CN106433919A - Tantalum alloy col-upsetting process lubricant composition - Google Patents
Tantalum alloy col-upsetting process lubricant composition Download PDFInfo
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- C10M—LUBRICATING COMPOSITIONS; USE OF CHEMICAL SUBSTANCES EITHER ALONE OR AS LUBRICATING INGREDIENTS IN A LUBRICATING COMPOSITION
- C10M169/00—Lubricating compositions characterised by containing as components a mixture of at least two types of ingredient selected from base-materials, thickeners or additives, covered by the preceding groups, each of these compounds being essential
- C10M169/04—Mixtures of base-materials and additives
- C10M169/048—Mixtures of base-materials and additives the additives being a mixture of compounds of unknown or incompletely defined constitution, non-macromolecular and macromolecular compounds
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- C10M—LUBRICATING COMPOSITIONS; USE OF CHEMICAL SUBSTANCES EITHER ALONE OR AS LUBRICATING INGREDIENTS IN A LUBRICATING COMPOSITION
- C10M2205/00—Organic macromolecular hydrocarbon compounds or fractions, whether or not modified by oxidation as ingredients in lubricant compositions
- C10M2205/02—Organic macromolecular hydrocarbon compounds or fractions, whether or not modified by oxidation as ingredients in lubricant compositions containing acyclic monomers
- C10M2205/026—Butene
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- C10M2209/00—Organic macromolecular compounds containing oxygen as ingredients in lubricant compositions
- C10M2209/02—Macromolecular compounds obtained by reactions only involving carbon-to-carbon unsaturated bonds
- C10M2209/08—Macromolecular compounds obtained by reactions only involving carbon-to-carbon unsaturated bonds containing monomers having an unsaturated radical bound to a carboxyl radical, e.g. acrylate type
- C10M2209/084—Acrylate; Methacrylate
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- C10M2209/00—Organic macromolecular compounds containing oxygen as ingredients in lubricant compositions
- C10M2209/10—Macromolecular compoundss obtained otherwise than by reactions only involving carbon-to-carbon unsaturated bonds
- C10M2209/103—Polyethers, i.e. containing di- or higher polyoxyalkylene groups
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- C10M2211/00—Organic non-macromolecular compounds containing halogen as ingredients in lubricant compositions
- C10M2211/08—Halogenated waxes
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- C10M2215/00—Organic non-macromolecular compounds containing nitrogen as ingredients in lubricant compositions
- C10M2215/02—Amines, e.g. polyalkylene polyamines; Quaternary amines
- C10M2215/04—Amines, e.g. polyalkylene polyamines; Quaternary amines having amino groups bound to acyclic or cycloaliphatic carbon atoms
- C10M2215/042—Amines, e.g. polyalkylene polyamines; Quaternary amines having amino groups bound to acyclic or cycloaliphatic carbon atoms containing hydroxy groups; Alkoxylated derivatives thereof
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- C10M2215/00—Organic non-macromolecular compounds containing nitrogen as ingredients in lubricant compositions
- C10M2215/22—Heterocyclic nitrogen compounds
- C10M2215/223—Five-membered rings containing nitrogen and carbon only
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- C10M2219/00—Organic non-macromolecular compounds containing sulfur, selenium or tellurium as ingredients in lubricant compositions
- C10M2219/04—Organic non-macromolecular compounds containing sulfur, selenium or tellurium as ingredients in lubricant compositions containing sulfur-to-oxygen bonds, i.e. sulfones, sulfoxides
- C10M2219/044—Sulfonic acids, Derivatives thereof, e.g. neutral salts
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- C10M2219/00—Organic non-macromolecular compounds containing sulfur, selenium or tellurium as ingredients in lubricant compositions
- C10M2219/06—Thio-acids; Thiocyanates; Derivatives thereof
- C10M2219/062—Thio-acids; Thiocyanates; Derivatives thereof having carbon-to-sulfur double bonds
- C10M2219/066—Thiocarbamic type compounds
- C10M2219/068—Thiocarbamate metal salts
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- C10M2219/00—Organic non-macromolecular compounds containing sulfur, selenium or tellurium as ingredients in lubricant compositions
- C10M2219/08—Thiols; Sulfides; Polysulfides; Mercaptals
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- C10M2219/00—Organic non-macromolecular compounds containing sulfur, selenium or tellurium as ingredients in lubricant compositions
- C10M2219/10—Heterocyclic compounds containing sulfur, selenium or tellurium compounds in the ring
- C10M2219/104—Heterocyclic compounds containing sulfur, selenium or tellurium compounds in the ring containing sulfur and carbon with nitrogen or oxygen in the ring
- C10M2219/106—Thiadiazoles
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- C10M2223/00—Organic non-macromolecular compounds containing phosphorus as ingredients in lubricant compositions
- C10M2223/06—Organic non-macromolecular compounds containing phosphorus as ingredients in lubricant compositions having phosphorus-to-carbon bonds
- C10M2223/065—Organic non-macromolecular compounds containing phosphorus as ingredients in lubricant compositions having phosphorus-to-carbon bonds containing sulfur
