CN204865075U - Polymer extraction separating centrifuge - Google Patents
Polymer extraction separating centrifuge Download PDFInfo
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- CN204865075U CN204865075U CN201520525993.4U CN201520525993U CN204865075U CN 204865075 U CN204865075 U CN 204865075U CN 201520525993 U CN201520525993 U CN 201520525993U CN 204865075 U CN204865075 U CN 204865075U
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- extraction
- extract
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- extraction box
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Abstract
The utility model discloses a polymer extraction separating centrifuge, including throwing liquid mouth, extraction box, thermometer, heating piece, supersonic generator, heavy crystal case, wire netting, heater, lower floor's extract collecting box, time -recorder, pump and upper extract collecting box, the extraction box on be equipped with thermometer and time -recorder, be equipped with heating piece in the extraction box, be equipped with supersonic generator in the extraction box, the extraction box lower extreme passes through lower floor's extract transmission pipe to be connected with the heavy crystal case, the heavy crystal case passes through the gas -supply pipe to be connected with lower floor extract collecting box, upper extract collecting box passes through upper extract to be transmitted to manage and is connected with the extraction box. The utility model discloses the temperature of the interior solution of extraction box is monitored at any time to the thermometer, and the time -recorder writes down the extraction time, guarantees the reaction degree of accuracy, and a heating quickening reaction time and extraction speed, supersonic generator make and react more thoroughly, and wire netting assurance heating is even, collects and attendes lower floor's extract, avoids extravagant, simple structure, convenient to use.
Description
Technical field
The utility model relates to a kind of chemical device, specifically a kind of macromolecule extract and separate machine.
Background technology
Usually need separate substance in chemical experiment, extract a kind of method often commonly used.Extraction utilizes
materialin two kinds of immiscible or sl. sol. solvents solubility or
distribution coefficientdifference, make solute substance in a kind of solvent, transfer to method another solvent.Control degree during extract and separate inaccurate, need manually to rock solution, be separated not thorough, difficulty during separatory.
Summary of the invention
The purpose of this utility model is to provide a kind of macromolecule extract and separate machine, to solve the problem proposed in above-mentioned background technology.
For achieving the above object, the utility model provides following technical scheme:
A kind of macromolecule extract and separate machine, comprise and throw liquid mouth, extraction box, thermometer, heat block, supersonic generator, recrystallization case, wire netting, heater, lower floor's extract collecting box, timer, pump and upper layer of extraction liquid collecting box, described extraction box top is provided with throws liquid mouth, extraction box is provided with thermometer and timer, heat block is provided with in extraction box, supersonic generator is provided with in extraction box, extraction box lower end is provided with lower floor's extract transfer tube, lower floor's extract transfer tube is provided with switch, lower floor's extract transfer tube bottom is provided with recrystallization case, recrystallization case is connected with lower floor extract collecting box by appendix, recrystallization case lower end is provided with heater, upper layer of extraction liquid collecting box is connected with extraction box by upper layer of extraction liquid transfer tube, upper layer of extraction liquid transfer tube arrival end is provided with filter screen, installation pump on upper layer of extraction liquid transfer tube.
As further program of the utility model: be provided with wire netting between described recrystallization case and heater.
As the utility model further scheme: described upper layer of extraction liquid transfer tube arrival end is arranged in extraction box.
Compared with prior art, the beneficial effects of the utility model are: the temperature of solution in extraction box monitored at any time by the utility model thermometer, timer record extraction time, ensure the reaction degree of accuracy, heat block heated solution is to suitable temperature, and accelerate reaction time and extraction rate, supersonic generator sends ultrasonic wave for agitating solution, make reaction more thorough, wire netting ensures homogeneous heating, collects levels extract, avoids waste, structure is simple, easy to use.
Accompanying drawing explanation
Fig. 1 is a kind of structural representation of macromolecule extract and separate machine.
In figure: 1, throw liquid mouth, 2, extraction box, 3, thermometer, 4, heat block, 5, supersonic generator, 6, switch, 7, lower floor's extract transfer tube, 8, recrystallization case, 9, wire netting, 10, heater, 11, appendix, 12, lower floor's extract collecting box, 13, filter screen, 14, timer, 15, pump, 16, upper layer of extraction liquid collecting box, 17, upper layer of extraction liquid transfer tube.
Detailed description of the invention
Be described in more detail below in conjunction with the technical scheme of detailed description of the invention to this patent.
Refer to Fig. 1, a kind of macromolecule extract and separate machine, comprise and throw liquid mouth 1, extraction box 2, thermometer 3, heat block 4, supersonic generator 5, recrystallization case 8, wire netting 9, heater 10, lower floor's extract collecting box 12, timer 14, pump 15 and upper layer of extraction liquid collecting box 16, described extraction box 2 top is provided with throws liquid mouth 1, solution is knocked down in extraction box 2 from throwing liquid mouth 1, extraction box 2 is provided with thermometer 3 and timer 14, the temperature of solution in extraction box 2 monitored at any time by thermometer 3, timer 14 records extraction time, ensure the reaction degree of accuracy, heat block 4 is provided with in extraction box 2, heat block 4 heated solution is to suitable temperature, accelerate reaction time and extraction rate, supersonic generator 5 is provided with in extraction box 2, supersonic generator 5 sends ultrasonic wave for agitating solution, make reaction more thorough, extraction box 2 lower end is provided with lower floor's extract transfer tube 7, lower floor's extract transfer tube 7 is provided with switch 6, lower floor's extract transfer tube 7 bottom is provided with recrystallization case 8, by-pass cock 6 makes lower floor's extract flow into recrystallization case 8 from lower floor's extract transfer tube 7, recrystallization case 8 is connected with lower floor extract collecting box 12 by appendix 11, recrystallization case 8 lower end is provided with heater 10, wire netting 9 is provided with between recrystallization case 8 and heater 10, wire netting 9 ensures homogeneous heating, add hot recrystallization case 8, make lower floor's extract volatilization, recrystallization separates out material in solution, lower floor's extract enters lower floor's extract collecting box 12 and collects, upper layer of extraction liquid collecting box 16 is connected with extraction box 2 by upper layer of extraction liquid transfer tube 17, upper layer of extraction liquid transfer tube 17 arrival end is arranged in extraction box 2, upper layer of extraction liquid transfer tube 17 arrival end is provided with filter screen 13, installation pump 15 on upper layer of extraction liquid transfer tube 17, upper layer of extraction liquid enters upper layer of extraction liquid collecting box 16 from upper layer of extraction liquid transfer tube 17 and collects.
