CN106431074A - Lightweight thermal-insulation fireproof material and preparation method thereof - Google Patents
Lightweight thermal-insulation fireproof material and preparation method thereof Download PDFInfo
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- CN106431074A CN106431074A CN201610760854.9A CN201610760854A CN106431074A CN 106431074 A CN106431074 A CN 106431074A CN 201610760854 A CN201610760854 A CN 201610760854A CN 106431074 A CN106431074 A CN 106431074A
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Classifications
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- C—CHEMISTRY; METALLURGY
- C04—CEMENTS; CONCRETE; ARTIFICIAL STONE; CERAMICS; REFRACTORIES
- C04B—LIME, MAGNESIA; SLAG; CEMENTS; COMPOSITIONS THEREOF, e.g. MORTARS, CONCRETE OR LIKE BUILDING MATERIALS; ARTIFICIAL STONE; CERAMICS; REFRACTORIES; TREATMENT OF NATURAL STONE
- C04B26/00—Compositions of mortars, concrete or artificial stone, containing only organic binders, e.g. polymer or resin concrete
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- C—CHEMISTRY; METALLURGY
- C04—CEMENTS; CONCRETE; ARTIFICIAL STONE; CERAMICS; REFRACTORIES
- C04B—LIME, MAGNESIA; SLAG; CEMENTS; COMPOSITIONS THEREOF, e.g. MORTARS, CONCRETE OR LIKE BUILDING MATERIALS; ARTIFICIAL STONE; CERAMICS; REFRACTORIES; TREATMENT OF NATURAL STONE
- C04B2111/00—Mortars, concrete or artificial stone or mixtures to prepare them, characterised by specific function, property or use
- C04B2111/00474—Uses not provided for elsewhere in C04B2111/00
- C04B2111/00482—Coating or impregnation materials
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- C—CHEMISTRY; METALLURGY
- C04—CEMENTS; CONCRETE; ARTIFICIAL STONE; CERAMICS; REFRACTORIES
- C04B—LIME, MAGNESIA; SLAG; CEMENTS; COMPOSITIONS THEREOF, e.g. MORTARS, CONCRETE OR LIKE BUILDING MATERIALS; ARTIFICIAL STONE; CERAMICS; REFRACTORIES; TREATMENT OF NATURAL STONE
- C04B2111/00—Mortars, concrete or artificial stone or mixtures to prepare them, characterised by specific function, property or use
- C04B2111/20—Resistance against chemical, physical or biological attack
- C04B2111/28—Fire resistance, i.e. materials resistant to accidental fires or high temperatures
-
- C—CHEMISTRY; METALLURGY
- C04—CEMENTS; CONCRETE; ARTIFICIAL STONE; CERAMICS; REFRACTORIES
- C04B—LIME, MAGNESIA; SLAG; CEMENTS; COMPOSITIONS THEREOF, e.g. MORTARS, CONCRETE OR LIKE BUILDING MATERIALS; ARTIFICIAL STONE; CERAMICS; REFRACTORIES; TREATMENT OF NATURAL STONE
- C04B2111/00—Mortars, concrete or artificial stone or mixtures to prepare them, characterised by specific function, property or use
- C04B2111/40—Porous or lightweight materials
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- Chemical & Material Sciences (AREA)
- Engineering & Computer Science (AREA)
- Ceramic Engineering (AREA)
- Materials Engineering (AREA)
- Structural Engineering (AREA)
- Organic Chemistry (AREA)
- Fireproofing Substances (AREA)
Abstract
The invention relates to a lightweight thermal-insulation fireproof material and a preparation method thereof; the lightweight thermal-insulation fireproof material comprises the components in parts by weight: 10 parts-30 parts of distilled water, 10 parts-20 parts of a water-based emulsion, 30 parts-50 parts of ammonium polyphosphate, 18 parts-24 parts of nano titanium dioxide, 10 parts-20 parts of a black mud powder, 5 parts-10 parts of sepiolite, 5 parts-10 parts of a zirconium silicate powder or a yttrium stabilized zirconia powder, 5 parts-10 parts of expanded perlite, 2 parts-5 parts of polyester fibers, 3 parts-7 parts of a film-forming auxiliary agent, 1 part-2 parts of citric acid, 1 part-2 parts of expandable graphite, and 0.2 part-0.6 part of kaolin. The fireproof material has the characteristics of high temperature resistance, sintering cracking resistance, no toxicity, no odor, green and environmental protection, good decorative performance, and convenient construction, can be spray-brushed, and can keep an original shape of a base material.
