CN106426975A - Preparation process of composite fishing rod - Google Patents

Preparation process of composite fishing rod Download PDF

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Publication number
CN106426975A
CN106426975A CN201610856493.8A CN201610856493A CN106426975A CN 106426975 A CN106426975 A CN 106426975A CN 201610856493 A CN201610856493 A CN 201610856493A CN 106426975 A CN106426975 A CN 106426975A
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solidification
control
drying
relative humidity
indoor
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CN201610856493.8A
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CN106426975B (en
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陈雨
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    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B29—WORKING OF PLASTICS; WORKING OF SUBSTANCES IN A PLASTIC STATE IN GENERAL
    • B29C—SHAPING OR JOINING OF PLASTICS; SHAPING OF MATERIAL IN A PLASTIC STATE, NOT OTHERWISE PROVIDED FOR; AFTER-TREATMENT OF THE SHAPED PRODUCTS, e.g. REPAIRING
    • B29C70/00—Shaping composites, i.e. plastics material comprising reinforcements, fillers or preformed parts, e.g. inserts
    • B29C70/04—Shaping composites, i.e. plastics material comprising reinforcements, fillers or preformed parts, e.g. inserts comprising reinforcements only, e.g. self-reinforcing plastics
    • B29C70/28—Shaping operations therefor
    • B29C70/30—Shaping by lay-up, i.e. applying fibres, tape or broadsheet on a mould, former or core; Shaping by spray-up, i.e. spraying of fibres on a mould, former or core
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B29—WORKING OF PLASTICS; WORKING OF SUBSTANCES IN A PLASTIC STATE IN GENERAL
    • B29C—SHAPING OR JOINING OF PLASTICS; SHAPING OF MATERIAL IN A PLASTIC STATE, NOT OTHERWISE PROVIDED FOR; AFTER-TREATMENT OF THE SHAPED PRODUCTS, e.g. REPAIRING
    • B29C35/00—Heating, cooling or curing, e.g. crosslinking or vulcanising; Apparatus therefor
    • B29C35/02—Heating or curing, e.g. crosslinking or vulcanizing during moulding, e.g. in a mould
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B29—WORKING OF PLASTICS; WORKING OF SUBSTANCES IN A PLASTIC STATE IN GENERAL
    • B29C—SHAPING OR JOINING OF PLASTICS; SHAPING OF MATERIAL IN A PLASTIC STATE, NOT OTHERWISE PROVIDED FOR; AFTER-TREATMENT OF THE SHAPED PRODUCTS, e.g. REPAIRING
    • B29C37/00—Component parts, details, accessories or auxiliary operations, not covered by group B29C33/00 or B29C35/00
    • B29C37/0092—Drying moulded articles or half products, e.g. preforms, during or after moulding or cooling
    • C—CHEMISTRY; METALLURGY
    • C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
    • C08L—COMPOSITIONS OF MACROMOLECULAR COMPOUNDS
    • C08L67/00—Compositions of polyesters obtained by reactions forming a carboxylic ester link in the main chain; Compositions of derivatives of such polymers
    • C08L67/02—Polyesters derived from dicarboxylic acids and dihydroxy compounds
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B29—WORKING OF PLASTICS; WORKING OF SUBSTANCES IN A PLASTIC STATE IN GENERAL
    • B29L—INDEXING SCHEME ASSOCIATED WITH SUBCLASS B29C, RELATING TO PARTICULAR ARTICLES
    • B29L2031/00—Other particular articles
    • B29L2031/70—Agricultural usage or equipment
    • B29L2031/7002—Agricultural usage or equipment for fishing
    • C—CHEMISTRY; METALLURGY
    • C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
    • C08K—Use of inorganic or non-macromolecular organic substances as compounding ingredients
    • C08K2201/00—Specific properties of additives
    • C08K2201/011—Nanostructured additives
    • C—CHEMISTRY; METALLURGY
    • C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
    • C08L—COMPOSITIONS OF MACROMOLECULAR COMPOUNDS
    • C08L2205/00—Polymer mixtures characterised by other features
    • C08L2205/03—Polymer mixtures characterised by other features containing three or more polymers in a blend
    • C08L2205/035—Polymer mixtures characterised by other features containing three or more polymers in a blend containing four or more polymers in a blend
    • C—CHEMISTRY; METALLURGY
    • C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
    • C08L—COMPOSITIONS OF MACROMOLECULAR COMPOUNDS
    • C08L2205/00—Polymer mixtures characterised by other features
    • C08L2205/14—Polymer mixtures characterised by other features containing polymeric additives characterised by shape
    • C08L2205/16—Fibres; Fibrils

