption extraction equipment.The technical problem to be solved in the present invention is to provide a kind of extraction efficiency height, energy consumption sucralose low energy consumption extraction equipment that is low and extracting liquid energy recycling.In order to solve above-mentioned technical problem, the invention provides such a sucralose low energy consumption extraction equipment, include base plate, left socle, waste water frame, support bar, right support, ethyl acetate recovery frame, the first valve, the first drain pipe, the second valve, second drain pipe etc.；First through hole and the second through hole are had on left socle, first through hole is located at the top of the second through hole, the mode being bolted on the right side of left socle is connected with second bearing seat and extraction frame, second bearing seat is located at the top of extraction frame.Invention achieves environmental protection, efficiently, low energy consumption, device structure is simple and the effect simple to operate of device.
Description
Technical field
The present invention relates to a kind of extraction equipment, more particularly, to a kind of sucralose low energy consumption extraction equipment.
Background technology
Sucralose, the one kind applied for a patent by the common development of Tai Lai company of Britain and London University and in 1976 is new
Sweeting agent.It is unique functional sweetener with sucrose as raw material, original brand name is, sugariness is up to 600 times of sucrose.This
Sweeting agent has a noenergy, and sugariness is high, and sweet taste is pure, the features such as high safety.Be at present classic functional sweetener it
One.The use of sucralose first will extract sucralose, and the extraction efficiency of present sucralose extraction equipment is low, extraction
Take not thorough and high energy consumption.
Chinese patent CN204428889U extracts thorough and extract waste problem for existing, discloses one kind
Three sucrose extraction equipment, it overcomes sucralose extraction by way of designing three extraction equipments and being serially connected extraction
The problem that not thorough and extract can waste, but because this equipment is complicated and operation is excessive, thus this equipment occupation of land face can be led to
Long-pending big, high energy consumption and the problem being difficult to use.
To sum up, need at present to research and develop the sucralose use that a kind of extraction efficiency is high, energy consumption is low and extracts liquid energy recycling
Low energy consumption extraction equipment, to overcome that sucralose extraction equipment extraction efficiency in prior art is low, high energy consumption and extract are a large amount of
The shortcoming wasting.
Content of the invention
（1）Technical problem to be solved
Sucralose extraction equipment extraction efficiency in prior art is low, high energy consumption and extract waste in a large number in order to overcome for the present invention
Shortcoming, the technical problem to be solved in the present invention is to provide that a kind of extraction efficiency is high, energy consumption is low and extraction liquid energy recycles
Sucralose low energy consumption extraction equipment.
（2）Technical scheme
In order to solve above-mentioned technical problem, the invention provides such a sucralose low energy consumption extraction equipment, include
Base plate, left socle, waste water frame, support bar, right support, ethyl acetate reclaim frame, the first valve, the first drain pipe, the second valve,
Second drain pipe, extract frame, supersonic generator, ethyl acetate feed tube, first bearing seat, first rotating shaft, first bevel gear,
Second bevel gear, the second rotating shaft, second bearing seat, handle, rubber blanket, the first feed tube, sealing ring, the 3rd valve, the 3rd go out
Liquid pipe, stirring vane and extraction frame；The mode that base plate top passes on left welding is connected with left socle, and left socle has first
Through hole and the second through hole, first through hole is located at the top of the second through hole, and the mode being bolted on the right side of left socle is connected with
Second bearing seat and extraction frame, second bearing seat is located at the top of extraction frame, and the bearing in second bearing seat passes through interference fit
Mode be connected with the second rotating shaft, the second rotating shaft pass through first through hole, the second rotating shaft is connected with by way of flat key connects
Second bevel gear, the second rotating shaft left end is connected with handle by way of welding, and handle periphery is connected with by way of glueing joint
Rubber blanket, extraction arch has third through-hole, is provided with sealing ring, the side that extraction arch is bolted in third through-hole
Formula is connected with first bearing seat, and the bearing in first bearing seat is connected with first rotating shaft by way of interference fit, first turn
It is connected with first bevel gear, first bevel gear and second bevel gear engagement, first rotating shaft by way of flat key connects above axle
Through third through-hole and sealing ring, first rotating shaft bottom and bottom are connected with stirring vane by way of welding, extraction frame