Description
Technical field
The present invention relates to new material technology field is and in particular to a kind of light insulating fire proof weight material and preparation method thereof.
Background technology
With the aggravation of global warming, people focus on mostly be building effect of heat insulation, can stop during the broiling summer
Outdoor temperature, and the effect of indoor heat insulating when using air-conditioning or heating installation, can be reached again.Along with people, building energy-saving is anticipated
The continuous improvement known, the requirement to building thermal insulation material and fire proofing material significantly increases, and provides a kind of fire proofing wood of environment-friendly light
Material is current research emphasis.
Content of the invention
The technical problem to be solved is for the deficiencies in the prior art, provide a kind of environment-friendly fireproof material and
Its preparation method.
The technical scheme that the present invention solves above-mentioned technical problem is as follows：A kind of light insulating fire proof weight material, in parts by weight,
Including 10 parts of -30 parts of distilled water, 10 parts of -20 parts of water-based emulsions, 30 parts of -50 parts of ammonium polyphosphates, 18 parts of -24 parts of Nanometer Titanium Dioxides
Powder, 10 parts -20 parts black mud powder, 5 parts of -10 parts of meerschaums, 5 parts of -10 parts of zirconium silicate powders or yttrium stable zirconium oxide powder, 5 parts -10 parts swollen
Swollen perlite, 2 parts of -5 parts of polyester fibers, 3 parts of -7 parts of coalescents, 1 part of -2 parts of citric acid, 1 part of -2 parts of expansible graphite, 0.2
- 0.6 part of Kaolin of part.
The invention has the beneficial effects as follows：The fire proofing material of the present invention have the characteristics that high temperature resistant, anti-hardening crack, and nontoxic nothing
Taste, environmental protection, decoration performance is good, easy construction, and spary can keep the original appearance of base material.
On the basis of technique scheme, the present invention can also do following improvement.
Further, in parts by weight, including 10 parts of distilled water, 10 parts of water-based emulsions, 30 parts of ammonium polyphosphates, 18 parts of nanometers
Titanium dioxide, 10 parts of black mud powder, 5 parts of meerschaums, 5 parts of zirconium silicate powders or yttrium stable zirconium oxide powder, 5 parts of expanded perlites, 2 parts of polyester
Fiber, 3 parts of coalescents, 1 part of citric acid, 1 part of expansible graphite, 0.2 part of Kaolin.
Further, in parts by weight, including 20 parts of distilled water, 15 parts of water-based emulsions, 40 parts of ammonium polyphosphates, 20 parts of nanometers
Titanium dioxide, 15 parts of black mud powder, 8 parts of meerschaums, 7 parts of zirconium silicate powders or yttrium stable zirconium oxide powder, 8 parts of expanded perlites, 3 parts of polyester
Fiber, 4 parts of coalescents, 1.5 parts of citric acids, 1.5 parts of expansible graphites, 0.4 part of Kaolin.
Further, in parts by weight, including 30 parts of distilled water, 20 parts of water-based emulsions, 50 parts of ammonium polyphosphates, 24 parts of nanometers
Titanium dioxide, 20 parts of black mud powder, 10 parts of meerschaums, 10 parts of zirconium silicate powders or yttrium stable zirconium oxide powder, 10 parts of expanded perlites, 5 parts
Polyester fiber, 7 parts of coalescents, 2 parts of citric acids, 2 parts of expansible graphites, 0.6 part of Kaolin.
A kind of preparation method of light insulating fire proof weight material as above, comprises the following steps：
Step 1), weigh distilled water, nanometer titanium dioxide, ammonium polyphosphate, zirconium silicate powder or yttrium by weight and stably aoxidize
Zirconium powder, citric acid, black mud powder, expanded perlite, polyester fiber and meerschaum, and mix homogeneously obtains mixed liquor；
Step 2), weigh water-based emulsion by weight, and water-based emulsion is added in mixed liquor, stir and make aqueouss
Emulsion evenly spreads in mixed liquor, obtains dispersion liquid；
Step 3), will add coalescents, expansible graphite and Kaolin in dispersion liquid, dispersed 50min-80min,
Filter fill.