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  • Chemical & Material Sciences (AREA)
  • Health & Medical Sciences (AREA)
  • Oral & Maxillofacial Surgery (AREA)
  • Mechanical Engineering (AREA)
  • Physics & Mathematics (AREA)
  • Composite Materials (AREA)
  • Engineering & Computer Science (AREA)
  • Thermal Sciences (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • Medicinal Chemistry (AREA)
  • Polymers & Plastics (AREA)
  • Organic Chemistry (AREA)
  • Treatments For Attaching Organic Compounds To Fibrous Goods (AREA)
  • Reinforced Plastic Materials (AREA)

Abstract

The invention discloses a preparation process of a composite fishing rod. The preparation process is characterized by comprising the following steps: (1) a composite material is fed in melting equipment for heating and melting to obtain a melt; (2) non-woven fabric is tailored by a set size, and the tailored non-woven fabric is dipped in the melt, so that the melt is combined with the non-woven fabric; and (3) the non-woven fabric dipped with the melt is wound on a core to be fed in curing equipment for curing, and then, the core is removed for painting and drying. The preparation process is simple in step and controllable; and the prepared fishing rod is smooth and compact in surface, and is excellent in mechanical performance.

Description

A kind of preparation technology of compound Herba Veronicastri
Technical field
The present invention relates to fishing gear technical field is and in particular to a kind of preparation technology of compound Herba Veronicastri.
Background technology
With the continuous improvement of people's living standard, fish and have become as a kind of important amusement of people, stress-relieving activity, competing Skill fishing frequent development also like a raging fire.Fishing rod in the market is mostly carbon fiber fishing rod, is all using no shuttle Spin carbon fiber longitudinal direction cloth tubulation, manufacture through resin pickup solidification.Carbon fiber content for fishing rod production aspect is how many, directly Determine value and the grade of fishing rod.General phosphorus content is 30%, 90% about, with the fishing rod of carbon fiber manufacture have light, solid, The high feature of tensile strength, but there is no insulation function.
Content of the invention
The technical problem to be solved is to provide a kind of processing step simple, the good compound fishing of controllability The preparation technology of pole.
The technical problem to be solved employs the following technical solutions to realize：
A kind of preparation technology of compound Herba Veronicastri, its step is as follows：
(1) composite is sent into fusion apparatus, fusing of heating, obtain melt；
(2) by non-woven fabrics by being sized carrying out cutting, and the non-woven fabrics cutting are immersed in melt, make melt with no Spin cloth to combine；
(3) nonwoven fabric roll being soaked with melt is wound on core, send into curing apparatus carry out cured, after the completion of remove Core, japanning is dried.
The curing process of above-mentioned cured is as follows：
First cure stage：Control the indoor solidification temperature of solidification at 65 DEG C, 99%, curing time control exists relative humidity 12 hours；
Second cure stage：Control the indoor solidification temperature of solidification at 70 DEG C, 99%, curing time control exists relative humidity 15 hours；
3rd cure stage：Control the indoor solidification temperature of solidification at 72 DEG C, 82%, curing time control exists relative humidity 5 hours；
First drying stage：Control the indoor baking temperature of solidification at 80 DEG C, 65%, drying time controls relative humidity 2 hours；
Second drying stage：Control the indoor baking temperature of solidification at 73 DEG C, 40%, drying time controls relative humidity 2 hours；
3rd drying stage：Control the indoor baking temperature of solidification at 85 DEG C, 0.5%, drying time controls relative humidity At 18 hours.This curing process relative energy-saving, the product total quality obtaining is stable, and qualification rate reaches 100%.
Above-mentioned japanning drying is to carry out in drying equipment.
Above-mentioned drying equipment is steam drying equipment.
Above-mentioned fusion apparatus are double screw extruder.
Above-mentioned composite is made up of the component of following mass percent：Polyethylene terephthalate 10%, carbon Fiber 60%, glass fibre 10%, methylvinylcyclosiloxane 5%, epoxy hardener 2%, nylon 3%, imitative spider silk are fine Dimension 1%, antistatic additive 1%, viscosifier 5%, glycerol 0.2%, bamboo fibre 0.8%, nano silicon 2%.
Above-mentioned viscosifier are made up of the component of following weight：Ethylene glycol 80g, glycidyl acrylate 15g, Colophonium 5g, n-butyl acrylate 10g, lauryl mercaptan 5g, lac resin 4g, microwax 2g, pure-acrylic emulsion 5g；This viscosifier is special Configured for regeneration insulation fishing rod, the speed of viscosity increasement is fast, and effect is good.