First feed tube is connected with by way of flange connects on left wall, the first feed tube passes through the left wall of extraction frame and second to lead to
Hole, the right wall of extraction frame is connected with ethyl acetate feed tube and the second drain pipe, ethyl acetate by way of flange connects
Feed tube is located at the top of the second drain pipe, and ethyl acetate feed tube and the second drain pipe both pass through the right wall of extraction frame, and second
Drain pipe is provided with the second valve, and extraction frame bottom is connected with the 3rd drain pipe, the 3rd drain pipe by way of flange connects
Pass through extraction frame bottom, the 3rd drain pipe is provided with the 3rd valve, and the mode that base plate top is bolted is connected with waste water
Frame, waste water frame is located at the right of left socle, and waste water frame is located at the lower section of the 3rd drain pipe, and base plate top is connected by way of welding
It is connected to support bar and right support, support bar is located at the left of right support, support bar is located at the right of waste water frame, support bar top is led to
Cross bolted mode and be connected with extraction frame, extract the left wall of frame and the right-hand member of the second drain pipe by way of flange connects
Connect, the right-hand member of the second drain pipe passes through the left wall extracting frame, and the mode that extraction inframe top is bolted is connected with super
Sonic generator, is connected with the first drain pipe below the right wall extracting frame, the first drain pipe passes through by way of flange connects
Extract below the right wall of frame, the first drain pipe is provided with the first valve, the mode that on the left of right support, lower section is bolted is even
It is connected to ethyl acetate and reclaims frame, by way of flange connects and ethyl acetate reclaims the left wall company of frame to the first drain pipe left end
Connect.
Preferably, also include filter screen, extract and be connected with filter screen, the material of filter screen by way of welding below inframe right wall
Matter is rustless steel, and filter screen is located at the left of the first drain pipe left end.
Preferably, also include sloping platform, extract inframe bottom and be connected with sloping platform by way of bonding, sloping platform is located at filter screen
Left, the main view cross sectional shape of sloping platform is right angled triangle, and the material of sloping platform is rustless steel.
Preferably, the material of left socle is Q235 steel.
Preferably, the three-dimensional shape of base plate is cuboid.
Preferably, the diameter ratio of first rotating shaft and the second rotating shaft is 1:2.
Operation principle：When sucralose is extracted from aqueous solution, trichlorine is contained from the first feed tube handle in elder generation
The solution of sucrose is put into, and puts into ethyl acetate from ethyl acetate feed tube simultaneously, when sucralose solution and the second of extraction inframe
When acetoacetic ester adds appropriate, ethyl acetate and sucralose solution stop adding extraction inframe, ethyl acetate and water to be sl. sol.,
And dissolubility in ethyl acetate for the sucralose is high, now so ethyl acetate can extract the sucralose in water outlet.With
This simultaneously workman the second rotating shaft is rotated by handle, rubber blanket can make the more preferable swing handle of workman, and the second rotating shaft passes through the
Plug tap gear driven first bevel gear rotates, and first bevel gear drives first rotating shaft to rotate, and first rotating shaft drives stirring vane to enter
Row rotates, thus improving the speed of the sucralose in ethyl acetate extraction water.After stirring vane stirring a period of time, workman
Stop operating handle, and at this moment ethyl acetate and water will separate, and the density ratio ethyl acetate of water is big, and water is by under ethyl acetate
Side, and ethyl acetate will extract the sucralose in water entirely.When ethyl acetate and water stratification, workman opens the 3rd valve
Door, the water of extraction inframe will flow to waste water inframe from the 3rd drain pipe, when the water extracting inframe flows to waste water frame entirely, Gong Renguan
Close the 3rd valve, at this moment workman opens the second valve, the ethyl acetate containing sucralose will flow to extraction from the second drain pipe
Inframe, when the ethyl acetate extracting inframe flows to extraction inframe entirely, workman closes the second valve, at this moment starts ultrasound wave and occurs
Device, makes supersonic generator send the ultrasound wave for 59KHZ for the frequency, the ultrasound wave that at this moment supersonic generator sends will make acetic acid
Sucralose crystallization in ethyl ester, thus departing from ethyl acetate, and then obtains pure sucralose.When in ethyl acetate no longer
When separating out sucralose crystallization, workman opens the first valve, and the ethyl acetate without sucralose will flow to from the first drain pipe
Ethyl acetate reclaim frame, when extract inframe ethyl acetate entirely flow to ethyl acetate reclaim frame when, workman close the first valve and
Supersonic generator, at this moment can extract sucralose from sucralose solution, and ethyl acetate can be made to reclaim profit simultaneously
With.