The invention has the beneficial effects as follows：The method of the present invention is simple, can reduce the destruction of effective ingredient.
Specific embodiment
Hereinafter the principle and feature of the present invention is described, example is served only for explaining the present invention, is not intended to limit
Determine the scope of the present invention.
Embodiment 1
A kind of light insulating fire proof weight material of the present embodiment, in parts by weight, including 10 parts of distilled water, 10 parts of aqueouss breasts
Liquid, 30 parts of ammonium polyphosphates, 18 parts of nanometer titanium dioxides, 10 parts of black mud powder, 5 parts of meerschaums, 5 parts of zirconium silicate powders or yttrium stably aoxidize
Zirconium powder, 5 parts of expanded perlites, 2 parts of polyester fibers, 3 parts of coalescents, 1 part of citric acid, 1 part of expansible graphite, 0.2 part of kaolinite
Soil.
The fire proofing material of the present embodiment have the characteristics that high temperature resistant, anti-hardening crack, and nonpoisonous and tasteless, environmental protection, ornamental
Good, the easy construction of energy, spary, the original appearance of base material can be kept.
A kind of preparation method of light insulating fire proof weight material of the present embodiment, comprises the following steps：
Step 1), weigh distilled water, nanometer titanium dioxide, ammonium polyphosphate, zirconium silicate powder or yttrium by weight and stably aoxidize
Zirconium powder, citric acid, black mud powder, expanded perlite, polyester fiber and meerschaum, and mix homogeneously obtains mixed liquor；
Step 2), weigh water-based emulsion by weight, and water-based emulsion is added in mixed liquor, stir and make aqueouss
Emulsion evenly spreads in mixed liquor, obtains dispersion liquid；
Step 3), will add coalescents, expansible graphite and Kaolin in dispersion liquid, dispersed 50min-80min,
Filter fill.
The method of the present embodiment is simple, can reduce the destruction of effective ingredient.
Embodiment 2
A kind of light insulating fire proof weight material of embodiment, in parts by weight, including 20 parts of distilled water, 15 parts of water-based emulsions,
40 parts of ammonium polyphosphates, 20 parts of nanometer titanium dioxides, 15 parts of black mud powder, 8 parts of meerschaums, 7 parts of zirconium silicate powders or yttrium stable zirconium oxide
Powder, 8 parts of expanded perlites, 3 parts of polyester fibers, 4 parts of coalescents, 1.5 parts of citric acids, 1.5 parts of expansible graphites, 0.4 part high
Ridge soil.
A kind of preparation method of light insulating fire proof weight material of the present embodiment, comprises the following steps：
Step 1), weigh distilled water, nanometer titanium dioxide, ammonium polyphosphate, zirconium silicate powder or yttrium by weight and stably aoxidize
Zirconium powder, citric acid, black mud powder, expanded perlite, polyester fiber and meerschaum, and mix homogeneously obtains mixed liquor；
Step 2), weigh water-based emulsion by weight, and water-based emulsion is added in mixed liquor, stir and make aqueouss
Emulsion evenly spreads in mixed liquor, obtains dispersion liquid；
Step 3), will add coalescents, expansible graphite and Kaolin in dispersion liquid, dispersed 50min-80min,
Filter fill.
The method of the present embodiment is simple, can reduce the destruction of effective ingredient.
Embodiment 3
A kind of light insulating fire proof weight material of embodiment, in parts by weight, including 30 parts of distilled water, 20 parts of water-based emulsions,
50 parts of ammonium polyphosphates, 24 parts of nanometer titanium dioxides, 20 parts of black mud powder, 10 parts of meerschaums, 10 parts of zirconium silicate powders or yttrium stably aoxidize
Zirconium powder, 10 parts of expanded perlites, 5 parts of polyester fibers, 7 parts of coalescents, 2 parts of citric acids, 2 parts of expansible graphites, 0.6 part of kaolinite
Soil.