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- C10M2227/00—Organic non-macromolecular compounds containing atoms of elements not provided for in groups C10M2203/00, C10M2207/00, C10M2211/00, C10M2215/00, C10M2219/00 or C10M2223/00 as ingredients in lubricant compositions
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- C10M2229/00—Organic macromolecular compounds containing atoms of elements not provided for in groups C10M2205/00, C10M2209/00, C10M2213/00, C10M2217/00, C10M2221/00 or C10M2225/00 as ingredients in lubricant compositions
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- C10N—INDEXING SCHEME ASSOCIATED WITH SUBCLASS C10M RELATING TO LUBRICATING COMPOSITIONS
- C10N2030/00—Specified physical or chemical properties which is improved by the additive characterising the lubricating composition, e.g. multifunctional additives
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- C10N2030/00—Specified physical or chemical properties which is improved by the additive characterising the lubricating composition, e.g. multifunctional additives
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- C10N2030/00—Specified physical or chemical properties which is improved by the additive characterising the lubricating composition, e.g. multifunctional additives
- C10N2030/10—Inhibition of oxidation, e.g. anti-oxidants
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- C10N2030/00—Specified physical or chemical properties which is improved by the additive characterising the lubricating composition, e.g. multifunctional additives
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- C10N2030/18—Anti-foaming property
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- C10N2030/00—Specified physical or chemical properties which is improved by the additive characterising the lubricating composition, e.g. multifunctional additives
- C10N2030/56—Boundary lubrication or thin film lubrication
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- C10N2040/00—Specified use or application for which the lubricating composition is intended
- C10N2040/20—Metal working
- C10N2040/24—Metal working without essential removal of material, e.g. forming, gorging, drawing, pressing, stamping, rolling or extruding; Punching metal
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Abstract
The invention discloses a tantalum alloy col-upsetting process lubricant composition which adopts VHVI12 base oil as base oil and cooperates with a variety of composite additives. The tantalum alloy col-upsetting process lubricant composition is prepared from an antioxidant, a metal deactivator, an anti-rust agent, an oily agent, a friction improver, an extreme pressure agent, an anti-abrasion agent, an antifoaming agent, a dispersant, an adhesive, an oxidation and corrosion inhibitor and the like. The composition has good bearing and abrasion resistance properties, compression resistance, low-temperature flow diffusivity, lubricity and cooling performance, an oil film is high in strength, oil film thickness is kept stable, no peculiar smell is produced, the composition is non-irritant to the skin, the roughness can be improved, the surfaces of machined parts are protected against rusting and oxidation, power consumption is reduced, the low-temperature fluidity is good, anti-foaming, demulsibility and thermal oxidation stability are good, production of precipitates and paint films is reduced, and formed parts are easy to clean.
Description
Technical field
A kind of present invention tantalum alloy cold heading technique lubricant compositions belong to metal working lubricant field.
Background technology
Tantalum, metallic element, the quality of tantalum is very hard, and hardness can reach 6-6.5.Up to 2996 DEG C of its fusing point.Main
In tantalite to be present in, with niobium symbiosis.The quality of tantalum is very hard, and tantalum is rich in ductility, can pull into filament formula thin foil.
Its thermal coefficient of expansion very little.Tantalum has very outstanding chemical property, has high corrosion resistance.Either in cold and hot bar
Under part, hydrochloric acid, red fuming nitric acid (RFNA) and " chloroazotic acid " are not reacted.May be utilized in fabricating evaporator boat etc., also can do the electrode of electron tube, whole
Stream device, electrolysis, electric capacity.Medically it is used for laminating or fine rule, the tissue that destroy is sewed and mend.The characteristic that tantalum has, makes its
Application is very wide.In the equipment producing various inorganic acids, tantalum can be substituted for stainless steel, and the life-span carries than stainless steel
High tens times.Additionally, chemical industry, electronics, electrically etc. in industry, tantalum can replace needs in the past by precious metal platinum undertake times
Business, makes required expense substantially reduce.Tantalum has been manufactured into electric capacity and has been provided in military equipment.Tantalum be rare metal mineral products resource it
One, it is electronics industry and the space technology indispensable strategic material of development.
Cold-heading processing is the forging method at normal temperatures metal bar material jumping-up (often for gathering stock) being shaped using mould.