Because also including filter screen, extracting and being connected with filter screen, the material of filter screen by way of welding below inframe right wall
For rustless steel, filter screen is located at the left of the first drain pipe left end, so filter screen can prevent the trichlorine crystallizing because of ultrasound wave
Sucrose blocks the first drain pipe, makes ethyl acetate be not plugged up extracting inframe, thus preferably recycling ethyl acetate.
Because also including sloping platform, extracting inframe bottom and being connected with sloping platform by way of bonding, sloping platform is located at filter screen
Left, the main view cross sectional shape of sloping platform is right angled triangle, and the material of sloping platform is rustless steel, so when the trichlorine in ethyl acetate
When sucrose is crystallized precipitation, sloping platform can make the ethyl acetate of extraction inframe faster and more thoroughly flow to second from the first drain pipe
Acetoacetic ester reclaims inframe, thus more rapid and more thorough recovery ethyl acetate.
（3）Beneficial effect
Invention achieves environmental protection, efficiently, low energy consumption, device structure is simple and the effect simple to operate of device, by super
The ultrasound wave that sonic generator sends makes the sucralose in ethyl acetate separate out in the way of crystallizing, thus in extraction trichlorine sugarcane
When sugared, ethyl acetate can be recycled.
Brief description
Fig. 1 is the first main structure diagram of the present invention.
Fig. 2 is the second main structure diagram of the present invention.
Fig. 3 is the third main structure diagram of the present invention.
Being labeled as in accompanying drawing：1- base plate, 2- left socle, 3- waste water frame, 4- support bar, 5- right support, 6- ethyl acetate
Reclaim frame, 7- first valve, 8- first drain pipe, 9- second valve, 10- second drain pipe, 11- extracts frame, 12- ultrasound wave is sent out
Raw device, 13- ethyl acetate feed tube, 14- first bearing seat, 15- first rotating shaft, 16- first bevel gear, 17- second bevel gear,
18- second rotating shaft, 19- second bearing seat, 20- first through hole, 21- handle, 22- rubber blanket, 23- first feed tube, 24- second
Through hole, 25- sealing ring, 26- third through-hole, 27- the 3rd valve, 28- the 3rd drain pipe, 29- stirring vane, 30- extracts frame,
31- filter screen, 32- sloping platform.
Specific embodiment
The present invention is further illustrated with reference to the accompanying drawings and examples.
Embodiment 1
A kind of sucralose low energy consumption extraction equipment, as Figure 1-3, includes base plate 1, left socle 2, waste water frame 3, supports
Bar 4, right support 5, ethyl acetate reclaim frame 6, the first valve 7, the first drain pipe 8, the second valve 9, the second drain pipe 10, extract
Frame 11, supersonic generator 12, ethyl acetate feed tube 13, first bearing seat 14, first rotating shaft 15, first bevel gear 16,
Two bevel gears 17, the second rotating shaft 18, second bearing seat 19, handle 21, rubber blanket 22, the first feed tube 23, sealing ring the 25, the 3rd
Valve 27, the 3rd drain pipe 28, stirring vane 29 and extraction frame 30；Base plate 1 top left side is connected with a left side by way of welding
Support 2, left socle 2 has first through hole 20 and the second through hole 24, and first through hole 20 is located at the top of the second through hole 24, left
The mode being bolted on the right side of frame 2 is connected with second bearing seat 19 and extraction frame 30, and second bearing seat 19 is located at extraction frame
30 top, the bearing in second bearing seat 19 is connected with the second rotating shaft 18 by way of interference fit, and the second rotating shaft 18 is worn
Cross first through hole 20, the second rotating shaft 18 is connected with by way of flat key connects second bevel gear 17, the second rotating shaft 18 left end
It is connected with handle 21 by way of welding, handle 21 periphery is connected with rubber blanket 22 by way of glueing joint, extraction frame 30 pushes up
Portion has third through-hole 26, is provided with sealing ring 25 in third through-hole 26, and the mode that extraction frame 30 top is bolted connects
There is first bearing seat 14, the bearing in first bearing seat 14 is connected with first rotating shaft 15 by way of interference fit, first turn
It is connected with first bevel gear 16 by way of flat key connects, first bevel gear 16 and second bevel gear 17 engage above axle 15,
First rotating shaft 15 is passed through third through-hole 26 and sealing ring 25, first rotating shaft 15 bottom and bottom to be connected with by way of welding and stirs
Mix blade 29, the left wall of extraction frame 30 is connected with the first feed tube 23 by way of flange connects, the first feed tube 23 is worn
Cross left wall and second through hole 24 of extraction frame 30, the right wall of extraction frame 30 is connected with ethyl acetate by way of flange connects
Feed tube 13 and the second drain pipe 10, ethyl acetate feed tube 13 is located at the top of the second drain pipe 10, ethyl acetate feed tube