A kind of preparation method of light insulating fire proof weight material of the present embodiment, comprises the following steps：
Step 1), weigh distilled water, nanometer titanium dioxide, ammonium polyphosphate, zirconium silicate powder or yttrium by weight and stably aoxidize
Zirconium powder, citric acid, black mud powder, expanded perlite, polyester fiber and meerschaum, and mix homogeneously obtains mixed liquor；
Step 2), weigh water-based emulsion by weight, and water-based emulsion is added in mixed liquor, stir and make aqueouss
Emulsion evenly spreads in mixed liquor, obtains dispersion liquid；
Step 3), will add coalescents, expansible graphite and Kaolin in dispersion liquid, dispersed 50min-80min,
Filter fill.
The method of the present embodiment is simple, can reduce the destruction of effective ingredient.
The resistance to elevated temperatures of the light insulating fire proof weight material in embodiment 1-3 is tested.Example 1-3 institute respectively
Then fire proofing material A-C is coated in wall by the fire proofing material stated, respectively fire proofing material A, fire proofing material B, fire proofing material C
One side on, and using identical temperature, high-temperature heating is carried out to the another side of wall and heat time heating time is identical, heating temperature
Spend for 150 DEG C, heat time heating time is 2h.Then the temperature of the another side of waterproof material is detected, testing result such as table 1 institute
Show.
The fire protecting performance of table 1 fire proofing material
As shown in Table 1, the fire proofing material of the present embodiment can fire-proof and thermal-insulation effect good.
The foregoing is only presently preferred embodiments of the present invention, not in order to limit the present invention, all spirit in the present invention and
Within principle, any modification, equivalent substitution and improvement made etc., should be included within the scope of the present invention.
Claims (5)
1. a kind of light insulating fire proof weight material is it is characterised in that in parts by weight, including 10 parts of -30 parts of distilled water, 10 part -20
Part water-based emulsion, 30 parts of -50 parts of ammonium polyphosphates, 18 parts of -24 parts of nanometer titanium dioxides, 10 parts -20 parts black mud powder, 5 parts of -10 parts of seas
Afrodite, 5 parts of -10 parts of zirconium silicate powders or yttrium stable zirconium oxide powder, 5 parts of -10 parts of expanded perlites, 2 parts of -5 parts of polyester fibers, 3 parts -
7 parts of coalescents, 1 part of -2 parts of citric acids, 1 part of -2 parts of expansible graphites, 0.2 part of -0.6 part of Kaolin.
2. a kind of light insulating fire proof weight material it is characterised in that in parts by weight, steams including 10 parts according to claim 1
Distilled water, 10 parts of water-based emulsions, 30 parts of ammonium polyphosphates, 18 parts of nanometer titanium dioxides, 10 parts of black mud powder, 5 parts of meerschaums, 5 parts of silicic acid
Zirconium powder or yttrium stable zirconium oxide powder, 5 parts of expanded perlites, 2 parts of polyester fibers, 3 parts of coalescents, 1 part of citric acid, 1 part can be swollen
Swollen graphite, 0.2 part of Kaolin.
3. a kind of light insulating fire proof weight material it is characterised in that in parts by weight, steams including 20 parts according to claim 1
Distilled water, 15 parts of water-based emulsions, 40 parts of ammonium polyphosphates, 20 parts of nanometer titanium dioxides, 15 parts of black mud powder, 8 parts of meerschaums, 7 parts of silicic acid
Zirconium powder or yttrium stable zirconium oxide powder, 8 parts of expanded perlites, 3 parts of polyester fibers, 4 parts of coalescents, 1.5 parts of citric acids, 1.5 parts
Expansible graphite, 0.4 part of Kaolin.
4. a kind of light insulating fire proof weight material it is characterised in that in parts by weight, steams including 30 parts according to claim 1
Distilled water, 20 parts of water-based emulsions, 50 parts of ammonium polyphosphates, 24 parts of nanometer titanium dioxides, 20 parts of black mud powder, 10 parts of meerschaums, 10 parts of silicon
Sour zirconium powder or yttrium stable zirconium oxide powder, 10 parts of expanded perlites, 5 parts of polyester fibers, 7 parts of coalescents, 2 parts of citric acids, 2 parts can
Expanded graphite, 0.6 part of Kaolin.
