CN204865075U - Polymer extraction separating centrifuge - Google Patents

Polymer extraction separating centrifuge Download PDF

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Publication number
CN204865075U
CN204865075U CN201520525993.4U CN201520525993U CN204865075U CN 204865075 U CN204865075 U CN 204865075U CN 201520525993 U CN201520525993 U CN 201520525993U CN 204865075 U CN204865075 U CN 204865075U
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CN
China
Prior art keywords
extraction
extract
box
lower floor
extraction box
Prior art date
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Expired - Fee Related
Application number
CN201520525993.4U
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Chinese (zh)
Inventor
赵春山
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Harbin University of Science and Technology
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Harbin University of Science and Technology
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Priority to CN201520525993.4U priority Critical patent/CN204865075U/en
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Publication of CN204865075U publication Critical patent/CN204865075U/en
Expired - Fee Related legal-status Critical Current
Anticipated expiration legal-status Critical

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Abstract

The utility model discloses a polymer extraction separating centrifuge, including throwing liquid mouth, extraction box, thermometer, heating piece, supersonic generator, heavy crystal case, wire netting, heater, lower floor's extract collecting box, time -recorder, pump and upper extract collecting box, the extraction box on be equipped with thermometer and time -recorder, be equipped with heating piece in the extraction box, be equipped with supersonic generator in the extraction box, the extraction box lower extreme passes through lower floor's extract transmission pipe to be connected with the heavy crystal case, the heavy crystal case passes through the gas -supply pipe to be connected with lower floor extract collecting box, upper extract collecting box passes through upper extract to be transmitted to manage and is connected with the extraction box. The utility model discloses the temperature of the interior solution of extraction box is monitored at any time to the thermometer, and the time -recorder writes down the extraction time, guarantees the reaction degree of accuracy, and a heating quickening reaction time and extraction speed, supersonic generator make and react more thoroughly, and wire netting assurance heating is even, collects and attendes lower floor's extract, avoids extravagant, simple structure, convenient to use.