13 and second drain pipe 10 both pass through the right wall of extraction frame 30, the second drain pipe 10 is provided with the second valve 9, extracts frame 30 bottom
It is connected with the 3rd drain pipe 28 by way of flange connects, the 3rd drain pipe 28 passes through extraction frame 30 bottom, the 3rd drain pipe
28 are provided with the 3rd valve 27, and the mode that base plate 1 top is bolted is connected with waste water frame 3, and waste water frame 3 is located at left socle
2 right, waste water frame 3 is located at the lower section of the 3rd drain pipe 28, and base plate 1 top is connected with support bar 4 He by way of welding
Right support 5, support bar 4 is located at the left of right support 5, and support bar 4 is located at the right of waste water frame 3, and bolt is passed through at support bar 4 top
The mode connecting is connected with extraction frame 11, extracts the left wall of frame 11 and the right-hand member of the second drain pipe 10 by way of flange connects
Connect, the right-hand member of the second drain pipe 10 passes through the left wall extracting frame 11, and the mode that extraction frame 11 inner top is bolted is even
It is connected to supersonic generator 12, by way of flange connects, below the right wall extracting frame 11, be connected with the first drain pipe 8, first
Drain pipe 8 passes through below the right wall extracting frame 11, and the first drain pipe 8 is provided with the first valve 7, and right support 5 passes through below left side
Bolted mode is connected with ethyl acetate and reclaims frame 6, and the first drain pipe 8 left end is by way of flange connects and acetic acid second
The left wall that ester reclaims frame 6 connects.
Also include filter screen 31, extract and be connected with filter screen 31 by way of welding below frame 11 inner right wall, filter screen 31
Material is rustless steel, and filter screen 31 is located at the left of the first drain pipe 8 left end.
Also include sloping platform 32, extract frame 11 inner bottom part and be connected with sloping platform 32 by way of bonding, sloping platform 32 is located at filter
The left of net 31, the main view cross sectional shape of sloping platform 32 is right angled triangle, and the material of sloping platform 32 is rustless steel.
The material of left socle 2 is Q235 steel.
The three-dimensional shape of base plate 1 is cuboid.
The diameter ratio of first rotating shaft 15 and the second rotating shaft 18 is 1:2.
Operation principle：When sucralose is extracted from aqueous solution, elder generation 23 from the first feed tube contains three
The solution of chlorine sucrose is put into, and puts into ethyl acetate from ethyl acetate feed tube 13 simultaneously, when the sucralose in extraction frame 30 is molten
When liquid and ethyl acetate add appropriate, ethyl acetate and sucralose solution stop adding in extraction frame 30, ethyl acetate and water
It is sl. sol., and dissolubility in ethyl acetate for the sucralose is high, now so ethyl acetate can extract three in water outlet
Chlorine sucrose.Meanwhile workman rotates the second rotating shaft 18 by handle 21, and rubber blanket 22 can make the more preferable swing handle of workman
21, the second rotating shaft 18 drives first bevel gear 16 to rotate by second bevel gear 17, and first bevel gear 16 drives first rotating shaft 15
Rotate, first rotating shaft 15 drives stirring vane 29 to be rotated, thus improving the speed of the sucralose in ethyl acetate extraction water
Degree.After stirring vane 29 stirring a period of time, workman stops operating handle 21, and at this moment ethyl acetate and water will separate, water
Density ratio ethyl acetate is big, and water is by the lower section positioned at ethyl acetate, and ethyl acetate will extract the sucralose in water entirely
Come.When ethyl acetate and water stratification, workman opens the 3rd valve 27, and the water in extraction frame 30 will flow to from the 3rd drain pipe 28
In waste water frame 3, when the water in extraction frame 30 flows to waste water frame 3 entirely, workman closes the 3rd valve 27, and at this moment workman opens second
Valve 9, the ethyl acetate containing sucralose will flow to the acetic acid in extraction frame 11, in extraction frame 30 from the second drain pipe 10
When ethyl ester flows in extraction frame 11 entirely, workman closes the second valve 9, at this moment starts supersonic generator 12, so that ultrasound wave is occurred
Device 12 sends the ultrasound wave that frequency is 59KHZ, and the ultrasound wave that at this moment supersonic generator 12 sends will make in ethyl acetate three
Chlorine crystallization of sucrose, thus departing from ethyl acetate, and then obtains pure sucralose.When no longer separating out trichlorine sugarcane in ethyl acetate
During sugar crystallization, workman opens the first valve 7, and the ethyl acetate without sucralose will flow to ethyl acetate from the first drain pipe 8
Reclaim frame 6, when extracting the ethyl acetate in frame 11 and entirely flowing to ethyl acetate and reclaim frame 6, workman closes the first valve 7 and ultrasonic
Wave producer 12, at this moment can extract sucralose from sucralose solution, and ethyl acetate can be made to recycle simultaneously.