The preparation method of above-mentioned composite is as follows：
(1) by polyethylene terephthalate, methylvinylcyclosiloxane, epoxy hardener, antistatic additive, glycerol Send in rotary drum with nano silicon and carry out mix and blend, rotary drum is heated up to 80-120 DEG C simultaneously, the time, at 40 minutes, presses Power, in 150-200Mpa, is taken out and is obtained compound；
(2) by viscosifier, glass fibre, imitative spider silk fiber, nylon and bamboo fibre, after being plastified by single screw extrusion machine High-temperature fusant reactor is transported to by mouth mould, adds compound, keep kettle temperature in 235～240 DEG C, pressure 2.0～2.5MPa Under the conditions of, obtain blend melt；
(3) blend melt is sent to dipping head, the temperature of dipping head is set as 280-360 DEG C, carbon fiber is led to Cross dipping head die hole, after dipping, pulled out dipping head, cooling, pelletizing, obtain composite.
Fishing rod of the present invention has insulation function, and advantage is good toughness, lightweight, is using the dimension material manufacture of high-tech carbon Become；There occurs some changes compared with the existing product character on market, more superior than pure carbon fishing rod in performance, show as：Matter Amount is lighter, and intensity is bigger, and the pole tip can bend 180 degree, and the soft pole tip is more conducive to the power of unloading, and prevents the big fish of ferociousness from causing when struggling Disconnected pole or broken string；Recreational fishing thunderbolt, electric shock accidentss can be avoided simultaneously to occur, effectively reduce in thundery sky outdoor fishing Unexpected rate.
The invention has the beneficial effects as follows：Present invention process step is simple, and technique is controlled, makes the fishing rod smooth surface made close Real, and there is excellent mechanical property.
Specific embodiment
In order that technological means, creation characteristic, reached purpose and effect that the present invention realizes are easy to understand, tie below Close specific embodiment, the present invention is expanded on further.
Embodiment 1
A kind of preparation technology of compound Herba Veronicastri, its step is as follows：
(1) composite is sent into fusion apparatus, fusing of heating, obtain melt；
(2) by non-woven fabrics by being sized carrying out cutting, and the non-woven fabrics cutting are immersed in melt, make melt with no Spin cloth to combine；
(3) nonwoven fabric roll being soaked with melt is wound on core, send into curing apparatus carry out cured, after the completion of remove Core, japanning is dried, and drying is to carry out in steam drying equipment；
The curing process of above-mentioned cured is as follows：
First cure stage：Control the indoor solidification temperature of solidification at 65 DEG C, 99%, curing time control exists relative humidity 12 hours；
Second cure stage：Control the indoor solidification temperature of solidification at 70 DEG C, 99%, curing time control exists relative humidity 15 hours；
3rd cure stage：Control the indoor solidification temperature of solidification at 72 DEG C, 82%, curing time control exists relative humidity 5 hours；
First drying stage：Control the indoor baking temperature of solidification at 80 DEG C, 65%, drying time controls relative humidity 2 hours；
Second drying stage：Control the indoor baking temperature of solidification at 73 DEG C, 40%, drying time controls relative humidity 2 hours；
3rd drying stage：Control the indoor baking temperature of solidification at 85 DEG C, 0.5%, drying time controls relative humidity At 18 hours.This curing process relative energy-saving, the product total quality obtaining is stable, and qualification rate reaches 100%.
Embodiment 2
A kind of preparation technology of compound Herba Veronicastri, its step is as follows：
(1) composite is sent into fusion apparatus, fusing of heating, obtain melt；
(2) by non-woven fabrics by being sized carrying out cutting, and the non-woven fabrics cutting are immersed in melt, make melt with no Spin cloth to combine；
(3) nonwoven fabric roll being soaked with melt is wound on core, send into curing apparatus carry out cured, after the completion of remove Core, japanning is dried.
The curing process of above-mentioned cured is as follows：
First cure stage：Control the indoor solidification temperature of solidification at 65 DEG C, 99%, curing time control exists relative humidity 12 hours；
Second cure stage：Control the indoor solidification temperature of solidification at 70 DEG C, 99%, curing time control exists relative humidity 15 hours；
3rd cure stage：Control the indoor solidification temperature of solidification at 72 DEG C, 82%, curing time control exists relative humidity 5 hours；
First drying stage：Control the indoor solidification temperature of solidification at 80 DEG C, 65%, drying time controls relative humidity 2 hours；