Cold-heading is another form of upsetting.More metal mold becomes theoretical, applies certain pressure to metal stock at normal temperatures,
It is allowed to be deformed in die cavity.Shape by the shape and size of regulation.Cold heading technique is widely used in middle finding and various
The standard component of type.
Cold heading technique be mainly characterized by no machining, stock utilization is high, and utilization rate reaches 80~90%, and metal material
Stream line will not be cut off, and therefore product intensity is higher than machining or casting part strength, in certain batch life
Under the conditions of product, cold-heading processing cost more much lower than other processing costs it is adaptable to typically require cutting members and securing member etc.
The Product processing of symmetrical shape.The dimensional accuracy of product, weight accuracy and mechanical property etc. are attained by higher requirement.
Lubricant should have the special feature that:Good carrying wear resistence, Squeezing ground (not plucking, pull, effectively extend punch die
Service life), low temperature flow diffusivity, lubricity, cooling, film strength is big, oil film thickness keeps stable, free from extraneous odour, no
Stimulate skin etc..Improve fineness, protect part to be processed surface not corrosion and oxidation, reduce power consumption, low temperature flow
Well, good anti-foaming property, resistance to emulsion, thermal oxide are qualitative good, reduce the generation of sediment and paint film, profiled member easy cleaning.
Content of the invention
The technical problem to be solved in the present invention is that offer is a kind of has good carrying wear resistence, Squeezing ground, low temperature flow
Diffusivity, lubricity, cooling, film strength is big, oil film thickness keeps stable, free from extraneous odour, does not stimulate skin, can improve bright and clean
Degree, protect part to be processed surface not corrosion and oxidation, minimizing power consumption, and low temperature flow is good, good anti-foaming property, anti-breast
The property changed, thermal oxide are qualitative good, reduce the generation of sediment and paint film, the tantalum alloy cold heading technique lubricant group of profiled member easy cleaning
Compound.
The present invention employs the following technical solutions solution above-mentioned technical problem:
A kind of tantalum alloy cold heading technique lubricant compositions, using oil based on VHVI 12 base oil, cooperation is multiple multiple
Close additive, the one-tenth of its respective mass percent is grouped into:
Component | Mass percentage content |
Base oil | Surplus |
Antioxidant | 0.05%~0.4% |
Metal deactivator | 0.03%~0.2% |
Antirust agent | 0.03%~0.3% |
Oiliness improver | 3%~8% |
Friction improver | 0.3%~1.5% |
Extreme pressure agent | 3%~5% |
Antiwear additive | 5%~8% |
Anti-foaming agent | 10~50ppm |
Dispersant | 2~4% |
Adhesive | 3~8% |
Oxidation and corrosion inhibitor | 0.3~0.8% |
Each constituent mass percentage summation is 100% above.
Antioxidant be the cupric antioxidant T543 of mass ratio 50% and 50% 2,6- di-t-butyl-α dimethylamino to first
Phenol T521's is compound;Metal deactivator is the benzotriazole derivative T551 of mass ratio 50% and 50% thiadiazoles derivative T561
Compound.
Antirust agent be the barium dinonyl napthalene sulphonate T705A of mass ratio 50% and 50% benzotriazole T706 compound
Thing.
Oiliness improver is sulfurized lard;Friction improver is dialkyldithiocarbamacompositions tungsten.
Extreme pressure agent is boronation phosphamidon ester T3011.
Antiwear additive is chlorinated paraffin T301;Anti-foaming agent is acrylic acid and ether copolymer T912.
Dispersant is boronation polyisobutene succinimide T154B.
Adsorbent is polyisobutene T603D.
Oxidation and corrosion inhibitor is double octyl group basic zinc salt T203 of sulphur phosphorus.
The beneficial effects of the present invention is:Tantalum alloy cold heading technique lubricant of the present invention have good carrying wear resistence,
Squeezing ground (not plucking, the service life pulled, effectively extend punch die), low temperature flow diffusivity, lubricity, cooling, oil film
Intensity is big, oil film thickness keeps stable, free from extraneous odour, does not stimulate skin etc..Improve fineness, protection part to be processed surface is stainless
Erosion and aoxidizing, reduces power consumption, low temperature flow is good, and good anti-foaming property, resistance to emulsion, thermal oxide are qualitative good, and it is heavy to reduce
Starch and the generation of paint film, profiled member easy cleaning.
Specific embodiment
Embodiment 1:
Following component is in harmonious proportion by mass percentage and forms:
Each constituent mass percentage summation is 100% above.
Embodiment 2:
Following component is in harmonious proportion by mass percentage and forms:
Each constituent mass percentage summation is 100% above.