Because also including filter screen 31, extracting and being connected with filter screen 31, filter screen by way of welding below frame 11 inner right wall
31 material is rustless steel, and filter screen 31 is located at the left of the first drain pipe 8 left end, so filter screen 31 can prevent because ultrasound wave
And the sucralose crystallizing blocks the first drain pipe 8, ethyl acetate is made to be not plugged up in extraction frame 11, thus preferably returning
Receipts utilize ethyl acetate.
Because also including sloping platform 32, extracting frame 11 inner bottom part and being connected with sloping platform 32, sloping platform 32 by way of bonding
In the left of filter screen 31, the main view cross sectional shape of sloping platform 32 is right angled triangle, and the material of sloping platform 32 is rustless steel, so working as second
When sucralose in acetoacetic ester is crystallized precipitation, sloping platform 32 can make ethyl acetate in extraction frame 11 faster and more thoroughly
Flow to ethyl acetate from the first drain pipe 8 to reclaim in frame 6, thus more rapid and more thorough recovery ethyl acetate.
Embodiment described above only have expressed the preferred embodiment of the present invention, and its description is more concrete and detailed, but simultaneously
Therefore the restriction to the scope of the claims of the present invention can not be interpreted as.It should be pointed out that for those of ordinary skill in the art
For, without departing from the inventive concept of the premise, some deformation, improvement and replacement can also be made, these broadly fall into this
Bright protection domain.Therefore, the protection domain of patent of the present invention should be defined by claims.
Claims (6)
1. a kind of sucralose low energy consumption extraction equipment is it is characterised in that include base plate（1）, left socle（2）, waste water frame
（3）, support bar（4）, right support（5）, ethyl acetate reclaim frame（6）, the first valve（7）, the first drain pipe（8）, the second valve
（9）, the second drain pipe（10）, extract frame（11）, supersonic generator（12）, ethyl acetate feed tube（13）, first bearing seat
（14）, first rotating shaft（15）, first bevel gear（16）, second bevel gear（17）, the second rotating shaft（18）, second bearing seat（19）、
Handle（21）, rubber blanket（22）, the first feed tube（23）, sealing ring（25）, the 3rd valve（27）, the 3rd drain pipe（28）, stir
Mix blade（29）With extraction frame（30）；Base plate（1）Top left side is connected with left socle by way of welding（2）, left socle（2）
On have first through hole（20）With the second through hole（24）, first through hole（20）Positioned at the second through hole（24）Top, left socle（2）
The mode that right side is bolted is connected with second bearing seat（19）With extraction frame（30）, second bearing seat（19）It is located at extraction
Frame（30）Top, second bearing seat（19）Interior bearing is connected with the second rotating shaft by way of interference fit（18）, second
Rotating shaft（18）Through first through hole（20）, the second rotating shaft（18）On be connected with second bevel gear by way of flat key connects
（17）, the second rotating shaft（18）Left end is connected with handle by way of welding（21）, handle（21）Periphery is by way of glueing joint
It is connected with rubber blanket（22）, extract frame（30）Top has third through-hole（26）, third through-hole（26）Inside it is provided with sealing ring（25）,
Extraction frame（30）The mode that top is bolted is connected with first bearing seat（14）, first bearing seat（14）Interior bearing leads to
The mode crossing interference fit is connected with first rotating shaft（15）, first rotating shaft（15）Top is connected with the by way of flat key connects