5. a kind of preparation method of light insulating fire proof weight material as described in any one as Claims 1-4 is it is characterised in that include
Following steps：
Step 1), weigh by weight distilled water, nanometer titanium dioxide, ammonium polyphosphate, zirconium silicate powder or yttrium stable zirconium oxide powder,
Citric acid, black mud powder, expanded perlite, polyester fiber and meerschaum, and mix homogeneously obtains mixed liquor；
Step 2), weigh water-based emulsion by weight, and water-based emulsion is added in mixed liquor, stir and make water-based emulsion
Evenly spread in mixed liquor, obtain dispersion liquid；
Step 3), coalescents, expansible graphite and Kaolin, dispersed 50min-80min will be added in dispersion liquid, filter
Fill.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201610760854.9A CN106431074A (en) | 2016-08-30 | 2016-08-30 | Lightweight thermal-insulation fireproof material and preparation method thereof |
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| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201610760854.9A CN106431074A (en) | 2016-08-30 | 2016-08-30 | Lightweight thermal-insulation fireproof material and preparation method thereof |
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| CN106431074A true CN106431074A (en) | 2017-02-22 |
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| CN201610760854.9A Pending CN106431074A (en) | 2016-08-30 | 2016-08-30 | Lightweight thermal-insulation fireproof material and preparation method thereof |
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Cited By (4)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN107344839A (en) * | 2017-08-15 | 2017-11-14 | 重庆市佰恒科技有限公司 | A kind of building heat preservation fire proofing material and preparation method thereof |
| CN107673671A (en) * | 2017-10-20 | 2018-02-09 | 广西银英生物质能源科技开发股份有限公司 | High-temperature-resistant fireproof material |
| CN107721261A (en) * | 2017-10-20 | 2018-02-23 | 广西银英生物质能源科技开发股份有限公司 | Heat-insulating fireproof material and preparation method thereof |
| CN107777986A (en) * | 2017-10-20 | 2018-03-09 | 广西银英生物质能源科技开发股份有限公司 | Environment-friendly fireproof material and preparation method thereof |
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| CN103881143A (en) * | 2014-02-20 | 2014-06-25 | 铜陵祥云消防科技有限责任公司 | Mullite composite flame retardant |
| CN104743974A (en) * | 2013-12-30 | 2015-07-01 | 天津赫得建材发展有限公司 | Fireproof material |
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| CN105440411A (en) * | 2015-12-19 | 2016-03-30 | 青岛大方智慧网络科技有限公司 | Fireproof material for strongbox |
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Patent Citations (6)
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|---|---|---|---|---|
| WO2006070960A1 (en) * | 2004-12-31 | 2006-07-06 | Kyung Dong Ceratech Co., Ltd. | Covering composite for fire resistance and sound absorption |
| CN102584115A (en) * | 2011-12-20 | 2012-07-18 | 汪洋 | Fireproof material, preparation method thereof and fireproof door |
| CN104743974A (en) * | 2013-12-30 | 2015-07-01 | 天津赫得建材发展有限公司 | Fireproof material |
| CN103881143A (en) * | 2014-02-20 | 2014-06-25 | 铜陵祥云消防科技有限责任公司 | Mullite composite flame retardant |
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Cited By (4)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN107344839A (en) * | 2017-08-15 | 2017-11-14 | 重庆市佰恒科技有限公司 | A kind of building heat preservation fire proofing material and preparation method thereof |
| CN107673671A (en) * | 2017-10-20 | 2018-02-09 | 广西银英生物质能源科技开发股份有限公司 | High-temperature-resistant fireproof material |
| CN107721261A (en) * | 2017-10-20 | 2018-02-23 | 广西银英生物质能源科技开发股份有限公司 | Heat-insulating fireproof material and preparation method thereof |
| CN107777986A (en) * | 2017-10-20 | 2018-03-09 | 广西银英生物质能源科技开发股份有限公司 | Environment-friendly fireproof material and preparation method thereof |
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Application publication date: 20170222 |