Description

A kind of macromolecule extract and separate machine
Technical field
The utility model relates to a kind of chemical device, specifically a kind of macromolecule extract and separate machine.
Background technology
Usually need separate substance in chemical experiment, extract a kind of method often commonly used.Extraction utilizes materialin two kinds of immiscible or sl. sol. solvents solubility or distribution coefficientdifference, make solute substance in a kind of solvent, transfer to method another solvent.Control degree during extract and separate inaccurate, need manually to rock solution, be separated not thorough, difficulty during separatory.
Summary of the invention
The purpose of this utility model is to provide a kind of macromolecule extract and separate machine, to solve the problem proposed in above-mentioned background technology.
For achieving the above object, the utility model provides following technical scheme:
A kind of macromolecule extract and separate machine, comprise and throw liquid mouth, extraction box, thermometer, heat block, supersonic generator, recrystallization case, wire netting, heater, lower floor's extract collecting box, timer, pump and upper layer of extraction liquid collecting box, described extraction box top is provided with throws liquid mouth, extraction box is provided with thermometer and timer, heat block is provided with in extraction box, supersonic generator is provided with in extraction box, extraction box lower end is provided with lower floor's extract transfer tube, lower floor's extract transfer tube is provided with switch, lower floor's extract transfer tube bottom is provided with recrystallization case, recrystallization case is connected with lower floor extract collecting box by appendix, recrystallization case lower end is provided with heater, upper layer of extraction liquid collecting box is connected with extraction box by upper layer of extraction liquid transfer tube, upper layer of extraction liquid transfer tube arrival end is provided with filter screen, installation pump on upper layer of extraction liquid transfer tube.
As further program of the utility model: be provided with wire netting between described recrystallization case and heater.
As the utility model further scheme: described upper layer of extraction liquid transfer tube arrival end is arranged in extraction box.
Compared with prior art, the beneficial effects of the utility model are: the temperature of solution in extraction box monitored at any time by the utility model thermometer, timer record extraction time, ensure the reaction degree of accuracy, heat block heated solution is to suitable temperature, and accelerate reaction time and extraction rate, supersonic generator sends ultrasonic wave for agitating solution, make reaction more thorough, wire netting ensures homogeneous heating, collects levels extract, avoids waste, structure is simple, easy to use.
Accompanying drawing explanation
Fig. 1 is a kind of structural representation of macromolecule extract and separate machine.
In figure: 1, throw liquid mouth, 2, extraction box, 3, thermometer, 4, heat block, 5, supersonic generator, 6, switch, 7, lower floor's extract transfer tube, 8, recrystallization case, 9, wire netting, 10, heater, 11, appendix, 12, lower floor's extract collecting box, 13, filter screen, 14, timer, 15, pump, 16, upper layer of extraction liquid collecting box, 17, upper layer of extraction liquid transfer tube.
Detailed description of the invention
Be described in more detail below in conjunction with the technical scheme of detailed description of the invention to this patent.
Refer to Fig. 1, a kind of macromolecule extract and separate machine, comprise and throw liquid mouth 1, extraction box 2, thermometer 3, heat block 4, supersonic generator 5, recrystallization case 8, wire netting 9, heater 10, lower floor's extract collecting box 12, timer 14, pump 15 and upper layer of extraction liquid collecting box 16, described extraction box 2 top is provided with throws liquid mouth 1, solution is knocked down in extraction box 2 from throwing liquid mouth 1, extraction box 2 is provided with thermometer 3 and timer 14, the temperature of solution in extraction box 2 monitored at any time by thermometer 3, timer 14 records extraction time, ensure the reaction degree of accuracy, heat block 4 is provided with in extraction box 2, heat block 4 heated solution is to suitable temperature, accelerate reaction time and extraction rate, supersonic generator 5 is provided with in extraction box 2, supersonic generator 5 sends ultrasonic wave for agitating solution, make reaction more thorough, extraction box 2 lower end is provided with lower floor's extract transfer tube 7, lower floor's extract transfer tube 7 is provided with switch 6, lower floor's extract transfer tube 7 bottom is provided with recrystallization case 8, by-pass cock 6 makes lower floor's extract flow into recrystallization case 8 from lower floor's extract transfer tube 7, recrystallization case 8 is connected with lower floor extract collecting box 12 by appendix 11, recrystallization case 8 lower end is provided with heater 10, wire netting 9 is provided with between recrystallization case 8 and heater 10, wire netting 9 ensures homogeneous heating, add hot recrystallization case 8, make lower floor's extract volatilization, recrystallization separates out material in solution, lower floor's extract enters lower floor's extract collecting box 12 and collects, upper layer of extraction liquid collecting box 16 is connected with extraction box 2 by upper layer of extraction liquid transfer tube 17, upper layer of extraction liquid transfer tube 17 arrival end is arranged in extraction box 2, upper layer of extraction liquid transfer tube 17 arrival end is provided with filter screen 13, installation pump 15 on upper layer of extraction liquid transfer tube 17, upper layer of extraction liquid enters upper layer of extraction liquid collecting box 16 from upper layer of extraction liquid transfer tube 17 and collects.
Operation principle of the present utility model is: the utility model solution is knocked down in extraction box from throwing liquid mouth, the temperature of solution in extraction box monitored at any time by thermometer, timer record extraction time, ensure the reaction degree of accuracy, heat block heated solution is to suitable temperature, accelerate reaction time and extraction rate, supersonic generator sends ultrasonic wave for agitating solution, make reaction more thorough, by-pass cock makes lower floor's extract flow into recrystallization case from lower floor's extract transfer tube, wire netting ensures homogeneous heating, add hot recrystallization case, make lower floor's extract volatilization, recrystallization separates out material in solution, lower floor's extract enters lower floor's extract collecting box and collects, upper layer of extraction liquid enters upper layer of extraction liquid collecting box from upper layer of extraction liquid transfer tube and collects.
Above the better embodiment of this patent is explained in detail, but this patent is not limited to above-mentioned embodiment, in the ken that one skilled in the relevant art possesses, can also makes a variety of changes under the prerequisite not departing from this patent aim.