Embodiment 3:Following component is in harmonious proportion by mass percentage and forms:
Each constituent mass percentage summation is 100% above.
Embodiment 2 product typical technology index:
Project | Index |
100 DEG C of kinematic viscosity mm2/s | 12.5 |
Flash-point (opening)/DEG C | 255 |
Pour point/DEG C | -16 |
Viscosity index (VI) | 131 |
Coefficient of friction | 0.09 |
Corrosion experiment (copper sheet, 100 DEG C, 3h)/level | 1 |
Oxidation stability (Rotary Oxygen elasticity, 150 DEG C) min | 420 |
FZG, level | 14 |
Tetra-ball machine test Pb/N | 952 |
Tetra-ball machine test PD/N | 8280 |
Terraced nurse agrees/N | 330 |
24 DEG C of foaming characteristics test | 300/0 |
96℃ | 200/0 |
24 DEG C afterwards | 200/0 |
Evaporation loss (Angelika Noack method, 250 DEG C, 1h) (m) % | 11 |
Mechanical admixture, % | No |
Moisture, % | Vestige |
Water-soluble acid and alkali | No |
Saturated hydrocarbons (m) % | 97 |
82 DEG C of demulsification number (40 37 3), min | 13 |
Claims (9)
1. a kind of tantalum alloy cold heading technique lubricant compositions it is characterised in that:Using oil based on VHVI 12 base oil,
Coordinate multiple compound additives, the one-tenth of its respective mass percent is grouped into:
Each constituent mass percentage summation is 100% above.
2. as claimed in claim 1 a kind of tantalum alloy cold heading technique lubricant compositions it is characterised in that antioxidant is quality
Cupric antioxidant T543 than 50% and 50% 2,6- di-t-butyl-α dimethylamino-p-cresol T521 compound;Metal deactivating
Agent be the benzotriazole derivative T551 of mass ratio 50% and 50% thiadiazoles derivative T561 compound.
3. as claimed in claim 1 a kind of tantalum alloy cold heading technique lubricant compositions it is characterised in that antirust agent is quality
Barium dinonyl napthalene sulphonate T705A than 50% and 50% benzotriazole T706 compound.
4. as claimed in claim 1 a kind of tantalum alloy cold heading technique lubricant compositions it is characterised in that oiliness improver be sulfuration
Lard;Friction improver is dialkyldithiocarbamacompositions tungsten.
5. as claimed in claim 1 a kind of tantalum alloy cold heading technique lubricant compositions it is characterised in that extreme pressure agent is boronation
Phosphamidon ester T3011.
6. as claimed in claim 1 a kind of tantalum alloy cold heading technique lubricant compositions it is characterised in that antiwear additive is chlorination
Paraffin T301;Anti-foaming agent is acrylic acid and ether copolymer T912.
7. as claimed in claim 1 a kind of tantalum alloy cold heading technique lubricant compositions it is characterised in that dispersant is boronation
Polyisobutene succinimide T154B.
8. as claimed in claim 1 a kind of tantalum alloy cold heading technique lubricant compositions it is characterised in that adsorbent is poly- different
Butylene T603D.
9. as claimed in claim 1 a kind of tantalum alloy cold heading technique lubricant compositions it is characterised in that oxidation and corrosion inhibitor is
Double octyl group basic zinc salt T203 of sulphur phosphorus.
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CN104403738A (en) * | 2014-09-30 | 2015-03-11 | 宁波保润石化有限公司 | Multi-station cold heading oil and preparation method thereof |
CN104962368A (en) * | 2015-07-20 | 2015-10-07 | 广西大学 | Rhenium bar rotary-swaging lubricant composition |
CN105132092A (en) * | 2015-07-20 | 2015-12-09 | 广西大学 | Lubricant composition for Al-Mg alloy precision die forging |
CN105238519A (en) * | 2015-10-19 | 2016-01-13 | 中国石油化工股份有限公司 | Lubricant composition and application thereof |
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2016
- 2016-09-21 CN CN201610839024.5A patent/CN106433919A/en active Pending
Patent Citations (4)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
CN104403738A (en) * | 2014-09-30 | 2015-03-11 | 宁波保润石化有限公司 | Multi-station cold heading oil and preparation method thereof |
CN104962368A (en) * | 2015-07-20 | 2015-10-07 | 广西大学 | Rhenium bar rotary-swaging lubricant composition |
CN105132092A (en) * | 2015-07-20 | 2015-12-09 | 广西大学 | Lubricant composition for Al-Mg alloy precision die forging |
CN105238519A (en) * | 2015-10-19 | 2016-01-13 | 中国石油化工股份有限公司 | Lubricant composition and application thereof |
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Application publication date: 20170222 |