Operation principle of the present utility model is: the utility model solution is knocked down in extraction box from throwing liquid mouth, the temperature of solution in extraction box monitored at any time by thermometer, timer record extraction time, ensure the reaction degree of accuracy, heat block heated solution is to suitable temperature, accelerate reaction time and extraction rate, supersonic generator sends ultrasonic wave for agitating solution, make reaction more thorough, by-pass cock makes lower floor's extract flow into recrystallization case from lower floor's extract transfer tube, wire netting ensures homogeneous heating, add hot recrystallization case, make lower floor's extract volatilization, recrystallization separates out material in solution, lower floor's extract enters lower floor's extract collecting box and collects, upper layer of extraction liquid enters upper layer of extraction liquid collecting box from upper layer of extraction liquid transfer tube and collects.
Above the better embodiment of this patent is explained in detail, but this patent is not limited to above-mentioned embodiment, in the ken that one skilled in the relevant art possesses, can also makes a variety of changes under the prerequisite not departing from this patent aim.
Claims (3)
1. a macromolecule extract and separate machine, comprise and throw liquid mouth, extraction box, thermometer, heat block, supersonic generator, recrystallization case, wire netting, heater, lower floor's extract collecting box, timer, pump and upper layer of extraction liquid collecting box, it is characterized in that, described extraction box top is provided with throws liquid mouth, extraction box is provided with thermometer and timer, heat block is provided with in extraction box, supersonic generator is provided with in extraction box, extraction box lower end is provided with lower floor's extract transfer tube, lower floor's extract transfer tube is provided with switch, lower floor's extract transfer tube bottom is provided with recrystallization case, recrystallization case is connected with lower floor extract collecting box by appendix, recrystallization case lower end is provided with heater, upper layer of extraction liquid collecting box is connected with extraction box by upper layer of extraction liquid transfer tube, upper layer of extraction liquid transfer tube arrival end is provided with filter screen, installation pump on upper layer of extraction liquid transfer tube.
2. a kind of macromolecule extract and separate machine according to claim 1, is characterized in that, be provided with wire netting between described recrystallization case and heater.
3. a kind of macromolecule extract and separate machine according to claim 1, is characterized in that, described upper layer of extraction liquid transfer tube arrival end is arranged in extraction box.
Priority Applications (1)
Application Number | Priority Date | Filing Date | Title |
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CN201520525993.4U CN204865075U (en) | 2015-07-20 | 2015-07-20 | Polymer extraction separating centrifuge |
Applications Claiming Priority (1)
Application Number | Priority Date | Filing Date | Title |
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CN201520525993.4U CN204865075U (en) | 2015-07-20 | 2015-07-20 | Polymer extraction separating centrifuge |
Publications (1)
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CN204865075U true CN204865075U (en) | 2015-12-16 |
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CN201520525993.4U Expired - Fee Related CN204865075U (en) | 2015-07-20 | 2015-07-20 | Polymer extraction separating centrifuge |
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Cited By (3)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
CN106474767A (en) * | 2016-12-27 | 2017-03-08 | 郑州艾莫弗信息技术有限公司 | A kind of efficient chemical industry extraction and stripping apparatus |
CN106474766A (en) * | 2016-11-30 | 2017-03-08 | 广东技术师范学院 | A kind of sucralose low energy consumption extraction equipment |
CN111995568A (en) * | 2020-09-15 | 2020-11-27 | 北京六合宁远科技有限公司 | Preparation method of poly-substituted fluorine-containing hexa-heterocyclic methylamine with protection groups |
-
2015
- 2015-07-20 CN CN201520525993.4U patent/CN204865075U/en not_active Expired - Fee Related
Cited By (4)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
CN106474766A (en) * | 2016-11-30 | 2017-03-08 | 广东技术师范学院 | A kind of sucralose low energy consumption extraction equipment |
CN106474767A (en) * | 2016-12-27 | 2017-03-08 | 郑州艾莫弗信息技术有限公司 | A kind of efficient chemical industry extraction and stripping apparatus |
CN111995568A (en) * | 2020-09-15 | 2020-11-27 | 北京六合宁远科技有限公司 | Preparation method of poly-substituted fluorine-containing hexa-heterocyclic methylamine with protection groups |
CN111995568B (en) * | 2020-09-15 | 2022-04-05 | 北京六合宁远科技有限公司 | Preparation method of poly-substituted fluorine-containing hexa-heterocyclic methylamine with protection groups |
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Legal Events
Date | Code | Title | Description |
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C14 | Grant of patent or utility model | ||
GR01 | Patent grant | ||
CF01 | Termination of patent right due to non-payment of annual fee |
Granted publication date: 20151216 Termination date: 20160720 |
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CF01 | Termination of patent right due to non-payment of annual fee |