Claims (3)

1. a macromolecule extract and separate machine, comprise and throw liquid mouth, extraction box, thermometer, heat block, supersonic generator, recrystallization case, wire netting, heater, lower floor's extract collecting box, timer, pump and upper layer of extraction liquid collecting box, it is characterized in that, described extraction box top is provided with throws liquid mouth, extraction box is provided with thermometer and timer, heat block is provided with in extraction box, supersonic generator is provided with in extraction box, extraction box lower end is provided with lower floor's extract transfer tube, lower floor's extract transfer tube is provided with switch, lower floor's extract transfer tube bottom is provided with recrystallization case, recrystallization case is connected with lower floor extract collecting box by appendix, recrystallization case lower end is provided with heater, upper layer of extraction liquid collecting box is connected with extraction box by upper layer of extraction liquid transfer tube, upper layer of extraction liquid transfer tube arrival end is provided with filter screen, installation pump on upper layer of extraction liquid transfer tube.
2. a kind of macromolecule extract and separate machine according to claim 1, is characterized in that, be provided with wire netting between described recrystallization case and heater.
3. a kind of macromolecule extract and separate machine according to claim 1, is characterized in that, described upper layer of extraction liquid transfer tube arrival end is arranged in extraction box.
CN201520525993.4U 2015-07-20 2015-07-20 Polymer extraction separating centrifuge Expired - Fee Related CN204865075U (en)

Priority Applications (1)

Application Number Priority Date Filing Date Title
CN201520525993.4U CN204865075U (en) 2015-07-20 2015-07-20 Polymer extraction separating centrifuge

Applications Claiming Priority (1)

Application Number Priority Date Filing Date Title
CN201520525993.4U CN204865075U (en) 2015-07-20 2015-07-20 Polymer extraction separating centrifuge

Publications (1)

Publication Number Publication Date
CN204865075U true CN204865075U (en) 2015-12-16

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Family Applications (1)

Application Number Title Priority Date Filing Date
CN201520525993.4U Expired - Fee Related CN204865075U (en) 2015-07-20 2015-07-20 Polymer extraction separating centrifuge

Country Status (1)

Country Link
CN (1) CN204865075U (en)

Cited By (3)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN106474767A (en) * 2016-12-27 2017-03-08 郑州艾莫弗信息技术有限公司 A kind of efficient chemical industry extraction and stripping apparatus
CN106474766A (en) * 2016-11-30 2017-03-08 广东技术师范学院 A kind of sucralose low energy consumption extraction equipment
CN111995568A (en) * 2020-09-15 2020-11-27 北京六合宁远科技有限公司 Preparation method of poly-substituted fluorine-containing hexa-heterocyclic methylamine with protection groups

Cited By (4)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN106474766A (en) * 2016-11-30 2017-03-08 广东技术师范学院 A kind of sucralose low energy consumption extraction equipment
CN106474767A (en) * 2016-12-27 2017-03-08 郑州艾莫弗信息技术有限公司 A kind of efficient chemical industry extraction and stripping apparatus
CN111995568A (en) * 2020-09-15 2020-11-27 北京六合宁远科技有限公司 Preparation method of poly-substituted fluorine-containing hexa-heterocyclic methylamine with protection groups
CN111995568B (en) * 2020-09-15 2022-04-05 北京六合宁远科技有限公司 Preparation method of poly-substituted fluorine-containing hexa-heterocyclic methylamine with protection groups

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Date Code Title Description
C14 Grant of patent or utility model
GR01 Patent grant
CF01 Termination of patent right due to non-payment of annual fee

Granted publication date: 20151216

Termination date: 20160720

CF01 Termination of patent right due to non-payment of annual fee