One bevel gear（16）, first bevel gear（16）And second bevel gear（17）Engagement, first rotating shaft（15）Through third through-hole（26）
And sealing ring（25）, first rotating shaft（15）Bottom and bottom are connected with stirring vane by way of welding（29）, extract frame
（30）Left wall on be connected with the first feed tube by way of flange connects（23）, the first feed tube（23）Pass through extraction frame
（30）Left wall and the second through hole（24）, extract frame（30）Right wall on be connected with ethyl acetate by way of flange connects and enter
Liquid pipe（13）With the second drain pipe（10）, ethyl acetate feed tube（13）Positioned at the second drain pipe（10）Top, ethyl acetate
Feed tube（13）With the second drain pipe（10）Both pass through extraction frame（30）Right wall, the second drain pipe（10）It is provided with the second valve
（9）, extract frame（30）Bottom is connected with the 3rd drain pipe by way of flange connects（28）, the 3rd drain pipe（28）Pass through extraction
Take frame（30）Bottom, the 3rd drain pipe（28）It is provided with the 3rd valve（27）, base plate（1）The mode that top is bolted is even
It is connected to waste water frame（3）, waste water frame（3）Positioned at left socle（2）Right, waste water frame（3）Positioned at the 3rd drain pipe（28）Lower section,
Base plate（1）Top is connected with support bar by way of welding（4）And right support（5）, support bar（4）Positioned at right support（5）'s
Left, support bar（4）Positioned at waste water frame（3）Right, support bar（4）The mode that top is bolted is connected with extraction frame
（11）, extract frame（11）Left wall and the second drain pipe（10）Right-hand member connect by way of flange connects, the second drain pipe
（10）Right-hand member pass through extract frame（11）Left wall, extract frame（11）The mode that inner top is bolted is connected with ultrasound wave
Generator（12）, extract frame（11）Right wall below be connected with the first drain pipe by way of flange connects（8）, first goes out liquid
Pipe（8）Pass through and extract frame（11）Right wall below, the first drain pipe（8）It is provided with the first valve（7）, right support（5）Under left side
The mode that side is bolted is connected with ethyl acetate and reclaims frame（6）, the first drain pipe（8）The side that left end is connected by flange
Formula and ethyl acetate reclaim frame（6）Left wall connect.
2. a kind of sucralose low energy consumption extraction equipment according to claim 1 is it is characterised in that also include filter screen
（31）, extract frame（11）It is connected with filter screen by way of welding below inner right wall（31）, filter screen（31）Material be rustless steel,
Filter screen（31）Positioned at the first drain pipe（8）The left of left end.
3. a kind of sucralose low energy consumption extraction equipment according to claim 2 is it is characterised in that also include sloping platform
（32）, extract frame（11）Inner bottom part is connected with sloping platform by way of bonding（32）, sloping platform（32）Positioned at filter screen（31）Left,
Sloping platform（32）Main view cross sectional shape be right angled triangle, sloping platform（32）Material be rustless steel.
4. a kind of sucralose according to claim 1 with low energy consumption extraction equipment it is characterised in that left socle（2）'s
Material is Q235 steel.
5. a kind of sucralose according to claim 1 with low energy consumption extraction equipment it is characterised in that base plate（1）Vertical
Shape is cuboid.
6. a kind of sucralose according to claim 1 with low energy consumption extraction equipment it is characterised in that first rotating shaft（15）
With the second rotating shaft（18）Diameter ratio be 1:2.