Second drying stage：Control the indoor solidification temperature of solidification at 73 DEG C, 40%, drying time controls relative humidity 2 hours；
3rd drying stage：Control the indoor solidification temperature of solidification at 85 DEG C, 0.5%, drying time controls relative humidity At 18 hours.This curing process relative energy-saving, the product total quality obtaining is stable, and qualification rate reaches 100%.
Embodiment 3
A kind of preparation technology of compound Herba Veronicastri, its step is as follows：
(1) composite is sent into fusion apparatus, fusing of heating, obtain melt；
(2) by non-woven fabrics by being sized carrying out cutting, and the non-woven fabrics cutting are immersed in melt, make melt with no Spin cloth to combine；
(3) nonwoven fabric roll being soaked with melt is wound on core, send into curing apparatus carry out cured, after the completion of remove Core, japanning is dried.
The curing process of above-mentioned cured is as follows：
First cure stage：Control the indoor solidification temperature of solidification at 65 DEG C, 99%, curing time control exists relative humidity 12 hours；
Second cure stage：Control the indoor solidification temperature of solidification at 70 DEG C, 99%, curing time control exists relative humidity 15 hours；
3rd cure stage：Control the indoor solidification temperature of solidification at 72 DEG C, 82%, curing time control exists relative humidity 5 hours；
First drying stage：Control the indoor solidification temperature of solidification at 80 DEG C, 65%, drying time controls relative humidity 2 hours；
Second drying stage：Control the indoor solidification temperature of solidification at 73 DEG C, 40%, drying time controls relative humidity 2 hours；
3rd drying stage：Control the indoor solidification temperature of solidification at 85 DEG C, 0.5%, drying time controls relative humidity At 18 hours.This curing process relative energy-saving, the product total quality obtaining is stable, and qualification rate reaches 100%.
Above-mentioned composite is made up of the component of following mass percent：Polyethylene terephthalate 10%, carbon Fiber 60%, glass fibre 10%, methylvinylcyclosiloxane 5%, epoxy hardener 2%, nylon 3%, imitative spider silk are fine Dimension 1%, antistatic additive 1%, viscosifier 5%, glycerol 0.2%, bamboo fibre 0.8%, nano silicon 2%.
Above-mentioned viscosifier are made up of the component of following weight：Ethylene glycol 80g, glycidyl acrylate 15g, Colophonium 5g, n-butyl acrylate 10g, lauryl mercaptan 5g, lac resin 4g, microwax 2g, pure-acrylic emulsion 5g；This viscosifier is special Configured for regeneration insulation fishing rod, the speed of viscosity increasement is fast, and effect is good.
The preparation method of above-mentioned composite is as follows：
(1) by polyethylene terephthalate, methylvinylcyclosiloxane, epoxy hardener, antistatic additive, glycerol Send in rotary drum with nano silicon and carry out mix and blend, rotary drum is heated up to 80-120 DEG C simultaneously, the time, at 40 minutes, presses Power, in 150-200Mpa, is taken out and is obtained compound；
(2) by viscosifier, glass fibre, imitative spider silk fiber, nylon and bamboo fibre, after being plastified by single screw extrusion machine High-temperature fusant reactor is transported to by mouth mould, adds compound, keep kettle temperature in 235～240 DEG C, pressure 2.0～2.5MPa Under the conditions of, obtain blend melt；
(3) blend melt is sent to dipping head, the temperature of dipping head is set as 280-360 DEG C, carbon fiber is led to Cross dipping head die hole, after dipping, pulled out dipping head, cooling, pelletizing, obtain composite.
By above-described embodiment, the fishing rod that example 1～3 is obtained is tested, and test performance is as shown in the table：
Performance Embodiment 1 Embodiment 2 Embodiment 3
Bending strength MPa 1560 1540 1680
Bending moduluses GPa 102 106 158
Interlaminar shear strength MPa 72 80 90.2
As can be seen from the above table, the embodiment of the present invention 1～3 comprehensive mechanical property is excellent, compared with the fishing rod of prior art, It has been obviously improved bending strength, bending moduluses, interlaminar shear strength.
Ultimate principle and principal character and the advantages of the present invention of the present invention have been shown and described above.The technology of the industry , it should be appreciated that the present invention is not restricted to the described embodiments, the simply explanation described in above-described embodiment and description is originally for personnel The principle of invention, without departing from the spirit and scope of the present invention, the present invention also has various changes and modifications, these changes Change and improvement both falls within scope of the claimed invention.Claimed scope by appending claims and its Equivalent thereof.