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| CN201611075763.8A CN106474766A (en) | 2016-11-30 | 2016-11-30 | A kind of sucralose low energy consumption extraction equipment |
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Cited By (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN107374189A (en) * | 2017-06-28 | 2017-11-24 | 安徽工程大学 | A kind of Intelligent bracelet height attraction type exhibiting device |
| CN108525343A (en) * | 2018-06-20 | 2018-09-14 | 宜昌市汇宜兴新能源科技有限公司 | A kind of extracting method of efficient tealeaves lutein |
| CN115364520A (en) * | 2022-09-06 | 2022-11-22 | 新琪安科技股份有限公司 | Novel sucralose mother liquor extraction process |
Citations (10)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN1106361A (en) * | 1994-02-02 | 1995-08-09 | 东北师范大学 | Treatment of Cr-bearing waste water |
| JP2000176438A (en) * | 1998-12-18 | 2000-06-27 | Electric Power Dev Co Ltd | Extraction method |
| CN204247225U (en) * | 2014-11-23 | 2015-04-08 | 青州市晨凯化工有限公司 | Chemical reaction stirred tank |
| CN204637643U (en) * | 2015-04-23 | 2015-09-16 | 赣州市豪鹏科技有限公司 | A kind of from waste and old electrokinetic cell reclaim sulfuric acid nickel environment-friendly type to strip device |
| CN105037449A (en) * | 2015-09-02 | 2015-11-11 | 常州市长宇实用气体有限公司 | Crystallization method for sucralose |
| CN204841485U (en) * | 2015-08-05 | 2015-12-09 | 杨斗华 | Laboratory agitating unit |
| CN204865075U (en) * | 2015-07-20 | 2015-12-16 | 哈尔滨理工大学 | Polymer extraction separating centrifuge |
| CN106083942A (en) * | 2016-07-02 | 2016-11-09 | 安徽广信农化股份有限公司 | A kind of method improving stability of trichlorosucrose |
| CN205700319U (en) * | 2016-06-28 | 2016-11-23 | 姬昂 | Medical ozone butter honey is mixed with device |
| CN206252883U (en) * | 2016-11-30 | 2017-06-16 | 广东技术师范学院 | A kind of Sucralose low energy consumption extraction equipment |
-
2016
- 2016-11-30 CN CN201611075763.8A patent/CN106474766A/en active Pending
Patent Citations (10)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN1106361A (en) * | 1994-02-02 | 1995-08-09 | 东北师范大学 | Treatment of Cr-bearing waste water |
| JP2000176438A (en) * | 1998-12-18 | 2000-06-27 | Electric Power Dev Co Ltd | Extraction method |
| CN204247225U (en) * | 2014-11-23 | 2015-04-08 | 青州市晨凯化工有限公司 | Chemical reaction stirred tank |
| CN204637643U (en) * | 2015-04-23 | 2015-09-16 | 赣州市豪鹏科技有限公司 | A kind of from waste and old electrokinetic cell reclaim sulfuric acid nickel environment-friendly type to strip device |
| CN204865075U (en) * | 2015-07-20 | 2015-12-16 | 哈尔滨理工大学 | Polymer extraction separating centrifuge |
| CN204841485U (en) * | 2015-08-05 | 2015-12-09 | 杨斗华 | Laboratory agitating unit |
| CN105037449A (en) * | 2015-09-02 | 2015-11-11 | 常州市长宇实用气体有限公司 | Crystallization method for sucralose |
| CN205700319U (en) * | 2016-06-28 | 2016-11-23 | 姬昂 | Medical ozone butter honey is mixed with device |
| CN106083942A (en) * | 2016-07-02 | 2016-11-09 | 安徽广信农化股份有限公司 | A kind of method improving stability of trichlorosucrose |
| CN206252883U (en) * | 2016-11-30 | 2017-06-16 | 广东技术师范学院 | A kind of Sucralose low energy consumption extraction equipment |
Cited By (6)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN107374189A (en) * | 2017-06-28 | 2017-11-24 | 安徽工程大学 | A kind of Intelligent bracelet height attraction type exhibiting device |
| CN107374189B (en) * | 2017-06-28 | 2020-04-24 | 安徽工程大学 | High attraction type display device of intelligence bracelet |
| CN108525343A (en) * | 2018-06-20 | 2018-09-14 | 宜昌市汇宜兴新能源科技有限公司 | A kind of extracting method of efficient tealeaves lutein |
| CN108525343B (en) * | 2018-06-20 | 2019-03-08 | 贵州通和茶叶有限公司 | A kind of extract equipment and application method of efficient tealeaves lutein |
| CN115364520A (en) * | 2022-09-06 | 2022-11-22 | 新琪安科技股份有限公司 | Novel sucralose mother liquor extraction process |
| CN115364520B (en) * | 2022-09-06 | 2023-06-02 | 新琪安科技股份有限公司 | Novel mother liquor extraction process for sucralose |
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