Claims (4)

1. a kind of preparation technology of compound Herba Veronicastri is it is characterised in that step is as follows：
(1) composite is sent into fusion apparatus, fusing of heating, obtain melt；
(2) by non-woven fabrics by being sized carrying out cutting, and the non-woven fabrics cutting are immersed in melt, make melt and non-woven fabrics In conjunction with；
(3) nonwoven fabric roll being soaked with melt is wound on core, send into curing apparatus carry out cured, after the completion of remove core Material, japanning is dried；
The curing process of above-mentioned cured is as follows：
First cure stage：Control the indoor solidification temperature of solidification at 65 DEG C, 99%, curing time control is little 12 for relative humidity When；
Second cure stage：Control the indoor solidification temperature of solidification at 70 DEG C, 99%, curing time control is little 15 for relative humidity When；
3rd cure stage：Control the indoor solidification temperature of solidification at 72 DEG C, 82%, curing time control is little 5 for relative humidity When；
First drying stage：Control the indoor baking temperature of solidification at 80 DEG C, 65%, drying time controls little 2 relative humidity When；
Second drying stage：Control the indoor baking temperature of solidification at 73 DEG C, 40%, drying time controls little 2 relative humidity When；
3rd drying stage：Control the indoor baking temperature of solidification at 85 DEG C, relative humidity 0.5%, controls 18 drying time Hour.
2. a kind of compound Herba Veronicastri according to claim 1 preparation technology it is characterised in that the drying of above-mentioned japanning be Carry out in drying equipment.
3. a kind of preparation technology of compound Herba Veronicastri according to claim 2 is it is characterised in that above-mentioned drying equipment is to steam Vapour drying equipment.
4. a kind of preparation technology of compound Herba Veronicastri according to claim 1 is it is characterised in that above-mentioned fusion apparatus are double Screw extruder.
CN201610856493.8A 2016-09-27 2016-09-27 A kind of preparation process of compound fishing rod Active CN106426975B (en)

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Cited By (2)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN106857435A (en) * 2017-02-28 2017-06-20 威海东澳渔具有限公司 A kind of fishing rod leads the preparation method of eye
CN106916392A (en) * 2017-03-24 2017-07-04 合肥悦兰信息技术有限公司 Laminated bow material for producing the light-duty bow and arrow of high resiliency

Citations (3)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
JPH0549372A (en) * 1991-08-19 1993-03-02 Shimano Inc Fishing rod and its production
CN1939711A (en) * 2005-09-29 2007-04-04 大和精工株式会社 Tubular member and producing method thereof
CN101513177A (en) * 2008-02-18 2009-08-26 周鸢 Fishing rod doped with carbon nanometer particles and preparation method thereof

Patent Citations (3)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
JPH0549372A (en) * 1991-08-19 1993-03-02 Shimano Inc Fishing rod and its production
CN1939711A (en) * 2005-09-29 2007-04-04 大和精工株式会社 Tubular member and producing method thereof
CN101513177A (en) * 2008-02-18 2009-08-26 周鸢 Fishing rod doped with carbon nanometer particles and preparation method thereof

Cited By (3)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN106857435A (en) * 2017-02-28 2017-06-20 威海东澳渔具有限公司 A kind of fishing rod leads the preparation method of eye
CN106857435B (en) * 2017-02-28 2021-01-22 威海东澳渔具有限公司 Preparation method of fishing rod guide hole
CN106916392A (en) * 2017-03-24 2017-07-04 合肥悦兰信息技术有限公司 Laminated bow material for producing the light-duty bow and arrow of high resiliency

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